Institute of Experimental Mineralogy Russian Academy of Sciences ------------------------------------------------- 142432, Chernogolovka, Moscow district A.V. Chichagov +7(496)52-22320 *** *** W W W - X R A Y P O L *** *********************** EPIDOTE 4, syn, t-epidote, f-epidote, s-epidote Ca(2)Al(2.4)Fe(0.6)Si(3)O(13) Monoclinic P 2(1)/m Z = 2 P2(1)/m 21 .2 .1902 Ref.Str.: Giuli G., Bonazzi P., Menchetti S. (1987) * Amer. Mineral., 84, 933-936 Reserv: N.A.D. Initial data from BDM-file Lattice parameters (cub. angs.,degr.): a = 8.891 alpha = 90.0 b = 5.624 beta = 115.43 c = 10.164 gamma = 90.0 Unit cell volume (cub. angs.) = 458.97 Molar volume ( cub.cm/mol.) = 138.23 Co-ordinates, thermal parameters, occupation for atomic positions: NoP x/a y/b z/c B(j) atom / occupation 1 0.7574 0.75 0.1517 0.0 Ca = 1.00 2 0.6047 0.75 0.4241 0.0 Ca = 1.00 3 0.0 0.0 0.0 0.0 Al = 0.92, Fe = 0.08 4 0.0 0.0 0.5 0.0 Al = 1.00 5 0.2936 0.25 0.2247 0.0 Al = 0.4 , Fe = 0.6 6 0.3383 0.75 0.0467 0.0 Si = 1.00 7 0.6832 0.25 0.2742 0.0 Si = 1.00 8 0.1834 0.75 0.3183 0.0 Si = 1.00 9 0.2345 0.9942 0.0416 0.0 O = 1.00 10 0.3017 0.9819 0.3535 0.0 O = 1.00 11 0.7937 0.0128 0.3419 0.0 O = 1.00 12 0.053 0.25 0.1298 0.0 O = 1.00 13 0.0418 0.75 0.1449 0.0 O = 1.00 14 0.0659 0.75 0.4059 0.0 O = 1.00 15 0.5138 0.75 0.1807 0.0 O = 1.00 16 0.523 0.25 0.3067 0.0 O = 1.00 17 0.6295 0.25 0.0996 0.0 O = 1.00 18 0.0796 0.25 0.4263 0.0 O = 1.00 Co-ordinates for all atomic positions : No NoP x/a y/b z/c 1 1 0.7574 0.75 0.1517 2 2 0.6047 0.75 0.4241 3 3 0.0 0.0 0.0 4 4 0.0 0.0 0.5 5 5 0.2936 0.25 0.2247 6 6 0.3383 0.75 0.0467 7 7 0.6832 0.25 0.2742 8 8 0.1834 0.75 0.3183 9 9 0.2345 0.9942 0.0416 10 10 0.3017 0.9819 0.3535 11 11 0.7937 0.0128 0.3419 12 12 0.053 0.25 0.1298 13 13 0.0418 0.75 0.1449 14 14 0.0659 0.75 0.4059 15 15 0.5138 0.75 0.1807 16 16 0.523 0.25 0.3067 17 17 0.6295 0.25 0.0996 18 18 0.0796 0.25 0.4263 19 1 0.2426 0.25 0.8483 20 2 0.3953 0.25 0.5759 21 3 0.0 0.5 0.0 22 4 0.0 0.5 0.5 23 5 0.7064 0.75 0.7753 24 6 0.6617 0.25 0.9533 25 7 0.3168 0.75 0.7258 26 8 0.8166 0.25 0.6817 27 9 0.7655 0.4942 0.9584 28 10 0.6983 0.4819 0.6465 29 11 0.2063 0.5128 0.6581 30 12 0.947 0.75 0.8702 31 13 0.9582 0.25 0.8551 32 14 0.9341 0.25 0.5941 33 15 0.4862 0.25 0.8193 34 16 0.477 0.75 0.6933 35 17 0.3705 0.75 0.9004 36 18 0.9204 0.75 0.5737 37 9 0.2345 0.5058 0.0416 38 10 0.3017 0.5181 0.3535 39 11 0.7937 0.4872 0.3419 40 9 0.7655 0.0058 0.9584 41 10 0.6983 0.0181 0.6465 42 11 0.2063 0.9872 0.6581 X-ray density (g/cm cub.) = 3.42 MU (1/cm) = 254.784 Mass attenuation coefficient (cm**2/g) = 74.47 Selected interatomic distances (cation-anion,anion-anion): NoP Atom Rad.sph. C.N. Distance NoP N. (angs.) (angs.) 1 Ca 2.88 7 2.3431 11 2.559 13 2.8481 14 2.3078 15 2.461 9 2.3431 11 2.461 9 2 Ca 2.88 8 2.7952 10 2.6291 11 2.2486 15 2.5416 10 2.5544 18 2.7952 10 2.6291 11 2.5416 10 3 Al ,Fe 2.592 6 1.9415 9 1.8454 12 1.9529 13 1.8454 12 1.9529 13 1.9415 9 4 Al 2.316 6 1.8493 11 1.9278 14 1.8693 18 1.9278 14 1.8693 18 1.8493 11 5 Al ,Fe 2.592 6 2.2292 9 1.9777 10 1.9324 12 1.8424 16 2.2292 9 1.9777 10 6 Si 2.1 4 1.643 9 1.5698 15 1.6306 17 1.643 9 7 Si 2.1 4 1.6241 11 1.5944 16 1.6277 17 1.6241 11 8 Si 2.1 4 1.6162 10 1.6689 13 1.638 14 1.6162 10 9 O 3.264 10 2.9639 10 2.5923 12 2.733 13 2.6525 15 3.158 16 2.7623 12 2.7745 13 2.6265 17 2.8772 9 2.7468 9 10 O 3.264 8 2.9639 9 2.8309 12 2.707 13 2.7091 14 2.6786 16 2.8241 18 3.0156 10 2.6084 10 11 O 3.264 9 2.6669 14 2.7495 15 2.6383 16 2.6245 17 2.6653 18 2.6759 14 2.5932 18 2.668 11 2.956 11 12 O 3.264 10 2.5923 9 2.8309 10 2.8203 13 2.8203 13 2.9199 18 2.7623 9 2.5465 13 2.5923 9 2.8309 10 2.7623 9 13 O 3.264 10 2.733 9 2.707 10 2.8203 12 2.8203 12 2.5681 14 2.7745 9 2.5465 12 2.733 9 2.707 10 2.7745 9 14 O 3.264 10 2.7091 10 2.6669 11 2.5681 13 2.8184 18 2.8184 18 2.6759 11 2.5451 18 2.7091 10 2.6669 11 2.6759 11 15 O 3.264 9 2.6525 9 2.7495 11 3.0764 16 3.0764 16 3.2208 17 3.2208 17 2.5733 17 2.6525 9 2.7495 11 16 O 3.264 9 3.158 9 2.6786 10 2.6383 11 3.0764 15 3.0764 15 2.6532 17 3.158 9 2.6786 10 2.6383 11 17 O 3.264 8 2.6245 11 3.2208 15 3.2208 15 2.6532 16 2.6265 9 2.5733 15 2.6245 11 2.6265 9 18 O 3.264 10 2.8241 10 2.6653 11 2.9199 12 2.8184 14 2.8184 14 2.5932 11 2.5451 14 2.8241 10 2.6653 11 2.5932 11 X-ray diffraction powder data (II), X-Ray W.L. = 1.54056(angs.): No H K L Theta 2*Theta S LPG MF F I int. ( degree ) *100 1 0 0 1 4.814 9.628 0.054 281.02 2 8.0 17.1 2 1 0 0 5.505 11.01 0.062 214.34 2 15.9 51.5 3 1 0 -1 5.543 11.086 0.063 211.37 2 11.1 24.6 4 1 0 1 8.754 17.507 0.099 83.42 2 8.2 5.3 5 1 0 -2 8.826 17.652 0.1 82.02 2 57.4 256.8 6 0 1 1 9.243 18.487 0.104 74.59 4 8.9 11.2 7 1 1 0 9.626 19.252 0.109 68.6 4 9.9 12.7 8 1 1 -1 9.648 19.297 0.109 68.28 4 14.8 28.2 9 0 0 2 9.662 19.324 0.109 68.08 2 2.3 0.3 10 2 0 -1 9.978 19.957 0.112 63.69 2 4.1 1.0 11 2 0 0 11.062 22.124 0.125 51.43 2 58.3 166.2 12 2 0 -2 11.139 22.278 0.125 50.69 2 58.5 164.8 13 1 1 1 11.814 23.629 0.133 44.83 4 25.4 54.8 14 1 1 -2 11.869 23.738 0.134 44.4 4 13.6 15.7 15 0 1 2 12.511 25.022 0.141 39.75 4 0.4 0.0 16 2 1 -1 12.76 25.52 0.143 38.13 4 64.8 304.5 17 1 0 2 13.078 26.156 0.147 36.2 2 55.9 107.5 18 1 0 -3 13.161 26.321 0.148 35.73 2 9.4 3.0 19 2 1 0 13.635 27.27 0.153 33.15 4 7.8 3.8 20 2 1 -2 13.699 27.397 0.154 32.82 4 5.6 2.0 21 2 0 1 13.897 27.794 0.156 31.83 2 60.1 109.1 22 2 0 -3 14.022 28.043 0.157 31.23 2 15.9 7.5 23 0 0 3 14.581 29.163 0.163 28.73 2 36.1 35.5 24 3 0 -1 15.243 30.487 0.171 26.13 2 22.9 13.0 25 3 0 -2 15.286 30.573 0.171 25.97 2 80.4 159.5 26 1 1 2 15.337 30.675 0.172 25.79 4 10.6 5.5 27 1 1 -3 15.409 30.817 0.172 25.53 4 138.9 935.4 28 0 2 0 15.898 31.796 0.178 23.87 2 127.5 368.3 29 2 1 1 16.051 32.101 0.179 23.38 4 47.5 100.2 30 2 1 -3 16.16 32.32 0.181 23.04 4 27.8 33.9 31 0 2 1 16.648 33.296 0.186 21.6 4 11.3 5.2 32 0 1 3 16.655 33.309 0.186 21.58 4 83.9 288.3 33 3 0 0 16.726 33.453 0.187 21.38 2 92.2 172.6 34 3 0 -3 16.845 33.69 0.188 21.06 2 13.3 3.5 35 1 2 0 16.872 33.745 0.188 20.98 4 70.4 197.5 36 1 2 -1 16.885 33.771 0.189 20.95 4 9.3 3.5 37 3 1 -1 17.245 34.49 0.192 20.01 4 103.4 406.3 38 3 1 -2 17.283 34.567 0.193 19.91 4 19.7 14.7 39 2 0 2 17.72 35.441 0.198 18.85 2 95.7 163.9 40 1 0 3 17.788 35.576 0.198 18.7 2 8.4 1.3 41 2 0 -4 17.871 35.742 0.199 18.51 2 12.5 2.8 42 1 0 -4 17.876 35.751 0.199 18.5 2 46.2 37.5 43 1 2 1 18.262 36.524 0.203 17.65 4 5.5 1.0 44 1 2 -2 18.299 36.597 0.204 17.57 4 55.7 103.6 45 3 1 0 18.586 37.172 0.207 16.98 4 15.6 7.9 46 3 1 -3 18.694 37.389 0.208 16.76 4 93.9 280.9 47 0 2 2 18.739 37.478 0.209 16.68 4 83.9 222.8 48 2 2 -1 18.913 37.826 0.21 16.34 4 37.1 42.6 49 3 0 1 19.426 38.852 0.216 15.4 2 16.8 4.1 50 2 1 2 19.498 38.995 0.217 15.27 4 22.8 15.0 51 2 2 0 19.538 39.077 0.217 15.2 4 11.4 3.7 52 1 1 3 19.56 39.12 0.217 15.17 4 40.3 46.8 53 2 2 -2 19.585 39.169 0.218 15.12 4 63.9 117.4 54 3 0 -4 19.6 39.2 0.218 15.1 2 27.5 10.8 55 0 0 4 19.614 39.227 0.218 15.08 2 11.5 1.9 56 2 1 -4 19.636 39.273 0.218 15.04 4 33.2 31.5 57 1 1 -4 19.641 39.282 0.218 15.03 4 27.5 21.6 58 4 0 -2 20.277 40.554 0.225 14.0 2 24.8 8.2 59 1 2 2 20.812 41.624 0.231 13.21 4 10.8 2.9 60 4 0 -1 20.846 41.692 0.231 13.16 2 108.8 147.8 61 1 2 -3 20.867 41.733 0.231 13.13 4 51.0 64.8 62 4 0 -3 20.934 41.867 0.232 13.04 2 40.9 20.7 63 3 1 1 21.081 42.162 0.233 12.84 4 3.1 0.2 64 3 1 -4 21.244 42.487 0.235 12.62 4 10.6 2.7 65 0 1 4 21.256 42.513 0.235 12.6 4 27.7 18.3 66 2 2 1 21.365 42.73 0.236 12.46 4 88.2 183.8 67 2 2 -3 21.451 42.902 0.237 12.34 4 85.1 169.9 68 0 2 3 21.842 43.683 0.241 11.85 4 78.6 139.1 69 4 1 -2 21.879 43.757 0.242 11.81 4 22.2 11.1 70 2 0 3 22.111 44.223 0.244 11.53 2 79.4 69.0 71 2 0 -5 22.278 44.557 0.246 11.34 2 24.8 6.6 72 3 2 -1 22.314 44.629 0.246 11.3 4 35.6 27.2 73 3 2 -2 22.345 44.691 0.247 11.26 4 27.1 15.6 74 4 1 -1 22.415 44.829 0.248 11.18 4 2.9 0.2 75 4 1 -3 22.497 44.994 0.248 11.09 4 0.8 0.0 76 4 0 0 22.565 45.13 0.249 11.01 2 78.9 65.2 77 4 0 -4 22.729 45.459 0.251 10.84 2 18.9 3.7 78 1 0 4 22.75 45.499 0.251 10.81 2 28.7 8.5 79 1 0 -5 22.841 45.683 0.252 10.72 2 39.2 15.7 80 3 0 2 22.986 45.971 0.253 10.56 2 19.9 4.0 81 3 0 -5 23.198 46.396 0.256 10.35 2 44.8 19.7 82 3 2 0 23.411 46.822 0.258 10.13 4 17.8 6.1 83 3 2 -3 23.501 47.002 0.259 10.05 4 21.6 8.9 84 2 1 3 23.613 47.226 0.26 9.94 4 43.1 35.1 85 2 1 -5 23.771 47.543 0.262 9.79 4 4.0 0.3 86 4 1 0 24.044 48.089 0.264 9.54 4 7.1 0.9 87 2 2 2 24.172 48.345 0.266 9.42 4 72.1 93.0 88 4 1 -4 24.201 48.402 0.266 9.4 4 3.3 0.2 89 1 1 4 24.22 48.44 0.266 9.38 4 50.4 45.2 90 1 2 3 24.225 48.45 0.266 9.38 4 24.1 10.3 91 2 2 -4 24.289 48.579 0.267 9.32 4 87.2 134.5 92 1 2 -4 24.293 48.586 0.267 9.32 4 55.9 55.2 93 1 1 -5 24.308 48.615 0.267 9.31 4 41.3 30.2 94 3 1 2 24.445 48.89 0.269 9.19 4 44.6 34.7 95 3 1 -5 24.648 49.295 0.271 9.02 4 9.3 1.5 96 0 3 1 24.795 49.59 0.272 8.9 4 4.3 0.3 97 0 0 5 24.809 49.618 0.272 8.88 2 15.0 1.9 98 1 3 0 24.957 49.914 0.274 8.76 4 25.5 10.8 99 1 3 -1 24.967 49.933 0.274 8.76 4 8.9 1.3 100 4 0 1 25.25 50.499 0.277 8.53 2 17.9 2.6 101 4 0 -5 25.476 50.951 0.279 8.36 2 14.7 1.7 102 3 2 1 25.523 51.046 0.28 8.33 4 22.3 7.9 103 3 2 -4 25.663 51.327 0.281 8.22 4 4.3 0.3 104 0 2 4 25.674 51.349 0.281 8.22 4 37.8 22.2 105 5 0 -2 25.776 51.552 0.282 8.14 2 76.3 45.0 106 5 0 -3 25.823 51.646 0.283 8.11 2 30.1 7.0 107 1 3 1 25.987 51.974 0.284 7.99 4 26.0 10.2 108 1 3 -2 26.015 52.03 0.285 7.97 4 15.3 3.5 109 0 1 5 26.192 52.384 0.287 7.85 4 40.2 24.1 110 4 2 -2 26.215 52.43 0.287 7.84 4 38.5 22.0 111 0 3 2 26.35 52.699 0.288 7.75 4 0.3 0.0 112 2 3 -1 26.483 52.966 0.289 7.66 4 51.8 39.1 113 4 1 1 26.616 53.232 0.291 7.57 4 11.8 2.0 114 4 2 -1 26.684 53.369 0.292 7.53 4 24.4 8.5 115 5 0 -1 26.747 53.494 0.292 7.49 2 10.5 0.8 116 4 2 -3 26.757 53.514 0.292 7.48 4 22.6 7.2 117 4 1 -5 26.834 53.668 0.293 7.43 4 67.2 63.8 118 5 0 -4 26.883 53.766 0.294 7.4 2 21.0 3.1 119 2 0 4 26.908 53.816 0.294 7.38 2 41.6 12.1 120 2 3 0 26.967 53.934 0.294 7.35 4 9.1 1.1 121 2 3 -2 27.003 54.006 0.295 7.32 4 2.3 0.1 122 2 0 -6 27.088 54.177 0.296 7.27 2 65.1 29.2 123 5 1 -2 27.124 54.248 0.296 7.25 4 45.8 28.9 124 3 0 3 27.165 54.33 0.296 7.23 2 19.8 2.7 125 5 1 -3 27.169 54.338 0.296 7.22 4 36.0 17.8 126 3 0 -6 27.407 54.814 0.299 7.08 2 77.2 40.0 127 2 2 3 27.745 55.489 0.302 6.89 4 0.9 0.0 128 2 2 -5 27.886 55.772 0.304 6.81 4 19.5 4.9 129 1 0 5 27.961 55.922 0.304 6.77 2 48.2 14.9 130 1 3 2 27.974 55.949 0.304 6.76 4 7.1 0.6 131 1 3 -3 28.018 56.037 0.305 6.74 4 95.2 115.8 132 1 0 -6 28.058 56.115 0.305 6.71 2 131.1 109.5 133 5 1 -1 28.062 56.125 0.305 6.71 4 100.3 128.3 134 4 2 0 28.13 56.26 0.306 6.67 4 51.2 33.2 135 5 1 -4 28.194 56.388 0.307 6.64 4 24.3 7.5 136 2 1 4 28.218 56.436 0.307 6.63 4 41.0 21.1 137 4 2 -4 28.27 56.54 0.307 6.6 4 107.1 143.7 138 1 2 4 28.287 56.575 0.308 6.59 4 74.9 70.3 139 1 2 -5 28.366 56.732 0.308 6.55 4 2.3 0.1 140 2 1 -6 28.393 56.786 0.309 6.54 4 33.4 13.8 141 2 3 1 28.42 56.841 0.309 6.52 4 37.1 17.0 142 3 1 3 28.467 56.935 0.309 6.5 4 21.4 5.7 143 3 2 2 28.489 56.979 0.31 6.49 4 61.5 46.6 144 2 3 -3 28.49 56.98 0.31 6.49 4 20.3 5.1 145 5 0 0 28.664 57.328 0.311 6.4 2 21.5 2.8 146 3 2 -5 28.672 57.343 0.311 6.39 4 14.2 2.4 147 3 1 -6 28.702 57.404 0.312 6.38 4 8.9 1.0 148 4 0 2 28.709 57.417 0.312 6.37 2 5.3 0.2 149 0 3 3 28.808 57.617 0.313 6.32 4 64.7 50.3 150 5 0 -5 28.88 57.76 0.314 6.29 2 17.0 1.7 151 4 0 -6 28.985 57.97 0.315 6.24 2 142.8 120.7 152 3 3 -1 29.197 58.393 0.317 6.14 4 88.2 90.5 153 3 3 -2 29.222 58.445 0.317 6.12 4 29.0 9.8 154 1 1 5 29.24 58.479 0.317 6.12 4 73.8 63.3 155 1 1 -6 29.334 58.667 0.318 6.07 4 22.4 5.8 156 5 1 0 29.923 59.847 0.324 5.81 4 57.5 36.4 157 4 1 2 29.967 59.934 0.324 5.79 4 77.5 66.0 158 0 2 5 30.072 60.145 0.325 5.74 4 6.9 0.5 159 3 3 0 30.11 60.219 0.326 5.73 4 21.1 4.9 160 5 1 -5 30.134 60.267 0.326 5.72 4 16.5 2.9 161 3 3 -3 30.185 60.37 0.326 5.69 4 67.8 49.7 162 0 0 6 30.233 60.465 0.327 5.67 2 38.8 8.1 163 4 1 -6 30.236 60.472 0.327 5.67 4 3.9 0.2 164 4 2 1 30.46 60.921 0.329 5.58 4 12.0 1.5 165 4 2 -5 30.66 61.321 0.331 5.5 4 47.7 23.8 166 2 3 2 30.753 61.507 0.332 5.46 4 20.4 4.3 167 1 3 3 30.798 61.596 0.332 5.45 4 21.1 4.6 168 2 3 -4 30.853 61.706 0.333 5.42 4 19.7 4.0 169 1 3 -4 30.856 61.712 0.333 5.42 4 12.5 1.6 170 5 2 -2 30.927 61.854 0.334 5.4 4 24.2 6.0 171 5 2 -3 30.968 61.936 0.334 5.38 4 6.3 0.4 172 6 0 -3 31.321 62.642 0.337 5.25 2 44.0 9.6 173 5 0 1 31.416 62.832 0.338 5.21 2 7.0 0.2 174 0 1 6 31.453 62.907 0.339 5.2 4 5.3 0.3 175 5 0 -6 31.702 63.404 0.341 5.11 2 46.9 10.7 176 6 0 -2 31.725 63.45 0.341 5.1 2 17.4 1.5 177 5 2 -1 31.794 63.588 0.342 5.08 4 29.7 8.5 178 6 0 -4 31.823 63.645 0.342 5.07 2 95.0 43.4 179 3 0 4 31.851 63.703 0.343 5.06 2 59.7 17.1 180 3 3 1 31.913 63.826 0.343 5.04 4 8.2 0.6 181 5 2 -4 31.916 63.832 0.343 5.03 4 112.0 120.0 182 2 2 4 31.938 63.876 0.343 5.03 4 62.6 37.4 183 3 3 -4 32.035 64.069 0.344 4.99 4 6.1 0.3 184 0 3 4 32.044 64.088 0.344 4.99 4 20.0 3.8 185 2 0 5 32.077 64.154 0.345 4.98 2 5.9 0.2 186 2 2 -6 32.1 64.201 0.345 4.97 4 69.7 45.9 187 3 0 -7 32.119 64.239 0.345 4.97 2 6.4 0.2 188 3 2 3 32.17 64.339 0.346 4.95 4 36.6 12.6 189 2 0 -7 32.271 64.542 0.347 4.92 2 21.1 2.1 190 3 2 -6 32.388 64.776 0.348 4.88 4 95.9 85.1 191 4 3 -2 32.515 65.03 0.349 4.84 4 12.9 1.5 192 6 1 -3 32.519 65.038 0.349 4.83 4 9.8 0.9 193 5 1 1 32.612 65.223 0.35 4.81 4 23.1 4.9 194 4 0 3 32.81 65.621 0.352 4.74 2 56.3 14.3 195 1 2 5 32.89 65.779 0.352 4.72 4 16.9 2.5 196 5 1 -6 32.892 65.784 0.353 4.72 4 14.8 2.0 197 6 1 -2 32.914 65.829 0.353 4.71 4 22.9 4.7 198 4 3 -1 32.927 65.854 0.353 4.71 4 6.7 0.4 199 1 2 -6 32.977 65.955 0.353 4.69 4 20.4 3.7 200 4 3 -3 32.991 65.981 0.353 4.69 4 2.2 0.0 201 6 1 -4 33.01 66.02 0.354 4.68 4 22.0 4.3 202 6 0 -1 33.015 66.03 0.354 4.68 2 13.1 0.8 203 3 1 4 33.038 66.077 0.354 4.67 4 0.9 0.0 204 4 0 -7 33.13 66.26 0.355 4.65 2 14.6 0.9 205 6 0 -5 33.206 66.413 0.355 4.62 2 35.6 5.6 206 0 4 0 33.22 66.44 0.356 4.62 2 232.8 237.7 207 2 1 5 33.26 66.519 0.356 4.61 4 72.4 45.9 208 3 1 -7 33.301 66.603 0.356 4.59 4 35.9 11.3 209 2 1 -7 33.45 66.9 0.358 4.55 4 42.9 15.9 210 1 0 6 33.474 66.948 0.358 4.54 2 16.8 1.2 211 5 2 0 33.53 67.06 0.359 4.53 4 53.6 24.7 212 4 2 2 33.571 67.142 0.359 4.52 4 135.7 157.9 213 1 0 -7 33.577 67.154 0.359 4.52 2 35.0 5.3 214 0 4 1 33.659 67.317 0.36 4.49 4 5.8 0.3 215 5 2 -5 33.728 67.456 0.36 4.47 4 10.2 0.9 216 1 4 0 33.793 67.585 0.361 4.46 4 8.2 0.6 217 1 4 -1 33.8 67.601 0.361 4.45 4 6.0 0.3 218 4 2 -6 33.824 67.648 0.361 4.45 4 37.2 11.7 219 2 3 3 33.865 67.73 0.362 4.44 4 33.2 9.3 220 4 1 3 33.98 67.96 0.363 4.4 4 1.0 0.0 221 2 3 -5 33.991 67.982 0.363 4.4 4 6.0 0.3 222 6 1 -1 34.181 68.362 0.365 4.35 4 39.6 13.0 223 4 3 0 34.209 68.418 0.365 4.34 4 5.3 0.2 224 4 1 -7 34.294 68.588 0.366 4.32 4 29.5 7.1 225 4 3 -4 34.334 68.669 0.366 4.31 4 7.1 0.4 226 1 3 4 34.35 68.699 0.366 4.31 4 49.7 20.2 227 6 1 -5 34.369 68.738 0.366 4.3 4 3.2 0.1 228 1 3 -5 34.42 68.84 0.367 4.29 4 31.4 8.0 229 3 3 2 34.531 69.062 0.368 4.26 4 25.2 5.1 230 1 1 6 34.632 69.265 0.369 4.23 4 6.3 0.3 231 1 4 1 34.652 69.305 0.369 4.23 4 3.0 0.1 232 1 4 -2 34.676 69.352 0.369 4.22 4 32.7 8.6 233 3 3 -5 34.695 69.389 0.369 4.22 4 15.9 2.0 234 1 1 -7 34.734 69.467 0.37 4.21 4 0.6 0.0 235 5 0 2 34.903 69.806 0.371 4.17 2 74.5 22.0 236 0 4 2 34.959 69.917 0.372 4.15 4 2.8 0.1 237 0 2 6 34.974 69.947 0.372 4.15 4 69.2 37.8 238 2 4 -1 35.072 70.144 0.373 4.13 4 1.2 0.0 239 6 0 0 35.142 70.284 0.374 4.11 2 28.5 3.2 240 5 0 -7 35.252 70.504 0.375 4.09 2 14.7 0.8 241 6 0 -6 35.42 70.841 0.376 4.05 2 13.7 0.7 242 2 4 0 35.484 70.968 0.377 4.03 4 33.3 8.5 243 2 4 -2 35.515 71.03 0.377 4.03 4 33.9 8.8 244 0 3 5 35.964 71.927 0.381 3.93 4 33.0 8.1 245 0 0 7 35.975 71.95 0.381 3.92 2 26.3 2.6 246 6 2 -3 35.986 71.973 0.381 3.92 4 46.5 16.1 247 5 1 2 36.04 72.081 0.382 3.91 4 21.7 3.5 248 5 2 1 36.075 72.15 0.382 3.9 4 21.5 3.4 249 6 1 0 36.276 72.552 0.384 3.86 4 12.0 1.1 250 4 3 1 36.318 72.637 0.384 3.85 4 11.6 1.0 251 5 2 -6 36.343 72.685 0.385 3.85 4 40.8 12.1 252 1 4 2 36.352 72.704 0.385 3.85 4 33.2 8.1 253 6 2 -2 36.364 72.728 0.385 3.84 4 74.3 40.3 254 5 1 -7 36.385 72.769 0.385 3.84 4 1.8 0.0 255 1 4 -3 36.39 72.78 0.385 3.84 4 7.7 0.4 256 6 2 -4 36.455 72.911 0.386 3.83 4 69.4 35.0 257 3 2 4 36.482 72.965 0.386 3.82 4 10.0 0.7 258 4 3 -5 36.502 73.003 0.386 3.82 4 56.2 22.9 259 6 1 -6 36.551 73.101 0.387 3.81 4 26.0 4.9 260 2 2 5 36.694 73.388 0.388 3.78 4 29.6 6.3 261 3 2 -7 36.734 73.468 0.388 3.77 4 11.9 1.0 262 2 4 1 36.74 73.48 0.388 3.77 4 40.1 11.5 263 5 3 -2 36.746 73.493 0.388 3.77 4 47.3 16.0 264 5 3 -3 36.784 73.569 0.389 3.76 4 25.2 4.5 265 2 4 -3 36.801 73.602 0.389 3.76 4 4.8 0.2 266 2 2 -7 36.877 73.753 0.39 3.74 4 21.0 3.1 267 3 0 5 37.026 74.051 0.391 3.72 2 69.6 17.1 268 0 4 3 37.08 74.16 0.391 3.7 4 17.6 2.2 269 0 1 7 37.098 74.197 0.392 3.7 4 55.3 21.5 270 3 0 -8 37.321 74.642 0.394 3.66 2 92.8 29.9 271 4 2 3 37.385 74.77 0.394 3.65 4 82.6 47.3 272 7 0 -3 37.413 74.826 0.394 3.64 2 33.0 3.8 273 3 4 -1 37.422 74.843 0.394 3.64 4 14.8 1.5 274 3 4 -2 37.444 74.888 0.395 3.64 4 56.6 22.2 275 7 0 -4 37.466 74.932 0.395 3.64 2 32.1 3.6 276 4 0 4 37.499 74.998 0.395 3.63 2 60.3 12.5 277 5 3 -1 37.547 75.094 0.396 3.62 4 94.6 61.5 278 6 2 -1 37.578 75.156 0.396 3.62 4 48.4 16.1 279 5 3 -4 37.66 75.32 0.397 3.6 4 13.8 1.3 280 2 0 6 37.662 75.323 0.397 3.6 2 62.3 13.3 281 2 3 4 37.681 75.361 0.397 3.6 4 35.3 8.5 282 4 2 -7 37.687 75.373 0.397 3.6 4 2.3 0.0 283 6 2 -5 37.759 75.518 0.397 3.58 4 89.9 55.0 284 2 3 -6 37.831 75.663 0.398 3.57 4 29.7 6.0 285 4 0 -8 37.861 75.721 0.398 3.57 2 28.4 2.7 286 2 0 -8 37.872 75.745 0.398 3.57 2 60.9 12.6 287 3 3 3 37.896 75.792 0.399 3.56 4 24.3 4.0 288 1 2 6 38.013 76.025 0.4 3.54 4 39.8 10.7 289 6 0 1 38.048 76.096 0.4 3.54 2 22.7 1.7 290 3 3 -6 38.099 76.198 0.401 3.53 4 14.0 1.3 291 1 2 -7 38.11 76.22 0.401 3.53 4 15.7 1.6 292 3 1 5 38.138 76.275 0.401 3.52 4 9.4 0.6 293 7 0 -2 38.194 76.387 0.401 3.51 2 8.1 0.2 294 3 4 0 38.232 76.464 0.402 3.51 4 64.3 27.5 295 3 4 -3 38.299 76.599 0.402 3.5 4 8.0 0.4 296 7 0 -5 38.351 76.702 0.403 3.49 2 13.5 0.6 297 6 0 -7 38.408 76.816 0.403 3.48 2 17.4 1.0 298 3 1 -8 38.43 76.86 0.403 3.47 4 2.7 0.0 299 7 1 -3 38.521 77.042 0.404 3.46 4 3.0 0.1 300 1 3 5 38.567 77.134 0.405 3.45 4 66.5 29.0 301 7 1 -4 38.574 77.147 0.405 3.45 4 22.9 3.4 302 4 1 4 38.606 77.212 0.405 3.45 4 14.8 1.4 303 1 3 -6 38.649 77.299 0.405 3.44 4 10.7 0.7 304 2 1 6 38.767 77.535 0.406 3.42 4 24.0 3.7 305 2 4 2 38.809 77.618 0.407 3.42 4 77.9 39.4 306 1 4 3 38.849 77.698 0.407 3.41 4 0.8 0.0 307 2 4 -4 38.898 77.797 0.408 3.4 4 2.9 0.1 308 1 4 -4 38.901 77.803 0.408 3.4 4 36.7 8.7 309 4 1 -8 38.965 77.929 0.408 3.39 4 8.1 0.4 310 2 1 -8 38.976 77.953 0.408 3.39 4 3.7 0.1 311 5 0 3 39.067 78.134 0.409 3.38 2 3.0 0.0 312 6 1 1 39.15 78.3 0.41 3.37 4 1.2 0.0 313 5 3 0 39.168 78.336 0.41 3.37 4 52.3 17.5 314 4 3 2 39.206 78.413 0.41 3.36 4 64.5 26.5 315 7 1 -2 39.295 78.589 0.411 3.35 4 10.6 0.7 316 5 3 -5 39.354 78.708 0.412 3.34 4 3.8 0.1 317 5 2 2 39.374 78.748 0.412 3.34 4 22.8 3.3 318 1 0 7 39.388 78.776 0.412 3.33 2 14.5 0.7 319 4 3 -6 39.445 78.889 0.412 3.33 4 4.2 0.1 320 7 1 -5 39.451 78.902 0.412 3.33 4 4.1 0.1 321 5 0 -8 39.476 78.953 0.413 3.32 2 2.3 0.0 322 1 0 -8 39.5 78.999 0.413 3.32 2 16.2 0.8 323 6 1 -7 39.507 79.015 0.413 3.32 4 77.9 38.2 324 6 2 0 39.603 79.205 0.414 3.31 4 19.5 2.4 325 5 2 -7 39.708 79.416 0.415 3.29 4 34.5 7.4 326 7 0 -1 39.792 79.583 0.415 3.28 2 19.1 1.1 327 3 4 1 39.859 79.719 0.416 3.27 4 14.3 1.3 328 6 2 -6 39.87 79.739 0.416 3.27 4 42.2 11.1 329 3 4 -4 39.97 79.941 0.417 3.26 4 33.6 7.0 330 0 4 4 39.979 79.958 0.417 3.26 4 5.9 0.2 331 7 0 -6 40.051 80.102 0.418 3.25 2 3.0 0.0 332 5 1 3 40.161 80.322 0.419 3.23 4 8.6 0.5 333 0 2 7 40.403 80.806 0.421 3.21 4 69.6 29.5 334 4 4 -2 40.411 80.821 0.421 3.2 4 4.8 0.1 335 1 1 7 40.48 80.96 0.421 3.2 4 17.4 1.8 336 0 3 6 40.533 81.066 0.422 3.19 4 0.3 0.0 337 5 1 -8 40.568 81.135 0.422 3.19 4 4.3 0.1 338 1 1 -8 40.591 81.182 0.422 3.18 4 2.1 0.0 339 4 4 -1 40.789 81.579 0.424 3.16 4 61.3 22.5 340 4 4 -3 40.848 81.697 0.425 3.15 4 21.6 2.8 341 7 1 -1 40.881 81.762 0.425 3.15 4 12.9 1.0 342 7 1 -6 41.139 82.278 0.427 3.12 4 37.2 8.2 343 3 2 5 41.418 82.836 0.429 3.09 4 35.2 7.3 344 6 3 -3 41.5 82.999 0.43 3.09 4 7.9 0.4 345 5 3 1 41.584 83.169 0.431 3.08 4 26.8 4.2 346 2 4 3 41.659 83.319 0.431 3.07 4 42.9 10.7 347 6 0 2 41.696 83.393 0.432 3.07 2 19.5 1.1 348 3 2 -8 41.705 83.409 0.432 3.07 4 40.7 9.6 349 2 4 -5 41.777 83.554 0.432 3.06 4 13.7 1.1 350 7 2 -3 41.794 83.588 0.433 3.06 4 52.4 15.9 351 5 3 -6 41.841 83.683 0.433 3.05 4 8.3 0.4 352 7 2 -4 41.845 83.691 0.433 3.05 4 3.8 0.1 353 6 3 -2 41.862 83.724 0.433 3.05 4 22.0 2.8 354 4 2 4 41.877 83.754 0.433 3.05 4 21.5 2.7 355 6 3 -4 41.95 83.9 0.434 3.04 4 23.1 3.1 356 3 3 4 41.976 83.952 0.434 3.04 4 8.7 0.4 357 4 4 0 41.98 83.961 0.434 3.04 4 50.1 14.5 358 2 2 6 42.035 84.071 0.435 3.04 4 26.0 3.9 359 4 4 -4 42.098 84.195 0.435 3.03 4 13.6 1.1 360 1 4 4 42.112 84.224 0.435 3.03 4 18.9 2.0 361 6 0 -8 42.136 84.273 0.435 3.03 2 72.9 15.3 362 0 0 8 42.171 84.342 0.436 3.02 2 2.7 0.0 363 1 4 -5 42.178 84.356 0.436 3.02 4 23.3 3.1 364 2 3 5 42.179 84.359 0.436 3.02 4 63.8 23.3 365 7 0 0 42.186 84.372 0.436 3.02 2 5.2 0.1 366 3 3 -7 42.218 84.436 0.436 3.02 4 34.2 6.7 367 4 2 -8 42.229 84.458 0.436 3.02 4 27.1 4.2 368 2 2 -8 42.241 84.481 0.436 3.02 4 28.9 4.8 369 3 4 2 42.282 84.564 0.437 3.01 4 12.6 0.9 370 2 3 -7 42.355 84.71 0.437 3.01 4 36.5 7.6 371 6 2 1 42.412 84.823 0.438 3.0 4 11.6 0.8 372 3 4 -5 42.436 84.871 0.438 3.0 4 28.2 4.5 373 7 0 -7 42.545 85.089 0.439 2.99 2 15.5 0.7 374 7 2 -2 42.554 85.107 0.439 2.99 4 23.2 3.1 375 7 2 -5 42.707 85.415 0.44 2.98 4 5.8 0.2 376 3 0 6 42.753 85.506 0.441 2.97 2 8.8 0.2 377 6 2 -7 42.763 85.526 0.441 2.97 4 8.3 0.4 378 6 1 2 42.776 85.552 0.441 2.97 4 14.8 1.2 379 4 0 5 42.798 85.597 0.441 2.97 2 7.7 0.2 380 4 3 3 42.846 85.692 0.441 2.97 4 4.1 0.1 381 6 3 -1 43.033 86.066 0.443 2.95 4 33.5 6.3 382 3 0 -9 43.082 86.164 0.443 2.95 2 17.4 0.9 383 4 3 -7 43.139 86.277 0.444 2.94 4 29.0 4.7 384 4 0 -9 43.208 86.415 0.444 2.94 2 5.7 0.1 385 6 3 -5 43.209 86.417 0.444 2.94 4 0.2 0.0 386 6 1 -8 43.215 86.43 0.444 2.94 4 32.0 5.7 387 0 1 8 43.249 86.499 0.445 2.94 4 52.5 15.3 388 7 1 0 43.264 86.528 0.445 2.93 4 71.5 28.5 389 5 2 3 43.408 86.815 0.446 2.92 4 6.3 0.2 390 1 3 6 43.455 86.91 0.446 2.92 4 11.0 0.7 391 1 3 -7 43.55 87.1 0.447 2.91 4 6.2 0.2 392 7 1 -7 43.622 87.244 0.448 2.91 4 65.8 24.0 393 0 5 1 43.625 87.25 0.448 2.91 4 7.0 0.3 394 0 4 5 43.636 87.272 0.448 2.91 4 9.0 0.4 395 1 2 7 43.723 87.446 0.449 2.9 4 6.7 0.2 396 1 5 0 43.749 87.498 0.449 2.9 4 4.1 0.1 397 1 5 -1 43.756 87.513 0.449 2.9 4 8.9 0.4 398 2 0 7 43.779 87.558 0.449 2.9 2 46.8 6.0 399 5 2 -8 43.809 87.619 0.449 2.9 4 61.1 20.5 400 3 1 6 43.83 87.66 0.45 2.9 4 38.1 8.0 401 1 2 -8 43.832 87.665 0.45 2.9 4 55.5 16.9 402 4 1 5 43.875 87.75 0.45 2.89 4 37.2 7.6 403 8 0 -4 43.877 87.754 0.45 2.89 2 14.1 0.5 404 5 0 4 43.915 87.829 0.45 2.89 2 3.6 0.0 405 4 4 1 43.974 87.948 0.451 2.89 4 4.7 0.1 406 2 0 -9 44.013 88.025 0.451 2.88 2 45.4 5.6 407 7 2 -1 44.119 88.239 0.452 2.88 4 27.7 4.2 408 4 4 -5 44.149 88.298 0.452 2.88 4 3.3 0.1 409 3 1 -9 44.158 88.316 0.452 2.87 4 17.8 1.7 410 8 0 -3 44.222 88.445 0.453 2.87 2 87.4 20.8 411 4 1 -9 44.284 88.567 0.453 2.87 4 80.7 35.5 412 8 0 -5 44.339 88.678 0.454 2.86 2 37.4 3.8 413 7 2 -6 44.375 88.75 0.454 2.86 4 33.0 5.9 414 5 4 -2 44.384 88.767 0.454 2.86 4 51.6 14.5 415 5 0 -9 44.389 88.778 0.454 2.86 2 12.3 0.4 416 5 4 -3 44.42 88.84 0.454 2.86 4 15.2 1.3 417 1 5 1 44.549 89.098 0.455 2.85 4 8.4 0.4 418 1 5 -2 44.571 89.142 0.456 2.85 4 2.4 0.0 419 5 3 2 44.784 89.568 0.457 2.84 4 27.8 4.2 420 0 5 2 44.836 89.672 0.458 2.84 4 1.3 0.0 421 2 1 7 44.854 89.708 0.458 2.84 4 29.3 4.6 422 2 5 -1 44.943 89.885 0.459 2.83 4 34.0 6.2 423 8 1 -4 44.952 89.904 0.459 2.83 4 20.4 2.2 424 5 1 4 44.99 89.979 0.459 2.83 4 10.8 0.6 X-ray diffraction powder data (I)...X-Ray wave length = 1.54056 (angs.): No H K L Theta 2*Theta d I int I int.n. I p.h.n. H(Si) ( degree ) (angstrem) *100 *100 1 0 0 1 4.814 9.628 9.17891 17.1 1.8 1.9 5.6 2 1 0 0 5.505 11.01 8.02929 51.5 5.5 5.6 5.6 3 1 0 -1 5.543 11.086 7.97433 24.6 2.6 2.7 5.6 4 1 0 -2 8.826 17.652 5.02022 256.8 27.5 27.7 5.6 5 0 1 1 9.243 18.487 4.79544 11.2 1.2 1.2 5.6 6 1 1 -1 9.648 19.297 4.59597 41.0 4.4 4.4 5.6 7 2 0 0 11.062 22.124 4.01464 166.2 17.8 17.9 5.6 8 2 0 -2 11.139 22.278 3.98717 164.8 17.6 17.7 5.6 9 1 1 1 11.814 23.629 3.76219 54.8 5.9 5.9 5.6 10 1 1 -2 11.869 23.738 3.74517 15.7 1.7 1.7 5.6 11 2 1 -1 12.76 25.52 3.48745 304.5 32.6 32.7 5.6 12 1 0 2 13.078 26.156 3.4041 107.5 11.5 11.5 5.6 13 2 0 1 13.897 27.794 3.20712 109.1 11.7 11.7 5.6 14 0 0 3 14.581 29.163 3.05964 35.5 3.8 3.8 5.6 15 3 0 -1 15.243 30.487 2.92971 13.0 1.4 1.4 5.6 16 3 0 -2 15.286 30.573 2.92165 159.5 17.0 17.1 5.6 17 1 1 -3 15.409 30.817 2.89903 935.4 100.0 100.0 5.6 18 0 2 0 15.898 31.796 2.812 368.3 39.4 39.3 5.6 19 2 1 1 16.051 32.101 2.78597 100.2 10.7 10.7 5.6 20 2 1 -3 16.16 32.32 2.76759 33.9 3.6 3.6 5.6 21 0 1 3 16.655 33.309 2.68765 293.5 31.4 31.3 5.6 22 3 0 0 16.726 33.453 2.67643 172.6 18.4 18.4 5.7 23 1 2 0 16.872 33.745 2.65395 204.5 21.9 21.8 5.7 24 3 1 -1 17.245 34.49 2.5983 406.3 43.4 43.3 5.7 25 3 1 -2 17.283 34.567 2.59267 14.7 1.6 1.6 5.7 26 2 0 2 17.72 35.441 2.53072 163.9 17.5 17.5 5.7 27 1 0 -4 17.876 35.751 2.50944 40.3 4.3 4.3 5.7 28 1 2 -2 18.299 36.597 2.45335 103.6 11.1 11.0 5.7 29 3 1 -3 18.694 37.389 2.40321 280.9 30.0 29.9 5.7 30 0 2 2 18.739 37.478 2.39772 222.8 23.8 23.7 5.7 31 2 2 -1 18.913 37.826 2.37645 42.6 4.6 4.5 5.7 32 2 1 2 19.498 38.995 2.30783 15.0 1.6 1.6 5.7 33 2 2 -2 19.585 39.169 2.29798 178.8 19.1 19.0 5.7 34 1 1 -4 19.641 39.282 2.29166 54.9 5.9 5.8 5.7 35 4 0 -1 20.846 41.692 2.16457 212.6 22.7 22.5 5.7 36 4 0 -3 20.934 41.867 2.15592 20.7 2.2 2.2 5.7 37 0 1 4 21.256 42.513 2.12467 21.0 2.2 2.2 5.7 38 2 2 1 21.365 42.73 2.11436 183.8 19.6 19.4 5.7 39 2 2 -3 21.451 42.902 2.10629 169.9 18.2 18.0 5.7 40 0 2 3 21.842 43.683 2.0704 139.1 14.9 14.7 5.7 41 4 1 -2 21.879 43.757 2.06709 11.1 1.2 1.2 5.7 42 2 0 3 22.111 44.223 2.04639 69.0 7.4 7.3 5.7 43 3 2 -1 22.314 44.629 2.02872 27.2 2.9 2.9 5.7 44 3 2 -2 22.345 44.691 2.02604 15.6 1.7 1.7 5.7 45 4 0 0 22.565 45.13 2.00732 65.2 7.0 6.9 5.7 46 1 0 4 22.75 45.499 1.99191 12.1 1.3 1.3 5.7 47 1 0 -5 22.841 45.683 1.98432 15.7 1.7 1.6 5.7 48 3 0 -5 23.198 46.396 1.95549 19.7 2.1 2.1 5.7 49 2 1 3 23.613 47.226 1.92304 35.1 3.8 3.7 5.7 50 2 2 2 24.172 48.345 1.8811 93.2 10.0 9.8 5.7 51 1 1 4 24.22 48.44 1.87762 55.5 5.9 5.8 5.7 52 2 2 -4 24.289 48.579 1.87258 219.9 23.5 23.1 5.7 53 3 1 2 24.445 48.89 1.86138 34.7 3.7 3.6 5.7 54 1 3 0 24.957 49.914 1.82557 12.1 1.3 1.3 5.7 55 0 2 4 25.674 51.349 1.77788 22.2 2.4 2.3 5.8 56 5 0 -2 25.776 51.552 1.77134 45.0 4.8 4.7 5.8 57 1 3 1 25.987 51.974 1.75796 13.8 1.5 1.4 5.8 58 0 1 5 26.192 52.384 1.74516 46.1 4.9 4.8 5.8 59 2 3 -1 26.483 52.966 1.72735 39.1 4.2 4.1 5.8 60 4 1 -5 26.834 53.668 1.7064 63.8 6.8 6.7 5.8 61 2 0 4 26.908 53.816 1.70205 15.2 1.6 1.6 5.8 62 2 0 -6 27.088 54.177 1.69157 29.2 3.1 3.0 5.8 63 5 1 -2 27.124 54.248 1.68952 28.9 3.1 3.0 5.8 64 5 1 -3 27.169 54.338 1.68694 20.5 2.2 2.1 5.8 65 3 0 -6 27.407 54.814 1.67341 40.0 4.3 4.2 5.8 66 1 0 5 27.961 55.922 1.64285 15.6 1.7 1.6 5.8 67 1 3 -3 28.018 56.037 1.63975 115.8 12.4 12.1 5.8 68 5 1 -1 28.062 56.125 1.63738 237.8 25.4 24.7 5.8 69 4 2 0 28.13 56.26 1.63377 33.2 3.6 3.5 5.8 70 2 1 4 28.218 56.436 1.62908 28.6 3.1 3.0 5.8 71 4 2 -4 28.27 56.54 1.62633 213.9 22.9 22.2 5.8 72 2 3 1 28.42 56.841 1.61845 30.8 3.3 3.2 5.8 73 3 2 2 28.489 56.979 1.61486 57.4 6.1 6.0 5.8 74 0 3 3 28.808 57.617 1.59848 50.3 5.4 5.2 5.8 75 4 0 -6 28.985 57.97 1.58959 120.7 12.9 12.5 5.8 76 3 3 -1 29.197 58.393 1.57906 100.3 10.7 10.4 5.8 77 1 1 5 29.24 58.479 1.57695 63.3 6.8 6.6 5.8 78 5 1 0 29.923 59.847 1.54414 36.4 3.9 3.8 5.8 79 4 1 2 29.967 59.934 1.5421 66.0 7.1 6.8 5.8 80 3 3 -3 30.185 60.37 1.53199 49.7 5.3 5.1 5.8 81 4 2 -5 30.66 61.321 1.51051 23.8 2.5 2.5 5.8 82 6 0 -3 31.321 62.642 1.48178 9.6 1.0 1.0 5.8 83 5 0 -6 31.702 63.404 1.46579 12.1 1.3 1.2 5.9 84 6 0 -4 31.823 63.645 1.46083 69.0 7.4 7.1 5.9 85 5 2 -4 31.916 63.832 1.45701 157.4 16.8 16.2 5.9 86 2 2 -6 32.1 64.201 1.44952 46.1 4.9 4.7 5.9 87 3 2 3 32.17 64.339 1.44673 12.6 1.3 1.3 5.9 88 3 2 -6 32.388 64.776 1.43804 85.1 9.1 8.7 5.9 89 4 0 3 32.81 65.621 1.42154 14.3 1.5 1.5 5.9 90 0 4 0 33.22 66.44 1.406 243.3 26.0 24.9 5.9 91 2 1 5 33.26 66.519 1.40451 45.9 4.9 4.7 5.9 92 3 1 -7 33.301 66.603 1.40295 11.3 1.2 1.2 5.9 93 2 1 -7 33.45 66.9 1.39743 17.1 1.8 1.7 5.9 94 5 2 0 33.53 67.06 1.39449 24.7 2.6 2.5 5.9 95 4 2 2 33.571 67.142 1.39298 163.2 17.4 16.7 5.9 96 4 2 -6 33.824 67.648 1.3838 11.7 1.3 1.2 5.9 97 6 1 -1 34.181 68.362 1.37107 13.2 1.4 1.3 5.9 98 1 3 4 34.35 68.699 1.36516 20.3 2.2 2.1 5.9 99 1 4 -2 34.676 69.352 1.3539 10.6 1.1 1.1 5.9 100 5 0 2 34.903 69.806 1.3462 22.0 2.3 2.2 5.9 101 0 2 6 34.974 69.947 1.34382 37.8 4.0 3.8 5.9 102 6 2 -3 35.986 71.973 1.31091 26.8 2.9 2.7 5.9 103 6 2 -2 36.364 72.728 1.29915 60.5 6.5 6.1 6.0 104 6 2 -4 36.455 72.911 1.29634 35.7 3.8 3.6 6.0 105 4 3 -5 36.502 73.003 1.29493 22.9 2.4 2.3 6.0 106 5 3 -2 36.746 73.493 1.2875 28.5 3.0 2.9 6.0 107 3 0 5 37.026 74.051 1.27917 17.1 1.8 1.7 6.0 108 0 1 7 37.098 74.197 1.27702 23.7 2.5 2.4 6.0 109 3 0 -8 37.321 74.642 1.2705 29.9 3.2 3.0 6.0 110 4 2 3 37.385 74.77 1.26865 51.0 5.5 5.1 6.0 111 3 4 -2 37.444 74.888 1.26693 27.2 2.9 2.7 6.0 112 4 0 4 37.499 74.998 1.26536 12.5 1.3 1.3 6.0 113 5 3 -1 37.547 75.094 1.26398 61.5 6.6 6.2 6.0 114 6 2 -1 37.578 75.156 1.26308 16.1 1.7 1.6 6.0 115 2 3 4 37.681 75.361 1.26015 23.1 2.5 2.3 6.0 116 6 2 -5 37.759 75.518 1.25793 55.0 5.9 5.5 6.0 117 2 0 -8 37.872 75.745 1.25472 16.5 1.8 1.7 6.0 118 1 2 6 38.013 76.025 1.25079 10.7 1.1 1.1 6.0 119 3 4 0 38.232 76.464 1.2447 27.5 2.9 2.8 6.0 120 1 3 5 38.567 77.134 1.23555 32.4 3.5 3.3 6.0 121 2 4 2 38.809 77.618 1.22906 39.4 4.2 4.0 6.0 122 5 3 0 39.168 78.336 1.21958 17.5 1.9 1.7 6.0 123 4 3 2 39.206 78.413 1.21857 26.5 2.8 2.7 6.0 124 6 1 -7 39.507 79.015 1.2108 38.2 4.1 3.8 6.0 125 6 2 -6 39.87 79.739 1.2016 12.3 1.3 1.2 6.0 126 0 2 7 40.403 80.806 1.18841 29.7 3.2 3.0 6.1 127 4 4 -1 40.789 81.579 1.17909 22.5 2.4 2.2 6.1 128 2 4 3 41.659 83.319 1.15884 10.7 1.1 1.1 6.1 129 3 2 -8 41.705 83.409 1.15781 10.7 1.1 1.1 6.1 130 7 2 -3 41.794 83.588 1.15579 17.0 1.8 1.7 6.1 131 4 4 0 41.98 83.961 1.1516 14.5 1.6 1.4 6.1 132 6 0 -8 42.136 84.273 1.14813 18.4 2.0 1.8 6.1 133 2 3 5 42.179 84.359 1.14718 26.5 2.8 2.6 6.1 134 3 3 -7 42.218 84.436 1.14633 15.7 1.7 1.5 6.1 135 7 1 0 43.264 86.528 1.1239 43.8 4.7 4.3 6.1 136 7 1 -7 43.622 87.244 1.11651 24.7 2.6 2.4 6.2 137 5 2 -8 43.809 87.619 1.1127 51.5 5.5 5.0 6.2 138 8 0 -3 44.222 88.445 1.10443 20.8 2.2 2.0 6.2 139 4 1 -9 44.284 88.567 1.10322 35.5 3.8 3.5 6.2 140 5 4 -2 44.384 88.767 1.10125 20.8 2.2 2.0 6.2 Reference: Chichagov A.V. et al. Information-Calculating System on Crystal Structure Data of Minerals (MINCRYST) - Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian) |