Institute of Experimental Mineralogy Russian Academy of Sciences ------------------------------------------------- 142432, Chernogolovka, Moscow district A.V. Chichagov +7(496)52-22320 *** *** W W W - X R A Y P O L *** *********************** RIOMARINAITE 1, syn Bi(OH)SO(4).H(2)O Monoclinic P 2(1)/n Z = 4 P2(1)/n 28 .5 .1907 Ref.Str.: Graunar M., Lazarini F. (1982) * Acta Cryst., B38, 2879-2881 Reserv: N.A.D. Initial data from BDM-file Lattice parameters (cub. angs.,degr.): a = 6.021 alpha = 90.0 b = 13.363 beta = 112.94 c = 6.495 gamma = 90.0 Unit cell volume (cub. angs.) = 481.25 Molar volume ( cub.cm/mol.) = 72.47 Co-ordinates, thermal parameters, occupation for atomic positions: NoP x/a y/b z/c B(j) atom / occupation 1 0.346 0.3791 0.4124 0.0 Bi = 1.00 2 0.8229 0.166 0.4085 0.0 S = 1.00 3 0.6932 0.2428 0.4673 0.0 O = 1.00 4 0.6515 0.1083 0.2027 0.0 O = 1.00 5 0.0232 0.2044 0.3608 0.0 O = 1.00 6 0.9165 0.0913 0.5962 0.0 O = 1.00 7 0.2942 0.542 0.4041 0.0 OH = 1.00 8 0.9379 0.4146 0.147 0.0 H(2)O = 1.00 Co-ordinates for all atomic positions : No NoP x/a y/b z/c 1 1 0.346 0.3791 0.4124 2 2 0.8229 0.166 0.4085 3 3 0.6932 0.2428 0.4673 4 4 0.6515 0.1083 0.2027 5 5 0.0232 0.2044 0.3608 6 6 0.9165 0.0913 0.5962 7 7 0.2942 0.542 0.4041 8 8 0.9379 0.4146 0.147 9 1 0.654 0.6209 0.5876 10 2 0.1771 0.834 0.5915 11 3 0.3068 0.7572 0.5327 12 4 0.3485 0.8917 0.7973 13 5 0.9768 0.7956 0.6392 14 6 0.0835 0.9087 0.4038 15 7 0.7058 0.458 0.5959 16 8 0.0621 0.5854 0.853 17 1 0.846 0.1209 0.9124 18 2 0.3229 0.334 0.9085 19 3 0.1932 0.2572 0.9673 20 4 0.1515 0.3917 0.7027 21 5 0.5232 0.2956 0.8608 22 6 0.4165 0.4087 0.0962 23 7 0.7942 0.958 0.9041 24 8 0.4379 0.0854 0.647 25 1 0.154 0.8791 0.0876 26 2 0.6771 0.666 0.0915 27 3 0.8068 0.7428 0.0327 28 4 0.8485 0.6083 0.2973 29 5 0.4768 0.7044 0.1392 30 6 0.5835 0.5913 0.9038 31 7 0.2058 0.042 0.0959 32 8 0.5621 0.9146 0.353 X-ray density (g/cm cub.) = 4.69 MU (1/cm) = 747.136 Mass attenuation coefficient (cm**2/g) = 159.239 Selected interatomic distances (cation-anion,anion-anion): NoP Atom Rad.sph. C.N. Distance NoP N. (angs.) (angs.) 1 Bi 3.24 9 2.6895 3 2.9719 5 2.1967 7 2.4356 8 2.2831 7 3.1279 3 2.5838 4 2.9057 5 2.2878 6 2 S 2.148 4 1.4288 3 1.5398 4 1.4509 5 1.5049 6 3 O 3.432 8 2.4312 4 2.4002 5 2.3937 6 2.9873 7 3.2592 4 3.1807 5 3.2202 6 3.0899 8 4 O 3.432 9 2.4312 3 2.4333 5 2.4394 6 3.2592 3 3.2335 5 3.1357 7 3.3401 8 2.6489 7 2.89 8 5 O 3.432 8 2.4002 3 2.4333 4 2.4084 6 3.0864 8 3.1807 3 3.2335 4 2.9327 8 3.2176 7 6 O 3.432 10 2.3937 3 2.4394 4 2.4084 5 3.0832 6 3.2202 3 2.977 7 3.0271 8 3.0266 8 3.0975 7 3.1617 8 7 OH 3.48 9 2.738 8 2.9873 3 2.5587 7 3.3469 8 3.1357 4 2.977 6 2.6489 4 3.2176 5 3.0975 6 8 H(2)O 3.6 11 3.0864 5 2.738 7 3.3469 7 3.2447 8 3.0899 3 3.3401 4 2.9327 5 3.0266 6 3.0271 6 2.89 4 3.1617 6 X-ray diffraction powder data (II), X-Ray W.L. = 1.54056(angs.): No H K L Theta 2*Theta S LPG MF F I int. ( degree ) *100 1 0 2 0 6.62 13.24 0.075 147.52 2 10.7 14.5 2 0 1 1 8.111 16.222 0.092 97.52 4 146.8 3627.6 3 1 0 -1 8.517 17.035 0.096 88.23 2 199.3 3027.0 4 1 1 0 8.65 17.301 0.098 85.48 4 134.9 2688.4 5 1 1 -1 9.145 18.29 0.103 76.25 4 41.1 222.8 6 0 2 1 9.953 19.906 0.112 64.03 4 112.9 1410.8 7 1 2 0 10.4 20.801 0.117 58.46 4 294.2 8740.9 8 1 2 -1 10.818 21.636 0.122 53.87 4 56.6 297.9 9 0 3 1 12.451 24.903 0.14 40.15 4 79.5 438.0 10 1 3 0 12.816 25.632 0.144 37.79 4 135.7 1202.4 11 1 0 1 12.898 25.797 0.145 37.28 2 19.3 12.0 12 1 3 -1 13.161 26.322 0.148 35.73 4 79.4 388.6 13 1 1 1 13.329 26.658 0.15 34.78 4 109.4 719.4 14 0 4 0 13.331 26.661 0.15 34.77 2 309.9 2882.9 15 1 1 -2 14.307 28.614 0.16 29.92 4 255.7 3379.8 16 1 2 1 14.551 29.101 0.163 28.86 4 3.4 0.6 17 0 0 2 14.925 29.851 0.167 27.34 2 152.5 548.8 18 2 1 -1 15.253 30.505 0.171 26.09 4 47.1 99.9 19 0 1 2 15.304 30.607 0.171 25.91 4 199.1 1773.3 20 0 4 1 15.313 30.627 0.171 25.87 4 60.8 165.3 21 1 2 -2 15.458 30.915 0.173 25.36 4 67.8 201.5 22 1 4 0 15.616 31.232 0.175 24.81 4 26.4 29.8 23 1 4 -1 15.905 31.81 0.178 23.84 4 191.4 1508.3 24 2 0 0 16.131 32.262 0.18 23.13 2 119.2 283.9 25 2 2 -1 16.343 32.686 0.183 22.49 4 166.9 1081.4 26 0 2 2 16.391 32.781 0.183 22.34 4 18.0 12.4 27 1 3 1 16.402 32.803 0.183 22.31 4 223.1 1917.2 28 2 1 0 16.484 32.969 0.184 22.07 4 184.6 1299.4 29 1 3 -2 17.221 34.442 0.192 20.07 4 195.6 1326.4 30 2 0 -2 17.231 34.462 0.192 20.04 2 155.0 416.0 31 2 2 0 17.506 35.012 0.195 19.36 4 1.9 0.1 32 2 1 -2 17.564 35.129 0.196 19.22 4 161.1 861.9 33 2 3 -1 18.029 36.058 0.201 18.15 4 46.1 66.6 34 0 3 2 18.073 36.146 0.201 18.06 4 85.2 226.1 35 0 5 1 18.402 36.803 0.205 17.36 4 185.0 1026.2 36 2 2 -2 18.534 37.068 0.206 17.08 4 20.3 12.2 37 1 5 0 18.66 37.319 0.208 16.83 4 73.1 155.3 38 1 4 1 18.719 37.438 0.208 16.72 4 23.0 15.3 39 1 5 -1 18.908 37.815 0.21 16.35 4 70.2 139.0 40 2 3 0 19.102 38.205 0.212 15.98 4 209.2 1207.6 41 1 4 -2 19.453 38.905 0.216 15.35 4 4.0 0.4 42 1 1 2 19.989 39.977 0.222 14.45 4 92.2 212.4 43 2 3 -2 20.06 40.12 0.223 14.34 4 185.4 851.4 44 2 4 -1 20.184 40.368 0.224 14.14 4 11.9 3.5 45 0 4 2 20.224 40.448 0.224 14.08 4 88.2 189.3 46 0 6 0 20.234 40.468 0.225 14.07 2 66.7 54.0 47 2 1 1 20.704 41.408 0.229 13.36 4 198.4 908.7 48 1 0 -3 20.853 41.707 0.231 13.15 2 205.7 480.6 49 1 2 2 20.862 41.724 0.231 13.14 4 255.0 1475.1 50 1 1 -3 21.138 42.276 0.234 12.76 4 109.7 265.1 51 2 4 0 21.165 42.329 0.234 12.72 4 78.0 133.7 52 1 5 1 21.38 42.76 0.237 12.44 4 161.2 557.8 53 2 2 1 21.554 43.107 0.238 12.21 4 131.0 361.9 54 0 6 1 21.657 43.315 0.24 12.08 4 145.0 438.9 55 1 6 0 21.883 43.766 0.242 11.8 4 235.6 1131.8 56 1 2 -3 21.974 43.947 0.243 11.69 4 31.4 19.9 57 1 5 -2 22.04 44.079 0.244 11.62 4 184.1 679.8 58 2 4 -2 22.048 44.096 0.244 11.61 4 193.0 746.8 59 1 6 -1 22.101 44.201 0.244 11.54 4 61.0 74.3 60 1 3 2 22.255 44.509 0.246 11.36 4 83.9 138.2 61 2 1 -3 22.472 44.944 0.248 11.12 4 199.1 761.3 62 3 0 -1 22.66 45.321 0.25 10.91 2 172.5 280.3 63 2 5 -1 22.702 45.405 0.251 10.86 4 59.1 65.6 64 0 5 2 22.739 45.477 0.251 10.83 4 184.2 634.5 65 2 3 1 22.913 45.825 0.253 10.64 4 97.0 172.9 66 3 1 -1 22.927 45.854 0.253 10.63 4 149.8 411.9 67 0 1 3 22.993 45.986 0.254 10.56 4 3.8 0.3 68 2 2 -3 23.269 46.539 0.256 10.27 4 66.5 78.4 69 1 3 -3 23.313 46.627 0.257 10.23 4 114.8 232.9 70 3 1 -2 23.552 47.105 0.259 10.0 4 83.7 120.9 71 2 5 0 23.599 47.197 0.26 9.95 4 174.1 521.1 72 3 2 -1 23.713 47.425 0.261 9.84 4 25.0 10.7 73 0 2 3 23.777 47.554 0.262 9.78 4 225.6 860.2 74 1 4 2 24.097 48.193 0.265 9.49 4 29.5 14.2 75 1 6 1 24.308 48.615 0.267 9.31 4 13.6 3.0 76 3 2 -2 24.323 48.645 0.267 9.29 4 257.9 1067.5 77 2 5 -2 24.412 48.824 0.268 9.22 4 159.4 404.2 78 2 3 -3 24.554 49.108 0.27 9.1 4 122.4 235.3 79 2 4 1 24.717 49.433 0.271 8.96 4 30.2 14.1 80 3 1 0 24.88 49.761 0.273 8.83 4 188.0 538.6 81 1 6 -2 24.907 49.813 0.273 8.8 4 28.1 12.0 82 3 3 -1 24.98 49.96 0.274 8.75 4 124.3 233.4 83 0 3 3 25.042 50.083 0.275 8.7 4 1.3 0.0 84 0 7 1 25.059 50.118 0.275 8.68 4 128.8 248.7 85 1 4 -3 25.095 50.191 0.275 8.65 4 171.5 439.6 86 1 7 0 25.261 50.522 0.277 8.53 4 73.5 79.4 87 1 7 -1 25.456 50.913 0.279 8.38 4 75.9 83.3 88 2 6 -1 25.512 51.024 0.28 8.34 4 212.0 647.2 89 0 6 2 25.545 51.091 0.28 8.31 4 9.3 1.3 90 3 3 -2 25.567 51.134 0.28 8.3 4 62.4 55.8 91 3 2 0 25.62 51.241 0.281 8.26 4 57.1 46.5 92 2 4 -3 26.273 52.547 0.287 7.8 4 17.0 3.9 93 1 5 2 26.32 52.641 0.288 7.76 4 43.6 25.5 94 2 6 0 26.336 52.672 0.288 7.75 4 12.4 2.0 95 3 0 -3 26.381 52.762 0.288 7.72 2 71.4 34.0 96 2 0 2 26.516 53.032 0.29 7.63 2 268.2 474.3 97 3 1 -3 26.619 53.238 0.291 7.57 4 119.8 187.6 98 3 4 -1 26.679 53.358 0.291 7.53 4 120.6 189.1 99 0 4 3 26.738 53.476 0.292 7.49 4 73.1 69.1 100 2 1 2 26.754 53.507 0.292 7.48 4 14.1 2.6 101 3 3 0 26.821 53.643 0.293 7.44 4 155.0 308.7 102 2 5 1 26.903 53.806 0.294 7.39 4 193.5 477.8 103 2 6 -2 27.089 54.178 0.296 7.27 4 25.1 7.9 104 3 4 -2 27.24 54.481 0.297 7.18 4 9.8 1.2 105 1 5 -3 27.26 54.52 0.297 7.17 4 61.2 46.4 106 1 0 3 27.303 54.605 0.298 7.14 2 172.3 183.0 107 3 2 -3 27.326 54.651 0.298 7.13 4 11.5 1.6 108 2 2 2 27.458 54.915 0.299 7.05 4 10.0 1.2 109 1 7 1 27.46 54.92 0.299 7.05 4 237.4 686.4 110 0 8 0 27.461 54.922 0.299 7.05 2 206.9 260.7 111 1 1 3 27.535 55.071 0.3 7.01 4 42.8 22.2 112 1 7 -2 28.011 56.021 0.305 6.74 4 142.5 236.3 113 1 2 3 28.226 56.453 0.307 6.62 4 73.4 61.6 114 2 5 -3 28.374 56.749 0.308 6.55 4 190.3 409.5 115 3 4 0 28.443 56.886 0.309 6.51 4 30.2 10.3 116 3 3 -3 28.477 56.953 0.309 6.49 4 119.6 160.3 117 2 7 -1 28.569 57.139 0.31 6.44 4 26.7 7.9 118 0 7 2 28.6 57.2 0.311 6.43 4 123.0 167.9 119 2 3 2 28.605 57.21 0.311 6.43 4 26.2 7.6 120 0 8 1 28.606 57.212 0.311 6.43 4 48.8 26.4 121 2 0 -4 28.725 57.449 0.312 6.37 2 208.6 239.3 122 3 5 -1 28.76 57.52 0.312 6.35 4 73.9 59.9 123 1 8 0 28.791 57.582 0.313 6.33 4 37.9 15.7 124 3 0 1 28.801 57.603 0.313 6.33 2 208.1 236.6 125 1 1 -4 28.807 57.614 0.313 6.33 4 66.1 47.8 126 0 5 3 28.816 57.633 0.313 6.32 4 22.0 5.3 127 1 6 2 28.872 57.744 0.313 6.29 4 182.5 361.9 128 2 1 -4 28.95 57.9 0.314 6.25 4 44.4 21.3 129 1 8 -1 28.969 57.939 0.314 6.25 4 208.5 468.7 130 3 1 1 29.026 58.053 0.315 6.22 4 37.0 14.7 131 3 5 -2 29.295 58.589 0.318 6.09 4 35.1 13.0 132 2 7 0 29.334 58.668 0.318 6.07 4 151.0 239.1 133 1 3 3 29.354 58.708 0.318 6.06 4 90.2 85.2 134 2 6 1 29.42 58.84 0.319 6.03 4 138.7 200.5 135 1 2 -4 29.478 58.957 0.319 6.01 4 202.8 426.6 136 2 2 -4 29.619 59.239 0.321 5.94 4 21.2 4.6 137 3 2 1 29.695 59.389 0.322 5.91 4 5.0 0.3 138 1 6 -3 29.757 59.514 0.322 5.88 4 54.3 30.0 139 2 7 -2 30.037 60.074 0.325 5.76 4 147.8 217.3 140 3 4 -3 30.039 60.079 0.325 5.76 4 70.7 49.7 141 2 4 2 30.164 60.327 0.326 5.7 4 217.0 464.0 142 3 5 0 30.445 60.89 0.329 5.59 4 159.5 245.5 143 1 3 -4 30.577 61.154 0.33 5.53 4 49.3 23.3 144 2 3 -4 30.715 61.43 0.332 5.48 4 73.8 51.5 145 3 3 1 30.789 61.577 0.332 5.45 4 60.8 34.8 146 2 6 -3 30.813 61.627 0.333 5.44 4 78.4 57.7 147 1 8 1 30.819 61.638 0.333 5.44 4 29.4 8.1 148 4 0 -2 30.888 61.777 0.333 5.41 2 278.7 363.0 149 1 4 3 30.889 61.778 0.333 5.41 4 192.5 346.1 150 0 0 4 31.006 62.011 0.334 5.37 2 187.3 162.6 151 4 1 -2 31.104 62.208 0.335 5.33 4 43.4 17.3 152 3 6 -1 31.18 62.361 0.336 5.3 4 66.6 40.7 153 0 1 4 31.221 62.442 0.336 5.28 4 156.2 222.5 154 0 6 3 31.234 62.468 0.337 5.28 4 252.4 580.7 155 1 8 -2 31.332 62.664 0.338 5.24 4 16.1 2.3 156 4 1 -1 31.493 62.986 0.339 5.18 4 134.6 162.2 157 3 1 -4 31.629 63.257 0.34 5.14 4 126.4 141.7 158 3 6 -2 31.69 63.38 0.341 5.11 4 238.0 500.4 159 1 7 2 31.714 63.428 0.341 5.11 4 69.8 43.0 160 4 2 -2 31.746 63.492 0.342 5.09 4 12.7 1.4 161 2 8 -1 31.855 63.709 0.343 5.06 4 65.1 37.0 162 0 2 4 31.861 63.723 0.343 5.05 4 12.0 1.3 163 0 8 2 31.884 63.767 0.343 5.05 4 94.6 78.1 164 3 5 -3 31.98 63.96 0.344 5.01 4 95.9 79.7 165 1 4 -4 32.077 64.155 0.345 4.98 4 26.2 5.9 166 2 5 2 32.1 64.2 0.345 4.97 4 18.9 3.1 167 4 2 -1 32.131 64.261 0.345 4.96 4 25.8 5.7 168 2 4 -4 32.212 64.423 0.346 4.93 4 215.0 394.1 169 2 7 1 32.233 64.467 0.346 4.93 4 49.7 21.0 170 3 2 -4 32.265 64.53 0.347 4.92 4 155.4 205.0 171 3 4 1 32.283 64.567 0.347 4.91 4 163.5 226.6 172 0 9 1 32.312 64.624 0.347 4.9 4 166.3 234.2 173 1 9 0 32.484 64.968 0.349 4.85 4 87.8 64.5 174 1 7 -3 32.553 65.106 0.349 4.82 4 163.6 222.9 175 2 8 0 32.573 65.146 0.349 4.82 4 86.6 62.4 176 1 9 -1 32.651 65.301 0.35 4.79 4 14.8 1.8 177 3 6 0 32.791 65.582 0.352 4.75 4 55.0 24.8 178 4 3 -2 32.8 65.6 0.352 4.75 4 43.9 15.8 179 1 5 3 32.801 65.602 0.352 4.75 4 63.3 32.9 180 4 1 -3 32.835 65.67 0.352 4.74 4 64.5 34.0 181 0 3 4 32.914 65.827 0.353 4.71 4 129.0 135.4 182 4 3 -1 33.178 66.357 0.355 4.63 4 115.5 106.7 183 2 8 -2 33.236 66.472 0.356 4.61 4 137.6 150.9 184 3 3 -4 33.31 66.621 0.356 4.59 4 119.0 112.3 185 4 2 -3 33.459 66.918 0.358 4.55 4 179.2 252.2 186 2 7 -3 33.559 67.119 0.359 4.52 4 63.0 31.0 187 4 0 0 33.757 67.515 0.361 4.47 2 166.5 106.9 188 3 7 -1 33.91 67.82 0.362 4.42 4 148.4 168.2 189 1 5 -4 33.953 67.906 0.363 4.41 4 60.1 27.5 190 0 7 3 33.961 67.923 0.363 4.41 4 26.4 5.3 191 4 1 0 33.963 67.926 0.363 4.41 4 98.4 73.7 192 2 1 3 34.047 68.093 0.363 4.39 4 123.4 115.4 193 2 5 -4 34.083 68.167 0.364 4.38 4 29.9 6.7 194 3 5 1 34.153 68.306 0.364 4.36 4 36.1 9.8 195 4 4 -2 34.247 68.495 0.365 4.33 4 225.3 379.8 196 3 6 -3 34.268 68.537 0.365 4.33 4 0.4 0.0 197 0 4 4 34.359 68.717 0.366 4.3 4 143.5 153.2 198 2 6 2 34.384 68.769 0.367 4.3 4 11.9 1.1 199 1 9 1 34.386 68.773 0.367 4.3 4 102.6 78.1 200 3 7 -2 34.398 68.797 0.367 4.29 4 33.8 8.5 201 4 3 -3 34.486 68.972 0.368 4.27 4 26.2 5.1 202 4 2 0 34.577 69.153 0.368 4.25 4 14.9 1.6 203 4 4 -1 34.618 69.236 0.369 4.24 4 36.0 9.5 204 2 2 3 34.66 69.319 0.369 4.23 4 41.1 12.3 205 3 4 -4 34.747 69.494 0.37 4.21 4 29.7 6.4 206 1 8 2 34.828 69.657 0.371 4.19 4 35.4 9.0 207 1 9 -2 34.871 69.743 0.371 4.18 4 132.9 127.4 208 3 1 2 34.88 69.76 0.371 4.17 4 102.3 75.4 209 1 6 3 35.062 70.125 0.373 4.13 4 65.1 30.3 210 0 10 0 35.2 70.399 0.374 4.1 2 55.4 10.9 211 2 8 1 35.324 70.649 0.375 4.07 4 30.4 6.5 212 2 9 -1 35.367 70.734 0.376 4.06 4 47.0 15.5 213 0 9 2 35.394 70.789 0.376 4.05 4 109.6 84.1 214 3 7 0 35.456 70.913 0.377 4.04 4 140.1 136.9 215 3 2 2 35.486 70.973 0.377 4.03 4 173.1 208.6 216 4 3 0 35.589 71.177 0.378 4.01 4 74.8 38.7 217 1 8 -3 35.631 71.261 0.378 4.0 4 167.4 193.5 218 2 3 3 35.671 71.341 0.379 3.99 4 85.7 50.6 219 1 1 4 35.895 71.791 0.381 3.94 4 184.4 231.5 220 4 4 -3 35.901 71.802 0.381 3.94 4 50.5 17.4 221 2 9 0 36.051 72.101 0.382 3.91 4 76.8 39.9 222 4 5 -2 36.068 72.135 0.382 3.91 4 21.9 3.2 223 0 5 4 36.176 72.352 0.383 3.88 4 126.5 107.3 224 1 6 -4 36.18 72.36 0.383 3.88 4 205.1 282.0 225 0 10 1 36.202 72.405 0.383 3.88 4 95.1 60.6 226 2 6 -4 36.307 72.614 0.384 3.86 4 35.2 8.2 227 4 0 -4 36.331 72.662 0.385 3.85 2 39.9 5.3 228 1 10 0 36.365 72.731 0.385 3.84 4 144.4 138.5 229 3 6 1 36.375 72.749 0.385 3.84 4 54.9 20.0 230 4 5 -1 36.43 72.86 0.385 3.83 4 160.6 170.7 231 3 3 2 36.487 72.975 0.386 3.82 4 96.5 61.4 232 1 2 4 36.495 72.989 0.386 3.82 4 26.8 4.7 233 1 10 -1 36.523 73.047 0.386 3.81 4 33.7 7.5 234 4 1 -4 36.53 73.06 0.386 3.81 4 177.2 206.7 235 3 5 -4 36.556 73.113 0.387 3.81 4 122.7 99.0 236 2 8 -3 36.597 73.194 0.387 3.8 4 46.2 14.0 237 2 1 -5 36.611 73.222 0.387 3.79 4 98.2 63.2 238 2 9 -2 36.684 73.368 0.388 3.78 4 62.9 25.8 239 3 7 -3 36.884 73.769 0.39 3.74 4 197.1 250.9 240 3 8 -1 36.935 73.869 0.39 3.73 4 155.3 155.4 241 0 8 3 36.984 73.968 0.391 3.72 4 96.3 59.7 242 4 4 0 36.986 73.971 0.391 3.72 4 179.2 206.5 243 2 7 2 36.997 73.994 0.391 3.72 4 5.3 0.2 244 2 4 3 37.066 74.132 0.391 3.71 4 5.6 0.2 245 1 0 -5 37.119 74.238 0.392 3.7 2 37.5 4.5 246 4 2 -4 37.125 74.25 0.392 3.7 4 3.4 0.1 247 2 2 -5 37.206 74.412 0.393 3.68 4 130.9 108.9 248 1 1 -5 37.317 74.633 0.394 3.66 4 125.8 100.0 249 3 8 -2 37.406 74.811 0.394 3.65 4 16.5 1.7 250 1 3 4 37.485 74.97 0.395 3.63 4 173.9 189.7 251 1 7 3 37.655 75.31 0.397 3.6 4 81.3 41.1 252 4 5 -3 37.687 75.375 0.397 3.6 4 95.0 56.1 253 3 4 2 37.871 75.743 0.398 3.57 4 16.8 1.7 254 1 2 -5 37.907 75.815 0.399 3.56 4 3.4 0.1 255 3 0 -5 38.004 76.008 0.4 3.54 2 201.7 124.5 256 4 3 -4 38.11 76.219 0.401 3.53 4 125.7 96.2 257 1 10 1 38.18 76.361 0.401 3.51 4 8.1 0.4 258 2 3 -5 38.189 76.379 0.401 3.51 4 58.0 20.4 259 3 1 -5 38.2 76.4 0.401 3.51 4 12.8 1.0 260 1 9 2 38.214 76.428 0.402 3.51 4 42.9 11.2 261 4 6 -2 38.243 76.486 0.402 3.5 4 10.5 0.7 262 4 1 1 38.32 76.64 0.402 3.49 4 46.1 12.8 263 0 6 4 38.35 76.699 0.403 3.49 4 3.4 0.1 264 3 8 0 38.43 76.86 0.403 3.47 4 6.9 0.3 265 4 6 -1 38.598 77.196 0.405 3.45 4 63.3 23.9 266 1 10 -2 38.646 77.293 0.405 3.44 4 28.0 4.7 267 2 9 1 38.693 77.386 0.406 3.43 4 178.7 189.5 268 3 6 -4 38.722 77.444 0.406 3.43 4 126.7 95.1 269 1 7 -4 38.744 77.488 0.406 3.43 4 52.9 16.6 270 4 5 0 38.754 77.507 0.406 3.43 4 137.0 111.1 271 3 2 -5 38.786 77.573 0.407 3.42 4 40.8 9.8 272 2 5 3 38.833 77.666 0.407 3.41 4 157.1 145.5 273 1 4 4 38.857 77.713 0.407 3.41 4 2.6 0.0 274 2 7 -4 38.868 77.736 0.407 3.41 4 51.7 15.7 275 1 3 -5 38.885 77.77 0.407 3.41 4 122.5 88.3 276 4 2 1 38.906 77.811 0.408 3.4 4 172.1 174.1 277 3 7 1 38.934 77.868 0.408 3.4 4 91.8 49.4 278 1 9 -3 38.989 77.978 0.408 3.39 4 67.9 27.0 279 2 10 -1 39.124 78.247 0.41 3.37 4 230.7 310.1 280 0 10 2 39.15 78.3 0.41 3.37 4 6.4 0.2 281 4 4 -4 39.474 78.949 0.413 3.32 4 25.1 3.6 282 2 4 -5 39.553 79.107 0.413 3.31 4 6.1 0.2 283 3 5 2 39.627 79.253 0.414 3.3 4 111.2 70.5 284 3 3 -5 39.758 79.515 0.415 3.29 4 22.0 2.7 285 2 10 0 39.784 79.568 0.415 3.28 4 26.7 4.0 286 3 8 -3 39.82 79.64 0.416 3.28 4 48.5 13.3 287 4 6 -3 39.833 79.665 0.416 3.28 4 160.6 146.0 288 4 3 1 39.876 79.752 0.416 3.27 4 61.4 21.3 289 2 9 -3 39.927 79.853 0.417 3.26 4 197.9 220.8 290 2 8 2 39.93 79.859 0.417 3.26 4 185.8 194.5 291 5 1 -2 39.97 79.94 0.417 3.26 4 115.8 75.4 292 1 4 -5 40.242 80.485 0.419 3.22 4 29.7 4.9 293 3 9 -1 40.255 80.511 0.419 3.22 4 68.9 26.4 294 0 1 5 40.277 80.553 0.42 3.22 4 108.3 65.2 295 0 9 3 40.304 80.607 0.42 3.22 4 21.3 2.5 296 0 11 1 40.317 80.634 0.42 3.22 4 112.5 70.3 297 2 10 -2 40.398 80.795 0.421 3.21 4 24.4 3.3 298 1 11 0 40.475 80.949 0.421 3.2 4 50.9 14.3 299 5 0 -3 40.543 81.087 0.422 3.19 2 155.5 66.6 300 5 2 -2 40.549 81.098 0.422 3.19 4 127.7 89.9 301 1 8 3 40.573 81.147 0.422 3.19 4 170.1 159.2 302 1 5 4 40.6 81.199 0.422 3.18 4 130.0 92.9 303 1 11 -1 40.628 81.255 0.423 3.18 4 95.1 49.6 304 3 9 -2 40.715 81.429 0.423 3.17 4 27.5 4.1 305 5 1 -3 40.736 81.472 0.424 3.17 4 13.7 1.0 306 4 7 -2 40.765 81.53 0.424 3.16 4 53.9 15.9 307 0 2 5 40.855 81.709 0.425 3.15 4 62.0 20.9 308 0 7 4 40.87 81.739 0.425 3.15 4 136.0 100.7 309 4 6 0 40.883 81.766 0.425 3.15 4 24.9 3.4 310 5 0 -1 40.937 81.873 0.425 3.14 2 56.6 8.7 311 2 6 3 40.961 81.923 0.426 3.14 4 80.8 35.5 312 3 4 -5 41.107 82.215 0.427 3.13 4 192.2 199.4 313 4 7 -1 41.114 82.228 0.427 3.13 4 109.3 64.6 314 5 1 -1 41.129 82.257 0.427 3.12 4 85.1 39.1 315 4 5 -4 41.211 82.422 0.428 3.12 4 149.4 120.1 316 4 4 1 41.225 82.45 0.428 3.11 4 45.4 11.1 317 3 7 -4 41.236 82.472 0.428 3.11 4 106.5 61.0 318 2 5 -5 41.289 82.578 0.428 3.11 4 110.6 65.6 319 5 2 -3 41.313 82.626 0.429 3.11 4 42.4 9.6 320 5 3 -2 41.51 83.021 0.43 3.09 4 125.1 83.4 321 1 8 -4 41.642 83.283 0.431 3.07 4 4.7 0.1 322 5 2 -1 41.704 83.409 0.432 3.07 4 0.9 0.0 323 3 9 0 41.717 83.434 0.432 3.06 4 105.1 58.5 324 3 6 2 41.745 83.491 0.432 3.06 4 173.6 159.3 325 2 8 -4 41.763 83.527 0.432 3.06 4 154.3 125.9 326 0 3 5 41.814 83.629 0.433 3.06 4 70.3 26.1 327 3 8 1 41.829 83.657 0.433 3.05 4 194.2 198.9 328 1 10 2 41.888 83.777 0.433 3.05 4 141.5 105.4 329 1 5 -5 41.972 83.944 0.434 3.04 4 84.0 37.1 330 4 1 -5 42.003 84.006 0.434 3.04 4 34.2 6.1 331 3 0 3 42.042 84.083 0.435 3.03 2 58.4 8.9 332 3 1 3 42.233 84.466 0.436 3.02 4 116.5 70.8 333 1 11 1 42.238 84.477 0.436 3.02 4 206.7 222.7 334 5 3 -3 42.271 84.541 0.437 3.01 4 14.7 1.1 335 4 7 -3 42.332 84.663 0.437 3.01 4 64.2 21.4 336 2 10 1 42.357 84.714 0.437 3.01 4 127.3 84.1 337 2 0 4 42.367 84.734 0.437 3.01 2 120.1 37.4 338 2 1 4 42.558 85.117 0.439 2.99 4 159.3 131.0 339 4 2 -5 42.577 85.154 0.439 2.99 4 152.0 119.2 340 1 10 -3 42.648 85.295 0.44 2.98 4 65.1 21.8 341 5 3 -1 42.661 85.322 0.44 2.98 4 137.1 96.8 342 1 11 -2 42.694 85.387 0.44 2.98 4 84.2 36.5 343 1 6 4 42.709 85.417 0.44 2.98 4 15.5 1.2 344 3 2 3 42.806 85.613 0.441 2.97 4 10.5 0.6 345 3 5 -5 42.831 85.662 0.441 2.97 4 4.7 0.1 346 5 4 -2 42.85 85.699 0.441 2.97 4 32.4 5.4 347 4 5 1 42.948 85.895 0.442 2.96 4 36.3 6.7 348 3 9 -3 43.083 86.166 0.443 2.95 4 103.4 54.5 349 2 2 4 43.131 86.262 0.444 2.94 4 7.2 0.3 350 0 4 5 43.152 86.305 0.444 2.94 4 2.8 0.0 351 2 11 -1 43.161 86.323 0.444 2.94 4 10.9 0.6 352 0 11 2 43.187 86.375 0.444 2.94 4 127.5 82.6 353 2 9 2 43.191 86.383 0.444 2.94 4 6.2 0.2 354 4 6 -4 43.315 86.63 0.445 2.93 4 29.0 4.3 355 4 7 0 43.371 86.742 0.446 2.93 4 56.1 15.9 356 2 6 -5 43.393 86.785 0.446 2.92 4 136.1 93.5 357 5 1 -4 43.407 86.815 0.446 2.92 4 158.2 126.4 358 2 7 3 43.449 86.898 0.446 2.92 4 92.0 42.7 359 4 3 -5 43.531 87.062 0.447 2.92 4 50.5 12.8 360 2 10 -3 43.57 87.139 0.447 2.91 4 65.3 21.4 361 5 4 -3 43.607 87.214 0.448 2.91 4 195.8 192.8 362 4 8 -2 43.636 87.271 0.448 2.91 4 138.6 96.4 363 0 8 4 43.739 87.479 0.449 2.9 4 75.7 28.7 364 3 3 3 43.76 87.52 0.449 2.9 4 136.5 93.3 365 0 12 0 43.766 87.532 0.449 2.9 2 146.9 54.0 366 2 11 0 43.81 87.62 0.449 2.9 4 124.5 77.5 367 1 9 3 43.827 87.654 0.45 2.9 4 49.4 12.2 368 3 10 -1 43.894 87.788 0.45 2.89 4 33.7 5.7 369 0 10 3 43.941 87.883 0.45 2.89 4 195.8 191.2 370 5 2 -4 43.979 87.958 0.451 2.89 4 91.9 42.1 371 4 8 -1 43.982 87.963 0.451 2.89 4 45.0 10.1 372 5 4 -1 43.996 87.992 0.451 2.88 4 87.5 38.1 373 1 6 -5 44.071 88.143 0.451 2.88 4 10.4 0.5 374 2 3 4 44.084 88.168 0.452 2.88 4 122.6 74.8 375 3 8 -4 44.103 88.205 0.452 2.88 4 8.2 0.3 376 5 1 0 44.185 88.371 0.452 2.87 4 36.2 6.5 377 3 7 2 44.227 88.454 0.453 2.87 4 80.9 32.5 378 4 0 2 44.237 88.473 0.453 2.87 2 112.4 31.3 379 3 10 -2 44.348 88.695 0.454 2.86 4 150.1 111.5 380 2 11 -2 44.415 88.83 0.454 2.86 4 94.4 44.0 381 4 1 2 44.427 88.854 0.454 2.86 4 121.7 73.1 382 5 5 -2 44.565 89.13 0.455 2.85 4 105.1 54.4 383 0 12 1 44.716 89.433 0.457 2.84 4 25.0 3.1 384 5 2 0 44.757 89.513 0.457 2.84 4 224.6 247.4 385 4 4 -5 44.864 89.729 0.458 2.84 4 56.9 15.9 386 0 5 5 44.867 89.734 0.458 2.84 4 131.6 84.8 387 1 12 0 44.872 89.744 0.458 2.83 4 51.3 12.9 388 1 9 -4 44.886 89.771 0.458 2.83 4 37.1 6.7 389 3 6 -5 44.927 89.854 0.458 2.83 4 72.3 25.6 390 5 3 -4 44.931 89.862 0.458 2.83 4 143.0 100.0 391 4 2 2 44.998 89.997 0.459 2.83 4 8.7 0.4 X-ray diffraction powder data (I)...X-Ray wave length = 1.54056 (angs.): No H K L Theta 2*Theta d I int I int.n. I p.h.n. H(Si) ( degree ) (angstrem) *100 *100 1 0 1 1 8.111 16.222 5.45939 3627.6 41.5 41.6 5.6 2 1 0 -1 8.517 17.035 5.20068 3027.0 34.6 34.7 5.6 3 1 1 0 8.65 17.301 5.12143 2688.4 30.8 30.8 5.6 4 1 1 -1 9.145 18.29 4.84657 222.8 2.5 2.6 5.6 5 0 2 1 9.953 19.906 4.45649 1410.8 16.1 16.1 5.6 6 1 2 0 10.4 20.801 4.26689 8740.9 100.0 100.0 5.6 7 1 2 -1 10.818 21.636 4.10399 297.9 3.4 3.4 5.6 8 0 3 1 12.451 24.903 3.57252 438.0 5.0 5.0 5.6 9 1 3 0 12.816 25.632 3.4726 1202.4 13.8 13.7 5.6 10 1 3 -1 13.161 26.322 3.38307 388.6 4.4 4.4 5.6 11 0 4 0 13.331 26.661 3.34075 3602.3 41.2 41.0 5.6 12 1 1 -2 14.307 28.614 3.11706 3379.8 38.7 38.4 5.6 13 0 0 2 14.925 29.851 2.99067 548.8 6.3 6.2 5.6 14 2 1 -1 15.253 30.505 2.92797 99.9 1.1 1.1 5.6 15 0 1 2 15.304 30.607 2.91847 1938.6 22.2 22.0 5.6 16 1 2 -2 15.458 30.915 2.89009 201.5 2.3 2.3 5.6 17 1 4 -1 15.905 31.81 2.81079 1508.3 17.3 17.1 5.6 18 2 0 0 16.131 32.262 2.77241 283.9 3.2 3.2 5.6 19 2 2 -1 16.343 32.686 2.73747 1081.4 12.4 12.3 5.6 20 1 3 1 16.402 32.803 2.72791 1929.7 22.1 21.9 5.6 21 2 1 0 16.484 32.969 2.7146 1299.4 14.9 14.7 5.6 22 1 3 -2 17.221 34.442 2.60181 1742.4 19.9 19.7 5.7 23 2 1 -2 17.564 35.129 2.55246 861.9 9.9 9.7 5.7 24 0 3 2 18.073 36.146 2.48294 226.1 2.6 2.6 5.7 25 0 5 1 18.402 36.803 2.44009 1026.2 11.7 11.6 5.7 26 1 5 0 18.66 37.319 2.40753 155.3 1.8 1.8 5.7 27 1 5 -1 18.908 37.815 2.37709 139.0 1.6 1.6 5.7 28 2 3 0 19.102 38.205 2.35374 1207.6 13.8 13.6 5.7 29 1 1 2 19.989 39.977 2.25337 212.4 2.4 2.4 5.7 30 2 3 -2 20.06 40.12 2.24568 851.4 9.7 9.6 5.7 31 0 4 2 20.224 40.448 2.22825 243.3 2.8 2.7 5.7 32 2 1 1 20.704 41.408 2.17874 908.7 10.4 10.2 5.7 33 1 2 2 20.862 41.724 2.163 1955.8 22.4 22.0 5.7 34 1 1 -3 21.138 42.276 2.13601 398.8 4.6 4.5 5.7 35 1 5 1 21.38 42.76 2.11297 557.8 6.4 6.3 5.7 36 2 2 1 21.554 43.107 2.09674 361.9 4.1 4.1 5.7 37 0 6 1 21.657 43.315 2.08717 438.9 5.0 4.9 5.7 38 1 6 0 21.883 43.766 2.06668 1131.8 12.9 12.7 5.7 39 2 4 -2 22.048 44.096 2.05199 1426.6 16.3 16.0 5.7 40 1 3 2 22.255 44.509 2.03388 138.2 1.6 1.5 5.7 41 2 1 -3 22.472 44.944 2.01522 761.3 8.7 8.5 5.7 42 3 0 -1 22.66 45.321 1.99933 280.3 3.2 3.1 5.7 43 0 5 2 22.739 45.477 1.99281 634.5 7.3 7.1 5.7 44 3 1 -1 22.927 45.854 1.97732 584.8 6.7 6.5 5.7 45 1 3 -3 23.313 46.627 1.94634 232.9 2.7 2.6 5.7 46 3 1 -2 23.552 47.105 1.92768 120.9 1.4 1.4 5.7 47 2 5 0 23.599 47.197 1.92413 521.1 6.0 5.8 5.7 48 0 2 3 23.777 47.554 1.91053 860.2 9.8 9.6 5.7 49 3 2 -2 24.323 48.645 1.87019 1070.5 12.2 11.9 5.7 50 2 5 -2 24.412 48.824 1.86374 404.2 4.6 4.5 5.7 51 2 3 -3 24.554 49.108 1.85364 235.3 2.7 2.6 5.7 52 3 1 0 24.88 49.761 1.83084 550.6 6.3 6.1 5.7 53 3 3 -1 24.98 49.96 1.82401 233.4 2.7 2.6 5.7 54 0 7 1 25.059 50.118 1.81862 248.7 2.8 2.8 5.7 55 1 4 -3 25.095 50.191 1.81615 439.6 5.0 4.9 5.7 56 2 6 -1 25.512 51.024 1.78843 647.2 7.4 7.2 5.8 57 2 0 2 26.516 53.032 1.72535 474.3 5.4 5.3 5.8 58 3 1 -3 26.619 53.238 1.71915 187.6 2.1 2.1 5.8 59 3 4 -1 26.679 53.358 1.71557 189.1 2.2 2.1 5.8 60 3 3 0 26.821 53.643 1.70714 308.7 3.5 3.4 5.8 61 2 5 1 26.903 53.806 1.70236 477.8 5.5 5.3 5.8 62 1 0 3 27.303 54.605 1.6793 184.7 2.1 2.0 5.8 63 0 8 0 27.461 54.922 1.67037 948.3 10.8 10.5 5.8 64 1 7 -2 28.011 56.021 1.64017 236.3 2.7 2.6 5.8 65 2 5 -3 28.374 56.749 1.62085 409.5 4.7 4.5 5.8 66 3 3 -3 28.477 56.953 1.61552 160.3 1.8 1.8 5.8 67 0 7 2 28.6 57.2 1.60912 202.0 2.3 2.2 5.8 68 2 0 -4 28.725 57.449 1.60274 239.3 2.7 2.6 5.8 69 1 1 -4 28.807 57.614 1.59856 305.4 3.5 3.4 5.8 70 1 6 2 28.872 57.744 1.59528 361.9 4.1 4.0 5.8 71 1 8 -1 28.969 57.939 1.59036 490.0 5.6 5.4 5.8 72 2 7 0 29.334 58.668 1.57231 324.2 3.7 3.6 5.8 73 2 6 1 29.42 58.84 1.56813 200.5 2.3 2.2 5.8 74 1 2 -4 29.478 58.957 1.56531 426.6 4.9 4.7 5.8 75 2 7 -2 30.037 60.074 1.53884 266.9 3.1 2.9 5.8 76 2 4 2 30.164 60.327 1.53298 464.0 5.3 5.1 5.8 77 3 5 0 30.445 60.89 1.52016 245.5 2.8 2.7 5.8 78 2 6 -3 30.813 61.627 1.50373 100.6 1.2 1.1 5.8 79 4 0 -2 30.888 61.777 1.50045 709.1 8.1 7.8 5.8 80 0 0 4 31.006 62.011 1.49533 162.6 1.9 1.8 5.8 81 0 6 3 31.234 62.468 1.4855 803.3 9.2 8.8 5.8 82 4 1 -1 31.493 62.986 1.47451 162.2 1.9 1.8 5.9 83 3 1 -4 31.629 63.257 1.46884 141.7 1.6 1.5 5.9 84 3 6 -2 31.69 63.38 1.4663 543.4 6.2 5.9 5.9 85 0 8 2 31.884 63.767 1.45833 116.3 1.3 1.3 5.9 86 2 4 -4 32.212 64.423 1.44505 415.1 4.7 4.5 5.9 87 3 4 1 32.283 64.567 1.44218 665.8 7.6 7.3 5.9 88 1 7 -3 32.553 65.106 1.43153 285.3 3.3 3.1 5.9 89 0 3 4 32.914 65.827 1.41759 135.4 1.5 1.5 5.9 90 4 3 -1 33.178 66.357 1.40755 106.7 1.2 1.2 5.9 91 2 8 -2 33.236 66.472 1.4054 150.9 1.7 1.6 5.9 92 3 3 -4 33.31 66.621 1.40262 112.3 1.3 1.2 5.9 93 4 2 -3 33.459 66.918 1.39711 252.2 2.9 2.7 5.9 94 4 0 0 33.757 67.515 1.3862 106.9 1.2 1.2 5.9 95 3 7 -1 33.91 67.82 1.3807 168.2 1.9 1.8 5.9 96 4 1 0 33.963 67.926 1.37881 106.5 1.2 1.2 5.9 97 2 1 3 34.047 68.093 1.37582 115.4 1.3 1.3 5.9 98 4 4 -2 34.247 68.495 1.36873 379.8 4.3 4.1 5.9 99 0 4 4 34.359 68.717 1.36485 232.4 2.7 2.5 5.9 100 1 9 -2 34.871 69.743 1.34727 202.8 2.3 2.2 5.9 101 0 9 2 35.394 70.789 1.3299 99.6 1.1 1.1 5.9 102 3 7 0 35.456 70.913 1.32788 136.9 1.6 1.5 5.9 103 3 2 2 35.486 70.973 1.32691 208.6 2.4 2.3 5.9 104 1 8 -3 35.631 71.261 1.32224 193.5 2.2 2.1 5.9 105 1 1 4 35.895 71.791 1.31378 248.9 2.8 2.7 5.9 106 1 6 -4 36.18 72.36 1.30484 449.9 5.1 4.8 5.9 107 1 10 0 36.365 72.731 1.29911 158.4 1.8 1.7 6.0 108 4 5 -1 36.43 72.86 1.29712 170.7 2.0 1.8 6.0 109 4 1 -4 36.53 73.06 1.29406 313.1 3.6 3.4 6.0 110 3 7 -3 36.884 73.769 1.28336 250.9 2.9 2.7 6.0 111 3 8 -1 36.935 73.869 1.28187 155.4 1.8 1.7 6.0 112 4 4 0 36.986 73.971 1.28036 266.4 3.0 2.9 6.0 113 2 2 -5 37.206 74.412 1.27387 108.9 1.2 1.2 6.0 114 1 1 -5 37.317 74.633 1.27063 100.0 1.1 1.1 6.0 115 1 3 4 37.485 74.97 1.26576 189.7 2.2 2.0 6.0 116 3 0 -5 38.004 76.008 1.25103 124.5 1.4 1.3 6.0 117 4 3 -4 38.11 76.219 1.24809 96.2 1.1 1.0 6.0 118 2 9 1 38.693 77.386 1.23216 284.6 3.3 3.0 6.0 119 4 5 0 38.754 77.507 1.23053 127.7 1.5 1.4 6.0 120 2 5 3 38.833 77.666 1.22841 145.6 1.7 1.5 6.0 121 4 2 1 38.906 77.811 1.22648 327.5 3.7 3.5 6.0 122 2 10 -1 39.124 78.247 1.22074 310.3 3.6 3.3 6.0 123 4 6 -3 39.833 79.665 1.20253 159.3 1.8 1.7 6.0 124 2 9 -3 39.927 79.853 1.20017 415.4 4.8 4.4 6.0 125 0 1 5 40.277 80.553 1.1915 99.1 1.1 1.0 6.1 126 1 8 3 40.573 81.147 1.18428 458.1 5.2 4.8 6.1 127 0 7 4 40.87 81.739 1.17718 125.0 1.4 1.3 6.1 128 3 4 -5 41.107 82.215 1.17158 303.0 3.5 3.2 6.1 129 4 5 -4 41.211 82.422 1.16916 192.1 2.2 2.0 6.1 130 3 6 2 41.745 83.491 1.15689 343.7 3.9 3.6 6.1 131 3 8 1 41.829 83.657 1.15501 225.0 2.6 2.4 6.1 132 1 10 2 41.888 83.777 1.15367 105.4 1.2 1.1 6.1 133 1 11 1 42.238 84.477 1.14588 293.5 3.4 3.1 6.1 134 2 10 1 42.357 84.714 1.14327 143.0 1.6 1.5 6.1 135 2 1 4 42.558 85.117 1.1389 250.2 2.9 2.6 6.1 136 5 3 -1 42.661 85.322 1.13668 118.6 1.4 1.2 6.1 137 5 1 -4 43.407 86.815 1.12093 235.8 2.7 2.5 6.1 138 5 4 -3 43.607 87.214 1.11682 289.2 3.3 3.0 6.2 139 0 12 0 43.766 87.532 1.11358 176.1 2.0 1.8 6.2 140 2 11 0 43.81 87.62 1.11269 89.7 1.0 0.9 6.2 141 0 10 3 43.941 87.883 1.11004 191.2 2.2 2.0 6.2 142 5 2 -4 43.979 87.958 1.10928 90.3 1.0 0.9 6.2 143 3 10 -2 44.348 88.695 1.10196 111.5 1.3 1.2 6.2 144 4 1 2 44.427 88.854 1.1004 117.1 1.3 1.2 6.2 145 5 2 0 44.757 89.513 1.094 247.4 2.8 2.6 6.2 146 0 5 5 44.867 89.734 1.09188 120.3 1.4 1.2 6.2 147 5 3 -4 44.931 89.862 1.09065 125.5 1.4 1.3 6.2 Reference: Chichagov A.V. et al. Information-Calculating System on Crystal Structure Data of Minerals (MINCRYST) - Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian) |