Institute of Experimental Mineralogy
                 Russian Academy of Sciences
     -------------------------------------------------
           142432, Chernogolovka, Moscow district
             A.V. Chichagov  +7(496)52-22320

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          ***      W W W - X R A Y P O L       ***
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PAVONITE

7, t-pavonite, analogue, at 323'K, DN

Cu(1.4)Ag(0.4)Bi(5.4)Se(9)


Monoclinic  C 2/m  Z = 2

R =0.037          NR =1004

3 .8 .23

Ref.Str.:

         Fraunhofer Ch., Paul Th., Oeckler O. (2022)

         * Dalton Transactions, doi:10.1039/D2DT01651F

         L: $Ag0.8 Bi10.8 Cu2.8 Se18$

         R: Structure data for this sample at all temperatures

         from 323'K up to 523'K see in the original. N.A.D.

                   Initial data from BDM-file 

   Lattice parameters (cub. angs.,degr.):

             a =  13.6967   alpha =   90.0 
             b =   4.1815   beta  =   99.5 
             c =  15.2646   gamma =   90.0 

    Unit cell volume (cub. angs.) =   862.25

    Molar volume ( cub.cm/mol.) =   259.68

  Co-ordinates, thermal parameters, occupation for atomic positions:

NoP   x/a     y/b     z/c    B(j)   atom  / occupation

   1 0.244   0.0     0.6222   0.0    Bi    = 1.00
   2 0.4513  0.0     0.1898   0.0    Bi    = 0.94, Bi    = 0.0 
   3 0.1517  0.0     0.0625   0.0    Bi    = 0.76, Ag    = 0.2 
   4 0.244   0.0     0.6222   0.0    Bi    = 1.00
   5 0.4025  0.0     0.3604   0.0    Se    = 1.00
   6 0.794   0.0     0.1247   0.0    Se    = 1.00
   7 0.1383  0.0     0.4551   0.0    Se    = 1.00
   8 0.095   0.0     0.2297   0.0    Se    = 1.00
   9 0.0     0.5     0.0      0.0    Se    = 1.00
  10 0.0231  0.0     0.56     0.0    Cu    = 0.08, Cu    = 0.0 
  11 0.4646  0.0     0.5227   0.0    Cu    = 0.24, Cu    = 0.0 
  12 0.0     0.3278  0.5      0.0    Cu    = 0.32, Cu    = 0.0 
  13 0.5024  0.0     0.2355   0.0    Cu    = 0.5 , Cu    = 0.0 


  Co-ordinates for all atomic positions :

   No       NoP      x/a        y/b       z/c 

     1       1     0.244      0.0        0.6222
     2       2     0.4513     0.0        0.1898
     3       3     0.1517     0.0        0.0625
     4       4     0.244      0.0        0.6222
     5       5     0.4025     0.0        0.3604
     6       6     0.794      0.0        0.1247
     7       7     0.1383     0.0        0.4551
     8       8     0.095      0.0        0.2297
     9       9     0.0        0.5        0.0   
    10      10     0.0231     0.0        0.56  
    11      11     0.4646     0.0        0.5227
    12      12     0.0        0.3278     0.5   
    13      13     0.5024     0.0        0.2355
    14       1     0.756      0.0        0.3778
    15       2     0.5487     0.0        0.8102
    16       3     0.8483     0.0        0.9375
    17       4     0.756      0.0        0.3778
    18       5     0.5975     0.0        0.6396
    19       6     0.206      0.0        0.8753
    20       7     0.8617     0.0        0.5449
    21       8     0.905      0.0        0.7703
    22      10     0.9769     0.0        0.44  
    23      11     0.5354     0.0        0.4773
    24      12     0.0        0.6722     0.5   
    25      13     0.4976     0.0        0.7645
    26       1     0.744      0.5        0.6222
    27       2     0.9513     0.5        0.1898
    28       3     0.6517     0.5        0.0625
    29       4     0.744      0.5        0.6222
    30       5     0.9025     0.5        0.3604
    31       6     0.294      0.5        0.1247
    32       7     0.6383     0.5        0.4551
    33       8     0.595      0.5        0.2297
    34       9     0.5        0.0        0.0   
    35      10     0.5231     0.5        0.56  
    36      11     0.9646     0.5        0.5227
    37      12     0.5        0.1722     0.5   
    38      13     0.0024     0.5        0.2355
    39       1     0.256      0.5        0.3778
    40       2     0.0487     0.5        0.8102
    41       3     0.3483     0.5        0.9375
    42       4     0.256      0.5        0.3778
    43       5     0.0975     0.5        0.6396
    44       6     0.706      0.5        0.8753
    45       7     0.3617     0.5        0.5449
    46       8     0.405      0.5        0.7703
    47      10     0.4769     0.5        0.44  
    48      11     0.0354     0.5        0.4773
    49      12     0.5        0.8278     0.5   
    50      13     0.9976     0.5        0.7645


X-ray density (g/cm cub.)   =      9.42

MU (1/cm) =    1744.958    Mass attenuation coefficient (cm**2/g) =    185.316

 Selected interatomic distances (cation-anion,anion-anion):

 NoP    Atom              Rad.sph.      C.N.    Distance     NoP N.
                           (angs.)               (angs.)

    1    Bi                  3.756        7
                                                 2.7181       7
                                                 2.9404       5
                                                 2.9404       5
                                                 2.9983       7
                                                 2.9983       7
                                                 3.5627       8
                                                 3.5627       8
    2   Bi   ,Bi             3.756        6
                                                 2.793        5
                                                 3.049        6
                                                 3.049        6
                                                 2.8675       8
                                                 2.8675       8
                                                 3.0785       9
    3   Bi   ,Ag             3.756        6
                                                 2.7875       8
                                                 2.9909       9
                                                 2.9909       9
                                                 3.0698       6
                                                 2.9081       6
                                                 2.9081       6
    4    Bi                  3.756        7
                                                 2.7181       7
                                                 2.9404       5
                                                 2.9404       5
                                                 2.9983       7
                                                 2.9983       7
                                                 3.5627       8
                                                 3.5627       8
    5    Se                  4.632       12
                                                 4.1815       5
                                                 4.1815       5
                                                 4.1127       7
                                                 4.3521       8
                                                 4.2142       6
                                                 4.2142       6
                                                 3.9175       7
                                                 3.9175       7
                                                 4.1278       8
                                                 4.1278       8
                                                 3.6248       7
                                                 3.6248       7
    6    Se                  4.632       12
                                                 4.1815       6
                                                 4.1815       6
                                                 4.1707       8
                                                 4.2109       9
                                                 4.2109       9
                                                 4.2142       5
                                                 4.2142       5
                                                 3.9756       8
                                                 3.9756       8
                                                 4.1598       9
                                                 4.3359       6
                                                 4.3359       6
    7    Se                  4.632       11
                                                 4.1127       5
                                                 4.1815       7
                                                 4.1815       7
                                                 3.3927       8
                                                 4.2365       7
                                                 3.9175       5
                                                 3.9175       5
                                                 3.6248       5
                                                 3.6248       5
                                                 3.7725       7
                                                 3.7725       7
    8    Se                  4.632       11
                                                 4.3521       5
                                                 4.1707       6
                                                 3.3927       7
                                                 4.1815       8
                                                 4.1815       8
                                                 4.1055       9
                                                 4.1055       9
                                                 4.1278       5
                                                 4.1278       5
                                                 3.9756       6
                                                 3.9756       6
    9    Se                  4.632       12
                                                 4.2109       6
                                                 4.2109       6
                                                 4.1055       8
                                                 4.1055       8
                                                 4.1815       9
                                                 4.1815       9
                                                 4.2109       6
                                                 4.2109       6
                                                 4.1055       8
                                                 4.1055       8
                                                 4.1598       6
                                                 4.1598       6
   10   Cu   ,Cu             3.492        4
                                                 2.4276       7
                                                 2.1838       7
                                                 2.545        5
                                                 2.545        5
   11   Cu   ,Cu             3.492        6
                                                 2.4837       5
                                                 2.329        5
                                                 3.4513       7
                                                 3.4513       7
                                                 2.5746       7
                                                 2.5746       7
   12   Cu   ,Cu             3.492        4
                                                 2.5229       7
                                                 2.5229       7
                                                 2.4298       5
                                                 2.4298       5
   13   Cu   ,Cu             3.492        3
                                                 2.5233       5
                                                 2.4546       8
                                                 2.4546       8

  X-ray diffraction powder data (II),  X-Ray W.L. =   1.54056(angs.):

  No   H   K   L   Theta 2*Theta    S       LPG   MF        F          I int.
                    ( degree )                                         *100

    1   0   0   1  2.933   5.865   0.033  761.03    2      184.9     7001.5
    2   0   0   2  5.873  11.746   0.066  188.03    2       38.9       76.7
    3   2   0   0  6.548  13.097   0.074  150.82    2      316.4     4061.0
    4   2   0  -1  6.721  13.442   0.076  143.06    2      293.0     3302.9
    5   2   0   1  7.613  15.225   0.086  111.01    2      434.1     5627.8
    6   2   0  -2  8.053  16.106   0.091   98.97    2      125.9      422.3
    7   0   0   3  8.829  17.659   0.1     81.96    2      124.1      339.6
    8   2   0   2  9.515  19.031   0.107   70.26    2      360.5     2456.1
    9   2   0  -3 10.105  20.211   0.114   62.05    2      386.7     2496.2
   10   1   1   0 11.118  22.237   0.125   50.89    4      121.3      402.6
   11   1   1  -1 11.366  22.732   0.128   48.6     4      168.1      738.7
   12   1   1   1 11.648  23.297   0.131   46.17    4      196.9      963.1
   13   0   0   4 11.809  23.619   0.133   44.87    2      468.4     2648.1
   14   2   0   3 11.875  23.75    0.134   44.35    2      658.5     5172.8
   15   1   1  -2 12.348  24.696   0.139   40.86    4      791.0    13755.6
   16   2   0  -4 12.546  25.091   0.141   39.52    2     1007.4    10788.7
   17   1   1   2 12.866  25.732   0.145   37.48    4      320.7     2073.8
   18   4   0  -1 13.024  26.048   0.146   36.52    2      491.9     2377.2
   19   4   0   0 13.184  26.368   0.148   35.59    2      382.5     1401.1
   20   4   0  -2 13.537  27.073   0.152   33.66    2      265.7      639.2
   21   1   1  -3 13.918  27.836   0.156   31.73    4      205.7      722.4
   22   4   0   1 13.996  27.992   0.157   31.36    2      202.2      344.9
   23   2   0   4 14.489  28.977   0.162   29.13    2      608.3     2899.0
   24   3   1  -1 14.528  29.055   0.163   28.96    4      599.4     5598.6
   25   3   1   0 14.56   29.119   0.163   28.83    4      750.6     8737.1
   26   1   1   3 14.611  29.222   0.164   28.61    4      398.4     2442.8
   27   4   0  -3 14.657  29.314   0.164   28.42    2      161.2      198.7
   28   0   0   5 14.822  29.644   0.166   27.75    2      606.1     2742.1
   29   3   1  -2 15.103  30.206   0.169   26.65    4      527.5     3990.3
   30   3   1   1 15.195  30.391   0.17    26.31    4     1085.2    16666.6
   31   2   0  -5 15.208  30.417   0.17    26.26    2      562.8     2237.1
   32   4   0   2 15.364  30.728   0.172   25.69    2       34.9        8.4
   33   1   1  -4 15.918  31.835   0.178   23.8     4       69.7       62.1
   34   3   1  -3 16.227  32.454   0.181   22.83    4      560.5     3858.8
   35   4   0  -4 16.27   32.541   0.182   22.7     2      413.4     1043.5
   36   3   1   2 16.371  32.743   0.183   22.4     4      230.5      640.3
   37   1   1   4 16.736  33.472   0.187   21.36    4       78.7       71.2
   38   4   0   3 17.169  34.338   0.192   20.2     2      221.8      267.4
   39   2   0   5 17.264  34.529   0.193   19.96    2      641.5     2209.1
   40   3   1  -4 17.807  35.614   0.199   18.65    4      299.6      901.0
   41   0   0   6 17.877  35.755   0.199   18.49    2       40.3        8.1
   42   3   1   3 17.993  35.987   0.201   18.23    4      254.3      634.5
   43   2   0  -6 18.019  36.038   0.201   18.18    2      218.6      233.6
   44   1   1  -5 18.225  36.45    0.203   17.73    4      312.4      931.0
   45   4   0  -5 18.263  36.525   0.203   17.65    2      410.7      800.6
   46   1   1   5 19.134  38.269   0.213   15.92    4      910.0     7094.3
   47   4   0   4 19.307  38.614   0.215   15.61    2      495.2     1029.9
   48   5   1  -1 19.645  39.289   0.218   15.02    4      306.5      759.1
   49   6   0  -1 19.723  39.446   0.219   14.89    2       93.3       34.8
   50   3   1  -5 19.75   39.501   0.219   14.84    4      433.5     1501.0
   51   5   1   0 19.843  39.685   0.22    14.69    4       47.3       17.6
   52   6   0  -2 19.909  39.819   0.221   14.58    2      105.0       43.3
   53   5   1  -2 19.918  39.836   0.221   14.57    4      586.1     2692.8
   54   3   1   4 19.97   39.939   0.222   14.48    4      133.0      137.8
   55   6   0   0 20.006  40.013   0.222   14.43    2      357.1      494.9
   56   2   0   6 20.162  40.324   0.224   14.18    2      335.8      430.1
   57   5   1   1 20.5    41.001   0.227   13.66    4      165.3      200.9
   58   4   0  -6 20.544  41.087   0.228   13.6     2       74.0       20.0
   59   6   0  -3 20.555  41.109   0.228   13.58    2      447.4      731.5
   60   5   1  -3 20.647  41.293   0.229   13.45    4      637.8     2943.1
   61   6   0   1 20.743  41.487   0.23    13.31    2      950.5     3234.2
   62   1   1  -6 20.761  41.521   0.23    13.28    4      599.3     2566.3
   63   2   0  -7 20.945  41.891   0.232   13.02    2      222.9      174.0
   64   0   0   7 20.986  41.973   0.232   12.97    2      703.5     1726.4
   65   5   1   2 21.584  43.167   0.239   12.17    4      491.0     1579.0
   66   0   2   0 21.618  43.237   0.239   12.13    2     1450.3     6863.4
   67   6   0  -4 21.625  43.25    0.239   12.12    2      844.9     2327.7
   68   4   0   5 21.701  43.402   0.24    12.03    2      539.7      942.2
   69   1   1   6 21.741  43.482   0.24    11.98    4      180.4      209.8
   70   5   1  -4 21.794  43.587   0.241   11.91    4      814.1     4248.0
   71   0   2   1 21.836  43.673   0.241   11.86    4      104.4       69.5
   72   6   0   2 21.896  43.793   0.242   11.79    2      578.0     1059.4
   73   3   1  -6 21.981  43.962   0.243   11.69    4      779.5     3819.8
   74   3   1   5 22.226  44.453   0.246   11.4     4      264.3      428.3
   75   0   2   2 22.481  44.961   0.248   11.11    4       15.0        1.3
   76   2   2   0 22.685  45.371   0.25    10.88    4      298.6      522.1
   77   2   2  -1 22.741  45.482   0.251   10.82    4      281.0      459.9
   78   5   1   3 23.044  46.088   0.254   10.5     4      883.5     4411.0
   79   2   2   1 23.049  46.098   0.254   10.5     4      399.6      901.8
   80   4   0  -7 23.052  46.104   0.254   10.5     2      480.1      650.8
   81   6   0  -5 23.074  46.148   0.254   10.47    2      594.5      995.9
   82   2   0   7 23.166  46.331   0.255   10.38    2       67.4       12.7
   83   2   2  -2 23.213  46.427   0.256   10.33    4      148.2      122.0
   84   5   1  -5 23.31   46.62    0.257   10.23    4      126.6       88.2
   85   6   0   3 23.417  46.834   0.258   10.13    2      108.1       31.8
   86   1   1  -7 23.477  46.955   0.259   10.07    4      643.6     2243.8
   87   0   2   3 23.523  47.046   0.259   10.03    4      145.7      114.5
   88   2   2   2 23.817  47.633   0.262    9.75    4      340.0      606.2
   89   2   0  -8 23.976  47.953   0.264    9.6     2      598.5      925.0
   90   2   2  -3 24.084  48.167   0.265    9.5     4      282.4      407.9
   91   0   0   8 24.161  48.323   0.266    9.43    2      305.2      236.4
   92   4   0   6 24.302  48.605   0.267    9.31    2      433.0      469.6
   93   3   1  -7 24.444  48.889   0.269    9.19    4       76.0       28.6
   94   1   1   7 24.517  49.034   0.269    9.13    4      543.2     1448.6
   95   3   1   6 24.712  49.424   0.271    8.96    4      632.2     1927.5
   96   5   1   4 24.832  49.664   0.273    8.87    4      160.7      123.2
   97   6   0  -6 24.851  49.701   0.273    8.85    2      236.0      132.5
   98   0   2   4 24.926  49.852   0.274    8.79    4      433.5      888.5
   99   2   2   3 24.961  49.921   0.274    8.76    4      520.9     1278.8
  100   5   1  -6 25.146  50.292   0.276    8.62    4      241.4      270.1
  101   6   0   4 25.256  50.513   0.277    8.53    2      374.7      322.1
  102   2   2  -4 25.321  50.642   0.278    8.48    4      809.7     2991.0
  103   4   2  -1 25.587  51.174   0.28     8.28    4      384.7      659.2
  104   4   2   0 25.678  51.356   0.281    8.21    4      290.5      372.9
  105   4   0  -8 25.75   51.499   0.282    8.16    2      688.7     1041.5
  106   7   1  -1 25.778  51.556   0.282    8.14    4      430.4      811.6
  107   7   1  -2 25.859  51.718   0.283    8.08    4       81.4       28.8
  108   4   2  -2 25.88   51.76    0.283    8.07    4      276.7      332.4
  109   7   1   0 26.078  52.157   0.285    7.93    4       84.6       30.5
  110   4   2   1 26.149  52.299   0.286    7.88    4      135.1       77.4
  111   2   0   8 26.274  52.548   0.287    7.8     2      415.2      361.5
  112   7   1  -3 26.32   52.639   0.288    7.77    4      226.4      214.1
  113   1   1  -8 26.351  52.701   0.288    7.74    4      224.6      210.2
  114   2   2   4 26.445  52.89    0.289    7.68    4      469.4      910.5
  115   4   2  -3 26.548  53.096   0.29     7.61    4      180.7      133.7
  116   0   2   5 26.649  53.299   0.291    7.55    4      559.1     1269.5
  117   7   1   1 26.751  53.503   0.292    7.48    4      246.4      244.3
  118   8   0  -1 26.779  53.558   0.292    7.46    2      341.5      234.2
  119   8   0  -2 26.79   53.58    0.293    7.46    2       88.5       15.7
  120   2   2  -5 26.89   53.779   0.294    7.4     4      508.7     1029.7
  121   5   1   5 26.903  53.806   0.294    7.39    4       23.7        2.2
  122   6   0  -7 26.912  53.824   0.294    7.38    2      181.1       65.1
  123   4   2   2 26.988  53.975   0.295    7.33    4        8.0        0.3
  124   4   0   7 27.081  54.163   0.296    7.28    2      324.4      206.0
  125   3   1  -8 27.107  54.213   0.296    7.26    4       49.3        9.5
  126   2   0  -9 27.113  54.226   0.296    7.26    2      407.8      324.6
  127   8   0   0 27.14   54.28    0.296    7.24    2      473.1      436.0
  128   7   1  -4 27.146  54.291   0.296    7.24    4       18.0        1.3
  129   8   0  -3 27.171  54.342   0.296    7.22    2     1040.0     2101.4
  130   5   1  -7 27.259  54.518   0.297    7.17    4      356.7      490.8
  131   6   0   5 27.372  54.744   0.298    7.1     2      472.2      426.0
  132   3   1   7 27.393  54.787   0.299    7.09    4      462.8      816.8
  133   0   0   9 27.418  54.835   0.299    7.08    2      342.5      223.3
  134   1   1   8 27.445  54.89    0.299    7.06    4      172.5      113.1
  135   4   2  -4 27.571  55.142   0.3      6.99    4      394.8      585.7
  136   7   1   2 27.778  55.557   0.303    6.87    4      356.0      468.4
  137   8   0   1 27.862  55.724   0.303    6.82    2      518.9      494.1
  138   8   0  -4 27.913  55.827   0.304    6.79    2       74.8       10.2
  139   4   2   3 28.17   56.341   0.306    6.65    4      230.1      189.5
  140   2   2   5 28.235  56.47    0.307    6.62    4      509.7      925.1
  141   7   1  -5 28.315  56.631   0.308    6.58    4      343.4      417.3
  142   4   0  -9 28.616  57.233   0.311    6.42    2       14.4        0.4
  143   0   2   6 28.656  57.313   0.311    6.4     4       76.2       20.0
  144   2   2  -6 28.755  57.51    0.312    6.35    4      147.9       74.8
  145   4   2  -5 28.925  57.851   0.314    6.27    4      399.6      538.3
  146   8   0   2 28.927  57.855   0.314    6.27    2      402.8      273.4
  147   8   0  -5 28.998  57.995   0.315    6.23    2      230.3       88.9
  148   7   1   3 29.135  58.269   0.316    6.17    4      391.6      508.6
  149   5   1   6 29.223  58.446   0.317    6.12    4      348.2      399.6
  150   6   0  -8 29.223  58.447   0.317    6.12    2      512.0      431.8
  151   1   1  -9 29.371  58.742   0.318    6.05    4      331.9      358.9
  152   2   0   9 29.493  58.986   0.32     6.0     2      386.7      241.3
  153   5   1  -8 29.617  59.233   0.321    5.94    4       91.3       26.7
  154   4   2   4 29.671  59.343   0.321    5.92    4      473.9      714.9
  155   6   0   6 29.732  59.464   0.322    5.89    2      105.3       17.6
  156   7   1  -6 29.804  59.607   0.323    5.86    4      541.0      922.6
  157   3   1  -9 29.949  59.898   0.324    5.8     4      323.2      325.8
  158   6   2  -1 29.975  59.95    0.324    5.78    4      122.6       46.8
  159   4   0   8 30.025  60.05    0.325    5.76    2      602.1      562.0
  160   6   2  -2 30.112  60.224   0.326    5.73    4       49.4        7.5
  161   6   2   0 30.184  60.368   0.326    5.7     4      352.8      381.3
  162   3   1   8 30.254  60.507   0.327    5.67    4      264.1      212.6
  163   2   2   6 30.299  60.598   0.327    5.65    4      252.5      193.7
  164   8   0   3 30.314  60.628   0.328    5.64    2       77.2        9.0
  165   2   0 -10 30.364  60.727   0.328    5.62    2      149.0       33.6
  166   8   0  -6 30.402  60.803   0.328    5.6     2      107.1       17.3
  167   1   1   9 30.519  61.038   0.33     5.56    4      349.5      365.2
  168   4   2  -6 30.584  61.168   0.33     5.53    4      106.1       33.5
  169   6   2  -3 30.592  61.185   0.33     5.53    4      351.3      366.9
  170   6   2   1 30.734  61.469   0.332    5.47    4      872.9     2242.9
  171   0   0  10 30.773  61.546   0.332    5.46    2       22.8        0.8
  172   7   1   4 30.794  61.589   0.332    5.45    4      165.9       80.6
  173   2   2  -7 30.887  61.774   0.333    5.41    4      235.6      161.6
  174   0   2   7 30.918  61.836   0.334    5.4     4      578.6      972.3
  175   6   2  -4 31.407  62.813   0.338    5.22    4      703.8     1389.8
  176   4   2   5 31.465  62.93    0.339    5.19    4      516.7      746.1
  177   7   1  -7 31.585  63.17    0.34     5.15    4      278.5      214.9
  178   6   2   2 31.616  63.232   0.34     5.14    4      465.0      597.9
  179   4   0 -10 31.645  63.291   0.341    5.13    2      717.9      711.2
  180   6   0  -9 31.761  63.522   0.342    5.09    2      348.5      166.3
  181   5   1   7 31.769  63.538   0.342    5.09    4      390.7      417.7
  182   8   0   4 31.998  63.997   0.344    5.01    2      581.1      454.9
  183   8   0  -7 32.102  64.205   0.345    4.97    2      350.4      164.2
  184   5   1  -9 32.197  64.394   0.346    4.94    4      601.2      960.5
  185   6   0   7 32.315  64.63    0.347    4.9     2      402.7      213.8
  186   4   2  -7 32.523  65.046   0.349    4.83    4      387.7      390.9
  187   1   1 -10 32.54   65.08    0.349    4.83    4       84.7       18.6
  188   6   2  -5 32.541  65.081   0.349    4.83    4      485.3      611.8
  189   9   1  -2 32.61   65.219   0.35     4.81    4      368.0      350.2
  190   2   2   7 32.614  65.228   0.35     4.8     4      101.5       26.6
  191   9   1  -1 32.661  65.322   0.35     4.79    4      322.0      267.2
  192   7   1   5 32.734  65.468   0.351    4.77    4      194.4       97.0
  193   6   2   3 32.815  65.629   0.352    4.74    4       57.9        8.6
  194   2   0  10 32.837  65.674   0.352    4.73    2      102.9       13.5
  195   9   1  -3 32.888  65.776   0.352    4.72    4      330.0      276.5
  196   3   1 -10 32.965  65.93    0.353    4.7     4      438.0      484.7
  197   9   1   0 33.041  66.083   0.354    4.67    4      169.9       72.5
  198   4   0   9 33.131  66.263   0.355    4.65    2      567.0      401.7
  199   2   2  -8 33.265  66.53    0.356    4.61    4      571.2      808.3
  200   3   1   9 33.288  66.576   0.356    4.6     4      170.5       71.9
  201   0   2   8 33.415  66.83    0.357    4.56    4      230.8      130.7
  202   9   1  -4 33.492  66.984   0.358    4.54    4      118.1       34.1
  203   4   2   6 33.53   67.059   0.359    4.53    4      344.2      288.7
  204   7   1  -8 33.638  67.275   0.36     4.5     4      418.9      424.7
  205   2   0 -11 33.744  67.488   0.361    4.47    2      320.3      123.3
  206   9   1   1 33.745  67.49    0.361    4.47    4       93.9       21.2
  207   1   1  10 33.746  67.491   0.361    4.47    4      477.8      548.8
  208   1   3   0 33.75   67.5     0.361    4.47    4       59.4        8.5
  209   1   3  -1 33.852  67.705   0.362    4.44    4      164.3       64.5
  210   8   0   5 33.96   67.92    0.363    4.41    2      220.8       57.9
  211   1   3   1 33.972  67.943   0.363    4.41    4      115.7       31.7
  212   6   2  -6 33.979  67.957   0.363    4.4     4      251.9      150.4
  213   8   0  -8 34.079  68.159   0.364    4.38    2      518.3      316.4
  214  10   0  -2 34.225  68.45    0.365    4.34    2       67.7        5.4
  215   0   0  11 34.25   68.499   0.365    4.33    2      349.9      142.7
  216   1   3  -2 34.278  68.556   0.366    4.33    4      642.6      961.0
  217   6   2   4 34.314  68.627   0.366    4.32    4      296.3      203.9
  218  10   0  -1 34.334  68.669   0.366    4.31    2        5.0        0.0
  219   9   1  -5 34.413  68.826   0.367    4.29    4      631.4      920.2
  220  10   0  -3 34.438  68.875   0.367    4.28    2      192.8       42.9
  221   6   0 -10 34.513  69.027   0.368    4.26    2        0.1        0.0
  222   1   3   2 34.515  69.029   0.368    4.26    4      211.4      102.5
  223   5   1   8 34.528  69.056   0.368    4.26    4      123.9       35.2
  224   4   2  -8 34.724  69.448   0.37     4.21    4      576.5      753.1
  225   9   1   2 34.762  69.525   0.37     4.2     4      872.6     1721.4
  226  10   0   0 34.765  69.529   0.37     4.2     2      508.5      292.3
  227   4   0 -11 34.841  69.682   0.371    4.18    2      357.0      143.5
  228   7   1   6 34.936  69.872   0.372    4.16    4      554.4      688.0
  229  10   0  -4 34.97   69.939   0.372    4.15    2      333.6      124.3
  230   5   1 -10 34.99   69.981   0.372    4.15    4      401.4      359.4
  231   1   3  -3 35.02   70.041   0.373    4.14    4      182.5       74.2
  232   6   0   8 35.111  70.222   0.373    4.12    2      575.1      366.4
  233   2   2   8 35.164  70.328   0.374    4.11    4      412.0      375.0
  234   3   3  -1 35.329  70.658   0.375    4.07    4      416.6      379.8
  235   3   3   0 35.345  70.691   0.376    4.06    4      530.0      614.2
  236   1   3   3 35.372  70.744   0.376    4.06    4      278.7      169.6
  237  10   0   1 35.51   71.02    0.377    4.03    2      284.1       87.4
  238   8   2  -1 35.592  71.184   0.378    4.01    4      268.5      155.4
  239   8   2  -2 35.601  71.202   0.378    4.01    4       40.6        3.5
  240   3   3  -2 35.63   71.26    0.378    4.0     4      363.3      283.9
  241   9   1  -6 35.64   71.279   0.378    4.0     4      354.7      270.6
  242   3   3   1 35.679  71.358   0.379    3.99    4      857.8     1579.0
  243   6   2  -7 35.705  71.41    0.379    3.98    4      198.8       84.7
  244  10   0  -5 35.815  71.63    0.38     3.96    2      210.5       47.2
  245   4   2   7 35.849  71.699   0.38     3.95    4      325.9      225.8
  246   1   1 -11 35.87   71.74    0.38     3.95    4      802.3     1366.8
  247   2   2  -9 35.876  71.753   0.38     3.95    4      404.5      347.3
  248   8   2   0 35.899  71.799   0.381    3.94    4      385.8      315.5
  249   8   2  -3 35.926  71.852   0.381    3.94    4      968.9     1987.3
  250   7   1  -9 35.947  71.894   0.381    3.93    4      269.6      153.7
  251   1   3  -4 36.072  72.144   0.382    3.9     4       86.2       15.6
  252   9   1   3 36.082  72.164   0.382    3.9     4      178.9       67.2
  253   6   2   5 36.098  72.196   0.382    3.9     4      387.3      314.6
  254   0   2   9 36.137  72.274   0.383    3.89    4      272.7      155.7
  255   3   1 -11 36.16   72.321   0.383    3.89    4      334.0      233.1
  256   8   0   6 36.184  72.369   0.383    3.88    2      184.3       35.5
  257   3   3  -3 36.245  72.489   0.384    3.87    4      394.8      324.5
  258   8   0  -9 36.318  72.636   0.384    3.85    2       14.8        0.2
  259   3   3   2 36.326  72.652   0.385    3.85    4      218.6       99.0
  260   2   0  11 36.328  72.655   0.385    3.85    2      202.2       42.3
  261   4   0  10 36.41   72.821   0.385    3.83    2      123.8       15.8
  262   3   1  10 36.503  73.006   0.386    3.82    4      492.9      498.8
  263   8   2   1 36.52   73.04    0.386    3.81    4      428.0      375.7
  264   1   3   4 36.535  73.069   0.386    3.81    4       31.7        2.1
  265  10   0   2 36.563  73.126   0.387    3.8     2      169.2       29.3
  266   8   2  -4 36.564  73.128   0.387    3.8     4       27.3        1.5
  267  10   0  -6 36.964  73.929   0.39     3.73    2      150.2       22.6
  268   1   1  11 37.14   74.279   0.392    3.69    4      244.1      118.5
  269   9   1  -7 37.161  74.322   0.392    3.69    4      467.0      433.0
  270   3   3  -4 37.167  74.335   0.392    3.69    4      197.0       77.1
  271   4   2  -9 37.175  74.35    0.392    3.69    4       50.1        5.0
  272   2   0 -12 37.277  74.555   0.393    3.67    2      116.3       13.3
  273   3   3   3 37.281  74.561   0.393    3.67    4      234.7      108.7
  274   7   1   7 37.388  74.777   0.394    3.65    4       62.3        7.6
  275   1   3  -5 37.422  74.845   0.394    3.64    4      207.5       84.4
  276   8   2   2 37.447  74.895   0.395    3.64    4      325.1      206.9
  277   6   0 -11 37.478  74.957   0.395    3.63    2      429.0      179.9
  278   5   1   9 37.5    75.0     0.395    3.63    4      259.1      131.1
  279   8   2  -5 37.509  75.018   0.395    3.63    4      245.3      117.4
  280   9   1   4 37.693  75.386   0.397    3.6     4      197.9       75.8
  281   6   2  -8 37.707  75.415   0.397    3.59    4      499.2      481.8
  282   0   0  12 37.877  75.753   0.399    3.56    2      541.6      281.2
  283  10   0   3 37.914  75.828   0.399    3.56    2       25.1        0.6
  284   2   2   9 37.945  75.891   0.399    3.55    4      385.7      284.4
  285   1   3   5 37.993  75.985   0.4      3.55    4      746.8     1063.8
  286   5   1 -11 37.997  75.994   0.4      3.54    4       12.5        0.3
  287   6   0   9 38.121  76.242   0.401    3.52    2       94.9        8.5
  288   6   2   6 38.157  76.313   0.401    3.52    4       59.8        6.8
  289   4   0 -12 38.219  76.437   0.402    3.51    2      467.9      206.7
  290   5   3  -1 38.321  76.643   0.402    3.49    4      275.8      142.9
  291   3   3  -5 38.39   76.781   0.403    3.48    4      379.2      269.4
  292  10   0  -7 38.409  76.819   0.403    3.48    2      560.6      294.0
  293   4   2   8 38.417  76.834   0.403    3.48    4      506.9      480.6
  294   5   3   0 38.451  76.902   0.404    3.47    4       71.4        9.5
  295   5   3  -2 38.5    77.0     0.404    3.46    4      500.1      466.1
  296   7   1 -10 38.505  77.009   0.404    3.46    4      728.2      988.0
  297   3   3   4 38.534  77.069   0.404    3.46    4      140.2       36.6
  298   8   0   7 38.662  77.325   0.406    3.44    2      142.0       18.7
  299   8   2   3 38.675  77.349   0.406    3.44    4       31.0        1.8
  300   2   2 -10 38.719  77.438   0.406    3.43    4       98.0       17.7
  301   8   2  -6 38.753  77.506   0.406    3.43    4      132.8       32.5
  302   8   0 -10 38.81   77.621   0.407    3.42    2      366.8      123.7
  303   5   3   1 38.887  77.775   0.408    3.41    4       97.1       17.3
  304   9   1  -8 38.967  77.934   0.408    3.39    4       12.3        0.3
  305   5   3  -3 38.986  77.972   0.408    3.39    4      539.9      531.9
  306   1   3  -6 39.063  78.125   0.409    3.38    4      443.0      356.9
  307   0   2  10 39.086  78.171   0.409    3.38    4       55.3        5.6
  308   1   1 -12 39.382  78.765   0.412    3.34    4       75.7       10.3
  309   3   1 -12 39.551  79.103   0.413    3.31    4      137.7       33.8
  310  10   0   4 39.555  79.11    0.413    3.31    2      371.6      123.1
  311   9   1   5 39.586  79.173   0.414    3.31    4      114.5       23.3
  312   5   3   2 39.628  79.256   0.414    3.3     4      360.0      230.3
  313   1   3   6 39.738  79.476   0.415    3.29    4      103.4       18.9
  314   5   3  -4 39.775  79.55    0.415    3.28    4      612.0      661.6
  315   4   2 -10 39.874  79.747   0.416    3.27    4      612.4      659.8
  316   4   0  11 39.882  79.763   0.416    3.27    2       95.2        8.0
  317   3   3  -6 39.906  79.813   0.416    3.27    4      658.2      761.5
  318   3   1  11 39.915  79.831   0.417    3.27    4      408.6      293.3
  319   6   2  -9 39.979  79.958   0.417    3.26    4      353.2      218.7
  320   2   0  12 39.994  79.988   0.417    3.26    2      892.2      697.1
  321   3   3   5 40.08   80.161   0.418    3.24    4      178.2       55.4
  322   7   1   8 40.09   80.179   0.418    3.24    4      723.7      913.8
  323  10   0  -8 40.142  80.284   0.418    3.24    2      211.3       38.9
  324   8   2   4 40.195  80.389   0.419    3.23    4      565.5      555.9
  325  11   1  -2 40.201  80.402   0.419    3.23    4      910.8     1441.6
  326   8   2  -7 40.289  80.579   0.42     3.22    4      283.2      138.9
  327  11   1  -3 40.346  80.691   0.42     3.21    4      284.4      139.8
  328  11   1  -1 40.36   80.72    0.42     3.21    4      318.4      175.1
  329   6   2   7 40.484  80.968   0.421    3.2     4      401.1      276.6
  330   6   0 -12 40.667  81.333   0.423    3.18    2      403.7      139.2
  331   5   3   3 40.669  81.338   0.423    3.17    4      676.3      781.3
  332   5   1  10 40.695  81.39    0.423    3.17    4      460.0      361.1
  333   1   1  12 40.727  81.454   0.424    3.17    4       93.9       15.0
  334  11   1  -4 40.794  81.588   0.424    3.16    4       91.5       14.3
  335  11   1   0 40.822  81.645   0.424    3.16    4      208.4       73.8
  336   5   3  -5 40.863  81.727   0.425    3.15    4      129.8       28.6
  337   2   2  10 40.963  81.926   0.426    3.14    4       58.2        5.7
  338   1   3  -7 40.987  81.973   0.426    3.14    4      485.3      397.9
  339   2   0 -13 40.997  81.994   0.426    3.14    2      497.0      208.6
  340   9   1  -9 41.052  82.104   0.426    3.13    4      368.6      229.0
  341   5   1 -12 41.23   82.459   0.428    3.11    4      203.6       69.4
  342   4   2   9 41.234  82.469   0.428    3.11    4      481.0      387.5
  343   7   1 -11 41.313  82.627   0.429    3.11    4      493.3      406.6
  344   6   0  10 41.358  82.716   0.429    3.1     2      267.2       59.5
  345   8   0   8 41.396  82.791   0.429    3.1     2      497.2      205.9
  346  10   0   5 41.481  82.962   0.43     3.09    2      454.3      171.4
  347  11   1  -5 41.543  83.087   0.43     3.08    4      275.1      125.5
  348   8   0 -11 41.558  83.117   0.431    3.08    2       99.7        8.2
  349  11   1   1 41.586  83.172   0.431    3.08    4       42.5        3.0
  350   0   0  13 41.692  83.384   0.432    3.07    2      321.7       85.4
  351   3   3  -7 41.71   83.421   0.432    3.07    4       91.8       13.9
  352   9   1   6 41.758  83.516   0.432    3.06    4      527.4      458.1
  353   1   3   7 41.765  83.531   0.432    3.06    4      473.1      368.5
  354   2   2 -11 41.802  83.604   0.433    3.06    4      257.0      108.6
  355   4   0 -13 41.804  83.608   0.433    3.06    2      200.7       33.1
  356   3   3   6 41.914  83.828   0.434    3.05    4      481.9      380.5
  357   8   2   5 42.003  84.006   0.434    3.04    4      234.9       90.2
  358   5   3   4 42.006  84.011   0.434    3.04    4       89.8       13.2
  359   8   2  -8 42.114  84.228   0.435    3.03    4      438.9      313.8
  360  10   0  -9 42.159  84.317   0.436    3.02    2      575.7      269.6
  361   5   3  -6 42.247  84.495   0.436    3.02    4      168.1       45.9
  362  10   2  -2 42.25   84.5     0.436    3.02    4       94.2       14.4
  363   0   2  11 42.273  84.546   0.437    3.01    4      354.8      204.1
  364  10   2  -1 42.352  84.705   0.437    3.01    4       29.6        1.4
  365  10   2  -3 42.449  84.898   0.438    3.0     4      142.3       32.7
  366  12   0  -2 42.45   84.9     0.438    3.0     2        8.3        0.1
  367   6   2 -10 42.52   85.04    0.439    2.99    4       34.1        1.9
  368  12   0  -3 42.538  85.076   0.439    2.99    2      312.9       78.8
  369  11   1  -6 42.592  85.184   0.439    2.99    4      454.7      332.1
  370  11   1   2 42.649  85.297   0.44     2.98    4      262.0      110.1
  371  12   0  -1 42.663  85.326   0.44     2.98    2      108.4        9.4
  372   7   3  -1 42.74   85.48    0.441    2.97    4      327.4      171.5
  373  10   2   0 42.756  85.511   0.441    2.97    4      502.7      404.2
  374   7   3  -2 42.804  85.608   0.441    2.97    4       38.0        2.3
  375   4   2 -11 42.828  85.656   0.441    2.97    4      361.7      208.9
  376  12   0  -4 42.927  85.854   0.442    2.96    2      465.1      172.2
  377  10   2  -4 42.949  85.897   0.442    2.96    4      271.2      117.1
  378   7   3   0 42.977  85.954   0.443    2.96    4      102.8       16.8
  379   7   1   9 43.048  86.096   0.443    2.95    4       68.6        7.5
  380   6   2   8 43.082  86.164   0.443    2.95    4      560.4      498.0
  381   1   1 -13 43.111  86.223   0.444    2.95    4      331.4      174.0
  382   3   1 -13 43.167  86.334   0.444    2.94    4      439.7      306.0
  383   7   3  -3 43.168  86.337   0.444    2.94    4      152.6       36.9
  384  12   0   0 43.176  86.353   0.444    2.94    2      308.5       75.3
  385   1   3  -8 43.193  86.386   0.444    2.94    4      146.4       33.9
  386   9   1 -10 43.417  86.834   0.446    2.92    4      481.5      364.6
  387  10   2   1 43.459  86.918   0.446    2.92    4      293.6      135.4
  388   7   3   1 43.514  87.028   0.447    2.92    4      234.6       86.3
  389   3   1  12 43.557  87.113   0.447    2.91    4       77.2        9.3
  390   4   0  12 43.579  87.157   0.447    2.91    2       64.3        3.2
  391  12   0  -5 43.616  87.231   0.448    2.91    2        9.1        0.1
  392   5   3   5 43.636  87.273   0.448    2.91    4       51.5        4.2
  393  10   0   6 43.691  87.382   0.448    2.9     2      247.9       48.0
  394  10   2  -5 43.748  87.496   0.449    2.9     4      160.3       40.1
  395   3   3  -8 43.801  87.603   0.449    2.9     4       77.3        9.3
  396   7   3  -4 43.833  87.666   0.45     2.9     4       17.0        0.4
  397   2   0  13 43.879  87.758   0.45     2.89    2      294.5       67.5
  398   5   3  -7 43.925  87.851   0.45     2.89    4      263.7      108.1
  399  11   1  -7 43.937  87.874   0.45     2.89    4      297.6      137.6
  400  12   0   1 43.99   87.979   0.451    2.89    2      365.6      103.7
  401  11   1   3 44.008  88.016   0.451    2.88    4      428.6      285.0
  402   3   3   7 44.035  88.07    0.451    2.88    4      349.2      189.1
  403   1   3   8 44.077  88.154   0.452    2.88    4      174.8       47.3
  404   8   2   6 44.1    88.199   0.452    2.88    4      204.4       64.7
  405   6   0 -13 44.101  88.203   0.452    2.88    2       22.2        0.4
  406   5   1  11 44.137  88.273   0.452    2.88    4      189.7       55.7
  407   9   1   7 44.211  88.423   0.453    2.87    4      462.9      331.1
  408   8   2  -9 44.227  88.454   0.453    2.87    4       45.1        3.1
  409   2   2  11 44.236  88.473   0.453    2.87    4      219.2       74.2
  410   4   2  10 44.315  88.631   0.453    2.87    4       79.3        9.7
  411   7   3   2 44.351  88.702   0.454    2.86    4      324.7      162.4
  412   7   1 -12 44.387  88.774   0.454    2.86    4       26.1        1.0
  413   8   0   9 44.396  88.793   0.454    2.86    2      471.2      170.9
  414  10   0 -10 44.461  88.922   0.455    2.86    2        1.0        0.0
  415  10   2   2 44.462  88.923   0.455    2.86    4      188.4       54.5
  416   1   1  13 44.547  89.095   0.455    2.85    4      197.7       60.0
  417   8   0 -12 44.575  89.15    0.456    2.85    2      448.9      154.5
  418  12   0  -6 44.604  89.208   0.456    2.85    2       14.9        0.2
  419   5   1 -13 44.714  89.428   0.457    2.84    4      249.6       95.3
  420   7   3  -5 44.797  89.594   0.457    2.84    4      315.6      152.1
  421  10   2  -6 44.846  89.693   0.458    2.84    4      171.6       44.9
  422   6   0  11 44.849  89.697   0.458    2.84    2      158.2       19.1
  423   2   0 -14 44.949  89.898   0.459    2.83    2      132.8       13.4


  X-ray diffraction powder data (I)...X-Ray wave length =  1.54056 (angs.):

  No   H   K   L   Theta 2*Theta    d           I int   I int.n.  I p.h.n.   H(Si)
                    ( degree )   (angstrem)     *100                         *100

    1   0   0   1   2.933   5.865 15.05521     7001.5     37.0     37.6     5.5
    2   2   0   0   6.548  13.097  6.75441     4061.0     21.5     21.7     5.6
    3   2   0  -1   6.721  13.442  6.5817      3302.9     17.5     17.7     5.6
    4   2   0   1   7.613  15.225  5.81458     5627.8     29.8     30.1     5.6
    5   2   0  -2   8.053  16.106  5.49866      422.3      2.2      2.3     5.6
    6   0   0   3   8.829  17.659  5.0184       339.6      1.8      1.8     5.6
    7   2   0   2   9.515  19.031  4.6595      2456.1     13.0     13.1     5.6
    8   2   0  -3  10.105  20.211  4.39006     2496.2     13.2     13.3     5.6
    9   1   1   0  11.118  22.237  3.99451      402.6      2.1      2.1     5.6
   10   1   1  -1  11.366  22.732  3.9085       738.7      3.9      3.9     5.6
   11   1   1   1  11.648  23.297  3.81504      963.1      5.1      5.1     5.6
   12   0   0   4  11.809  23.619  3.7638      2648.1     14.0     14.1     5.6
   13   2   0   3  11.875  23.75   3.7433      5172.8     27.4     27.5     5.6
   14   1   1  -2  12.348  24.696  3.60204    13755.6     72.8     73.1     5.6
   15   2   0  -4  12.546  25.091  3.5461     10788.7     57.1     57.3     5.6
   16   1   1   2  12.866  25.732  3.45928     2073.8     11.0     11.0     5.6
   17   4   0  -1  13.024  26.048  3.41801     2377.2     12.6     12.6     5.6
   18   4   0   0  13.184  26.368  3.3772      1401.1      7.4      7.4     5.6
   19   4   0  -2  13.537  27.073  3.29085      639.2      3.4      3.4     5.6
   20   1   1  -3  13.918  27.836  3.20241      722.4      3.8      3.8     5.6
   21   4   0   1  13.996  27.992  3.18494      344.9      1.8      1.8     5.6
   22   2   0   4  14.489  28.977  3.07881     2899.0     15.3     15.4     5.6
   23   3   1  -1  14.528  29.055  3.07071     5598.6     29.6     29.6     5.6
   24   3   1   0  14.56   29.119  3.06411     8737.1     46.2     46.3     5.6
   25   1   1   3  14.611  29.222  3.05354     2442.8     12.9     12.9     5.6
   26   4   0  -3  14.657  29.314  3.04424      198.7      1.1      1.1     5.6
   27   0   0   5  14.822  29.644  3.01104     2742.1     14.5     14.5     5.6
   28   3   1  -2  15.103  30.206  2.95632     3990.3     21.1     21.1     5.6
   29   3   1   1  15.195  30.391  2.93874    18903.7    100.0    100.0     5.6
   30   3   1  -3  16.227  32.454  2.7565      3858.8     20.4     20.4     5.6
   31   4   0  -4  16.27   32.541  2.74933     1043.5      5.5      5.5     5.6
   32   3   1   2  16.371  32.743  2.73284      640.3      3.4      3.4     5.6
   33   4   0   3  17.169  34.338  2.60942      267.4      1.4      1.4     5.7
   34   2   0   5  17.264  34.529  2.59544     2209.1     11.7     11.6     5.7
   35   3   1  -4  17.807  35.614  2.51879      901.0      4.8      4.7     5.7
   36   3   1   3  17.993  35.987  2.49357      868.1      4.6      4.6     5.7
   37   1   1  -5  18.225  36.45   2.46292      931.0      4.9      4.9     5.7
   38   4   0  -5  18.263  36.525  2.45803      800.6      4.2      4.2     5.7
   39   1   1   5  19.134  38.269  2.34995     7094.3     37.5     37.3     5.7
   40   4   0   4  19.307  38.614  2.32975     1029.9      5.4      5.4     5.7
   41   5   1  -1  19.645  39.289  2.29125      759.1      4.0      4.0     5.7
   42   3   1  -5  19.75   39.501  2.27945     1535.8      8.1      8.1     5.7
   43   5   1  -2  19.918  39.836  2.26106     2736.1     14.5     14.3     5.7
   44   6   0   0  20.006  40.013  2.25147      494.9      2.6      2.6     5.7
   45   2   0   6  20.162  40.324  2.2348       430.1      2.3      2.3     5.7
   46   5   1   1  20.5    41.001  2.19945      200.9      1.1      1.1     5.7
   47   6   0  -3  20.555  41.109  2.1939       751.5      4.0      3.9     5.7
   48   5   1  -3  20.647  41.293  2.18454     2943.1     15.6     15.4     5.7
   49   6   0   1  20.743  41.487  2.17482     5800.4     30.7     30.4     5.7
   50   0   0   7  20.986  41.973  2.15074     1726.4      9.1      9.0     5.7
   51   5   1   2  21.584  43.167  2.09396     1579.0      8.4      8.3     5.7
   52   0   2   0  21.618  43.237  2.09075     9191.2     48.6     48.0     5.7
   53   4   0   5  21.701  43.402  2.08316      942.2      5.0      4.9     5.7
   54   1   1   6  21.741  43.482  2.07955      209.8      1.1      1.1     5.7
   55   5   1  -4  21.794  43.587  2.07474     4248.0     22.5     22.2     5.7
   56   6   0   2  21.896  43.793  2.06548     1059.4      5.6      5.5     5.7
   57   3   1  -6  21.981  43.962  2.05794     3819.8     20.2     19.9     5.7
   58   3   1   5  22.226  44.453  2.03634      428.3      2.3      2.2     5.7
   59   2   2   0  22.685  45.371  1.99726      522.1      2.8      2.7     5.7
   60   2   2  -1  22.741  45.482  1.99263      459.9      2.4      2.4     5.7
   61   5   1   3  23.044  46.088  1.96782     5963.5     31.5     31.1     5.7
   62   6   0  -5  23.074  46.148  1.96542      995.9      5.3      5.2     5.7
   63   1   1  -7  23.477  46.955  1.9335      2243.8     11.9     11.7     5.7
   64   2   2   2  23.817  47.633  1.90752      606.2      3.2      3.2     5.7
   65   2   0  -8  23.976  47.953  1.89555      925.0      4.9      4.8     5.7
   66   2   2  -3  24.084  48.167  1.88761      407.9      2.2      2.1     5.7
   67   0   0   8  24.161  48.323  1.8819       236.4      1.3      1.2     5.7
   68   4   0   6  24.302  48.605  1.87165      469.6      2.5      2.4     5.7
   69   1   1   7  24.517  49.034  1.85626     1448.6      7.7      7.5     5.7
   70   3   1   6  24.712  49.424  1.84253     1927.5     10.2     10.0     5.7
   71   6   0  -6  24.851  49.701  1.83289      255.7      1.4      1.3     5.7
   72   0   2   4  24.926  49.852  1.8277       888.5      4.7      4.6     5.7
   73   2   2   3  24.961  49.921  1.82533     1278.8      6.8      6.6     5.7
   74   5   1  -6  25.146  50.292  1.81274      270.1      1.4      1.4     5.8
   75   6   0   4  25.256  50.513  1.80533      322.1      1.7      1.7     5.8
   76   2   2  -4  25.321  50.642  1.80102     2991.0     15.8     15.5     5.8
   77   4   2  -1  25.587  51.174  1.78354      659.2      3.5      3.4     5.8
   78   4   2   0  25.678  51.356  1.77767      372.9      2.0      1.9     5.8
   79   4   0  -8  25.75   51.499  1.77305     1853.1      9.8      9.6     5.8
   80   4   2  -2  25.88   51.76   1.76472      361.2      1.9      1.9     5.8
   81   2   0   8  26.274  52.548  1.74011      361.5      1.9      1.9     5.8
   82   7   1  -3  26.32   52.639  1.7373       214.1      1.1      1.1     5.8
   83   1   1  -8  26.351  52.701  1.7354       210.2      1.1      1.1     5.8
   84   2   2   4  26.445  52.89   1.72964      910.5      4.8      4.7     5.8
   85   0   2   5  26.649  53.299  1.71735     1269.5      6.7      6.6     5.8
   86   7   1   1  26.751  53.503  1.71127      478.5      2.5      2.5     5.8
   87   2   2  -5  26.89   53.779  1.70312     1097.1      5.8      5.7     5.8
   88   4   0   7  27.081  54.163  1.69197      215.5      1.1      1.1     5.8
   89   8   0   0  27.14   54.28   1.6886       760.6      4.0      3.9     5.8
   90   8   0  -3  27.171  54.342  1.6868      2102.7     11.1     10.8     5.8
   91   5   1  -7  27.259  54.518  1.68178      490.8      2.6      2.5     5.8
   92   3   1   7  27.393  54.787  1.67417     1579.2      8.4      8.1     5.8
   93   4   2  -4  27.571  55.142  1.66421      585.7      3.1      3.0     5.8
   94   7   1   2  27.778  55.557  1.65278      468.4      2.5      2.4     5.8
   95   8   0   1  27.862  55.724  1.64822      494.1      2.6      2.5     5.8
   96   4   2   3  28.17   56.341  1.63162      189.5      1.0      1.0     5.8
   97   2   2   5  28.235  56.47   1.62819      925.1      4.9      4.8     5.8
   98   7   1  -5  28.315  56.631  1.62395      417.3      2.2      2.1     5.8
   99   4   2  -5  28.925  57.851  1.59257      811.7      4.3      4.2     5.8
  100   7   1   3  29.135  58.269  1.58213      508.6      2.7      2.6     5.8
  101   6   0  -8  29.223  58.447  1.57775      831.4      4.4      4.3     5.8
  102   1   1  -9  29.371  58.742  1.57052      358.9      1.9      1.8     5.8
  103   2   0   9  29.493  58.986  1.5646       241.3      1.3      1.2     5.8
  104   4   2   4  29.671  59.343  1.55604      714.9      3.8      3.7     5.8
  105   7   1  -6  29.804  59.607  1.54977      922.6      4.9      4.7     5.8
  106   3   1  -9  29.949  59.898  1.54295      372.6      2.0      1.9     5.8
  107   4   0   8  30.025  60.05   1.5394       562.0      3.0      2.9     5.8
  108   6   2   0  30.184  60.368  1.53205      381.3      2.0      2.0     5.8
  109   3   1   8  30.254  60.507  1.52885      212.6      1.1      1.1     5.8
  110   2   2   6  30.299  60.598  1.52677      202.8      1.1      1.0     5.8
  111   1   1   9  30.519  61.038  1.51681      365.2      1.9      1.9     5.8
  112   6   2  -3  30.592  61.185  1.51354      400.4      2.1      2.0     5.8
  113   6   2   1  30.734  61.469  1.50723     2242.9     11.9     11.5     5.8
  114   0   2   7  30.918  61.836  1.49914      972.3      5.1      5.0     5.8
  115   6   2  -4  31.407  62.813  1.47816     1389.8      7.4      7.1     5.9
  116   4   2   5  31.465  62.93   1.47569      746.1      3.9      3.8     5.9
  117   7   1  -7  31.585  63.17   1.47067      214.9      1.1      1.1     5.9
  118   6   2   2  31.616  63.232  1.46937      597.9      3.2      3.0     5.9
  119   4   0 -10  31.645  63.291  1.46815      711.2      3.8      3.6     5.9
  120   5   1   7  31.769  63.538  1.46304      584.0      3.1      3.0     5.9
  121   8   0   4  31.998  63.997  1.45365      454.9      2.4      2.3     5.9
  122   5   1  -9  32.197  64.394  1.44563      960.5      5.1      4.9     5.9
  123   6   0   7  32.315  64.63   1.44093      213.8      1.1      1.1     5.9
  124   6   2  -5  32.541  65.081  1.43202     1021.3      5.4      5.2     5.9
  125   9   1  -2  32.61   65.219  1.42932      376.9      2.0      1.9     5.9
  126   9   1  -1  32.661  65.322  1.42732      267.2      1.4      1.4     5.9
  127   9   1  -3  32.888  65.776  1.41857      276.5      1.5      1.4     5.9
  128   3   1 -10  32.965  65.93   1.41562      484.7      2.6      2.5     5.9
  129   4   0   9  33.131  66.263  1.40932      401.7      2.1      2.0     5.9
  130   2   2  -8  33.265  66.53   1.40431      880.3      4.7      4.5     5.9
  131   4   2   6  33.53   67.059  1.39451      288.7      1.5      1.5     5.9
  132   7   1  -8  33.638  67.275  1.39055      424.7      2.2      2.1     5.9
  133   1   1  10  33.746  67.491  1.38662      701.8      3.7      3.5     5.9
  134   6   2  -6  33.979  67.957  1.37825      240.0      1.3      1.2     5.9
  135   8   0  -8  34.079  68.159  1.37467      316.4      1.7      1.6     5.9
  136   1   3  -2  34.278  68.556  1.36767     1109.1      5.9      5.6     5.9
  137   6   2   4  34.314  68.627  1.36642      203.9      1.1      1.0     5.9
  138   9   1  -5  34.413  68.826  1.36296      963.0      5.1      4.9     5.9
  139   4   2  -8  34.724  69.448  1.35226      753.1      4.0      3.8     5.9
  140   9   1   2  34.762  69.525  1.35095     2013.7     10.7     10.1     5.9
  141   7   1   6  34.936  69.872  1.34509      688.0      3.6      3.5     5.9
  142   5   1 -10  34.99   69.981  1.34326      483.7      2.6      2.4     5.9
  143   6   0   8  35.111  70.222  1.33924      366.4      1.9      1.8     5.9
  144   2   2   8  35.164  70.328  1.33748      375.0      2.0      1.9     5.9
  145   3   3   0  35.345  70.691  1.3315      1163.6      6.2      5.9     5.9
  146   3   3  -2  35.63   71.26   1.32227      554.5      2.9      2.8     5.9
  147   3   3   1  35.679  71.358  1.32068     1663.7      8.8      8.4     5.9
  148   2   2  -9  35.876  71.753  1.31439     1939.9     10.3      9.7     5.9
  149   8   2  -3  35.926  71.852  1.31281     2456.5     13.0     12.3     5.9
  150   6   2   5  36.098  72.196  1.3074       397.4      2.1      2.0     5.9
  151   3   1 -11  36.16   72.321  1.30545      424.3      2.2      2.1     5.9
  152   3   3  -3  36.245  72.489  1.30283      324.5      1.7      1.6     5.9
  153   3   1  10  36.503  73.006  1.29489      874.6      4.6      4.4     6.0
  154   9   1  -7  37.161  74.322  1.27518      633.5      3.4      3.2     6.0
  155   8   2   2  37.447  74.895  1.26684      291.3      1.5      1.5     6.0
  156   6   0 -11  37.478  74.957  1.26594      311.0      1.6      1.6     6.0
  157   6   2  -8  37.707  75.415  1.25939      557.5      2.9      2.8     6.0
  158   0   0  12  37.877  75.753  1.2546       281.2      1.5      1.4     6.0
  159   2   2   9  37.945  75.891  1.25267      284.4      1.5      1.4     6.0
  160   1   3   5  37.993  75.985  1.25135     1064.1      5.6      5.3     6.0
  161   4   0 -12  38.219  76.437  1.24507      206.7      1.1      1.0     6.0
  162   4   2   8  38.417  76.834  1.23963     1044.0      5.5      5.2     6.0
  163   7   1 -10  38.505  77.009  1.23724     1490.6      7.9      7.4     6.0
  164   5   3  -3  38.986  77.972  1.22436      531.9      2.8      2.6     6.0
  165   1   3  -6  39.063  78.125  1.22234      362.5      1.9      1.8     6.0
  166   5   3   2  39.628  79.256  1.20771      230.3      1.2      1.1     6.0
  167   5   3  -4  39.775  79.55   1.20399      661.6      3.5      3.3     6.0
  168   4   2 -10  39.874  79.747  1.2015       667.8      3.5      3.3     6.0
  169   3   3  -6  39.906  79.813  1.20068     1054.8      5.6      5.2     6.0
  170   2   0  12  39.994  79.988  1.19849      915.8      4.8      4.5     6.0
  171   7   1   8  40.09   80.179  1.19611      969.3      5.1      4.8     6.0
  172  11   1  -2  40.201  80.402  1.19337     1997.6     10.6      9.8     6.0
  173  11   1  -1  40.36   80.72   1.18946      314.9      1.7      1.6     6.1
  174   6   2   7  40.484  80.968  1.18645      276.6      1.5      1.4     6.1
  175   5   1  10  40.695  81.39   1.18135     1281.7      6.8      6.3     6.1
  176   1   3  -7  40.987  81.973  1.17442      612.2      3.2      3.0     6.1
  177   9   1  -9  41.052  82.104  1.17287      229.0      1.2      1.1     6.1
  178   4   2   9  41.234  82.469  1.16862      457.0      2.4      2.2     6.1
  179   7   1 -11  41.313  82.627  1.16678      406.6      2.2      2.0     6.1
  180   8   0   8  41.396  82.791  1.16487      205.9      1.1      1.0     6.1
  181   9   1   6  41.758  83.516  1.1566       826.6      4.4      4.0     6.1
  182   3   3   6  41.914  83.828  1.15309      380.5      2.0      1.9     6.1
  183   8   2  -8  42.114  84.228  1.14863      313.8      1.7      1.5     6.1
  184  10   0  -9  42.159  84.317  1.14764      269.6      1.4      1.3     6.1
  185   0   2  11  42.273  84.546  1.14511      264.4      1.4      1.3     6.1
  186  11   1  -6  42.592  85.184  1.13817      332.1      1.8      1.6     6.1
  187  10   2   0  42.756  85.511  1.13464      575.7      3.0      2.8     6.1
  188   4   2 -11  42.828  85.656  1.1331       211.2      1.1      1.0     6.1
  189  12   0  -4  42.927  85.854  1.131        289.3      1.5      1.4     6.1
  190   6   2   8  43.082  86.164  1.12772      672.0      3.6      3.3     6.1
  191   3   1 -13  43.167  86.334  1.12593      452.1      2.4      2.2     6.1
  192   9   1 -10  43.417  86.834  1.12073      364.6      1.9      1.8     6.1
  193  11   1  -7  43.937  87.874  1.11012      245.7      1.3      1.2     6.2
  194  11   1   3  44.008  88.016  1.1087       577.8      3.1      2.8     6.2
  195   9   1   7  44.211  88.423  1.10465      408.4      2.2      2.0     6.2
  196   8   0 -12  44.575  89.15   1.09752      214.5      1.1      1.0     6.2

Reference:
Chichagov A.V. et al.
Information-Calculating System on Crystal Structure Data of Minerals
(MINCRYST)
- Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian)