Institute of Experimental Mineralogy
                 Russian Academy of Sciences
     -------------------------------------------------
           142432, Chernogolovka, Moscow district
             A.V. Chichagov  +7(496)52-22320

                            ***

          ***      W W W - X R A Y P O L       ***
                  ***********************
GOBELINITE

2, t-ktenasite, f-ktenasite

CoCu(4)[SO(4)](2)(OH)(6).6H(2)O


Monoclinic  P 2(1)/c  Z = 2

R =0.0289          NR =1998

18 .10 .24

Ref.Str.:

         Mills S.J., Kolitsch U., Favreau G., Birch W.D., Galea-Clolus V.,

         Henrich J.M. (2020) * Eur. J. Mineral., 32, 637–644

         https://doi.org/10.5194/ejm-32-637-2020

         L: $Co0.92 Ni0.21 Mg0.01 Cu3.79 S2.08 O20 H18$

         R: Locality - Eisenzecher Zug, Siegerland, North Rhine-Westphalia, Germany.

         IMA2018-167. N.A.D.

                   Initial data from BDM-file 

   Lattice parameters (cub. angs.,degr.):

             a =   5.611    alpha =   90.0 
             b =   6.103    beta  =   95.18
             c =  23.808    gamma =   90.0 

    Unit cell volume (cub. angs.) =   811.95

    Molar volume ( cub.cm/mol.) =   244.53

  Co-ordinates, thermal parameters, occupation for atomic positions:

NoP   x/a     y/b     z/c    B(j)   atom  / occupation

   1 0.0     0.0     0.0      0.0    Co    = 0.92, Ni    = 0.08
   2 0.9922  0.1003  0.249    0.0    Cu    = 0.95, Zn    = 0.05
   3 0.499   0.8496  0.2474   0.0    Cu    = 0.95, Zn    = 0.05
   4 0.3647  0.0578  0.374    0.0    S     = 1.00
   5 0.3383  0.0963  0.3121   0.0    O     = 1.00
   6 0.6051  0.1045  0.2094   0.0    O     = 1.00
   7 0.8418  0.3545  0.2884   0.0    O     = 1.00
   8 0.1613  0.3469  0.2153   0.0    O     = 1.00
   9 0.1314  0.994   0.3922   0.0    O     = 1.00
  10 0.4473  0.2624  0.4023   0.0    O     = 1.00
  11 0.5423  0.8839  0.3864   0.0    O     = 1.00
  12 0.9149  0.0606  0.0826   0.0    O     = 1.00
  13 0.3248  0.1595  0.0178   0.0    O     = 1.00
  14 0.1401  0.7019  0.0286   0.0    O     = 1.00
  15 0.562   0.121   0.1802   0.0    H     = 1.00
  16 0.863   0.359   0.3206   0.0    H     = 1.00
  17 0.153   0.361   0.1842   0.0    H     = 1.00
  18 0.895   0.19    0.0889   0.0    H     = 1.00
  19 0.8     0.98    0.0898   0.0    H     = 1.00
  20 0.421   0.184   0.993    0.0    H     = 1.00
  21 0.361   0.231   0.0461   0.0    H     = 1.00
  22 0.032   0.632   0.0424   0.0    H     = 1.00
  23 0.259   0.716   0.0478   0.0    H     = 1.00


  Co-ordinates for all atomic positions :

   No       NoP      x/a        y/b       z/c 

     1       1     0.0        0.0        0.0   
     2       2     0.9922     0.1003     0.249 
     3       3     0.499      0.8496     0.2474
     4       4     0.3647     0.0578     0.374 
     5       5     0.3383     0.0963     0.3121
     6       6     0.6051     0.1045     0.2094
     7       7     0.8418     0.3545     0.2884
     8       8     0.1613     0.3469     0.2153
     9       9     0.1314     0.994      0.3922
    10      10     0.4473     0.2624     0.4023
    11      11     0.5423     0.8839     0.3864
    12      12     0.9149     0.0606     0.0826
    13      13     0.3248     0.1595     0.0178
    14      14     0.1401     0.7019     0.0286
    15      15     0.562      0.121      0.1802
    16      16     0.863      0.359      0.3206
    17      17     0.153      0.361      0.1842
    18      18     0.895      0.19       0.0889
    19      19     0.8        0.98       0.0898
    20      20     0.421      0.184      0.993 
    21      21     0.361      0.231      0.0461
    22      22     0.032      0.632      0.0424
    23      23     0.259      0.716      0.0478
    24       1     0.0        0.5        0.5   
    25       2     0.0078     0.6003     0.251 
    26       3     0.501      0.3496     0.2526
    27       4     0.6353     0.5578     0.126 
    28       5     0.6617     0.5963     0.1879
    29       6     0.3949     0.6045     0.2906
    30       7     0.1582     0.8545     0.2116
    31       8     0.8387     0.8469     0.2847
    32       9     0.8686     0.494      0.1078
    33      10     0.5527     0.7624     0.0977
    34      11     0.4577     0.3839     0.1136
    35      12     0.0851     0.5606     0.4174
    36      13     0.6752     0.6595     0.4822
    37      14     0.8599     0.2019     0.4714
    38      15     0.438      0.621      0.3198
    39      16     0.137      0.859      0.1794
    40      17     0.847      0.861      0.3158
    41      18     0.105      0.69       0.4111
    42      19     0.2        0.48       0.4102
    43      20     0.579      0.684      0.507 
    44      21     0.639      0.731      0.4539
    45      22     0.968      0.132      0.4576
    46      23     0.741      0.216      0.4522
    47       2     0.9922     0.3997     0.749 
    48       3     0.499      0.6504     0.7474
    49       4     0.3647     0.4422     0.874 
    50       5     0.3383     0.4037     0.8121
    51       6     0.6051     0.3955     0.7094
    52       7     0.8418     0.1455     0.7884
    53       8     0.1613     0.1531     0.7153
    54       9     0.1314     0.506      0.8922
    55      10     0.4473     0.2376     0.9023
    56      11     0.5423     0.6161     0.8864
    57      12     0.9149     0.4394     0.5826
    58      13     0.3248     0.3405     0.5178
    59      14     0.1401     0.7981     0.5286
    60      15     0.562      0.379      0.6802
    61      16     0.863      0.141      0.8206
    62      17     0.153      0.139      0.6842
    63      18     0.895      0.31       0.5889
    64      19     0.8        0.52       0.5898
    65      20     0.421      0.316      0.493 
    66      21     0.361      0.269      0.5461
    67      22     0.032      0.868      0.5424
    68      23     0.259      0.784      0.5478
    69       2     0.0078     0.8997     0.751 
    70       3     0.501      0.1504     0.7526
    71       4     0.6353     0.9422     0.626 
    72       5     0.6617     0.9037     0.6879
    73       6     0.3949     0.8955     0.7906
    74       7     0.1582     0.6455     0.7116
    75       8     0.8387     0.6531     0.7847
    76       9     0.8686     0.006      0.6078
    77      10     0.5527     0.7376     0.5977
    78      11     0.4577     0.1161     0.6136
    79      12     0.0851     0.9394     0.9174
    80      13     0.6752     0.8405     0.9822
    81      14     0.8599     0.2981     0.9714
    82      15     0.438      0.879      0.8198
    83      16     0.137      0.641      0.6794
    84      17     0.847      0.639      0.8158
    85      18     0.105      0.81       0.9111
    86      19     0.2        0.02       0.9102
    87      20     0.579      0.816      0.007 
    88      21     0.639      0.769      0.9539
    89      22     0.968      0.368      0.9576
    90      23     0.741      0.284      0.9522


X-ray density (g/cm cub.)   =      2.93

MU (1/cm) =     154.449    Mass attenuation coefficient (cm**2/g) =     52.776

 Selected interatomic distances (cation-anion,anion-anion):

 NoP    Atom              Rad.sph.      C.N.    Distance     NoP N.
                           (angs.)               (angs.)

    1   Co   ,Ni             2.568        6
                                                 2.098       12
                                                 2.0758      13
                                                 2.0725      14
                                                 2.098       12
                                                 2.0758      13
                                                 2.0725      14
    2   Cu   ,Zn             2.808        6
                                                 2.3466       5
                                                 2.2885       6
                                                 2.0354       7
                                                 1.9864       8
                                                 2.0143       7
                                                 1.9981       8
    3   Cu   ,Zn             2.808        6
                                                 2.3882       5
                                                 1.9214       6
                                                 2.338        5
                                                 1.9358       6
                                                 2.0223       7
                                                 2.029        8
    4    S                   1.98         4
                                                 1.4851       5
                                                 1.4684       9
                                                 1.4743      10
                                                 1.4677      11
    5    O                   3.264       10
                                                 2.9817       6
                                                 3.2061       7
                                                 2.8688       8
                                                 2.4029       9
                                                 2.4032      10
                                                 2.3988      11
                                                 3.1641       6
                                                 3.066        6
                                                 2.9133       7
                                                 3.2047       8
    6    O                   3.264        8
                                                 2.9817       5
                                                 2.6795       7
                                                 2.9107       8
                                                 3.066        5
                                                 3.1641       5
                                                 2.9399       7
                                                 2.643        8
                                                 2.9071      11
    7    O                   3.264        7
                                                 3.2061       5
                                                 2.6795       6
                                                 2.6096       8
                                                 2.9133       5
                                                 2.9399       6
                                                 3.0064       8
                                                 3.0991       8
    8    O                   3.264        9
                                                 2.8688       5
                                                 2.9107       6
                                                 2.6096       7
                                                 3.2047       5
                                                 2.643        6
                                                 3.0991       7
                                                 3.0064       7
                                                 3.0483       9
                                                 3.0666      11
    9    O                   3.264        6
                                                 2.4029       5
                                                 2.4095      10
                                                 2.4174      11
                                                 3.0483       8
                                                 2.7297      12
                                                 2.8288      14
   10    O                   3.264        6
                                                 2.4032       5
                                                 2.4095       9
                                                 2.4083      11
                                                 2.7755      12
                                                 2.7411      14
                                                 2.9328      13
   11    O                   3.264        7
                                                 2.3988       5
                                                 2.4174       9
                                                 2.4083      10
                                                 2.9071       6
                                                 3.0666       8
                                                 2.7064      13
                                                 3.2224      14
   12    O                   3.264        6
                                                 2.9453      13
                                                 2.887       14
                                                 2.7297       9
                                                 2.7755      10
                                                 2.9574      13
                                                 3.0098      14
   13    O                   3.264        7
                                                 2.9453      12
                                                 2.998       14
                                                 2.7064      11
                                                 2.9328      10
                                                 2.9574      12
                                                 2.9453      13
                                                 2.8671      14
   14    O                   3.264        8
                                                 2.887       12
                                                 2.998       13
                                                 2.8288       9
                                                 2.7411      10
                                                 3.2224      11
                                                 3.0098      12
                                                 2.8671      13
                                                 3.1645      14
   15    H                   1.632        1
                                                 0.7213       6
   16    H                   1.632        1
                                                 0.7661       7
   17    H                   1.632        1
                                                 0.7417       8
   18    H                   1.632        1
                                                 0.8134      12
   19    H                   1.632        1
                                                 0.8408      12
   20    H                   1.632        1
                                                 0.8485      13
   21    H                   1.632        1
                                                 0.813       13
   22    H                   1.632        1
                                                 0.8328      14
   23    H                   1.632        1
                                                 0.7786      14

  X-ray diffraction powder data (II),  X-Ray W.L. =   1.78892(angs.):

  No   H   K   L   Theta 2*Theta    S       LPG   MF        F          I int.
                    ( degree )                                         *100

    1   0   0   2  4.327   8.654   0.042  348.37    2      176.3     3284.1
    2   0   0   4  8.679  17.358   0.084   84.9     2      225.9     1314.7
    3   0   1   1  8.704  17.409   0.085   84.39    4        8.5        3.7
    4   1   0   0  9.211  18.421   0.089   75.13    2        2.2        0.1
    5   0   1   2  9.488  18.976   0.092   70.68    4       25.6       28.1
    6   1   0  -2  9.828  19.655   0.095   65.73    2        6.5        0.9
    7   1   0   2 10.545  21.091   0.102   56.81    2      126.1      273.9
    8   0   1   3 10.671  21.342   0.104   55.43    4      114.9      443.9
    9   1   0  -4 12.112  24.225   0.117   42.55    2      106.1      145.4
   10   0   1   4 12.143  24.286   0.118   42.32    4        6.5        1.1
   11   1   1   0 12.535  25.069   0.121   39.59    4       21.0       10.6
   12   1   1  -1 12.579  25.159   0.122   39.3     4      103.2      253.7
   13   1   1   1 12.87   25.74    0.125   37.45    4       46.9       49.9
   14   1   1  -2 13.001  26.003   0.126   36.66    4       16.2        5.9
   15   0   0   6 13.082  26.164   0.127   36.18    2      199.2      435.5
   16   1   0   4 13.278  26.556   0.128   35.06    2      103.6      114.2
   17   1   1   2 13.56   27.12    0.131   33.54    4       24.1       11.9
   18   1   1  -3 13.768  27.536   0.133   32.47    4       40.8       32.8
   19   0   1   5 13.82   27.639   0.134   32.21    4      116.9      267.1
   20   1   1   3 14.558  29.116   0.141   28.83    4       16.1        4.5
   21   1   1  -4 14.83   29.659   0.143   27.72    4       23.4        9.2
   22   1   0  -6 15.376  30.753   0.148   25.64    2      125.1      121.8
   23   0   1   6 15.643  31.287   0.151   24.71    4        4.4        0.3
   24   1   1   4 15.81   31.621   0.152   24.15    4       22.5        7.4
   25   1   1  -5 16.135  32.269   0.155   23.12    4       58.7       48.4
   26   1   0   6 16.785  33.57    0.161   21.22    2       75.8       37.0
   27   0   2   0 17.045  34.09    0.164   20.52    2       63.3       25.0
   28   0   2   1 17.19   34.38    0.165   20.15    4       15.2        2.8
   29   1   1   5 17.27   34.539   0.166   19.95    4       38.6       18.1
   30   0   0   8 17.565  35.13    0.169   19.22    2      286.7      479.3
   31   0   1   7 17.578  35.157   0.169   19.19    4       31.4       11.5
   32   0   2   2 17.618  35.237   0.169   19.09    4       18.8        4.1
   33   1   1  -6 17.636  35.272   0.169   19.05    4       42.7       21.0
   34   0   2   3 18.313  36.626   0.176   17.54    4       41.4       18.3
   35   2   0   0 18.671  37.342   0.179   16.81    2      248.9      315.9
   36   2   0  -2 18.796  37.592   0.18    16.56    2       87.6       38.5
   37   1   1   6 18.895  37.791   0.181   16.37    4       13.0        1.7
   38   1   0  -8 19.184  38.367   0.184   15.83    2       38.7        7.2
   39   0   2   4 19.249  38.499   0.184   15.71    4       38.7       14.2
   40   1   1  -7 19.296  38.593   0.185   15.63    4       51.8       25.5
   41   1   2   0 19.51   39.021   0.187   15.25    4      110.8      113.6
   42   1   2  -1 19.541  39.081   0.187   15.2     4      164.5      249.7
   43   2   0   2 19.601  39.202   0.188   15.1     2      199.6      182.5
   44   0   1   8 19.603  39.205   0.188   15.09    4       11.5        1.2
   45   1   2   1 19.738  39.476   0.189   14.87    4      132.9      159.4
   46   1   2  -2 19.828  39.656   0.19    14.72    4       57.2       29.3
   47   2   0  -4 19.96   39.92    0.191   14.5     2       93.6       38.6
   48   1   2   2 20.216  40.432   0.193   14.09    4       71.0       43.1
   49   1   2  -3 20.363  40.725   0.195   13.87    4      232.9      456.6
   50   0   2   5 20.4    40.799   0.195   13.81    4        3.2        0.1
   51   2   1  -1 20.549  41.098   0.196   13.59    4       18.0        2.7
   52   2   1   0 20.615  41.23    0.197   13.49    4       90.4       66.9
   53   1   1   7 20.658  41.317   0.197   13.43    4       64.9       34.3
   54   2   1  -2 20.73   41.461   0.198   13.33    4       54.9       24.3
   55   1   0   8 20.741  41.483   0.198   13.31    2       44.4        8.0
   56   2   1   1 20.926  41.853   0.2     13.05    4       72.2       41.3
   57   1   2   3 20.931  41.861   0.2     13.04    4       33.6        8.9
   58   1   1  -8 21.088  42.176   0.201   12.83    4       68.9       36.9
   59   1   2  -4 21.13   42.26    0.202   12.77    4       76.1       44.9
   60   2   1  -3 21.154  42.308   0.202   12.74    4        2.2        0.0
   61   2   0   4 21.471  42.942   0.205   12.32    2      286.0      305.7
   62   2   1   2 21.474  42.949   0.205   12.31    4       42.5       13.5
   63   0   1   9 21.703  43.406   0.207   12.02    4       18.1        2.4
   64   0   2   6 21.737  43.473   0.207   11.98    4       22.6        3.7
   65   2   1  -4 21.808  43.616   0.208   11.89    4       20.3        3.0
   66   1   2   4 21.863  43.726   0.208   11.83    4       88.5       56.2
   67   2   0  -6 22.025  44.05    0.21    11.63    2      141.2       70.3
   68   1   2  -5 22.11   44.22    0.21    11.53    4      216.4      327.7
   69   0   0  10 22.163  44.325   0.211   11.47    2       26.0        2.4
   70   2   1   3 22.245  44.49    0.212   11.38    4       47.6       15.6
   71   1   1   8 22.537  45.074   0.214   11.05    4       26.1        4.6
   72   2   1  -5 22.677  45.354   0.216   10.89    4       56.1       20.8
   73   1   1  -9 22.991  45.982   0.218   10.56    4       62.4       24.9
   74   1   2   5 22.992  45.984   0.218   10.56    4      180.1      207.9
   75   2   1   4 23.221  46.442   0.22    10.32    4        0.6        0.0
   76   0   2   7 23.236  46.473   0.221   10.31    4       44.2       12.2
   77   1   2  -6 23.282  46.564   0.221   10.26    4       67.5       28.4
   78   1   0 -10 23.345  46.69    0.222   10.2     2       55.6        9.6
   79   2   1  -6 23.743  47.485   0.225    9.82    4        2.5        0.0
   80   0   1  10 23.873  47.746   0.226    9.7     4        5.8        0.2
   81   2   0   6 24.105  48.21    0.228    9.48    2      254.3      186.1
   82   1   2   6 24.298  48.595   0.23     9.31    4       53.9       16.4
   83   2   1   5 24.384  48.768   0.231    9.24    4       52.8       15.6
   84   1   1   9 24.516  49.032   0.232    9.13    4       16.9        1.6
   85   1   2  -7 24.626  49.253   0.233    9.03    4      269.8      399.1
   86   2   0  -8 24.813  49.626   0.235    8.88    2      229.7      142.1
   87   0   2   8 24.879  49.759   0.235    8.83    4       61.2       20.1
   88   2   1  -7 24.987  49.974   0.236    8.74    4        6.7        0.2
   89   1   1 -10 24.993  49.985   0.236    8.74    4       37.4        7.4
   90   1   0  10 25.017  50.034   0.236    8.72    2       22.0        1.3
   91   2   2  -1 25.67   51.339   0.242    8.22    4       10.8        0.6
   92   2   1   6 25.716  51.432   0.243    8.19    4       10.0        0.5
   93   2   2   0 25.725  51.45    0.243    8.18    4       37.1        6.8
   94   1   2   7 25.762  51.524   0.243    8.15    4      158.1      123.7
   95   2   2  -2 25.823  51.645   0.243    8.11    4       29.0        4.1
   96   2   2   1 25.988  51.977   0.245    7.99    4       14.0        0.9
   97   0   1  11 26.109  52.218   0.246    7.91    4       54.3       14.1
   98   1   2  -8 26.125  52.251   0.246    7.9     4       94.3       42.6
   99   2   2  -3 26.181  52.363   0.247    7.86    4        5.4        0.1
  100   0   3   1 26.187  52.373   0.247    7.86    4       16.4        1.3
  101   2   1  -8 26.392  52.785   0.248    7.72    4       34.5        5.6
  102   2   2   2 26.454  52.909   0.249    7.68    4       55.5       14.4
  103   0   3   2 26.494  52.989   0.249    7.65    4       13.5        0.8
  104   1   1  10 26.587  53.175   0.25     7.59    4        1.0        0.0
  105   0   2   9 26.65   53.3     0.251    7.55    4       22.9        2.4
  106   2   2  -4 26.74   53.48    0.252    7.49    4       26.8        3.3
  107   0   0  12 26.916  53.832   0.253    7.38    2      141.0       44.5
  108   0   3   3 27.001  54.003   0.254    7.33    4       57.7       14.8
  109   1   1 -11 27.084  54.169   0.255    7.27    4       82.0       29.7
  110   2   2   3 27.116  54.233   0.255    7.26    4       60.6       16.2
  111   2   1   7 27.201  54.403   0.256    7.2     4       15.5        1.0
  112   2   0   8 27.345  54.691   0.257    7.12    2      252.8      138.0
  113   1   2   8 27.369  54.738   0.257    7.1     4       87.7       33.2
  114   2   2  -5 27.491  54.981   0.258    7.03    4       36.7        5.7
  115   0   3   4 27.701  55.402   0.26     6.91    4       43.0        7.8
  116   1   2  -9 27.764  55.528   0.26     6.88    4      223.5      208.4
  117   1   0 -12 27.796  55.592   0.261    6.86    2       58.0        7.0
  118   1   3   0 27.899  55.798   0.262    6.8     4       23.3        2.2
  119   1   3  -1 27.922  55.844   0.262    6.79    4       81.6       27.4
  120   2   1  -9 27.945  55.89    0.262    6.78    4        8.0        0.3
  121   2   2   4 27.965  55.93    0.262    6.76    4       92.3       35.0
  122   1   3   1 28.073  56.145   0.263    6.71    4       37.6        5.7
  123   1   3  -2 28.141  56.283   0.264    6.67    4        0.7        0.0
  124   2   0 -10 28.178  56.356   0.264    6.65    2       77.8       12.2
  125   0   1  12 28.413  56.825   0.266    6.53    4        8.6        0.3
  126   2   2  -6 28.423  56.846   0.266    6.52    4       30.2        3.6
  127   1   3   2 28.441  56.882   0.266    6.51    4       17.1        1.2
  128   0   2  10 28.537  57.075   0.267    6.46    4       45.6        8.2
  129   1   3  -3 28.554  57.109   0.267    6.45    4       68.7       18.5
  130   0   3   5 28.583  57.166   0.267    6.44    4       36.2        5.1
  131   3   0  -2 28.64   57.281   0.268    6.41    2        5.8        0.1
  132   3   0   0 28.698  57.396   0.268    6.38    2       19.8        0.8
  133   1   1  11 28.746  57.492   0.269    6.36    4        5.7        0.1
  134   2   1   8 28.827  57.654   0.27     6.32    4       19.4        1.4
  135   2   2   5 28.989  57.979   0.271    6.24    4        5.9        0.1
  136   1   3   3 28.999  57.997   0.271    6.23    4       33.6        4.3
  137   1   2   9 29.107  58.214   0.272    6.18    4      150.0       84.3
  138   1   3  -4 29.156  58.311   0.272    6.16    4       23.7        2.1
  139   1   1 -12 29.263  58.526   0.273    6.11    4       26.2        2.5
  140   3   0  -4 29.352  58.705   0.274    6.06    2       17.5        0.6
  141   3   0   2 29.523  59.046   0.275    5.98    2      102.3       19.0
  142   2   2  -7 29.526  59.052   0.275    5.98    4       29.8        3.2
  143   1   2 -10 29.531  59.062   0.276    5.98    4       37.4        5.1
  144   1   0  12 29.577  59.153   0.276    5.96    2       77.7       10.9
  145   2   1 -10 29.632  59.265   0.276    5.94    4        4.3        0.1
  146   0   3   6 29.638  59.276   0.276    5.93    4       23.6        2.0
  147   1   3   4 29.739  59.479   0.277    5.89    4       20.7        1.5
  148   1   3  -5 29.938  59.876   0.279    5.8     4       54.7       10.5
  149   3   1  -1 30.015  60.029   0.28     5.77    4       24.1        2.0
  150   3   1  -2 30.081  60.161   0.28     5.74    4       18.0        1.1
  151   3   1   0 30.137  60.273   0.281    5.72    4        5.7        0.1
  152   2   2   6 30.18   60.359   0.281    5.7     4       62.3       13.4
  153   3   1  -3 30.334  60.668   0.282    5.63    4       85.5       25.0
  154   3   1   1 30.445  60.891   0.283    5.59    4       55.0       10.3
  155   0   2  11 30.534  61.068   0.284    5.55    4        7.6        0.2
  156   2   1   9 30.583  61.166   0.284    5.53    4       72.5       17.6
  157   1   3   5 30.655  61.311   0.285    5.5     4       72.9       17.7
  158   3   1  -4 30.772  61.544   0.286    5.46    4       61.6       12.6
  159   0   1  13 30.787  61.573   0.286    5.45    4      131.9       57.5
  160   2   2  -8 30.79   61.58    0.286    5.45    4       60.4       12.1
  161   3   0  -6 30.8    61.601   0.286    5.44    2      100.1       16.6
  162   0   3   7 30.856  61.712   0.287    5.42    4       26.9        2.4
  163   1   3  -6 30.894  61.788   0.287    5.41    4       29.7        2.9
  164   3   1   2 30.938  61.875   0.287    5.39    4        8.9        0.3
  165   1   2  10 30.967  61.934   0.288    5.38    4       46.3        7.0
  166   1   1  12 30.99   61.98    0.288    5.37    4       22.9        1.7
  167   3   0   4 31.076  62.153   0.289    5.34    2       34.5        1.9
  168   2   0  10 31.087  62.173   0.289    5.33    2      192.3       59.8
  169   3   1  -5 31.39   62.779   0.291    5.22    4        0.7        0.0
  170   1   2 -11 31.419  62.837   0.291    5.21    4      217.7      149.8
  171   2   1 -11 31.446  62.893   0.292    5.2     4       40.5        5.2
  172   2   2   7 31.525  63.051   0.292    5.17    4       35.6        4.0
  173   1   1 -13 31.527  63.054   0.292    5.17    4       17.7        1.0
  174   3   1   3 31.608  63.216   0.293    5.14    4       54.5        9.3
  175   1   3   6 31.738  63.476   0.294    5.1     4       31.9        3.1
  176   0   0  14 31.879  63.759   0.295    5.05    2      156.6       37.5
  177   1   3  -7 32.014  64.029   0.296    5.0     4        3.2        0.0
  178   2   0 -12 32.027  64.054   0.296    5.0     2      227.3       78.3
  179   3   1  -6 32.182  64.364   0.298    4.94    4       43.0        5.6
  180   2   2  -9 32.206  64.412   0.298    4.94    4       19.7        1.2
  181   0   3   8 32.228  64.456   0.298    4.93    4       38.7        4.5
  182   3   1   4 32.451  64.903   0.3      4.86    4       23.2        1.6
  183   2   1  10 32.461  64.923   0.3      4.85    4       21.6        1.4
  184   1   0 -14 32.537  65.075   0.301    4.83    2       96.6       13.7
  185   0   2  12 32.636  65.272   0.301    4.8     4       19.2        1.1
  186   2   3  -1 32.901  65.801   0.304    4.71    4       43.0        5.3
  187   3   0  -8 32.929  65.858   0.304    4.71    2       87.3       10.9
  188   1   2  11 32.943  65.887   0.304    4.7     4      184.6       97.2
  189   2   3   0 32.948  65.896   0.304    4.7     4       42.4        5.1
  190   1   3   7 32.979  65.959   0.304    4.69    4       56.3        9.0
  191   2   2   8 33.019  66.037   0.305    4.68    4        0.3        0.0
  192   2   3  -2 33.032  66.063   0.305    4.68    4       27.8        2.2
  193   3   1  -7 33.142  66.285   0.306    4.64    4       27.7        2.2
  194   2   3   1 33.174  66.348   0.306    4.63    4       50.5        7.2
  195   0   1  14 33.236  66.472   0.306    4.61    4        0.0        0.0
  196   1   3  -8 33.292  66.584   0.307    4.6     4        0.8        0.0
  197   3   0   6 33.301  66.602   0.307    4.59    2       61.8        5.3
  198   1   1  13 33.322  66.644   0.307    4.59    4       27.5        2.1
  199   2   3  -3 33.34   66.68    0.307    4.58    4       44.9        5.6
  200   2   1 -12 33.381  66.761   0.308    4.57    4        6.1        0.1
  201   1   2 -12 33.422  66.844   0.308    4.56    4      116.2       37.3
  202   3   1   5 33.461  66.921   0.308    4.55    4       71.7       14.2
  203   2   3   2 33.576  67.152   0.309    4.52    4       49.8        6.8
  204   0   3   9 33.746  67.492   0.311    4.47    4       13.6        0.5
  205   2   2 -10 33.765  67.531   0.311    4.46    4       39.4        4.2
  206   2   3  -4 33.824  67.648   0.311    4.45    4       39.6        4.2
  207   1   1 -14 33.88   67.761   0.312    4.43    4       28.9        2.2
  208   3   2  -1 34.121  68.243   0.314    4.37    4      270.6      194.0
  209   2   3   3 34.152  68.303   0.314    4.36    4       43.5        5.0
  210   3   2  -2 34.183  68.366   0.314    4.35    4       55.5        8.1
  211   3   2   0 34.235  68.47    0.314    4.34    4      126.1       41.8
  212   3   1  -8 34.264  68.528   0.315    4.33    4        7.4        0.1
  213   1   3   8 34.373  68.745   0.316    4.3     4       37.0        3.6
  214   3   2  -3 34.419  68.839   0.316    4.29    4      209.4      114.1
  215   1   0  14 34.438  68.876   0.316    4.28    2        9.1        0.1
  216   2   1  11 34.459  68.918   0.316    4.28    4       14.5        0.5
  217   2   3  -5 34.479  68.959   0.316    4.27    4       46.4        5.6
  218   3   2   1 34.524  69.048   0.317    4.26    4      213.0      117.3
  219   3   1   6 34.629  69.259   0.318    4.24    4       36.4        3.4
  220   2   2   9 34.652  69.305   0.318    4.23    4       20.0        1.0
  221   1   3  -9 34.72   69.439   0.318    4.21    4       55.2        7.8
  222   3   2  -4 34.829  69.659   0.319    4.19    4       80.4       16.4
  223   0   2  13 34.843  69.686   0.319    4.18    4       21.0        1.1
  224   2   3   4 34.897  69.793   0.32     4.17    4       43.2        4.7
  225   3   2   2 34.985  69.97    0.321    4.15    4        8.4        0.2
  226   1   2  12 35.034  70.068   0.321    4.14    4      151.5       57.6
  227   2   0  12 35.279  70.558   0.323    4.08    2      234.6       68.1
  228   2   3  -6 35.302  70.604   0.323    4.07    4       21.0        1.1
  229   0   3  10 35.404  70.808   0.324    4.05    4        6.3        0.1
  230   3   2  -5 35.41   70.82    0.324    4.05    4      151.0       56.0
  231   2   1 -13 35.433  70.867   0.324    4.04    4       52.9        6.9
  232   2   2 -11 35.463  70.927   0.324    4.04    4        4.5        0.0
  233   1   2 -13 35.54   71.079   0.325    4.02    4      190.3       88.3
  234   3   1  -9 35.541  71.083   0.325    4.02    4       62.7        9.6
  235   3   2   3 35.616  71.232   0.326    4.0     4      142.6       49.4
  236   3   0 -10 35.68   71.36    0.326    3.99    2        8.1        0.1
  237   1   1  14 35.747  71.493   0.327    3.97    4       23.2        1.3
  238   0   1  15 35.77   71.539   0.327    3.97    4       11.5        0.3
  239   2   3   5 35.807  71.613   0.327    3.96    4        6.1        0.1
  240   0   4   0 35.891  71.782   0.328    3.94    2      144.6       25.0
  241   1   3   9 35.912  71.823   0.328    3.94    4       32.1        2.5
  242   3   1   7 35.952  71.904   0.328    3.93    4       29.8        2.1
  243   0   4   1 35.977  71.953   0.328    3.92    4      163.4       63.6
  244   3   0   8 36.141  72.282   0.33     3.89    2        4.0        0.0
  245   3   2  -6 36.158  72.316   0.33     3.89    4       11.0        0.3
  246   0   4   2 36.234  72.467   0.33     3.87    4      221.5      115.2
  247   2   3  -7 36.287  72.575   0.331    3.86    4       74.7       13.1
  248   1   3 -10 36.292  72.584   0.331    3.86    4       11.6        0.3
  249   2   0 -14 36.324  72.648   0.331    3.85    2      212.0       52.5
  250   1   1 -15 36.328  72.655   0.331    3.85    4       28.9        1.9
  251   3   2   4 36.413  72.826   0.332    3.83    4       82.4       15.8
  252   2   2  10 36.422  72.845   0.332    3.83    4       12.3        0.4
  253   2   1  12 36.574  73.149   0.333    3.8     4        5.3        0.1
  254   0   4   3 36.66   73.32    0.334    3.78    4      100.9       23.4
  255   2   3   6 36.877  73.754   0.335    3.74    4        5.2        0.1
  256   3   1 -10 36.969  73.939   0.336    3.73    4       12.5        0.4
  257   3   2  -7 37.069  74.138   0.337    3.71    4      183.8       76.0
  258   0   0  16 37.127  74.254   0.337    3.7     2      187.6       39.4
  259   0   2  14 37.159  74.317   0.338    3.69    4       37.1        3.1
  260   0   3  11 37.198  74.397   0.338    3.68    4       48.2        5.2
  261   1   2  13 37.24   74.48    0.338    3.68    4      217.6      105.6
  262   0   4   4 37.254  74.508   0.338    3.67    4      147.9       48.7
  263   2   2 -12 37.296  74.593   0.339    3.67    4        6.3        0.1
  264   3   2   5 37.372  74.745   0.339    3.65    4      163.3       59.1
  265   1   4   0 37.424  74.847   0.34     3.64    4       49.5        5.4
  266   3   1   8 37.424  74.849   0.34     3.64    4       14.8        0.5
  267   2   3  -8 37.432  74.863   0.34     3.64    4        0.6        0.0
  268   1   4  -1 37.443  74.887   0.34     3.64    4       31.3        2.2
  269   1   4   1 37.573  75.145   0.341    3.62    4       60.9        8.1
  270   1   3  10 37.593  75.185   0.341    3.61    4        3.5        0.0
  271   2   1 -14 37.605  75.21    0.341    3.61    4       69.1       10.5
  272   1   0 -16 37.612  75.225   0.341    3.61    2        5.9        0.0
  273   1   4  -2 37.632  75.264   0.341    3.61    4       17.2        0.6
  274   1   2 -14 37.773  75.546   0.342    3.58    4       19.6        0.8
  275   1   4   2 37.89   75.78    0.343    3.56    4       59.5        7.7
  276   1   4  -3 37.988  75.976   0.344    3.55    4        9.3        0.2
  277   1   3 -11 38.006  76.012   0.344    3.54    4       28.1        1.7
  278   0   4   5 38.013  76.026   0.344    3.54    4       73.7       11.7
  279   2   3   7 38.104  76.208   0.345    3.53    4       35.0        2.6
  280   3   2  -8 38.14   76.281   0.345    3.52    4       91.7       18.0
  281   1   1  15 38.272  76.544   0.346    3.5     4       94.0       18.8
  282   2   2  11 38.327  76.654   0.347    3.49    4       29.5        1.8
  283   1   4   3 38.374  76.748   0.347    3.48    4        9.0        0.2
  284   0   1  16 38.398  76.796   0.347    3.48    4       24.1        1.2
  285   3   2   6 38.491  76.981   0.348    3.47    4       20.2        0.9
  286   1   4  -4 38.511  77.022   0.348    3.46    4       17.7        0.7
  287   3   1 -11 38.544  77.089   0.348    3.46    4       62.6        8.2
  288   2   3  -9 38.731  77.461   0.35     3.43    4       46.9        4.6
  289   2   1  13 38.811  77.621   0.35     3.42    4       57.5        6.8
  290   1   1 -16 38.878  77.756   0.351    3.41    4       47.5        4.7
  291   0   4   6 38.934  77.867   0.351    3.4     4      145.4       43.6
  292   3   0 -12 39.013  78.025   0.352    3.39    2       29.0        0.9
  293   1   4   4 39.023  78.045   0.352    3.39    4       33.1        2.3
  294   3   1   9 39.043  78.086   0.352    3.38    4       24.3        1.2
  295   0   3  12 39.129  78.258   0.353    3.37    4       16.8        0.6
  296   1   4  -5 39.198  78.396   0.353    3.36    4        9.9        0.2
  297   2   2 -13 39.264  78.528   0.354    3.35    4       31.7        2.0
  298   3   2  -9 39.368  78.737   0.355    3.34    4      178.5       64.5
  299   1   3  11 39.414  78.829   0.355    3.33    4        7.8        0.1
  300   2   3   8 39.484  78.969   0.355    3.32    4       56.1        6.4
  301   3   0  10 39.559  79.118   0.356    3.31    2        9.1        0.1
  302   1   2  14 39.566  79.132   0.356    3.31    4       45.2        4.1
  303   0   2  15 39.589  79.177   0.356    3.31    4        4.2        0.0
  304   4   0  -2 39.635  79.27    0.357    3.3     2      151.2       22.9
  305   1   0  16 39.662  79.324   0.357    3.3     2       24.9        0.6
  306   3   2   7 39.765  79.53    0.358    3.28    4      152.1       46.1
  307   4   0   0 39.811  79.623   0.358    3.28    2      101.4       10.2
  308   1   4   5 39.834  79.669   0.358    3.28    4       28.3        1.6
  309   1   3 -12 39.861  79.721   0.358    3.27    4        8.4        0.1
  310   2   1 -15 39.899  79.799   0.359    3.27    4       31.3        1.9
  311   2   0  14 39.928  79.856   0.359    3.26    2       96.7        9.3
  312   0   4   7 40.014  80.027   0.359    3.25    4      135.4       36.2
  313   1   4  -6 40.047  80.095   0.36     3.25    4       52.2        5.4
  314   4   0  -4 40.121  80.242   0.36     3.24    2      231.1       52.5
  315   1   2 -15 40.128  80.256   0.36     3.24    4      134.2       35.4
  316   2   3 -10 40.182  80.364   0.361    3.23    4        5.2        0.1
  317   3   1 -12 40.265  80.531   0.361    3.22    4        8.7        0.1
  318   2   2  12 40.367  80.735   0.362    3.21    4       48.1        4.5
  319   3   3  -1 40.516  81.032   0.363    3.19    4       29.8        1.7
  320   3   3  -2 40.574  81.148   0.364    3.19    4       61.4        7.3
  321   3   3   0 40.623  81.247   0.364    3.18    4       21.4        0.9
  322   4   0   2 40.649  81.298   0.364    3.18    2       96.1        8.9
  323   3   2 -10 40.751  81.501   0.365    3.17    4       35.3        2.4
  324   3   3  -3 40.797  81.594   0.365    3.16    4       27.1        1.4
  325   1   4   6 40.807  81.613   0.365    3.16    4       31.0        1.8
  326   3   1  10 40.807  81.615   0.365    3.16    4       39.1        2.9
  327   4   1  -2 40.883  81.765   0.366    3.15    4        3.1        0.0
  328   4   1  -1 40.888  81.776   0.366    3.15    4       60.9        7.1
  329   3   3   1 40.895  81.79    0.366    3.15    4       13.5        0.3
  330   1   1  16 40.91   81.82    0.366    3.15    4        7.8        0.1
  331   2   3   9 41.017  82.033   0.367    3.14    4       10.3        0.2
  332   4   1  -3 41.042  82.084   0.367    3.13    4       16.4        0.5
  333   1   4  -7 41.057  82.114   0.367    3.13    4       31.0        1.8
  334   4   1   0 41.058  82.116   0.367    3.13    4        6.4        0.1
  335   2   0 -16 41.086  82.172   0.367    3.13    2      215.6       44.1
  336   0   1  17 41.135  82.27    0.368    3.12    4        7.4        0.1
  337   2   1  14 41.174  82.348   0.368    3.12    4        0.0        0.0
  338   3   3  -4 41.184  82.368   0.368    3.12    4       17.1        0.6
  339   3   2   8 41.193  82.386   0.368    3.12    4       87.1       14.4
  340   0   3  13 41.197  82.394   0.368    3.12    4       21.9        0.9
  341   0   4   8 41.251  82.502   0.369    3.11    4       82.4       12.8
  342   4   0  -6 41.265  82.53    0.369    3.11    2      145.1       19.9
  343   3   3   2 41.331  82.663   0.369    3.1     4       31.0        1.8
  344   4   1  -4 41.366  82.731   0.369    3.1     4       17.5        0.6
  345   2   2 -14 41.369  82.738   0.369    3.1     4        1.1        0.0
  346   1   3  12 41.378  82.756   0.37     3.1     4       50.3        4.8
  347   4   1   1 41.392  82.785   0.37     3.1     4       48.9        4.5
  348   1   1 -17 41.545  83.089   0.371    3.08    4       67.0        8.4
  349   3   3  -5 41.735  83.469   0.372    3.06    4       19.7        0.7
  350   2   3 -11 41.785  83.571   0.372    3.06    4       58.8        6.4
  351   4   1  -5 41.853  83.706   0.373    3.05    4       14.4        0.4
  352   1   3 -13 41.858  83.716   0.373    3.05    4       43.0        3.4
  353   2   4  -1 41.866  83.732   0.373    3.05    4       68.3        8.6
  354   4   1   2 41.89   83.78    0.373    3.05    4       16.8        0.5
  355   2   4   0 41.909  83.819   0.373    3.05    4       93.8       16.2
  356   3   3   3 41.931  83.861   0.374    3.04    4        0.1        0.0
  357   1   4   7 41.938  83.877   0.374    3.04    4       23.5        1.0
  358   2   4  -2 41.986  83.972   0.374    3.04    4      145.9       39.3
  359   1   2  15 42.02   84.041   0.374    3.04    4      199.5       73.3
  360   2   4   1 42.117  84.234   0.375    3.03    4      114.4       24.0
  361   3   1 -13 42.133  84.266   0.375    3.03    4       18.9        0.7
  362   4   0   4 42.139  84.278   0.375    3.03    2      184.1       31.1
  363   0   2  16 42.144  84.287   0.375    3.03    4       81.3       12.1
  364   1   4  -8 42.226  84.452   0.376    3.02    4       60.5        6.7
  365   2   4  -3 42.27   84.541   0.376    3.01    4       36.8        2.5
  366   3   2 -11 42.287  84.574   0.376    3.01    4      104.4       19.9
  367   2   1 -16 42.325  84.65    0.376    3.01    4       14.7        0.4
  368   3   3  -6 42.448  84.896   0.377    3.0     4        1.1        0.0
  369   2   4   2 42.488  84.977   0.378    3.0     4      175.3       55.8
  370   4   1  -6 42.503  85.007   0.378    2.99    4       55.7        5.6
  371   2   2  13 42.548  85.096   0.378    2.99    4       69.5        8.8
  372   4   1   3 42.551  85.102   0.378    2.99    4        7.3        0.1
  373   1   2 -16 42.614  85.228   0.378    2.98    4       49.0        4.3
  374   0   4   9 42.645  85.291   0.379    2.98    4       66.7        8.1
  375   3   3   4 42.692  85.384   0.379    2.98    4       32.1        1.9
  376   2   3  10 42.701  85.402   0.379    2.98    4        5.2        0.0
  377   2   4  -4 42.718  85.436   0.379    2.98    4       51.4        4.8
  378   3   1  11 42.72   85.439   0.379    2.98    4       29.3        1.5
  379   0   0  18 42.768  85.535   0.38     2.97    2      134.8       16.4
  380   3   2   9 42.776  85.551   0.38     2.97    4      120.4       26.1
  381   3   0 -14 42.919  85.839   0.381    2.96    2       35.4        1.1
  382   2   4   3 43.023  86.045   0.381    2.95    4      130.7       30.6
  383   4   0  -8 43.057  86.115   0.382    2.95    2      198.6       35.3
  384   1   0 -18 43.112  86.224   0.382    2.95    2        5.3        0.0
  385   1   4   8 43.229  86.457   0.383    2.94    4       15.5        0.4
  386   4   1  -7 43.316  86.631   0.383    2.93    4       74.8        9.9
  387   3   3  -7 43.323  86.646   0.384    2.93    4       12.2        0.3
  388   2   4  -5 43.328  86.656   0.384    2.93    4      102.2       18.6
  389   4   1   4 43.374  86.747   0.384    2.93    4       24.3        1.0
  390   0   3  14 43.409  86.818   0.384    2.92    4       54.1        5.2
  391   1   3  13 43.488  86.975   0.385    2.92    4       66.2        7.8
  392   2   3 -12 43.542  87.084   0.385    2.91    4       12.3        0.3
  393   1   4  -9 43.553  87.106   0.385    2.91    4       14.6        0.4
  394   3   0  12 43.554  87.107   0.385    2.91    2       38.2        1.3
  395   3   3   5 43.615  87.231   0.386    2.91    4       27.6        1.3
  396   2   2 -15 43.618  87.236   0.386    2.91    4        7.6        0.1
  397   2   1  15 43.674  87.348   0.386    2.91    4        8.3        0.1
  398   1   1  17 43.676  87.353   0.386    2.91    4       21.5        0.8
  399   2   4   4 43.719  87.439   0.386    2.9     4      129.4       29.5
  400   3   2 -12 43.979  87.958   0.388    2.89    4       54.3        5.2
  401   0   1  18 44.001  88.001   0.388    2.88    4        9.5        0.2
  402   1   3 -14 44.003  88.006   0.388    2.88    4       15.6        0.4
  403   2   4  -6 44.101  88.202   0.389    2.88    4      131.9       30.4
  404   3   1 -14 44.152  88.304   0.389    2.88    4       60.9        6.5
  405   0   4  10 44.197  88.394   0.39     2.87    4      141.3       34.8
  406   4   0   6 44.274  88.549   0.39     2.87    2      128.4       14.3
  407   4   1  -8 44.29   88.579   0.39     2.87    4       36.9        2.4
  408   1   1 -18 44.344  88.688   0.391    2.86    4       15.8        0.4
  409   4   1   5 44.358  88.716   0.391    2.86    4       35.0        2.1
  410   3   3  -8 44.359  88.719   0.391    2.86    4       27.4        1.3
  411   3   2  10 44.515  89.029   0.392    2.85    4        2.3        0.0
  412   2   3  11 44.541  89.081   0.392    2.85    4       36.9        2.4
  413   2   4   5 44.579  89.157   0.392    2.85    4      112.9       22.1
  414   4   2  -2 44.589  89.178   0.392    2.85    4       14.9        0.4
  415   4   2  -1 44.594  89.188   0.392    2.85    4       30.7        1.6
  416   1   2  16 44.616  89.232   0.393    2.85    4       65.0        7.3
  417   1   4   9 44.678  89.356   0.393    2.84    4       32.8        1.9
  418   3   3   6 44.7    89.4     0.393    2.84    4       62.5        6.7
  419   4   2  -3 44.747  89.493   0.394    2.84    4       26.5        1.2
  420   4   2   0 44.763  89.525   0.394    2.84    4        1.8        0.0
  421   3   1  12 44.785  89.57    0.394    2.84    4       10.0        0.2
  422   0   2  17 44.839  89.678   0.394    2.84    4       63.3        6.9
  423   2   2  14 44.877  89.755   0.394    2.83    4       81.9       11.5
  424   2   1 -17 44.895  89.79    0.395    2.83    4       20.9        0.8


  X-ray diffraction powder data (I)...X-Ray wave length =  1.78892 (angs.):

  No   H   K   L   Theta 2*Theta    d           I int   I int.n.  I p.h.n.   H(Si)
                    ( degree )   (angstrem)     *100                         *100

    1   0   0   2   4.327   8.654 11.85538     3284.1    100.0    100.0     5.6
    2   0   0   4   8.679  17.358  5.92769     1318.3     40.1     39.9     5.6
    3   1   0   2  10.545  21.091  4.8874       273.9      8.3      8.3     5.6
    4   0   1   3  10.671  21.342  4.83049      443.9     13.5     13.4     5.6
    5   1   0  -4  12.112  24.225  4.26277      145.4      4.4      4.4     5.6
    6   1   1  -1  12.579  25.159  4.10693      253.7      7.7      7.6     5.6
    7   1   1   1  12.87   25.74   4.01566       49.9      1.5      1.5     5.6
    8   0   0   6  13.082  26.164  3.95179      435.5     13.3     13.1     5.6
    9   1   0   4  13.278  26.556  3.89442      114.2      3.5      3.4     5.6
   10   0   1   5  13.82   27.639  3.7446       267.1      8.1      8.0     5.6
   11   1   0  -6  15.376  30.753  3.37328      121.8      3.7      3.7     5.6
   12   1   1  -5  16.135  32.269  3.21868       48.4      1.5      1.4     5.6
   13   1   0   6  16.785  33.57   3.09737       37.0      1.1      1.1     5.7
   14   0   0   8  17.565  35.13   2.96385      490.8     14.9     14.7     5.7
   15   2   0   0  18.671  37.342  2.79404      315.9      9.6      9.4     5.7
   16   2   0  -2  18.796  37.592  2.77607       38.5      1.2      1.1     5.7
   17   1   2   0  19.51   39.021  2.6782       113.6      3.5      3.4     5.7
   18   1   2  -1  19.541  39.081  2.67422      249.7      7.6      7.4     5.7
   19   2   0   2  19.601  39.202  2.66632      183.7      5.6      5.5     5.7
   20   1   2   1  19.738  39.476  2.64853      159.4      4.9      4.7     5.7
   21   2   0  -4  19.96   39.92   2.62024       38.6      1.2      1.1     5.7
   22   1   2   2  20.216  40.432  2.58841       43.1      1.3      1.3     5.7
   23   1   2  -3  20.363  40.725  2.57056      456.6     13.9     13.6     5.7
   24   2   1   0  20.615  41.23   2.54046       66.9      2.0      2.0     5.7
   25   1   1   7  20.658  41.317  2.53535       34.3      1.0      1.0     5.7
   26   2   1   1  20.926  41.853  2.50432       50.2      1.5      1.5     5.7
   27   1   1  -8  21.088  42.176  2.486         36.9      1.1      1.1     5.7
   28   1   2  -4  21.13   42.26   2.48127       45.0      1.4      1.3     5.7
   29   2   0   4  21.471  42.942  2.4437       319.2      9.7      9.5     5.7
   30   1   2   4  21.863  43.726  2.40197       56.2      1.7      1.7     5.7
   31   2   0  -6  22.025  44.05   2.38518       70.3      2.1      2.1     5.7
   32   1   2  -5  22.11   44.22   2.37644      327.7     10.0      9.7     5.7
   33   1   2   5  22.992  45.984  2.28995      232.8      7.1      6.9     5.7
   34   2   0   6  24.105  48.21   2.1901       186.1      5.7      5.5     5.7
   35   1   2  -7  24.626  49.253  2.14653      399.1     12.2     11.8     5.7
   36   2   0  -8  24.813  49.626  2.13138      142.1      4.3      4.2     5.7
   37   1   2   7  25.762  51.524  2.05797      123.7      3.8      3.6     5.8
   38   1   2  -8  26.125  52.251  2.03131       56.7      1.7      1.7     5.8
   39   0   0  12  26.916  53.832  1.9759        44.5      1.4      1.3     5.8
   40   2   0   8  27.345  54.691  1.94721      171.2      5.2      5.0     5.8
   41   1   2  -9  27.764  55.528  1.92014      208.4      6.3      6.1     5.8
   42   2   2   4  27.965  55.93   1.90745       35.0      1.1      1.0     5.8
   43   1   2   9  29.107  58.214  1.83879       84.3      2.6      2.5     5.8
   44   3   0  -6  30.8    61.601  1.74683       98.7      3.0      2.9     5.8
   45   2   0  10  31.087  62.173  1.73233       61.8      1.9      1.8     5.8
   46   1   2 -11  31.419  62.837  1.71587      155.0      4.7      4.5     5.9
   47   0   0  14  31.879  63.759  1.69363       37.5      1.1      1.1     5.9
   48   2   0 -12  32.027  64.054  1.68664       78.3      2.4      2.3     5.9
   49   1   2  11  32.943  65.887  1.64481      118.5      3.6      3.4     5.9
   50   1   2 -12  33.422  66.844  1.62393       37.3      1.1      1.1     5.9
   51   3   2  -1  34.121  68.243  1.59455      194.0      5.9      5.6     5.9
   52   3   2   0  34.235  68.47   1.58989       42.0      1.3      1.2     5.9
   53   3   2  -3  34.419  68.839  1.58242      114.2      3.5      3.3     5.9
   54   3   2   1  34.524  69.048  1.57823      117.3      3.6      3.4     5.9
   55   1   2  12  35.034  70.068  1.55812       57.6      1.8      1.6     5.9
   56   2   0  12  35.279  70.558  1.54869       69.2      2.1      2.0     5.9
   57   3   2  -5  35.41   70.82   1.54371       62.9      1.9      1.8     5.9
   58   1   2 -13  35.54   71.079  1.53882       97.9      3.0      2.8     5.9
   59   3   2   3  35.616  71.232  1.53595       49.4      1.5      1.4     5.9
   60   0   4   1  35.977  71.953  1.5226        65.7      2.0      1.9     5.9
   61   0   4   2  36.234  72.467  1.51327      115.2      3.5      3.3     5.9
   62   2   0 -14  36.324  72.648  1.51002       54.5      1.7      1.5     6.0
   63   3   2  -7  37.069  74.138  1.48389       76.0      2.3      2.2     6.0
   64   0   0  16  37.127  74.254  1.48192       39.4      1.2      1.1     6.0
   65   1   2  13  37.24   74.48   1.47806      154.4      4.7      4.4     6.0
   66   3   2   5  37.372  74.745  1.47359       59.1      1.8      1.7     6.0
   67   0   4   6  38.934  77.867  1.42335       43.6      1.3      1.2     6.0
   68   3   2  -9  39.368  78.737  1.41015       64.5      2.0      1.8     6.0
   69   3   2   7  39.765  79.53   1.39838       46.1      1.4      1.3     6.0
   70   0   4   7  40.014  80.027  1.39114       36.2      1.1      1.0     6.0
   71   4   0  -4  40.121  80.242  1.38804       87.9      2.7      2.5     6.0
   72   2   0 -16  41.086  82.172  1.36103       46.0      1.4      1.3     6.1
   73   2   4  -2  41.986  83.972  1.33711       39.3      1.2      1.1     6.1
   74   1   2  15  42.02   84.041  1.33622       73.3      2.2      2.0     6.1
   75   4   0   4  42.139  84.278  1.33316       67.9      2.1      1.9     6.1
   76   2   4   2  42.488  84.977  1.32426       61.5      1.9      1.7     6.1
   77   3   2   9  42.776  85.551  1.31707       42.5      1.3      1.2     6.1
   78   4   0  -8  43.057  86.115  1.31012       35.3      1.1      1.0     6.1
   79   0   4  10  44.197  88.394  1.28306       34.8      1.1      1.0     6.2

Reference:
Chichagov A.V. et al.
Information-Calculating System on Crystal Structure Data of Minerals
(MINCRYST)
- Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian)