Institute of Experimental Mineralogy
                 Russian Academy of Sciences
     -------------------------------------------------
           142432, Chernogolovka, Moscow district
             A.V. Chichagov  +7(496)52-22320

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          ***      W W W - X R A Y P O L       ***
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PROTOFERRO_ANTHOPHYLLITE

1, f-amphiboles, sf-Mg-Fe-amphiboles, s-anthophyllite

[Fe(0.8)Mn(0.2)](2)[Fe(0.96)Mg(0.02)](5)[Si(4)O(11)](2)(OH)(2)


Orthorhombic  P nmn  Z = 2

Pnmn

23 .10 .1998

Ref.Str.:

         Sueno S., Matsuura S., Gibbs G.V., Bounsen M.B. (1998)

         * Phys. Chem. Minerals, 25, 366-377

Reserv:

         N.A.D.

                   Initial data from BDM-file 

   Lattice parameters (cub. angs.,degr.):

             a =   9.388    alpha =   90.0 
             b =  18.387    beta  =   90.0 
             c =   5.347    gamma =   90.0 

    Unit cell volume (cub. angs.) =   922.98

    Molar volume ( cub.cm/mol.) =   277.97

  Co-ordinates, thermal parameters, occupation for atomic positions:

NoP   x/a     y/b     z/c    B(j)   atom  / occupation

   1 0.0     0.0883  0.5      0.55   Fe    = 1.00
   2 0.0     0.18    0.0      0.45   Fe    = 0.95, Mg    = 0.05
   3 0.0     0.0     0.0      0.54   Fe    = 1.00
   4 0.0     0.2588  0.5      0.75   Fe    = 0.8 , Mn    = 0.2 
   5 0.285   0.0835  0.1635   0.45   Si    = 1.00
   6 0.2972  0.1667  0.6611   0.49   Si    = 1.00
   7 0.1127  0.0881  0.1621   0.65   O     = 1.00
   8 0.1254  0.1741  0.6646   0.69   O     = 1.00
   9 0.1139  0.0     0.6613   0.74   O     = 1.00
  10 0.1163  0.2583  0.1912   0.85   O     = 1.00
  11 0.3472  0.1247  0.4083   0.89   O     = 1.00
  12 0.3478  0.1211  0.9123   1.07   O     = 1.00
  13 0.3397  0.0     0.1722   1.0    O     = 1.00


  Co-ordinates for all atomic positions :

   No       NoP      x/a        y/b       z/c 

     1       1     0.0        0.0883     0.5   
     2       2     0.0        0.18       0.0   
     3       3     0.0        0.0        0.0   
     4       4     0.0        0.2588     0.5   
     5       5     0.285      0.0835     0.1635
     6       6     0.2972     0.1667     0.6611
     7       7     0.1127     0.0881     0.1621
     8       8     0.1254     0.1741     0.6646
     9       9     0.1139     0.0        0.6613
    10      10     0.1163     0.2583     0.1912
    11      11     0.3472     0.1247     0.4083
    12      12     0.3478     0.1211     0.9123
    13      13     0.3397     0.0        0.1722
    14       1     0.0        0.9117     0.5   
    15       2     0.0        0.82       0.0   
    16       4     0.0        0.7412     0.5   
    17       5     0.715      0.9165     0.8365
    18       6     0.7028     0.8333     0.3389
    19       7     0.8873     0.9119     0.8379
    20       8     0.8746     0.8259     0.3354
    21       9     0.8861     0.0        0.3387
    22      10     0.8837     0.7417     0.8088
    23      11     0.6528     0.8753     0.5917
    24      12     0.6522     0.8789     0.0877
    25      13     0.6603     0.0        0.8278
    26       5     0.285      0.9165     0.1635
    27       6     0.2972     0.8333     0.6611
    28       7     0.1127     0.9119     0.1621
    29       8     0.1254     0.8259     0.6646
    30      10     0.1163     0.7417     0.1912
    31      11     0.3472     0.8753     0.4083
    32      12     0.3478     0.8789     0.9123
    33       5     0.715      0.0835     0.8365
    34       6     0.7028     0.1667     0.3389
    35       7     0.8873     0.0881     0.8379
    36       8     0.8746     0.1741     0.3354
    37      10     0.8837     0.2583     0.8088
    38      11     0.6528     0.1247     0.5917
    39      12     0.6522     0.1211     0.0877
    40       1     0.5        0.5883     0.0   
    41       2     0.5        0.68       0.5   
    42       3     0.5        0.5        0.5   
    43       4     0.5        0.7588     0.0   
    44       5     0.215      0.5835     0.6635
    45       6     0.2028     0.6667     0.1611
    46       7     0.3873     0.5881     0.6621
    47       8     0.3746     0.6741     0.1646
    48       9     0.3861     0.5        0.1613
    49      10     0.3837     0.7583     0.6912
    50      11     0.1528     0.6247     0.9083
    51      12     0.1522     0.6211     0.4123
    52      13     0.1603     0.5        0.6722
    53       1     0.5        0.4117     0.0   
    54       2     0.5        0.32       0.5   
    55       4     0.5        0.2412     0.0   
    56       5     0.785      0.4165     0.3365
    57       6     0.7972     0.3333     0.8389
    58       7     0.6127     0.4119     0.3379
    59       8     0.6254     0.3259     0.8354
    60       9     0.6139     0.5        0.8387
    61      10     0.6163     0.2417     0.3088
    62      11     0.8472     0.3753     0.0917
    63      12     0.8478     0.3789     0.5877
    64      13     0.8397     0.5        0.3278
    65       5     0.215      0.4165     0.6635
    66       6     0.2028     0.3333     0.1611
    67       7     0.3873     0.4119     0.6621
    68       8     0.3746     0.3259     0.1646
    69      10     0.3837     0.2417     0.6912
    70      11     0.1528     0.3753     0.9083
    71      12     0.1522     0.3789     0.4123
    72       5     0.785      0.5835     0.3365
    73       6     0.7972     0.6667     0.8389
    74       7     0.6127     0.5881     0.3379
    75       8     0.6254     0.6741     0.8354
    76      10     0.6163     0.7583     0.3088
    77      11     0.8472     0.6247     0.0917
    78      12     0.8478     0.6211     0.5877


X-ray density (g/cm cub.)   =      3.58

MU (1/cm) =     489.895    Mass attenuation coefficient (cm**2/g) =    136.731

 Selected interatomic distances (cation-anion,anion-anion):

 NoP    Atom              Rad.sph.      C.N.    Distance     NoP N.
                           (angs.)               (angs.)

    1    Fe                  2.592        6
                                                 2.0937       7
                                                 2.1562       8
                                                 2.1268       9
                                                 2.1268       9
                                                 2.0937       7
                                                 2.1562       8
    2   Fe   ,Mg             2.592        6
                                                 2.1736       7
                                                 2.148        8
                                                 2.0763      10
                                                 2.1736       7
                                                 2.148        8
                                                 2.0763      10
    3    Fe                  2.592        6
                                                 2.1201       7
                                                 2.1031       9
                                                 2.1201       7
                                                 2.1031       9
                                                 2.1201       7
                                                 2.1201       7
    4   Fe   ,Mn             2.724        6
                                                 2.1415       8
                                                 1.9795      10
                                                 2.1415       8
                                                 1.9795      10
                                                 2.6717      12
                                                 2.6717      12
    5    Si                  2.1          4
                                                 1.6198       7
                                                 1.6212      11
                                                 1.6216      12
                                                 1.6196      13
    6    Si                  2.1          4
                                                 1.6187       8
                                                 1.626       11
                                                 1.6531      12
                                                 1.6084      10
    7    O                   3.264       12
                                                 3.1199       8
                                                 3.0969       8
                                                 3.1223       9
                                                 3.1296       9
                                                 3.1335      10
                                                 2.6519      11
                                                 2.6502      12
                                                 2.6774      13
                                                 2.8357       9
                                                 3.2398       7
                                                 2.7355       7
                                                 2.8906       8
    8    O                   3.264       11
                                                 3.0969       7
                                                 3.1199       7
                                                 3.203        9
                                                 3.2144      10
                                                 2.9684      10
                                                 2.6531      11
                                                 2.6577      12
                                                 2.8906       7
                                                 2.9398       8
                                                 2.8531      10
                                                 2.7286      10
    9    O                   3.264        9
                                                 3.1296       7
                                                 3.1223       7
                                                 3.203        8
                                                 2.8357       7
                                                 2.7475       9
                                                 3.1296       7
                                                 3.1223       7
                                                 3.203        8
                                                 2.8357       7
   10    O                   3.264        8
                                                 3.1335       7
                                                 2.9684       8
                                                 3.2144       8
                                                 2.8531       8
                                                 2.9915      10
                                                 2.7286       8
                                                 2.6521      11
                                                 2.5354      12
   11    O                   3.264        7
                                                 2.6519       7
                                                 2.6531       8
                                                 2.6957      12
                                                 2.6529      12
                                                 2.6184      13
                                                 3.0319      11
                                                 2.6521      10
   12    O                   3.264        7
                                                 2.6502       7
                                                 2.6577       8
                                                 2.6529      11
                                                 2.6957      11
                                                 2.6258      13
                                                 3.0077      12
                                                 2.5354      10
   13    O                   3.264        6
                                                 2.6774       7
                                                 2.6184      11
                                                 2.6258      12
                                                 2.6774       7
                                                 2.6184      11
                                                 2.6258      12

  X-ray diffraction powder data (II),  X-Ray W.L. =   1.54056(angs.):

  No   H   K   L   Theta 2*Theta    S       LPG   MF        F          I int.
                    ( degree )                                         *100

    1   0   2   0  4.806   9.612   0.054  281.92    2       68.8      313.4
    2   1   1   0  5.286  10.572   0.06   232.68    4      140.9     2168.1
    3   0   1   1  8.628  17.257   0.097   85.92    4       39.7       63.7
    4   1   3   0  8.632  17.264   0.097   85.84    4        9.3        3.4
    5   2   0   0  9.445  18.89    0.107   71.35    2      107.4      193.2
    6   1   0   1  9.543  19.086   0.108   69.84    4       43.5       61.9
    7   0   4   0  9.647  19.293   0.109   68.3     2       90.3      130.7
    8   1   1   1  9.846  19.692   0.111   65.48    8       45.2      125.9
    9   2   2   0 10.617  21.235   0.12    56.01    4       71.9      135.9
   10   1   2   1 10.705  21.41    0.121   55.06    8       11.3        6.6
   11   0   3   1 11.021  22.043   0.124   51.82    4       33.4       27.1
   12   1   3   1 12.007  24.015   0.135   43.33    8      111.0      501.3
   13   2   0   1 12.613  25.225   0.142   39.08    4       13.4        3.3
   14   2   1   1 12.847  25.693   0.144   37.59    8       10.2        3.7
   15   1   5   0 13.001  26.001   0.146   36.66    4       39.7       27.1
   16   2   2   1 13.526  27.052   0.152   33.72    8       79.2      198.7
   17   2   4   0 13.564  27.129   0.152   33.51    4      158.6      396.0
   18   1   4   1 13.634  27.268   0.153   33.15    8       14.5        6.5
   19   3   1   0 14.459  28.918   0.162   29.26    4      256.8      905.9
   20   0   6   0 14.558  29.116   0.163   28.83    2       51.6       18.0
   21   2   3   1 14.593  29.185   0.164   28.69    8       85.8      198.4
   22   0   5   1 14.727  29.455   0.165   28.13    4       87.1      100.2
   23   1   5   1 15.494  30.987   0.173   25.23    8      140.9      470.1
   24   2   4   1 15.977  31.954   0.179   23.61    8        9.5        2.0
   25   3   3   0 16.044  32.088   0.179   23.4     4      112.0      137.9
   26   3   0   1 16.571  33.142   0.185   21.82    4       34.7       12.3
   27   0   0   2 16.745  33.49    0.187   21.33    2      131.1       86.0
   28   3   1   1 16.754  33.508   0.187   21.31    8       25.8       13.3
   29   3   2   1 17.293  34.586   0.193   19.89    8       72.8       99.1
   30   1   0   2 17.432  34.864   0.194   19.54    4      173.3      275.7
   31   0   2   2 17.461  34.921   0.195   19.47    4       35.5       11.5
   32   2   6   0 17.468  34.937   0.195   19.45    4       51.6       24.3
   33   1   6   1 17.524  35.048   0.195   19.32    8      210.0      800.1
   34   1   1   2 17.607  35.214   0.196   19.12    8      104.7      197.0
   35   2   5   1 17.613  35.226   0.196   19.11    8      226.5      920.4
   36   1   7   0 17.729  35.457   0.198   18.83    4       25.5        5.8
   37   1   2   2 18.124  36.247   0.202   17.95    8        2.6        0.1
   38   3   3   1 18.16   36.32    0.202   17.87    8       26.4       11.7
   39   3   5   0 18.857  37.714   0.21    16.45    4       50.0       19.3
   40   1   3   2 18.957  37.915   0.211   16.25    8       12.0        2.2
   41   0   7   1 19.07   38.14    0.212   16.04    4       16.7        2.1
   42   4   0   0 19.159  38.319   0.213   15.88    2      105.8       41.7
   43   3   4   1 19.317  38.633   0.215   15.59    8        9.5        1.3
   44   2   0   2 19.364  38.728   0.215   15.51    4      293.8      628.7
   45   2   6   1 19.448  38.897   0.216   15.36    8       79.3       90.7
   46   0   4   2 19.469  38.939   0.216   15.32    4       14.5        1.5
   47   2   1   2 19.524  39.049   0.217   15.23    8       56.5       45.6
   48   0   8   0 19.581  39.162   0.218   15.13    2       56.5       11.3
   49   1   7   1 19.686  39.372   0.219   14.95    8       90.9      116.1
   50   4   2   0 19.799  39.598   0.22    14.76    4       25.3        4.4
   51   2   2   2 19.998  39.997   0.222   14.44    8       39.3       21.0
   52   1   4   2 20.075  40.15    0.223   14.32    8       16.3        3.6
   53   3   5   1 20.724  41.447   0.23    13.34    8        0.1        0.0
   54   2   3   2 20.768  41.537   0.23    13.27    8       39.1       19.0
   55   4   0   1 21.003  42.007   0.233   12.94    4       19.0        2.2
   56   4   1   1 21.153  42.306   0.234   12.74    8       18.7        4.2
   57   1   5   2 21.441  42.881   0.237   12.36    8       26.8        8.3
   58   2   7   1 21.446  42.891   0.237   12.35    8       94.8      104.2
   59   4   2   1 21.598  43.195   0.239   12.16    8       56.7       36.7
   60   4   4   0 21.623  43.247   0.239   12.12    4       35.5        7.2
   61   2   4   2 21.809  43.618   0.241   11.89    8       30.3       10.2
   62   2   8   0 21.911  43.821   0.242   11.77    4       47.7       12.6
   63   1   8   1 21.957  43.913   0.243   11.71    8       67.7       50.4
   64   3   0   2 22.268  44.537   0.246   11.35    4       19.5        2.0
   65   4   3   1 22.322  44.645   0.247   11.29    8       37.0       14.5
   66   3   6   1 22.344  44.687   0.247   11.26    8      208.9      461.4
   67   3   1   2 22.411  44.823   0.247   11.19    8      114.1      136.7
   68   0   6   2 22.479  44.959   0.248   11.11    4       30.6        4.9
   69   3   7   0 22.511  45.022   0.249   11.07    4       49.8       12.9
   70   1   9   0 22.697  45.394   0.25    10.87    4       64.0       20.9
   71   3   2   2 22.836  45.672   0.252   10.72    8       10.0        1.0
   72   1   6   2 23.02   46.04    0.254   10.53    8       12.5        1.5
   73   2   5   2 23.091  46.182   0.255   10.46    8       52.0       26.5
   74   4   4   1 23.307  46.614   0.257   10.24    8       12.6        1.5
   75   3   3   2 23.531  47.062   0.259   10.02    8       36.9       12.8
   76   2   8   1 23.578  47.156   0.26     9.97    8       11.5        1.2
   77   0   9   1 23.805  47.609   0.262    9.76    4       54.0       13.4
   78   3   7   1 24.146  48.293   0.266    9.45    8       34.8       10.8
   79   1   9   1 24.323  48.645   0.267    9.29    8       73.0       46.5
   80   5   1   0 24.354  48.709   0.268    9.27    4       39.3        6.7
   81   4   6   0 24.418  48.836   0.268    9.21    4       45.4        8.9
   82   3   4   2 24.478  48.956   0.269    9.16    8       69.9       42.0
   83   4   5   1 24.528  49.056   0.269    9.12    8      170.3      248.3
   84   2   6   2 24.587  49.174   0.27     9.07    8       30.2        7.8
   85   0  10   0 24.767  49.534   0.272    8.92    2       82.6       14.3
   86   1   7   2 24.785  49.57    0.272    8.9     8        8.4        0.6
   87   5   3   0 25.408  50.817   0.279    8.41    4       48.0        9.1
   88   3   5   2 25.657  51.314   0.281    8.23    8       17.5        2.4
   89   0   1   3 25.734  51.469   0.282    8.17    4       26.5        2.7
   90   5   0   1 25.773  51.546   0.282    8.15    4       35.1        4.7
   91   2   9   1 25.83   51.66    0.283    8.1     8       36.7       10.3
   92   4   0   2 25.895  51.79    0.283    8.06    4      228.5      197.6
   93   5   1   1 25.901  51.802   0.284    8.05    8       12.9        1.3
   94   4   6   1 25.962  51.924   0.284    8.01    8      102.4       78.9
   95   4   1   2 26.023  52.045   0.285    7.97    8       62.4       29.1
   96   1   0   3 26.097  52.194   0.286    7.92    4       39.5        5.8
   97   3   8   1 26.108  52.217   0.286    7.91    8       61.4       28.0
   98   1   1   3 26.224  52.448   0.287    7.83    8        1.1        0.0
   99   0   8   2 26.229  52.458   0.287    7.83    4       47.8        8.4
  100   2   7   2 26.273  52.545   0.287    7.8     8       33.9        8.4
  101   5   2   1 26.283  52.566   0.287    7.79    8        6.5        0.3
  102   4   2   2 26.403  52.806   0.289    7.71    8       58.3       24.6
  103   1   2   3 26.603  53.206   0.291    7.58    8       58.7       24.5
  104   1   8   2 26.713  53.425   0.292    7.51    8       89.8       56.9
  105   2  10   0 26.739  53.477   0.292    7.49    4       33.5        3.9
  106   0   3   3 26.749  53.497   0.292    7.48    4      131.5       60.8
  107   3   9   0 26.761  53.522   0.292    7.48    4        3.0        0.0
  108   1  10   1 26.778  53.556   0.292    7.47    8       34.4        8.3
  109   5   3   1 26.911  53.822   0.294    7.38    8       21.7        3.3
  110   4   3   2 27.029  54.058   0.295    7.31    8       16.6        1.9
  111   3   6   2 27.048  54.095   0.295    7.3     8        2.2        0.0
  112   1   3   3 27.226  54.451   0.297    7.19    8        2.0        0.0
  113   5   5   0 27.428  54.855   0.299    7.07    4       27.3        2.5
  114   2   0   3 27.534  55.069   0.3      7.01    4       10.3        0.3
  115   4   7   1 27.587  55.175   0.301    6.98    8       39.6       10.3
  116   2   1   3 27.657  55.314   0.301    6.94    8       35.5        8.2
  117   5   4   1 27.774  55.547   0.302    6.87    8        3.4        0.1
  118   4   4   2 27.889  55.779   0.304    6.81    8       94.4       57.0
  119   1  11   0 27.909  55.818   0.304    6.8     4      234.5      175.4
  120   4   8   0 27.974  55.949   0.304    6.76    4       85.1       23.0
  121   2   2   3 28.022  56.044   0.305    6.73    8       13.6        1.2
  122   1   4   3 28.082  56.163   0.306    6.7     8        8.0        0.4
  123   2   8   2 28.128  56.256   0.306    6.68    8       21.0        2.8
  124   2  10   1 28.191  56.383   0.307    6.64    8       52.2       17.0
  125   3   9   1 28.213  56.426   0.307    6.63    8       32.1        6.4
  126   2   3   3 28.624  57.248   0.311    6.42    8       31.2        5.9
  127   3   7   2 28.631  57.261   0.311    6.41    8       21.1        2.7
  128   0   5   3 28.702  57.405   0.312    6.38    4      286.2      245.2
  129   1   9   2 28.787  57.574   0.313    6.33    8       29.7        5.3
  130   5   5   1 28.857  57.714   0.313    6.3     8        6.0        0.2
  131   0  11   1 28.869  57.738   0.313    6.29    4       19.9        1.2
  132   4   5   2 28.97   57.94    0.314    6.24    8       17.6        1.8
  133   1   5   3 29.158  58.316   0.316    6.15    8        7.0        0.3
  134   1  11   1 29.323  58.646   0.318    6.08    8       30.3        5.3
  135   4   8   1 29.387  58.773   0.319    6.05    8       14.4        1.2
  136   2   4   3 29.453  58.907   0.319    6.02    8       14.4        1.2
  137   6   0   0 29.492  58.983   0.32     6.0     2      229.0       73.9
  138   3   0   3 29.825  59.651   0.323    5.85    4       27.8        2.1
  139   3   1   3 29.942  59.883   0.324    5.8     8        0.2        0.0
  140   6   2   0 29.959  59.917   0.324    5.79    4       39.1        4.1
  141   5   0   2 30.087  60.174   0.325    5.74    4       26.6        1.9
  142   2   9   2 30.138  60.277   0.326    5.71    8       45.3       11.0
  143   5   6   1 30.148  60.295   0.326    5.71    8      281.7      425.5
  144   0  12   0 30.18   60.359   0.326    5.7     2      325.1      141.3
  145   5   1   2 30.203  60.405   0.327    5.69    8      152.3      123.9
  146   4   6   2 30.258  60.515   0.327    5.66    8       27.7        4.1
  147   5   7   0 30.284  60.567   0.327    5.65    4        8.1        0.2
  148   3   2   3 30.289  60.578   0.327    5.65    8       38.2        7.7
  149   3   8   2 30.39   60.78    0.328    5.61    8       32.4        5.5
  150   1   6   3 30.44   60.881   0.329    5.59    8      225.5      266.9
  151   3  10   1 30.451  60.901   0.329    5.58    8       86.5       39.2
  152   2   5   3 30.499  60.998   0.329    5.56    8       77.3       31.2
  153   5   2   2 30.548  61.097   0.33     5.54    8       10.2        0.5
  154   0  10   2 30.56   61.12    0.33     5.54    4       37.2        3.6
  155   2  11   1 30.66   61.319   0.331    5.5     8       17.7        1.6
  156   6   0   1 30.86   61.72    0.333    5.42    4        7.9        0.2
  157   3   3   3 30.863  61.726   0.333    5.42    8        6.6        0.2
  158   6   1   1 30.974  61.948   0.334    5.38    8        0.2        0.0
  159   1  10   2 30.999  61.997   0.334    5.37    8       13.4        0.9
  160   5   3   2 31.12   62.239   0.335    5.32    8       46.5       10.8
  161   6   2   1 31.315  62.63    0.337    5.25    8       37.2        6.8
  162   6   4   0 31.335  62.669   0.338    5.24    4        1.7        0.0
  163   4   9   1 31.347  62.693   0.338    5.24    8        0.7        0.0
  164   0   7   3 31.485  62.97    0.339    5.19    4      146.1       52.0
  165   3  11   0 31.496  62.992   0.339    5.18    4      157.3       60.2
  166   5   7   1 31.631  63.263   0.34     5.13    8       25.5        3.1
  167   3   4   3 31.657  63.313   0.341    5.13    8       17.0        1.4
  168   4   7   2 31.738  63.477   0.341    5.1     8       22.2        2.4
  169   2   6   3 31.749  63.498   0.342    5.09    8        9.6        0.4
  170   6   3   1 31.878  63.756   0.343    5.05    8       11.2        0.6
  171   5   4   2 31.909  63.819   0.343    5.04    8       73.5       25.6
  172   1   7   3 31.916  63.833   0.343    5.03    8        9.4        0.4
  173   2  12   0 31.926  63.851   0.343    5.03    4       60.9        8.8
  174   1  12   1 31.961  63.922   0.344    5.02    8       34.8        5.7
  175   4  10   0 32.153  64.305   0.345    4.95    4       26.0        1.6
  176   2  10   2 32.294  64.588   0.347    4.91    8       42.1        8.2
  177   3   9   2 32.314  64.628   0.347    4.9     8        0.3        0.0
  178   6   4   1 32.658  65.315   0.35     4.79    8        4.7        0.1
  179   3   5   3 32.661  65.322   0.35     4.79    8        3.9        0.1
  180   3  11   1 32.816  65.631   0.352    4.74    8       12.5        0.7
  181   4   0   3 32.865  65.731   0.352    4.73    4        5.7        0.1
  182   5   5   2 32.909  65.819   0.353    4.71    8        3.0        0.0
  183   4   1   3 32.976  65.951   0.353    4.69    8       12.9        0.7
  184   2   7   3 33.192  66.384   0.355    4.63    8       20.2        1.8
  185   2  12   1 33.236  66.472   0.356    4.61    8        7.6        0.3
  186   5   8   1 33.297  66.594   0.356    4.6     8       61.7       16.4
  187   4   2   3 33.305  66.61    0.356    4.59    8        4.9        0.1
  188   1  11   2 33.342  66.684   0.357    4.58    8      149.5       96.2
  189   4   8   2 33.401  66.802   0.357    4.57    8       21.0        1.9
  190   1  13   0 33.419  66.837   0.358    4.56    4        1.1        0.0
  191   4  10   1 33.458  66.917   0.358    4.55    8       47.3        9.5
  192   6   6   0 33.556  67.112   0.359    4.52    4       21.9        1.0
  193   1   8   3 33.574  67.148   0.359    4.52    8       59.6       15.1
  194   6   5   1 33.646  67.292   0.36     4.5     8      145.9       89.8
  195   4   3   3 33.851  67.701   0.362    4.44    8       26.1        2.8
  196   5   9   0 33.861  67.723   0.362    4.44    4       38.6        3.1
  197   3   6   3 33.867  67.734   0.362    4.43    8      189.3      149.2
  198   5   6   2 34.111  68.222   0.364    4.37    8       35.3        5.1
  199   0  13   1 34.287  68.574   0.366    4.32    4       10.7        0.2
  200   3  10   2 34.395  68.789   0.367    4.29    8        5.9        0.1
  201   2  11   2 34.591  69.181   0.369    4.25    8        7.2        0.2
  202   4   4   3 34.608  69.215   0.369    4.24    8        3.0        0.0
  203   1  13   1 34.7    69.4     0.37     4.22    8       21.8        1.9
  204   6   0   2 34.779  69.558   0.37     4.2     4      199.2       78.2
  205   2   8   3 34.819  69.638   0.371    4.19    8       11.2        0.5
  206   6   6   1 34.835  69.67    0.371    4.18    8      167.1      109.8
  207   6   1   2 34.886  69.772   0.371    4.17    8      117.0       53.6
  208   0   9   3 34.996  69.993   0.372    4.15    4       77.2       11.6
  209   5   9   1 35.135  70.271   0.374    4.11    8       10.6        0.4
  210   7   1   0 35.161  70.321   0.374    4.11    4      138.9       37.2
  211   0   0   4 35.186  70.372   0.374    4.1     2       38.5        1.4
  212   6   2   2 35.207  70.414   0.374    4.1     8       33.2        4.3
  213   4   9   2 35.237  70.474   0.375    4.09    8       57.6       12.7
  214   3   7   3 35.266  70.532   0.375    4.08    8        0.7        0.0
  215   3  12   1 35.309  70.617   0.375    4.07    8       31.4        3.8
  216   1   9   3 35.406  70.812   0.376    4.05    8        6.0        0.1
  217   0  12   2 35.41   70.82    0.376    4.05    4       19.1        0.7
  218   5   7   2 35.506  71.011   0.377    4.03    8        0.5        0.0
  219   4   5   3 35.57   71.139   0.378    4.01    8      120.5       54.7
  220   1   0   4 35.595  71.189   0.378    4.01    4      175.0       57.6
  221   0   2   4 35.612  71.224   0.378    4.0     4       43.8        3.6
  222   1   1   4 35.701  71.401   0.379    3.98    8       91.4       31.2
  223   4  11   1 35.718  71.436   0.379    3.98    8        2.1        0.0
  224   6   3   2 35.739  71.478   0.379    3.98    8       77.0       22.1
  225   1  12   2 35.817  71.635   0.38     3.96    8      179.6      119.9
  226   0  14   0 35.909  71.818   0.381    3.94    2       75.5        5.3
  227   2  13   1 35.927  71.853   0.381    3.93    8       11.6        0.5
  228   7   3   0 36.011  72.021   0.382    3.92    4       61.9        7.1
  229   1   2   4 36.018  72.037   0.382    3.92    8        0.6        0.0
  230   6   7   1 36.217  72.435   0.384    3.87    8       51.2        9.5
  231   7   0   1 36.309  72.618   0.384    3.86    4       27.9        1.4
  232   7   1   1 36.414  72.828   0.385    3.83    8        5.5        0.1
  233   6   4   2 36.478  72.956   0.386    3.82    8       13.4        0.6
  234   1   3   4 36.545  73.091   0.387    3.81    8       33.2        3.9
  235   6   8   0 36.552  73.103   0.387    3.81    4       49.5        4.4
  236   5   0   3 36.576  73.151   0.387    3.8     4       12.8        0.3
  237   2   9   3 36.622  73.245   0.387    3.79    8       51.3        9.4
  238   3  11   2 36.628  73.256   0.387    3.79    8      125.4       56.0
  239   5   1   3 36.681  73.361   0.388    3.78    8        2.1        0.0
  240   3  13   0 36.702  73.403   0.388    3.78    4       21.2        0.8
  241   7   2   1 36.729  73.459   0.388    3.77    8       43.1        6.6
  242   4   6   3 36.731  73.461   0.388    3.77    8        6.0        0.1
  243   2   0   4 36.809  73.617   0.389    3.76    4      232.5       95.3
  244   3   8   3 36.851  73.702   0.389    3.75    8       49.2        8.5
  245   0   4   4 36.877  73.755   0.39     3.74    4       95.5       16.0
  246   4  12   0 36.896  73.791   0.39     3.74    4      146.0       37.4
  247   2   1   4 36.913  73.827   0.39     3.74    8       29.4        3.0
  248   5   2   3 36.995  73.99    0.391    3.72    8       66.0       15.2
  249   2  12   2 37.028  74.057   0.391    3.71    8      179.8      112.8
  250   5   8   2 37.087  74.173   0.391    3.7     8       19.0        1.3
  251   5  10   1 37.141  74.283   0.392    3.69    8       15.4        0.8
  252   2   2   4 37.227  74.454   0.393    3.68    8       30.9        3.3
  253   4  10   2 37.241  74.481   0.393    3.68    8       30.0        3.1
  254   7   3   1 37.252  74.505   0.393    3.67    8       23.4        1.9
  255   1   4   4 37.278  74.557   0.393    3.67    8       54.0       10.0
  256   1  10   3 37.406  74.812   0.394    3.65    8       69.8       16.7
  257   6   5   2 37.42   74.84    0.394    3.64    8       31.8        3.5
  258   5   3   3 37.517  75.034   0.395    3.63    8        3.5        0.0
  259   2  14   0 37.519  75.038   0.395    3.63    4       54.7        5.1
  260   1  14   1 37.552  75.104   0.396    3.62    8        1.5        0.0
  261   7   5   0 37.687  75.374   0.397    3.6     4        9.1        0.1
  262   2   3   4 37.748  75.495   0.397    3.59    8       28.5        2.7
  263   6   8   1 37.787  75.573   0.398    3.58    8       16.8        0.9
  264   3  13   1 37.935  75.87    0.399    3.55    8       23.2        1.8
  265   7   4   1 37.98   75.961   0.399    3.55    8        4.1        0.1
  266   4   7   3 38.085  76.171   0.4      3.53    8       60.7       12.2
  267   5  11   0 38.095  76.191   0.4      3.53    4       16.2        0.4
  268   4  12   1 38.127  76.253   0.401    3.52    8        5.9        0.1
  269   1   5   4 38.213  76.426   0.402    3.51    8        7.2        0.2
  270   5   4   3 38.243  76.486   0.402    3.5     8        4.2        0.1
  271   1  13   2 38.43   76.86    0.403    3.47    8       16.4        0.9
  272   2   4   4 38.472  76.945   0.404    3.47    8        4.7        0.1
  273   6   6   2 38.56   77.12    0.405    3.45    8       49.7        8.0
  274   2  10   3 38.599  77.197   0.405    3.45    8       11.3        0.4
  275   3   9   3 38.617  77.234   0.405    3.45    8        1.0        0.0
  276   2  14   1 38.743  77.486   0.406    3.43    8       38.4        4.8
  277   3   0   4 38.8    77.6     0.407    3.42    4        2.1        0.0
  278   5   9   2 38.849  77.698   0.407    3.41    8       47.5        7.2
  279   3   1   4 38.903  77.806   0.408    3.4     8       41.1        5.4
  280   7   5   1 38.91   77.819   0.408    3.4     8       34.7        3.8
  281   0   6   4 38.952  77.904   0.408    3.4     4       35.3        2.0
  282   3  12   2 39.016  78.032   0.409    3.39    8       15.2        0.7
  283   5   5   3 39.17   78.341   0.41     3.37    8        1.4        0.0
  284   0  11   3 39.181  78.361   0.41     3.36    4       36.4        2.1
  285   3   2   4 39.211  78.423   0.41     3.36    8       13.2        0.6
  286   5  11   1 39.314  78.628   0.411    3.35    8       13.6        0.6
  287   1  15   0 39.325  78.651   0.411    3.34    4       18.9        0.6
  288   1   6   4 39.346  78.692   0.412    3.34    8        3.6        0.0
  289   2   5   4 39.398  78.796   0.412    3.33    8       17.7        1.0
  290   4  11   2 39.411  78.823   0.412    3.33    8       84.9       22.6
  291   6   9   1 39.539  79.078   0.413    3.31    8       12.2        0.5
  292   1  11   3 39.574  79.148   0.414    3.31    8        7.6        0.2
  293   2  13   2 39.613  79.226   0.414    3.3     8       55.3        9.5
  294   4   8   3 39.629  79.258   0.414    3.3     8        0.9        0.0
  295   3   3   4 39.724  79.447   0.415    3.29    8       15.5        0.7
  296   6   7   2 39.894  79.789   0.416    3.27    8        2.6        0.0
  297   7   0   2 39.983  79.966   0.417    3.26    4       39.2        2.3
  298   7   6   1 40.037  80.073   0.418    3.25    8       78.1       18.6
  299   7   1   2 40.085  80.17    0.418    3.24    8       31.8        3.1
  300   0  15   1 40.143  80.285   0.418    3.24    4       27.8        1.2
  301   7   7   0 40.157  80.313   0.419    3.24    4       45.0        3.1
  302   6  10   0 40.272  80.544   0.42     3.22    4       28.6        1.2
  303   5   6   3 40.295  80.591   0.42     3.22    8        8.6        0.2
  304   7   2   2 40.391  80.782   0.421    3.21    8        4.3        0.1
  305   3   4   4 40.438  80.876   0.421    3.2     8       34.0        3.5
  306   2   6   4 40.521  81.043   0.422    3.19    8       21.7        1.4
  307   1  15   1 40.533  81.067   0.422    3.19    8       60.0       10.8
  308   3  10   3 40.563  81.125   0.422    3.19    8       13.5        0.5
  309   1   7   4 40.673  81.347   0.423    3.17    8       14.1        0.6
  310   4  13   1 40.69   81.38    0.423    3.17    8       11.7        0.4
  311   3  14   1 40.705  81.41    0.423    3.17    8       22.6        1.5
  312   2  11   3 40.748  81.496   0.424    3.17    8       19.7        1.2
  313   5  10   2 40.792  81.583   0.424    3.16    8        3.1        0.0
  314   0  14   2 40.802  81.604   0.424    3.16    4       42.3        2.7
  315   7   3   2 40.9    81.799   0.425    3.15    8       21.8        1.4
  316   6   0   3 40.926  81.852   0.425    3.15    4       10.4        0.2
  317   8   0   0 41.026  82.051   0.426    3.14    2      171.7       21.7
  318   6   1   3 41.027  82.055   0.426    3.14    8       17.7        0.9
  319   1  14   2 41.191  82.383   0.427    3.12    8        0.2        0.0
  320   6   2   3 41.332  82.663   0.429    3.1     8       13.3        0.5
  321   3   5   4 41.352  82.705   0.429    3.1     8       24.9        1.8
  322   7   7   1 41.359  82.718   0.429    3.1     8       13.8        0.6
  323   4   9   3 41.36   82.72    0.429    3.1     8       10.3        0.3
  324   6   8   2 41.42   82.841   0.429    3.09    8       20.7        1.2
  325   8   2   0 41.431  82.863   0.43     3.09    4       28.9        1.2
  326   6  10   1 41.474  82.947   0.43     3.09    8       32.9        3.1
  327   4   0   4 41.54   83.08    0.43     3.08    4      165.5       39.6
  328   3  13   2 41.565  83.13    0.431    3.08    8       42.9        5.3
  329   7   4   2 41.61   83.219   0.431    3.08    8        3.0        0.0
  330   5   7   3 41.616  83.232   0.431    3.07    8        0.6        0.0
  331   4   1   4 41.641  83.283   0.431    3.07    8       74.0       15.8
  332   5  12   1 41.656  83.313   0.431    3.07    8       30.0        2.6
  333   2  15   1 41.701  83.403   0.432    3.07    8       26.6        2.0
  334   4  12   2 41.753  83.505   0.432    3.06    8      140.1       56.4
  335   0   8   4 41.806  83.611   0.433    3.06    4       18.9        0.5
  336   6   3   3 41.838  83.676   0.433    3.05    8       47.6        6.5
  337   2   7   4 41.84   83.681   0.433    3.05    8       14.7        0.6
  338   1  12   3 41.913  83.826   0.434    3.05    8       31.3        2.8
  339   4   2   4 41.945  83.89    0.434    3.04    8       22.1        1.4
  340   0  16   0 42.089  84.178   0.435    3.03    2       44.2        1.4
  341   1   8   4 42.194  84.387   0.436    3.02    8        5.4        0.1
  342   8   0   1 42.223  84.446   0.436    3.02    4        8.5        0.1
  343   4  14   0 42.228  84.456   0.436    3.02    4       20.2        0.6
  344   8   1   1 42.324  84.648   0.437    3.01    8        8.3        0.2
  345   2  14   2 42.356  84.712   0.437    3.01    8       41.5        4.9
  346   3  15   0 42.445  84.89    0.438    3.0     4        9.0        0.1
  347   4   3   4 42.45   84.9     0.438    3.0     8       41.1        4.8
  348   3   6   4 42.465  84.93    0.438    3.0     8        1.6        0.0
  349   7   5   2 42.519  85.039   0.439    2.99    8       27.7        2.2
  350   6   4   3 42.545  85.091   0.439    2.99    8        8.0        0.2
  351   8   2   1 42.627  85.254   0.44     2.98    8       37.1        3.9
  352   8   4   0 42.644  85.289   0.44     2.98    4       51.0        3.6
  353   3  11   3 42.69   85.379   0.44     2.98    8        5.0        0.1
  354   7   8   1 42.875  85.75    0.442    2.96    8       41.2        4.7
  355   5  11   2 42.917  85.833   0.442    2.96    8      183.2       93.3
  356   5  13   0 42.987  85.974   0.443    2.96    4       76.4        8.1
  357   2  12   3 43.075  86.149   0.443    2.95    8        3.0        0.0
  358   5   8   3 43.131  86.261   0.444    2.94    8       27.2        2.0
  359   8   3   1 43.131  86.262   0.444    2.94    8       37.0        3.8
  360   6   9   2 43.138  86.276   0.444    2.94    8       42.2        4.9
  361   4   4   4 43.156  86.312   0.444    2.94    8       21.1        1.2
  362   4  10   3 43.279  86.559   0.445    2.93    8        2.1        0.0
  363   2   8   4 43.354  86.709   0.446    2.93    8       10.0        0.3
  364   7   9   0 43.396  86.793   0.446    2.92    4      104.5       15.0
  365   4  14   1 43.42   86.841   0.446    2.92    8       39.9        4.4
  366   6   5   3 43.453  86.905   0.446    2.92    8       76.3       16.0
  367   6  11   1 43.594  87.187   0.448    2.91    8        7.1        0.1
  368   7   6   2 43.628  87.256   0.448    2.91    8       37.5        3.8
  369   2  16   0 43.636  87.272   0.448    2.91    4       70.2        6.7
  370   3  15   1 43.637  87.273   0.448    2.91    8       19.1        1.0
  371   1  16   1 43.668  87.336   0.448    2.91    8       50.5        6.9
  372   3   7   4 43.775  87.55    0.449    2.9     8       11.4        0.4
  373   8   4   1 43.836  87.672   0.45     2.89    8       10.6        0.3
  374   1   9   4 43.907  87.814   0.45     2.89    8       14.7        0.6
  375   0  13   3 44.047  88.094   0.451    2.88    4       21.8        0.6
  376   4   5   4 44.062  88.124   0.451    2.88    8       19.7        1.0
  377   1  15   2 44.118  88.237   0.452    2.88    8        7.3        0.1
  378   5  13   1 44.178  88.355   0.452    2.87    8       10.5        0.3
  379   4  13   2 44.273  88.547   0.453    2.87    8       76.0       15.6
  380   3  14   2 44.288  88.577   0.453    2.87    8       10.1        0.3
  381   1  13   3 44.433  88.866   0.454    2.86    8        4.7        0.1
  382   6   6   3 44.559  89.119   0.455    2.85    8        4.8        0.1
  383   7   9   1 44.586  89.173   0.456    2.85    8       25.9        1.8
  384   8   6   0 44.658  89.316   0.456    2.85    4       54.5        4.0
  385   6  12   0 44.718  89.436   0.457    2.84    4       72.0        6.9
  386   8   5   1 44.741  89.482   0.457    2.84    8       94.8       24.0
  387   2  16   1 44.826  89.652   0.458    2.84    8       23.5        1.5
  388   5   9   3 44.841  89.683   0.458    2.84    8        1.1        0.0
  389   7   7   2 44.936  89.872   0.458    2.83    8        5.4        0.1


  X-ray diffraction powder data (I)...X-Ray wave length =  1.54056 (angs.):

  No   H   K   L   Theta 2*Theta    d           I int   I int.n.  I p.h.n.   H(Si)
                    ( degree )   (angstrem)     *100                         *100

    1   0   2   0   4.806   9.612  9.1935       313.4     14.5     14.5     5.6
    2   1   1   0   5.286  10.572  8.36121     2168.1    100.0    100.0     5.6
    3   0   1   1   8.628  17.257  5.13431       67.2      3.1      3.1     5.6
    4   2   0   0   9.445  18.89   4.694        193.2      8.9      8.9     5.6
    5   1   0   1   9.543  19.086  4.64624       61.9      2.9      2.8     5.6
    6   0   4   0   9.647  19.293  4.59675      130.7      6.0      6.0     5.6
    7   1   1   1   9.846  19.692  4.50465      125.9      5.8      5.8     5.6
    8   2   2   0  10.617  21.235  4.1806       135.9      6.3      6.2     5.6
    9   0   3   1  11.021  22.043  4.0292        27.1      1.3      1.2     5.6
   10   1   3   1  12.007  24.015  3.70259      501.3     23.1     22.9     5.6
   11   1   5   0  13.001  26.001  3.42408       27.1      1.2      1.2     5.6
   12   2   2   1  13.526  27.052  3.29344      198.7      9.2      9.1     5.6
   13   2   4   0  13.564  27.129  3.28424      396.0     18.3     18.1     5.6
   14   3   1   0  14.459  28.918  3.08497      905.9     41.8     41.3     5.6
   15   2   3   1  14.593  29.185  3.05734      198.4      9.1      9.0     5.6
   16   0   5   1  14.727  29.455  3.02998      100.2      4.6      4.6     5.6
   17   1   5   1  15.494  30.987  2.88351      470.1     21.7     21.4     5.6
   18   3   3   0  16.044  32.088  2.78707      137.9      6.4      6.3     5.6
   19   0   0   2  16.745  33.49   2.6735        99.3      4.6      4.5     5.7
   20   3   2   1  17.293  34.586  2.59129       99.1      4.6      4.5     5.7
   21   1   0   2  17.432  34.864  2.57127      275.7     12.7     12.5     5.7
   22   2   6   0  17.468  34.937  2.56606       35.8      1.7      1.6     5.7
   23   1   6   1  17.524  35.048  2.55817      800.1     36.9     36.3     5.7
   24   2   5   1  17.613  35.226  2.54569     1117.4     51.5     50.6     5.7
   25   4   0   0  19.159  38.319  2.347         41.7      1.9      1.9     5.7
   26   2   0   2  19.364  38.728  2.32312      628.7     29.0     28.4     5.7
   27   2   6   1  19.448  38.897  2.31345       92.2      4.3      4.2     5.7
   28   2   1   2  19.524  39.049  2.3048        45.6      2.1      2.1     5.7
   29   1   7   1  19.686  39.372  2.2866       116.1      5.4      5.2     5.7
   30   2   7   1  21.446  42.891  2.10679      112.6      5.2      5.1     5.7
   31   4   2   1  21.598  43.195  2.09267       43.9      2.0      2.0     5.7
   32   1   8   1  21.957  43.913  2.0601        50.4      2.3      2.3     5.7
   33   3   6   1  22.344  44.687  2.0262       475.9     22.0     21.4     5.7
   34   3   1   2  22.411  44.823  2.02038      136.7      6.3      6.1     5.7
   35   2   5   2  23.091  46.182  1.96404       26.5      1.2      1.2     5.7
   36   1   9   1  24.323  48.645  1.87019       46.5      2.1      2.1     5.7
   37   3   4   2  24.478  48.956  1.85904       42.0      1.9      1.9     5.7
   38   4   5   1  24.528  49.056  1.85547      248.3     11.5     11.1     5.7
   39   4   0   2  25.895  51.79   1.76378      198.8      9.2      8.8     5.8
   40   4   6   1  25.962  51.924  1.75954       78.9      3.6      3.5     5.8
   41   4   1   2  26.023  52.045  1.75572       29.1      1.3      1.3     5.8
   42   3   8   1  26.108  52.217  1.75036       33.8      1.6      1.5     5.8
   43   4   2   2  26.403  52.806  1.73219       24.6      1.1      1.1     5.8
   44   1   2   3  26.603  53.206  1.72013       24.5      1.1      1.1     5.8
   45   1   8   2  26.713  53.425  1.71358       60.8      2.8      2.7     5.8
   46   0   3   3  26.749  53.497  1.71144       60.8      2.8      2.7     5.8
   47   1  11   0  27.909  55.818  1.64566      232.4     10.7     10.3     5.8
   48   4   8   0  27.974  55.949  1.64212       23.0      1.1      1.0     5.8
   49   2  10   1  28.191  56.383  1.6305        23.4      1.1      1.0     5.8
   50   0   5   3  28.702  57.405  1.60388      245.2     11.3     10.8     5.8
   51   6   0   0  29.492  58.983  1.56467       73.9      3.4      3.3     5.8
   52   5   6   1  30.148  60.295  1.53372      436.5     20.1     19.2     5.8
   53   0  12   0  30.18   60.359  1.53225      265.3     12.2     11.7     5.8
   54   1   6   3  30.44   60.881  1.52036      306.2     14.1     13.5     5.8
   55   2   5   3  30.499  60.998  1.51773       31.2      1.4      1.4     5.8
   56   3  11   0  31.496  62.992  1.47439      112.2      5.2      4.9     5.9
   57   5   4   2  31.909  63.819  1.45727       34.7      1.6      1.5     5.9
   58   1  11   2  33.342  66.684  1.40144       96.2      4.4      4.2     5.9
   59   6   5   1  33.646  67.292  1.39024       89.8      4.1      3.9     5.9
   60   3   6   3  33.867  67.734  1.38225      155.2      7.2      6.7     5.9
   61   6   0   2  34.779  69.558  1.3504        78.2      3.6      3.4     5.9
   62   6   6   1  34.835  69.67   1.34849      109.8      5.1      4.8     5.9
   63   6   1   2  34.886  69.772  1.34677       53.6      2.5      2.3     5.9
   64   7   1   0  35.161  70.321  1.33759       38.6      1.8      1.7     5.9
   65   1   0   4  35.595  71.189  1.3234       115.9      5.3      5.0     5.9
   66   1   1   4  35.701  71.401  1.31999       31.2      1.4      1.3     5.9
   67   6   3   2  35.739  71.478  1.31877       22.1      1.0      1.0     5.9
   68   1  12   2  35.817  71.635  1.31626      119.9      5.5      5.2     5.9
   69   3  11   2  36.628  73.256  1.29107       65.3      3.0      2.8     6.0
   70   2   0   4  36.809  73.617  1.28563       95.3      4.4      4.1     6.0
   71   4  12   0  36.896  73.791  1.28303       65.0      3.0      2.8     6.0
   72   2  12   2  37.028  74.057  1.27909      112.8      5.2      4.8     6.0
   73   4  11   2  39.411  78.823  1.21326       22.6      1.0      1.0     6.0
   74   8   0   0  41.026  82.051  1.1735        22.6      1.0      1.0     6.1
   75   4   0   4  41.54   83.08   1.16156       44.9      2.1      1.9     6.1
   76   4  12   2  41.753  83.505  1.15672       56.4      2.6      2.4     6.1
   77   5  11   2  42.917  85.833  1.13121       93.3      4.3      3.9     6.1
   78   8   5   1  44.741  89.482  1.0943        30.9      1.4      1.3     6.2

Reference:
Chichagov A.V. et al.
Information-Calculating System on Crystal Structure Data of Minerals
(MINCRYST)
- Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian)