Institute of Experimental Mineralogy Russian Academy of Sciences ------------------------------------------------- 142432, Chernogolovka, Moscow district A.V. Chichagov +7(496)52-22320 *** *** W W W - X R A Y P O L *** *********************** NAUJAKASITE 2 Na(6)Fe[(Si,Al)(8)Si(4)O(26)] Monoclinic C 2/m Z = 2 C2/m 15 .8 .8 Ref.Str.: Basso R., dal Negro A., Giusta A.D., Ungaretti L. (1975) * Gronlands Geologiske Undersogelse, Bulletin, 116, 11-24 R: from Tuperssuatsiait Bay, Illimaussaq complex, Narsaq, Greenland. N.A.D. Initial data from BDM-file Lattice parameters (cub. angs.,degr.): a = 15.025 alpha = 90.0 b = 7.991 beta = 113.67 c = 10.468 gamma = 90.0 Unit cell volume (cub. angs.) = 1151.1 Molar volume ( cub.cm/mol.) = 346.68 Co-ordinates, thermal parameters, occupation for atomic positions: NoP x/a y/b z/c B(j) atom / occupation 1 0.2299 0.5 0.4403 0.0 Na = 1.00 2 0.343 0.5 0.1126 0.0 Na = 1.00 3 0.4643 0.0 0.165 0.0 Na = 1.00 4 0.0 0.0 0.0 0.0 Fe = 1.00 5 0.0584 0.1953 0.3415 0.0 Al = 0.5 , Si = 0.5 6 0.1463 0.3014 0.6507 0.0 Al = 0.5 , Si = 0.5 7 0.1505 0.3081 0.1315 0.0 Si = 1.00 8 0.101 0.1789 0.0102 0.0 O = 1.00 9 0.2681 0.2937 0.2103 0.0 O = 1.00 10 0.107 0.312 0.2509 0.0 O = 1.00 11 0.1318 0.5 0.0647 0.0 O = 1.00 12 0.1393 0.1973 0.5071 0.0 O = 1.00 13 0.036 0.0 0.2759 0.0 O = 1.00 14 0.0445 0.2932 0.6771 0.0 O = 1.00 15 0.1769 0.5 0.6338 0.0 O = 1.00 Co-ordinates for all atomic positions : No NoP x/a y/b z/c 1 1 0.2299 0.5 0.4403 2 2 0.343 0.5 0.1126 3 3 0.4643 0.0 0.165 4 4 0.0 0.0 0.0 5 5 0.0584 0.1953 0.3415 6 6 0.1463 0.3014 0.6507 7 7 0.1505 0.3081 0.1315 8 8 0.101 0.1789 0.0102 9 9 0.2681 0.2937 0.2103 10 10 0.107 0.312 0.2509 11 11 0.1318 0.5 0.0647 12 12 0.1393 0.1973 0.5071 13 13 0.036 0.0 0.2759 14 14 0.0445 0.2932 0.6771 15 15 0.1769 0.5 0.6338 16 1 0.7701 0.5 0.5597 17 2 0.657 0.5 0.8874 18 3 0.5357 0.0 0.835 19 5 0.9416 0.8047 0.6585 20 6 0.8537 0.6986 0.3493 21 7 0.8495 0.6919 0.8685 22 8 0.899 0.8211 0.9898 23 9 0.7319 0.7063 0.7897 24 10 0.893 0.688 0.7491 25 11 0.8682 0.5 0.9353 26 12 0.8607 0.8027 0.4929 27 13 0.964 0.0 0.7241 28 14 0.9555 0.7068 0.3229 29 15 0.8231 0.5 0.3662 30 5 0.0584 0.8047 0.3415 31 6 0.1463 0.6986 0.6507 32 7 0.1505 0.6919 0.1315 33 8 0.101 0.8211 0.0102 34 9 0.2681 0.7063 0.2103 35 10 0.107 0.688 0.2509 36 12 0.1393 0.8027 0.5071 37 14 0.0445 0.7068 0.6771 38 5 0.9416 0.1953 0.6585 39 6 0.8537 0.3014 0.3493 40 7 0.8495 0.3081 0.8685 41 8 0.899 0.1789 0.9898 42 9 0.7319 0.2937 0.7897 43 10 0.893 0.312 0.7491 44 12 0.8607 0.1973 0.4929 45 14 0.9555 0.2932 0.3229 46 1 0.7299 0.0 0.4403 47 2 0.843 0.0 0.1126 48 3 0.9643 0.5 0.165 49 4 0.5 0.5 0.0 50 5 0.5584 0.3047 0.3415 51 6 0.6463 0.1986 0.6507 52 7 0.6505 0.1919 0.1315 53 8 0.601 0.3211 0.0102 54 9 0.7681 0.2063 0.2103 55 10 0.607 0.188 0.2509 56 11 0.6318 0.0 0.0647 57 12 0.6393 0.3027 0.5071 58 13 0.536 0.5 0.2759 59 14 0.5445 0.2068 0.6771 60 15 0.6769 0.0 0.6338 61 1 0.2701 0.0 0.5597 62 2 0.157 0.0 0.8874 63 3 0.0357 0.5 0.835 64 5 0.4416 0.6953 0.6585 65 6 0.3537 0.8014 0.3493 66 7 0.3495 0.8081 0.8685 67 8 0.399 0.6789 0.9898 68 9 0.2319 0.7937 0.7897 69 10 0.393 0.812 0.7491 70 11 0.3682 0.0 0.9353 71 12 0.3607 0.6973 0.4929 72 13 0.464 0.5 0.7241 73 14 0.4555 0.7932 0.3229 74 15 0.3231 0.0 0.3662 75 5 0.5584 0.6953 0.3415 76 6 0.6463 0.8014 0.6507 77 7 0.6505 0.8081 0.1315 78 8 0.601 0.6789 0.0102 79 9 0.7681 0.7937 0.2103 80 10 0.607 0.812 0.2509 81 12 0.6393 0.6973 0.5071 82 14 0.5445 0.7932 0.6771 83 5 0.4416 0.3047 0.6585 84 6 0.3537 0.1986 0.3493 85 7 0.3495 0.1919 0.8685 86 8 0.399 0.3211 0.9898 87 9 0.2319 0.2063 0.7897 88 10 0.393 0.188 0.7491 89 12 0.3607 0.3027 0.4929 90 14 0.4555 0.2068 0.3229 X-ray density (g/cm cub.) = 2.72 MU (1/cm) = 132.106 Mass attenuation coefficient (cm**2/g) = 48.604 Selected interatomic distances (cation-anion,anion-anion): NoP Atom Rad.sph. C.N. Distance NoP N. (angs.) (angs.) 1 Na 2.808 5 2.5803 10 2.456 15 2.5803 10 2.4047 12 2.4047 12 2 Na 2.808 5 2.4401 9 2.4401 9 2.7113 13 2.2962 8 2.2962 8 3 Na 2.808 5 2.4728 10 2.2536 11 2.3782 14 2.4728 10 2.3782 14 4 Fe 2.592 4 2.0562 8 2.0562 8 2.0562 8 2.0562 8 5 Al ,Si 2.316 4 1.6907 10 1.6706 12 1.6837 13 1.6729 14 6 Al ,Si 2.316 4 1.684 12 1.6612 14 1.6812 15 1.6871 9 7 Si 2.1 4 1.5726 8 1.6265 9 1.6267 10 1.6618 11 8 O 3.264 6 2.7037 9 2.7029 10 2.629 11 3.2094 13 2.8592 8 2.9558 8 9 O 3.264 6 2.7037 8 2.6243 10 2.5939 11 2.7877 15 2.718 12 2.6711 14 10 O 3.264 7 2.7029 8 2.6243 9 2.6035 11 2.6876 12 2.7653 13 3.0046 10 2.6739 14 11 O 3.264 6 2.629 8 2.5939 9 2.6035 10 2.629 8 2.5939 9 2.6035 10 12 O 3.264 7 2.6876 10 2.7814 13 2.7961 14 2.7069 15 3.1532 12 2.767 14 2.718 9 13 O 3.264 8 2.7653 10 2.7814 12 3.2094 8 2.7699 14 2.7653 10 2.7814 12 3.2094 8 2.7699 14 14 O 3.264 6 2.7961 12 2.76 15 2.7699 13 2.6739 10 2.767 12 2.6711 9 15 O 3.264 6 2.7069 12 2.76 14 2.7069 12 2.76 14 2.7877 9 2.7877 9 X-ray diffraction powder data (II), X-Ray W.L. = 1.78892(angs.): No H K L Theta 2*Theta S LPG MF F I int. ( degree ) *100 1 0 0 1 5.353 10.706 0.052 226.8 2 11.2 4.3 2 2 0 -1 7.236 14.472 0.07 123.1 2 82.3 125.9 3 1 1 0 7.437 14.874 0.072 116.42 4 15.0 7.9 4 2 0 0 7.47 14.939 0.073 115.39 2 64.9 73.4 5 1 1 -1 8.25 16.5 0.08 94.2 4 3.4 0.3 6 1 1 1 10.029 20.058 0.097 63.03 4 58.4 64.9 7 2 0 -2 10.344 20.688 0.1 59.13 2 103.9 96.4 8 0 0 2 10.754 21.508 0.104 54.54 2 51.6 21.9 9 2 0 1 10.836 21.672 0.105 53.69 2 5.4 0.2 10 1 1 -2 11.802 23.604 0.114 44.93 4 29.4 11.7 11 3 1 -1 12.199 24.398 0.118 41.92 4 62.7 49.7 12 0 2 0 12.936 25.873 0.125 37.05 2 177.1 175.4 13 3 1 0 12.994 25.987 0.126 36.7 4 104.5 121.1 14 3 1 -2 13.708 27.416 0.132 32.77 4 45.7 20.7 15 4 0 -1 13.791 27.582 0.133 32.35 2 81.3 32.3 16 0 2 1 14.036 28.072 0.136 31.17 4 108.8 111.4 17 1 1 2 14.336 28.672 0.138 29.79 4 174.3 273.2 18 4 0 -2 14.591 29.182 0.141 28.69 2 197.6 169.1 19 2 2 -1 14.884 29.769 0.144 27.5 4 67.2 37.5 20 2 0 -3 14.889 29.778 0.144 27.48 2 179.8 134.1 21 2 2 0 15.003 30.007 0.145 27.03 4 17.5 2.5 22 4 0 0 15.07 30.14 0.145 26.78 2 146.2 86.3 23 2 0 2 15.475 30.95 0.149 25.29 2 142.1 77.1 24 3 1 1 15.77 31.541 0.152 24.29 4 63.5 29.5 25 0 0 3 16.253 32.507 0.156 22.75 2 123.1 52.1 26 1 1 -3 16.481 32.962 0.159 22.08 4 31.3 6.5 27 2 2 -2 16.677 33.354 0.16 21.52 4 135.7 119.6 28 0 2 2 16.944 33.887 0.163 20.79 4 127.7 102.4 29 3 1 -3 16.958 33.915 0.163 20.75 4 136.5 116.8 30 2 2 1 16.998 33.995 0.163 20.65 4 181.8 205.9 31 4 0 -3 17.206 34.413 0.165 20.11 2 25.2 1.9 32 4 0 1 18.028 36.056 0.173 18.16 2 105.5 30.5 33 5 1 -1 18.673 37.347 0.179 16.8 4 153.4 119.4 34 5 1 -2 18.84 37.679 0.181 16.48 4 105.0 54.9 35 4 2 -1 19.088 38.176 0.183 16.01 4 50.6 12.4 36 1 1 3 19.342 38.684 0.185 15.55 4 129.2 78.4 37 4 2 -2 19.695 39.39 0.188 14.94 4 134.5 81.6 38 3 1 2 19.786 39.572 0.189 14.79 4 74.2 24.6 39 2 2 -3 19.925 39.85 0.191 14.56 4 107.1 50.4 40 1 3 0 20.001 40.002 0.191 14.43 4 37.4 6.1 41 2 0 -4 20.021 40.042 0.191 14.4 2 55.2 6.6 42 4 2 0 20.066 40.131 0.192 14.33 4 181.5 142.6 43 5 1 0 20.105 40.209 0.192 14.27 4 10.9 0.5 44 1 3 -1 20.34 40.68 0.194 13.9 4 63.7 17.0 45 2 2 2 20.383 40.766 0.195 13.84 4 95.1 37.8 46 5 1 -3 20.57 41.141 0.196 13.56 4 42.7 7.5 47 2 0 3 20.657 41.315 0.197 13.43 2 188.9 72.3 48 0 2 3 21.002 42.004 0.2 12.94 4 62.8 15.4 49 6 0 -2 21.005 42.01 0.2 12.94 2 114.5 25.6 50 4 0 -4 21.045 42.091 0.201 12.88 2 170.0 56.2 51 1 3 1 21.182 42.364 0.202 12.7 4 22.5 1.9 52 3 1 -4 21.252 42.505 0.203 12.6 4 13.3 0.7 53 6 0 -1 21.269 42.538 0.203 12.58 2 5.2 0.1 54 1 1 -4 21.686 43.372 0.207 12.05 4 141.2 72.5 55 4 2 -3 21.776 43.552 0.207 11.93 4 33.4 4.0 56 0 0 4 21.912 43.824 0.209 11.77 2 54.3 5.2 57 4 0 2 22.086 44.171 0.21 11.56 2 82.8 12.0 58 1 3 -2 22.143 44.285 0.211 11.49 4 37.1 4.8 59 6 0 -3 22.202 44.404 0.211 11.42 2 13.6 0.3 60 3 3 -1 22.373 44.746 0.213 11.23 4 66.7 15.1 61 4 2 1 22.455 44.911 0.214 11.14 4 10.8 0.4 62 3 3 0 22.85 45.699 0.217 10.71 4 40.7 5.4 63 5 1 1 22.883 45.766 0.217 10.67 4 12.5 0.5 64 6 0 0 22.954 45.909 0.218 10.6 2 77.3 9.6 65 3 3 -2 23.295 46.589 0.221 10.25 4 192.4 114.6 66 5 1 -4 23.581 47.162 0.224 9.97 4 112.5 38.1 67 1 3 2 23.698 47.397 0.225 9.86 4 169.1 85.1 68 2 2 -4 24.146 48.291 0.229 9.45 4 105.8 31.9 69 3 1 3 24.556 49.113 0.232 9.09 4 110.4 33.5 70 3 3 1 24.661 49.322 0.233 9.01 4 7.4 0.1 71 6 0 -4 24.692 49.384 0.234 8.98 2 87.1 10.3 72 2 2 3 24.697 49.393 0.234 8.98 4 58.5 9.3 73 1 1 4 24.767 49.533 0.234 8.92 4 41.0 4.5 74 6 2 -2 25.0 49.999 0.236 8.73 4 35.3 3.3 75 4 2 -4 25.035 50.07 0.237 8.7 4 80.6 17.1 76 1 3 -3 25.157 50.315 0.238 8.61 4 59.3 9.1 77 6 2 -1 25.231 50.462 0.238 8.55 4 114.8 34.0 78 3 3 -3 25.497 50.994 0.241 8.35 4 47.6 5.7 79 2 0 -5 25.535 51.069 0.241 8.32 2 75.1 7.1 80 7 1 -2 25.563 51.127 0.241 8.3 4 23.3 1.4 81 4 0 -5 25.682 51.365 0.242 8.21 2 107.7 14.4 82 0 2 4 25.797 51.594 0.243 8.13 4 30.4 2.3 83 6 0 1 25.843 51.686 0.244 8.09 2 89.4 9.8 84 4 2 2 25.95 51.9 0.245 8.02 4 1.6 0.0 85 6 2 -3 26.054 52.107 0.246 7.95 4 36.5 3.2 86 7 1 -1 26.145 52.291 0.246 7.88 4 101.8 24.6 87 2 0 4 26.214 52.428 0.247 7.84 2 39.5 1.8 88 3 1 -5 26.214 52.428 0.247 7.84 4 18.9 0.8 89 7 1 -3 26.251 52.502 0.247 7.81 4 43.9 4.5 90 0 4 0 26.598 53.197 0.25 7.58 2 263.2 79.3 91 5 1 2 26.684 53.368 0.251 7.53 4 105.8 25.4 92 6 2 0 26.723 53.447 0.251 7.5 4 74.3 12.5 93 5 3 -1 26.761 53.522 0.252 7.48 4 75.3 12.8 94 4 0 3 26.876 53.753 0.253 7.4 2 26.4 0.8 95 5 3 -2 26.887 53.773 0.253 7.4 4 179.8 72.2 96 0 4 1 27.216 54.433 0.256 7.19 4 14.3 0.4 97 1 3 3 27.27 54.54 0.256 7.16 4 107.0 24.7 98 1 1 -5 27.275 54.551 0.256 7.16 4 59.5 7.7 99 5 1 -5 27.557 55.114 0.259 6.99 4 48.2 4.9 100 3 3 2 27.612 55.224 0.259 6.96 4 44.8 4.2 101 2 4 -1 27.718 55.435 0.26 6.9 4 19.5 0.8 102 2 4 0 27.79 55.579 0.261 6.86 4 23.0 1.1 103 0 0 5 27.806 55.612 0.261 6.85 2 34.3 1.2 104 5 3 0 27.86 55.721 0.261 6.82 4 28.7 1.7 105 7 1 0 27.941 55.882 0.262 6.78 4 5.4 0.1 106 7 1 -4 28.143 56.287 0.264 6.67 4 58.4 6.9 107 6 0 -5 28.222 56.444 0.264 6.63 2 116.0 13.5 108 5 3 -3 28.226 56.452 0.264 6.62 4 54.4 5.9 109 6 2 -4 28.29 56.581 0.265 6.59 4 36.4 2.6 110 8 0 -2 28.474 56.949 0.267 6.49 2 209.6 43.0 111 3 3 -4 28.768 57.537 0.269 6.34 4 96.8 17.9 112 8 0 -3 28.786 57.571 0.269 6.34 2 108.6 11.3 113 2 4 -2 28.842 57.684 0.27 6.31 4 12.7 0.3 114 0 4 2 29.016 58.033 0.271 6.22 4 4.8 0.0 115 2 4 1 29.052 58.104 0.271 6.21 4 90.0 15.2 116 2 2 -5 29.06 58.12 0.272 6.2 4 121.6 27.7 117 1 3 -4 29.117 58.234 0.272 6.17 4 76.2 10.8 118 4 2 -5 29.195 58.39 0.273 6.14 4 22.9 1.0 119 6 2 1 29.343 58.686 0.274 6.07 4 68.5 8.6 120 8 0 -1 29.344 58.688 0.274 6.07 2 17.3 0.3 121 2 2 4 29.684 59.367 0.277 5.91 4 40.5 2.9 122 6 0 2 29.691 59.382 0.277 5.91 2 212.8 40.4 123 3 1 4 29.884 59.768 0.279 5.82 4 37.7 2.5 124 5 3 1 30.095 60.19 0.28 5.73 4 91.7 14.6 125 8 0 -4 30.254 60.508 0.282 5.67 2 89.1 6.8 126 4 2 3 30.296 60.591 0.282 5.65 4 2.7 0.0 127 4 4 -1 30.48 60.96 0.284 5.57 4 32.2 1.7 128 1 1 5 30.572 61.145 0.284 5.54 4 76.0 9.6 129 5 3 -4 30.675 61.35 0.285 5.49 4 44.4 3.3 130 7 1 1 30.81 61.62 0.286 5.44 4 78.6 10.2 131 4 4 -2 30.913 61.826 0.287 5.4 4 16.7 0.5 132 4 0 -6 30.924 61.847 0.287 5.4 2 87.2 6.2 133 2 4 -3 31.079 62.159 0.289 5.34 4 41.2 2.7 134 7 1 -5 31.095 62.191 0.289 5.33 4 19.9 0.6 135 0 2 5 31.159 62.318 0.289 5.31 4 60.7 5.9 136 4 4 0 31.181 62.363 0.289 5.3 4 44.7 3.2 137 5 1 3 31.276 62.552 0.29 5.26 4 16.8 0.4 138 8 0 0 31.332 62.664 0.291 5.24 2 83.6 5.5 139 2 4 2 31.413 62.827 0.291 5.21 4 17.3 0.5 140 2 0 -6 31.424 62.847 0.291 5.21 2 67.8 3.6 141 3 3 3 31.496 62.992 0.292 5.18 4 73.5 8.4 142 6 2 -5 31.547 63.095 0.292 5.16 4 169.4 44.7 143 1 3 4 31.675 63.35 0.294 5.12 4 77.6 9.3 144 3 1 -6 31.709 63.417 0.294 5.11 4 7.5 0.1 145 8 2 -2 31.783 63.567 0.294 5.08 4 92.0 13.0 146 0 4 3 31.872 63.743 0.295 5.05 4 20.1 0.6 147 8 2 -3 32.075 64.15 0.297 4.98 4 25.4 1.0 148 2 0 5 32.151 64.303 0.297 4.95 2 76.0 4.3 149 4 0 4 32.252 64.503 0.298 4.92 2 6.8 0.0 150 5 1 -6 32.293 64.586 0.299 4.91 4 83.3 10.3 151 7 3 -2 32.357 64.714 0.299 4.89 4 23.6 0.8 152 4 4 -3 32.455 64.909 0.3 4.86 4 12.1 0.2 153 6 0 -6 32.593 65.185 0.301 4.81 2 71.3 3.7 154 8 2 -1 32.599 65.199 0.301 4.81 4 6.8 0.1 155 8 0 -5 32.787 65.573 0.303 4.75 2 62.6 2.8 156 7 3 -1 32.86 65.72 0.303 4.73 4 12.6 0.2 157 3 3 -5 32.92 65.839 0.304 4.71 4 154.3 33.8 158 6 2 2 32.927 65.853 0.304 4.71 4 62.5 5.6 159 7 3 -3 32.952 65.904 0.304 4.7 4 134.5 25.7 160 4 4 1 32.976 65.952 0.304 4.69 4 11.8 0.2 161 1 1 -6 33.266 66.533 0.307 4.61 4 93.0 12.0 162 9 1 -3 33.312 66.624 0.307 4.59 4 24.4 0.8 163 5 3 2 33.329 66.658 0.307 4.59 4 52.6 3.8 164 9 1 -2 33.331 66.662 0.307 4.59 4 6.2 0.1 165 8 2 -4 33.458 66.917 0.308 4.55 4 113.5 17.7 166 1 3 -5 33.848 67.696 0.311 4.44 4 28.9 1.1 167 0 0 6 34.04 68.08 0.313 4.39 2 197.6 25.9 168 4 2 -6 34.093 68.186 0.313 4.37 4 13.3 0.2 169 5 3 -5 34.096 68.193 0.313 4.37 4 40.2 2.1 170 1 5 0 34.293 68.587 0.315 4.32 4 9.7 0.1 171 2 4 -4 34.307 68.614 0.315 4.32 4 36.6 1.7 172 8 0 1 34.33 68.661 0.315 4.31 2 118.6 9.2 173 6 0 3 34.332 68.664 0.315 4.31 2 61.0 2.4 174 9 1 -4 34.372 68.743 0.316 4.3 4 22.1 0.6 175 9 1 -1 34.427 68.855 0.316 4.29 4 66.7 5.8 176 7 3 0 34.437 68.873 0.316 4.28 4 200.2 51.9 177 8 2 0 34.481 68.963 0.316 4.27 4 8.3 0.1 178 1 5 -1 34.529 69.058 0.317 4.26 4 21.7 0.6 179 2 2 -6 34.569 69.137 0.317 4.25 4 88.3 10.0 180 7 1 2 34.606 69.211 0.317 4.24 4 111.2 15.8 181 7 3 -4 34.616 69.233 0.318 4.24 4 168.6 36.4 182 2 4 3 34.751 69.503 0.319 4.21 4 62.5 5.0 183 7 1 -6 34.964 69.927 0.32 4.15 4 6.2 0.0 184 6 4 -2 34.998 69.995 0.321 4.15 4 17.3 0.4 185 4 4 -4 35.026 70.053 0.321 4.14 4 114.3 16.3 186 1 5 1 35.124 70.248 0.322 4.12 4 32.4 1.3 187 6 4 -1 35.187 70.373 0.322 4.1 4 54.3 3.7 188 2 2 5 35.263 70.526 0.323 4.08 4 16.5 0.3 189 4 2 4 35.359 70.718 0.323 4.06 4 14.3 0.2 190 0 4 4 35.652 71.305 0.326 3.99 4 32.0 1.2 191 6 2 -6 35.685 71.37 0.326 3.99 4 73.3 6.5 192 3 1 5 35.741 71.481 0.327 3.98 4 50.8 3.1 193 4 4 2 35.779 71.559 0.327 3.97 4 30.2 1.1 194 1 5 -2 35.821 71.643 0.327 3.96 4 64.8 5.0 195 6 4 -3 35.865 71.73 0.328 3.95 4 49.5 2.9 196 8 2 -5 35.871 71.742 0.328 3.95 4 47.0 2.6 197 3 5 -1 35.991 71.983 0.329 3.92 4 103.9 12.8 198 3 3 4 36.18 72.36 0.33 3.88 4 286.2 96.0 199 8 0 -6 36.273 72.545 0.331 3.86 2 61.2 2.2 200 3 5 0 36.346 72.693 0.331 3.85 4 126.0 18.4 201 6 4 0 36.425 72.85 0.332 3.83 4 70.5 5.8 202 9 1 -5 36.466 72.931 0.332 3.82 4 45.6 2.4 203 9 1 0 36.556 73.112 0.333 3.81 4 11.5 0.2 204 10 0 -3 36.557 73.113 0.333 3.81 2 69.6 2.8 205 5 1 4 36.559 73.118 0.333 3.8 4 8.5 0.1 206 3 5 -2 36.682 73.364 0.334 3.78 4 121.3 16.8 207 4 0 -7 36.736 73.473 0.334 3.77 2 47.6 1.3 208 1 3 5 36.806 73.613 0.335 3.76 4 40.4 1.8 209 1 1 6 36.829 73.658 0.335 3.75 4 43.8 2.2 210 10 0 -2 36.866 73.731 0.335 3.75 2 91.9 4.8 211 1 5 2 36.99 73.979 0.336 3.72 4 238.4 63.9 212 7 3 1 37.023 74.047 0.337 3.72 4 66.8 5.0 213 0 2 6 37.076 74.153 0.337 3.71 4 121.4 16.5 214 7 3 -5 37.285 74.57 0.339 3.67 4 43.4 2.1 215 10 0 -4 37.287 74.573 0.339 3.67 2 233.0 30.0 216 8 2 1 37.356 74.713 0.339 3.65 4 41.1 1.9 217 6 2 3 37.358 74.716 0.339 3.65 4 112.3 13.9 218 5 3 3 37.451 74.901 0.34 3.64 4 115.6 14.7 219 6 0 -7 37.708 75.415 0.342 3.59 2 54.1 1.6 220 5 1 -7 37.716 75.432 0.342 3.59 4 0.2 0.0 221 3 5 1 37.735 75.471 0.342 3.59 4 86.1 8.0 222 3 1 -7 37.75 75.499 0.342 3.59 4 71.4 5.5 223 6 4 -4 37.759 75.519 0.342 3.58 4 5.6 0.0 224 2 0 -7 37.775 75.55 0.342 3.58 2 2.0 0.0 225 3 3 -6 37.849 75.699 0.343 3.57 4 113.9 14.0 226 1 5 -3 38.126 76.253 0.345 3.52 4 43.5 2.0 227 10 0 -1 38.205 76.409 0.346 3.51 2 52.2 1.4 228 4 0 5 38.209 76.418 0.346 3.51 2 129.2 8.8 229 8 0 2 38.241 76.482 0.346 3.5 2 20.5 0.2 230 5 3 -6 38.39 76.78 0.347 3.48 4 163.0 27.9 231 3 5 -3 38.397 76.793 0.347 3.48 4 126.0 16.7 232 2 4 -5 38.427 76.853 0.347 3.48 4 62.4 4.1 233 4 4 -5 38.545 77.089 0.348 3.46 4 63.9 4.3 234 2 0 6 38.568 77.136 0.349 3.45 2 160.6 13.4 235 6 4 1 38.674 77.348 0.349 3.44 4 70.9 5.2 236 2 4 4 38.973 77.946 0.352 3.39 4 30.0 0.9 237 10 0 -5 39.035 78.07 0.352 3.38 2 248.5 31.5 238 7 1 3 39.24 78.48 0.354 3.36 4 2.1 0.0 239 8 2 -6 39.24 78.48 0.354 3.36 4 95.3 9.2 240 1 3 -6 39.297 78.594 0.354 3.35 4 69.8 4.9 241 9 3 -3 39.34 78.68 0.354 3.34 4 49.5 2.5 242 9 3 -2 39.357 78.715 0.354 3.34 4 73.9 5.5 243 5 5 -1 39.419 78.838 0.355 3.33 4 140.4 19.8 244 4 4 3 39.514 79.028 0.356 3.32 4 12.6 0.2 245 10 2 -3 39.516 79.033 0.356 3.32 4 123.8 15.3 246 5 5 -2 39.522 79.044 0.356 3.32 4 63.5 4.0 247 9 1 -6 39.533 79.066 0.356 3.32 4 102.3 10.5 248 9 1 1 39.656 79.313 0.357 3.3 4 44.3 2.0 249 7 1 -7 39.667 79.335 0.357 3.3 4 106.0 11.2 250 4 2 -7 39.692 79.383 0.357 3.29 4 11.8 0.1 251 6 0 4 39.712 79.423 0.357 3.29 2 146.2 10.6 252 1 1 -7 39.767 79.534 0.358 3.28 4 60.8 3.7 253 10 2 -2 39.818 79.636 0.358 3.28 4 63.8 4.0 254 1 5 3 39.838 79.676 0.358 3.28 4 87.7 7.6 255 3 5 2 40.123 80.245 0.36 3.24 4 80.7 6.4 256 10 2 -4 40.229 80.458 0.361 3.23 4 47.0 2.2 257 0 4 5 40.284 80.569 0.361 3.22 4 0.3 0.0 258 5 5 0 40.33 80.66 0.362 3.21 4 8.2 0.1 259 9 3 -4 40.336 80.672 0.362 3.21 4 26.7 0.7 260 9 3 -1 40.389 80.777 0.362 3.21 4 23.0 0.5 261 10 0 0 40.541 81.083 0.363 3.19 2 201.6 19.6 262 7 3 2 40.557 81.114 0.363 3.19 4 66.3 4.2 263 6 4 -5 40.634 81.268 0.364 3.18 4 26.1 0.7 264 5 5 -3 40.637 81.275 0.364 3.18 4 41.1 1.6 265 6 2 -7 40.641 81.282 0.364 3.18 4 69.5 4.6 266 8 0 -7 40.642 81.283 0.364 3.18 2 16.4 0.1 267 2 2 -7 40.707 81.414 0.365 3.17 4 105.5 10.6 268 0 0 7 40.774 81.547 0.365 3.16 2 19.6 0.2 269 8 4 -2 40.847 81.694 0.366 3.15 4 63.7 3.9 270 7 3 -6 40.897 81.793 0.366 3.15 4 67.1 4.3 271 3 5 -4 41.097 82.194 0.367 3.13 4 57.2 3.1 272 8 4 -3 41.111 82.223 0.368 3.13 4 55.4 2.9 273 10 2 -1 41.128 82.256 0.368 3.12 4 22.0 0.5 274 4 2 5 41.132 82.265 0.368 3.12 4 9.5 0.1 275 8 2 2 41.163 82.327 0.368 3.12 4 156.9 23.2 276 1 5 -4 41.395 82.789 0.37 3.1 4 186.1 32.4 277 2 2 6 41.484 82.969 0.37 3.09 4 30.2 0.9 278 8 4 -1 41.589 83.179 0.371 3.08 4 2.4 0.0 279 11 1 -3 41.635 83.27 0.371 3.07 4 36.9 1.3 280 3 3 5 41.636 83.273 0.371 3.07 4 17.8 0.3 281 10 0 -6 41.767 83.534 0.372 3.06 2 155.8 11.2 282 6 4 2 41.889 83.778 0.373 3.05 4 78.9 5.7 283 10 2 -5 41.944 83.887 0.374 3.04 4 21.9 0.4 284 11 1 -4 42.06 84.119 0.374 3.03 4 28.3 0.7 285 0 6 0 42.191 84.381 0.375 3.02 2 275.0 34.5 286 11 1 -2 42.214 84.427 0.376 3.02 4 137.1 17.1 287 3 1 6 42.219 84.439 0.376 3.02 4 17.9 0.3 288 5 5 1 42.24 84.48 0.376 3.02 4 35.9 1.2 289 9 3 -5 42.33 84.661 0.376 3.01 4 32.3 0.9 290 8 4 -4 42.379 84.758 0.377 3.0 4 68.6 4.3 291 9 3 0 42.417 84.835 0.377 3.0 4 33.3 1.0 292 5 3 4 42.42 84.84 0.377 3.0 4 40.8 1.5 293 5 1 5 42.561 85.122 0.378 2.99 4 41.7 1.6 294 6 2 4 42.61 85.221 0.378 2.99 4 96.5 8.4 295 1 3 6 42.68 85.36 0.379 2.98 4 24.9 0.6 296 0 6 1 42.691 85.383 0.379 2.98 4 46.5 1.9 297 5 5 -4 42.748 85.496 0.379 2.97 4 109.2 10.7 298 4 4 -6 42.967 85.935 0.381 2.96 4 49.1 2.2 299 8 0 3 43.027 86.054 0.381 2.95 2 31.3 0.4 300 2 6 -1 43.103 86.206 0.382 2.95 4 70.5 4.4 301 2 6 0 43.162 86.324 0.382 2.94 4 32.8 1.0 302 4 0 -8 43.214 86.428 0.383 2.94 2 249.5 27.6 303 8 4 0 43.33 86.659 0.384 2.93 4 34.0 1.0 304 2 4 -6 43.411 86.822 0.384 2.92 4 66.2 3.9 305 10 2 0 43.43 86.86 0.384 2.92 4 114.5 11.6 306 3 5 3 43.476 86.952 0.385 2.92 4 104.0 9.5 307 11 1 -5 43.484 86.967 0.385 2.92 4 37.3 1.2 308 8 2 -7 43.529 87.058 0.385 2.92 4 59.9 3.2 309 5 3 -7 43.536 87.073 0.385 2.91 4 22.3 0.4 310 9 1 -7 43.538 87.076 0.385 2.91 4 48.2 2.0 311 3 3 -7 43.569 87.138 0.385 2.91 4 58.5 3.0 312 6 0 -8 43.592 87.185 0.385 2.91 2 22.5 0.2 313 1 5 4 43.636 87.271 0.386 2.91 4 0.6 0.0 314 0 2 7 43.66 87.32 0.386 2.91 4 118.9 12.4 315 9 1 2 43.694 87.388 0.386 2.9 4 47.2 2.0 316 1 1 7 43.701 87.402 0.386 2.9 4 0.7 0.0 317 11 1 -1 43.79 87.581 0.387 2.9 4 68.9 4.2 318 10 0 1 43.848 87.695 0.387 2.89 2 112.4 5.5 319 5 1 -8 43.88 87.759 0.387 2.89 4 59.7 3.1 320 2 6 -2 44.042 88.084 0.389 2.88 4 9.4 0.1 321 2 4 5 44.064 88.127 0.389 2.88 4 40.4 1.4 322 4 4 4 44.154 88.308 0.389 2.87 4 29.2 0.7 323 0 6 2 44.19 88.38 0.39 2.87 4 24.8 0.5 324 2 6 1 44.22 88.44 0.39 2.87 4 24.2 0.5 325 7 5 -2 44.249 88.499 0.39 2.87 4 24.4 0.5 326 6 4 -6 44.463 88.925 0.392 2.86 4 14.5 0.2 327 3 1 -8 44.47 88.941 0.392 2.86 4 28.7 0.7 328 8 4 -5 44.639 89.278 0.393 2.85 4 72.0 4.5 329 10 2 -6 44.645 89.291 0.393 2.85 4 163.8 23.1 330 7 5 -1 44.706 89.412 0.393 2.84 4 117.0 11.7 331 7 1 4 44.722 89.445 0.393 2.84 4 70.5 4.3 332 3 5 -5 44.76 89.521 0.394 2.84 4 48.5 2.0 333 2 0 -8 44.774 89.548 0.394 2.84 2 79.7 2.7 334 7 5 -3 44.79 89.58 0.394 2.84 4 102.1 8.9 335 4 0 6 44.874 89.749 0.394 2.83 2 101.4 4.4 X-ray diffraction powder data (I)...X-Ray wave length = 1.78892 (angs.): No H K L Theta 2*Theta d I int I int.n. I p.h.n. H(Si) ( degree ) (angstrem) *100 *100 1 0 0 1 5.353 10.706 9.58736 4.3 1.6 1.6 5.6 2 2 0 -1 7.236 14.472 7.10121 125.9 46.1 46.5 5.6 3 1 1 0 7.437 14.874 6.91037 7.9 2.9 2.9 5.6 4 2 0 0 7.47 14.939 6.88049 73.4 26.9 27.1 5.6 5 1 1 1 10.029 20.058 5.13622 64.9 23.7 23.9 5.6 6 2 0 -2 10.344 20.688 4.98157 96.4 35.3 35.5 5.6 7 0 0 2 10.754 21.508 4.79368 21.9 8.0 8.1 5.6 8 1 1 -2 11.802 23.604 4.37327 11.7 4.3 4.3 5.6 9 3 1 -1 12.199 24.398 4.233 49.7 18.2 18.3 5.6 10 0 2 0 12.936 25.873 3.9955 175.4 64.2 64.3 5.6 11 3 1 0 12.994 25.987 3.97818 121.1 44.3 44.4 5.6 12 3 1 -2 13.708 27.416 3.77456 20.7 7.6 7.6 5.6 13 4 0 -1 13.791 27.582 3.75219 32.3 11.8 11.8 5.6 14 0 2 1 14.036 28.072 3.68805 111.4 40.8 40.8 5.6 15 1 1 2 14.336 28.672 3.61243 273.2 100.0 100.0 5.6 16 4 0 -2 14.591 29.182 3.55061 169.1 61.9 61.9 5.6 17 2 0 -3 14.889 29.778 3.48111 171.6 62.8 62.7 5.6 18 4 0 0 15.07 30.14 3.44025 86.3 31.6 31.6 5.6 19 2 0 2 15.475 30.95 3.3523 77.1 28.2 28.2 5.6 20 3 1 1 15.77 31.541 3.2911 29.5 10.8 10.8 5.6 21 0 0 3 16.253 32.507 3.19579 52.1 19.1 19.0 5.6 22 1 1 -3 16.481 32.962 3.15288 6.5 2.4 2.4 5.6 23 2 2 -2 16.677 33.354 3.11683 119.6 43.8 43.6 5.7 24 3 1 -3 16.958 33.915 3.06674 219.1 80.2 79.8 5.7 25 2 2 1 16.998 33.995 3.05973 205.9 75.4 75.0 5.7 26 4 0 1 18.028 36.056 2.89017 30.5 11.2 11.1 5.7 27 5 1 -1 18.673 37.347 2.79367 119.4 43.7 43.4 5.7 28 5 1 -2 18.84 37.679 2.76991 54.9 20.1 19.9 5.7 29 4 2 -1 19.088 38.176 2.73517 12.4 4.5 4.5 5.7 30 1 1 3 19.342 38.684 2.7006 78.4 28.7 28.4 5.7 31 4 2 -2 19.695 39.39 2.65407 81.6 29.9 29.6 5.7 32 3 1 2 19.786 39.572 2.64239 24.6 9.0 8.9 5.7 33 2 2 -3 19.925 39.85 2.62466 50.4 18.4 18.3 5.7 34 2 0 -4 20.021 40.042 2.61261 12.7 4.6 4.6 5.7 35 4 2 0 20.066 40.131 2.60702 142.6 52.2 51.6 5.7 36 1 3 -1 20.34 40.68 2.57329 17.0 6.2 6.2 5.7 37 2 2 2 20.383 40.766 2.56811 37.8 13.8 13.7 5.7 38 5 1 -3 20.57 41.141 2.54572 7.5 2.7 2.7 5.7 39 2 0 3 20.657 41.315 2.53548 72.3 26.5 26.2 5.7 40 6 0 -2 21.005 42.01 2.49537 41.0 15.0 14.8 5.7 41 4 0 -4 21.045 42.091 2.49078 56.2 20.6 20.3 5.7 42 1 1 -4 21.686 43.372 2.42062 72.5 26.5 26.2 5.7 43 4 2 -3 21.776 43.552 2.4111 4.0 1.5 1.5 5.7 44 0 0 4 21.912 43.824 2.39684 5.2 1.9 1.9 5.7 45 4 0 2 22.086 44.171 2.37894 12.0 4.4 4.3 5.7 46 1 3 -2 22.143 44.285 2.37311 4.8 1.7 1.7 5.7 47 3 3 -1 22.373 44.746 2.34991 15.1 5.5 5.4 5.7 48 3 3 0 22.85 45.699 2.30346 5.4 2.0 1.9 5.7 49 6 0 0 22.954 45.909 2.2935 9.6 3.5 3.4 5.7 50 3 3 -2 23.295 46.589 2.26183 114.6 41.9 41.2 5.7 51 5 1 -4 23.581 47.162 2.2359 38.1 13.9 13.7 5.7 52 1 3 2 23.698 47.397 2.22546 85.1 31.1 30.6 5.7 53 2 2 -4 24.146 48.291 2.18663 31.9 11.7 11.5 5.7 54 3 1 3 24.556 49.113 2.15228 33.5 12.3 12.0 5.7 55 6 0 -4 24.692 49.384 2.1412 19.5 7.2 7.0 5.7 56 1 1 4 24.767 49.533 2.13514 4.5 1.7 1.6 5.7 57 6 2 -2 25.0 49.999 2.1165 3.3 1.2 1.2 5.7 58 4 2 -4 25.035 50.07 2.1137 17.1 6.2 6.1 5.7 59 1 3 -3 25.157 50.315 2.10408 9.1 3.3 3.3 5.8 60 6 2 -1 25.231 50.462 2.09835 34.0 12.4 12.2 5.8 61 3 3 -3 25.497 50.994 2.07789 5.7 2.1 2.0 5.8 62 2 0 -5 25.535 51.069 2.07504 8.4 3.1 3.0 5.8 63 4 0 -5 25.682 51.365 2.06391 14.4 5.3 5.1 5.8 64 6 0 1 25.843 51.686 2.05194 9.8 3.6 3.5 5.8 65 6 2 -3 26.054 52.107 2.03651 3.2 1.2 1.1 5.8 66 7 1 -1 26.145 52.291 2.02987 24.6 9.0 8.8 5.8 67 7 1 -3 26.251 52.502 2.02225 4.5 1.7 1.6 5.8 68 0 4 0 26.598 53.197 1.99775 79.3 29.0 28.3 5.8 69 5 1 2 26.684 53.368 1.99182 25.4 9.3 9.1 5.8 70 6 2 0 26.723 53.447 1.98909 12.5 4.6 4.5 5.8 71 5 3 -1 26.761 53.522 1.98649 12.8 4.7 4.6 5.8 72 5 3 -2 26.887 53.773 1.97789 72.2 26.4 25.7 5.8 73 1 3 3 27.27 54.54 1.95219 32.4 11.9 11.5 5.8 74 5 1 -5 27.557 55.114 1.93342 4.9 1.8 1.7 5.8 75 3 3 2 27.612 55.224 1.92986 4.2 1.5 1.5 5.8 76 7 1 -4 28.143 56.287 1.89633 6.9 2.5 2.4 5.8 77 6 0 -5 28.222 56.444 1.89147 19.4 7.1 6.9 5.8 78 8 0 -2 28.474 56.949 1.87609 43.0 15.8 15.3 5.8 79 3 3 -4 28.768 57.537 1.85854 29.2 10.7 10.4 5.8 80 2 2 -5 29.06 58.12 1.8415 42.8 15.7 15.2 5.8 81 1 3 -4 29.117 58.234 1.8382 10.8 4.0 3.8 5.8 82 6 2 1 29.343 58.686 1.8253 8.9 3.2 3.1 5.8 83 6 0 2 29.691 59.382 1.80581 43.3 15.9 15.3 5.8 84 5 3 1 30.095 60.19 1.78381 14.6 5.3 5.1 5.8 85 8 0 -4 30.254 60.508 1.7753 6.8 2.5 2.4 5.8 86 1 1 5 30.572 61.145 1.75857 9.6 3.5 3.4 5.8 87 5 3 -4 30.675 61.35 1.75328 3.3 1.2 1.2 5.8 88 7 1 1 30.81 61.62 1.74634 10.2 3.7 3.6 5.8 89 4 0 -6 30.924 61.847 1.74055 6.2 2.3 2.2 5.8 90 2 4 -3 31.079 62.159 1.7327 3.4 1.2 1.2 5.8 91 0 2 5 31.159 62.318 1.72871 9.1 3.3 3.2 5.8 92 8 0 0 31.332 62.664 1.72012 5.5 2.0 1.9 5.8 93 2 0 -6 31.424 62.847 1.71562 3.6 1.3 1.3 5.9 94 3 3 3 31.496 62.992 1.71207 8.4 3.1 3.0 5.9 95 6 2 -5 31.547 63.095 1.70958 44.7 16.4 15.7 5.9 96 1 3 4 31.675 63.35 1.70341 9.3 3.4 3.3 5.9 97 8 2 -2 31.783 63.567 1.6982 13.0 4.7 4.6 5.9 98 2 0 5 32.151 64.303 1.68081 4.3 1.6 1.5 5.9 99 5 1 -6 32.293 64.586 1.67423 10.3 3.8 3.6 5.9 100 6 0 -6 32.593 65.185 1.66052 3.8 1.4 1.3 5.9 101 8 0 -5 32.787 65.573 1.65179 2.8 1.0 1.0 5.9 102 3 3 -5 32.92 65.839 1.64585 39.4 14.4 13.8 5.9 103 7 3 -3 32.952 65.904 1.64441 25.9 9.5 9.1 5.9 104 1 1 -6 33.266 66.533 1.63065 12.0 4.4 4.2 5.9 105 5 3 2 33.329 66.658 1.62792 3.9 1.4 1.4 5.9 106 8 2 -4 33.458 66.917 1.62236 17.7 6.5 6.2 5.9 107 0 0 6 34.04 68.08 1.59789 25.9 9.5 9.0 5.9 108 6 0 3 34.332 68.664 1.58596 13.3 4.9 4.6 5.9 109 7 3 0 34.437 68.873 1.58173 57.6 21.1 20.1 5.9 110 2 2 -6 34.569 69.137 1.57644 10.0 3.7 3.5 5.9 111 7 3 -4 34.616 69.233 1.57453 52.2 19.1 18.2 5.9 112 2 4 3 34.751 69.503 1.56919 5.0 1.8 1.7 5.9 113 4 4 -4 35.026 70.053 1.55842 16.3 6.0 5.7 5.9 114 6 4 -1 35.187 70.373 1.55223 3.7 1.3 1.3 5.9 115 6 2 -6 35.685 71.37 1.53337 6.5 2.4 2.2 5.9 116 3 1 5 35.741 71.481 1.5313 3.1 1.1 1.1 5.9 117 1 5 -2 35.821 71.643 1.52831 5.0 1.8 1.7 5.9 118 6 4 -3 35.865 71.73 1.52669 5.5 2.0 1.9 5.9 119 3 5 -1 35.991 71.983 1.52206 12.8 4.7 4.4 5.9 120 3 3 4 36.18 72.36 1.5152 96.0 35.1 33.2 5.9 121 3 5 0 36.346 72.693 1.50922 18.4 6.7 6.4 6.0 122 6 4 0 36.425 72.85 1.50641 5.8 2.1 2.0 6.0 123 10 0 -3 36.557 73.113 1.50174 2.9 1.0 1.0 6.0 124 3 5 -2 36.682 73.364 1.49732 16.8 6.2 5.8 6.0 125 1 1 6 36.829 73.658 1.49218 4.0 1.5 1.4 6.0 126 10 0 -2 36.866 73.731 1.49091 4.8 1.7 1.7 6.0 127 1 5 2 36.99 73.979 1.48663 63.9 23.4 22.0 6.0 128 7 3 1 37.023 74.047 1.48547 5.0 1.8 1.7 6.0 129 0 2 6 37.076 74.153 1.48365 16.5 6.0 5.7 6.0 130 10 0 -4 37.287 74.573 1.47649 32.1 11.8 11.1 6.0 131 6 2 3 37.358 74.716 1.47408 15.8 5.8 5.4 6.0 132 5 3 3 37.451 74.901 1.47096 14.7 5.4 5.1 6.0 133 3 5 1 37.735 75.471 1.4615 15.2 5.6 5.2 6.0 134 3 3 -6 37.849 75.699 1.45776 14.0 5.1 4.8 6.0 135 4 0 5 38.209 76.418 1.4461 10.3 3.8 3.5 6.0 136 5 3 -6 38.39 76.78 1.44032 44.6 16.3 15.3 6.0 137 2 4 -5 38.427 76.853 1.43917 4.1 1.5 1.4 6.0 138 2 0 6 38.568 77.136 1.43472 17.7 6.5 6.1 6.0 139 6 4 1 38.674 77.348 1.4314 5.2 1.9 1.8 6.0 140 10 0 -5 39.035 78.07 1.42024 31.5 11.5 10.8 6.0 141 8 2 -6 39.24 78.48 1.41402 9.2 3.4 3.1 6.0 142 1 3 -6 39.297 78.594 1.41229 4.9 1.8 1.7 6.0 143 9 3 -2 39.357 78.715 1.41047 8.0 2.9 2.7 6.0 144 5 5 -1 39.419 78.838 1.40863 19.8 7.3 6.8 6.0 145 10 2 -3 39.516 79.033 1.40573 29.9 10.9 10.2 6.0 146 7 1 -7 39.667 79.335 1.40125 13.1 4.8 4.5 6.0 147 6 0 4 39.712 79.423 1.39995 10.6 3.9 3.6 6.0 148 1 1 -7 39.767 79.534 1.39833 3.7 1.3 1.3 6.0 149 1 5 3 39.838 79.676 1.39624 11.6 4.3 4.0 6.0 150 3 5 2 40.123 80.245 1.388 6.4 2.3 2.2 6.0 151 10 0 0 40.541 81.083 1.3761 23.8 8.7 8.1 6.1 152 6 2 -7 40.641 81.282 1.37331 6.4 2.3 2.2 6.1 153 2 2 -7 40.707 81.414 1.37148 10.6 3.9 3.6 6.1 154 8 4 -2 40.847 81.694 1.36759 3.9 1.4 1.3 6.1 155 7 3 -6 40.897 81.793 1.36622 4.3 1.6 1.5 6.1 156 3 5 -4 41.097 82.194 1.36074 6.0 2.2 2.0 6.1 157 8 2 2 41.163 82.327 1.35893 23.2 8.5 7.9 6.1 158 1 5 -4 41.395 82.789 1.3527 32.4 11.8 11.0 6.1 159 10 0 -6 41.767 83.534 1.34282 11.2 4.1 3.8 6.1 160 6 4 2 41.889 83.778 1.33963 5.7 2.1 1.9 6.1 161 0 6 0 42.191 84.381 1.33183 51.9 19.0 17.5 6.1 162 8 4 -4 42.379 84.758 1.32703 4.3 1.6 1.4 6.1 163 6 2 4 42.61 85.221 1.32119 8.4 3.1 2.8 6.1 164 5 5 -4 42.748 85.496 1.31776 10.7 3.9 3.6 6.1 165 2 6 -1 43.103 86.206 1.30901 4.4 1.6 1.5 6.1 166 4 0 -8 43.214 86.428 1.30631 27.6 10.1 9.3 6.1 167 10 2 0 43.43 86.86 1.30109 15.4 5.6 5.2 6.1 168 3 5 3 43.476 86.952 1.29999 10.8 3.9 3.6 6.1 169 8 2 -7 43.529 87.058 1.29872 5.6 2.1 1.9 6.1 170 3 3 -7 43.569 87.138 1.29777 3.2 1.2 1.1 6.2 171 0 2 7 43.66 87.32 1.29562 12.4 4.5 4.2 6.2 172 11 1 -1 43.79 87.581 1.29253 4.2 1.5 1.4 6.2 173 10 0 1 43.848 87.695 1.29119 5.5 2.0 1.8 6.2 174 5 1 -8 43.88 87.759 1.29044 3.1 1.1 1.0 6.2 175 10 2 -6 44.645 89.291 1.27286 27.5 10.1 9.2 6.2 176 7 5 -1 44.706 89.412 1.2715 16.0 5.9 5.3 6.2 177 7 5 -3 44.79 89.58 1.26962 13.7 5.0 4.5 6.2 178 4 0 6 44.874 89.749 1.26774 4.4 1.6 1.5 6.2 Reference: Chichagov A.V. et al. Information-Calculating System on Crystal Structure Data of Minerals (MINCRYST) - Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian) |