Institute of Experimental Mineralogy Russian Academy of Sciences ------------------------------------------------- 142432, Chernogolovka, Moscow district A.V. Chichagov +7(496)52-22320 *** *** W W W - X R A Y P O L *** *********************** ZOISITE 8, t-zoisite, f-epidote, at 7.766 GPa Ca(2)Al(3)[Si(3)O(12)]OH Orthorhombic P nma Z = 4 Pnma 24 .1 .13 Ref.Str.: Alvaro M., Angel R.J., Camara F. (2012) * Amer. Mineral., 97, 1165-1176 R: from Merelani Hills, Tanzania. N.A.D. Initial data from BDM-file Lattice parameters (cub. angs.,degr.): a = 16.0271 alpha = 90.0 b = 5.4473 beta = 90.0 c = 9.8119 gamma = 90.0 Unit cell volume (cub. angs.) = 856.62 Molar volume ( cub.cm/mol.) = 128.99 Co-ordinates, thermal parameters, occupation for atomic positions: NoP x/a y/b z/c B(j) atom / occupation 1 0.4104 0.75 0.2788 0.0 Si = 1.00 2 0.0799 0.25 0.1048 0.0 Si = 1.00 3 0.16 0.25 0.4353 0.0 Si = 1.00 4 0.2485 0.9985 0.1865 0.0 Al = 1.00 5 0.1053 0.75 0.2999 0.0 Al = 1.00 6 0.3651 0.25 0.4353 0.0 Ca = 1.00 7 0.4554 0.25 0.1094 0.0 Ca = 1.00 8 0.1278 0.9933 0.1466 0.0 O = 1.00 9 0.1015 0.0116 0.4328 0.0 O = 1.00 10 0.3586 0.9958 0.239 0.0 O = 1.00 11 0.2191 0.75 0.3038 0.0 O = 1.00 12 0.2275 0.25 0.3113 0.0 O = 1.00 13 0.269 0.75 0.0576 0.0 O = 1.00 14 0.9899 0.25 0.1712 0.0 O = 1.00 15 0.9947 0.75 0.305 0.0 O = 1.00 16 0.4204 0.75 0.442 0.0 O = 1.00 17 0.2605 0.25 0.0646 0.0 OH = 1.00 Co-ordinates for all atomic positions : No NoP x/a y/b z/c 1 1 0.4104 0.75 0.2788 2 2 0.0799 0.25 0.1048 3 3 0.16 0.25 0.4353 4 4 0.2485 0.9985 0.1865 5 5 0.1053 0.75 0.2999 6 6 0.3651 0.25 0.4353 7 7 0.4554 0.25 0.1094 8 8 0.1278 0.9933 0.1466 9 9 0.1015 0.0116 0.4328 10 10 0.3586 0.9958 0.239 11 11 0.2191 0.75 0.3038 12 12 0.2275 0.25 0.3113 13 13 0.269 0.75 0.0576 14 14 0.9899 0.25 0.1712 15 15 0.9947 0.75 0.305 16 16 0.4204 0.75 0.442 17 17 0.2605 0.25 0.0646 18 1 0.0896 0.25 0.7788 19 2 0.4201 0.75 0.6048 20 3 0.34 0.75 0.9353 21 4 0.2515 0.0015 0.6865 22 5 0.3947 0.25 0.7999 23 6 0.1349 0.75 0.9353 24 7 0.0446 0.75 0.6094 25 8 0.3722 0.0067 0.6466 26 9 0.3985 0.9884 0.9328 27 10 0.1414 0.0042 0.739 28 11 0.2809 0.25 0.8038 29 12 0.2725 0.75 0.8113 30 13 0.231 0.25 0.5576 31 14 0.5101 0.75 0.6712 32 15 0.5053 0.25 0.805 33 16 0.0796 0.25 0.942 34 17 0.2395 0.75 0.5646 35 4 0.2515 0.4985 0.6865 36 8 0.3722 0.4933 0.6466 37 9 0.3985 0.5116 0.9328 38 10 0.1414 0.4958 0.739 39 4 0.2485 0.5015 0.1865 40 8 0.1278 0.5067 0.1466 41 9 0.1015 0.4884 0.4328 42 10 0.3586 0.5042 0.239 43 1 0.9104 0.75 0.2212 44 2 0.5799 0.25 0.3952 45 3 0.66 0.25 0.0647 46 4 0.7485 0.9985 0.3135 47 5 0.6053 0.75 0.2001 48 6 0.8651 0.25 0.0647 49 7 0.9554 0.25 0.3906 50 8 0.6278 0.9933 0.3534 51 9 0.6015 0.0116 0.0672 52 10 0.8586 0.9958 0.261 53 11 0.7191 0.75 0.1962 54 12 0.7275 0.25 0.1887 55 13 0.769 0.75 0.4424 56 14 0.4899 0.25 0.3288 57 15 0.4947 0.75 0.195 58 16 0.9204 0.75 0.058 59 17 0.7605 0.25 0.4354 60 1 0.5896 0.25 0.7212 61 2 0.9201 0.75 0.8952 62 3 0.84 0.75 0.5647 63 4 0.7515 0.0015 0.8135 64 5 0.8947 0.25 0.7001 65 6 0.6349 0.75 0.5647 66 7 0.5446 0.75 0.8906 67 8 0.8722 0.0067 0.8534 68 9 0.8985 0.9884 0.5672 69 10 0.6414 0.0042 0.761 70 11 0.7809 0.25 0.6962 71 12 0.7725 0.75 0.6887 72 13 0.731 0.25 0.9424 73 14 0.0101 0.75 0.8288 74 15 0.0053 0.25 0.695 75 16 0.5796 0.25 0.558 76 17 0.7395 0.75 0.9354 77 4 0.7515 0.4985 0.8135 78 8 0.8722 0.4933 0.8534 79 9 0.8985 0.5116 0.5672 80 10 0.6414 0.4958 0.761 81 4 0.7485 0.5015 0.3135 82 8 0.6278 0.5067 0.3534 83 9 0.6015 0.4884 0.0672 84 10 0.8586 0.5042 0.261 X-ray density (g/cm cub.) = 3.52 MU (1/cm) = 189.36 Mass attenuation coefficient (cm**2/g) = 53.767 Selected interatomic distances (cation-anion,anion-anion): NoP Atom Rad.sph. C.N. Distance NoP N. (angs.) (angs.) 1 Si 2.148 4 1.6234 10 1.6093 16 1.6234 10 1.5812 15 2 Si 2.148 4 1.6471 8 1.5828 14 1.5974 16 1.6471 8 3 Si 2.148 4 1.6022 9 1.6278 12 1.6534 13 1.6022 9 4 Al 2.364 6 1.9745 8 1.8377 10 1.8384 11 1.8682 12 1.8814 13 1.8287 17 5 Al 2.364 6 2.0369 8 1.9326 9 1.8243 11 1.7733 15 2.0369 8 1.9326 9 6 Ca 2.928 9 2.3744 10 2.5184 12 2.8651 16 2.8651 16 2.4633 8 2.4613 13 2.4633 8 2.3744 10 2.257 14 7 Ca 2.928 9 2.4378 10 2.4219 9 2.4219 9 2.4378 10 2.709 9 2.2225 14 2.9189 15 2.9189 15 2.709 9 8 O 3.312 10 2.8414 9 2.5053 11 2.6684 12 2.7641 13 2.6265 14 2.9534 15 2.6694 17 2.5656 16 2.7966 8 2.6507 8 9 O 3.312 10 2.8414 8 2.6805 11 2.6806 12 2.556 15 3.072 10 2.7375 13 2.9317 17 2.5973 9 2.85 9 3.2684 15 10 O 3.312 10 2.6825 11 2.6145 12 2.6501 13 2.5964 16 2.7051 17 3.072 9 2.7694 10 2.6779 10 2.6687 14 2.5956 15 11 O 3.312 10 2.5053 8 2.6805 9 2.6825 10 2.728 12 2.728 12 2.5446 13 2.5797 17 2.5053 8 2.6805 9 2.6825 10 12 O 3.312 10 2.6684 8 2.6806 9 2.6145 10 2.728 11 2.728 11 2.4777 17 2.4173 13 2.6684 8 2.6806 9 2.6145 10 13 O 3.312 10 2.7641 8 2.6501 10 2.5446 11 2.7279 17 2.7279 17 2.7375 9 2.4173 12 2.7375 9 2.7641 8 2.6501 10 14 O 3.312 9 2.6265 8 3.0245 15 3.0245 15 2.6691 16 2.6265 8 2.6687 10 3.1453 16 3.1453 16 2.6687 10 15 O 3.312 11 2.9534 8 2.556 9 3.0245 14 3.0245 14 2.9534 8 2.556 9 2.5956 10 2.7003 16 3.2684 9 3.2684 9 2.5956 10 16 O 3.312 9 2.5964 10 2.5656 8 2.6691 14 3.139 17 2.5656 8 2.5964 10 3.1453 14 3.1453 14 2.7003 15 17 OH 3.36 11 2.6694 8 2.7051 10 2.4777 12 2.7279 13 2.7279 13 2.9317 9 2.5797 11 3.139 16 2.9317 9 2.6694 8 2.7051 10 X-ray diffraction powder data (II), X-Ray W.L. = 1.54056(angs.): No H K L Theta 2*Theta S LPG MF F I int. ( degree ) *100 1 1 0 1 5.281 10.563 0.06 233.07 4 4.5 2.5 2 2 0 0 5.516 11.032 0.062 213.49 2 40.5 95.3 3 2 0 1 7.129 14.258 0.081 126.89 4 4.2 1.2 4 0 0 2 9.033 18.067 0.102 78.2 2 91.1 177.0 5 0 1 1 9.308 18.615 0.105 73.53 4 16.5 10.8 6 3 0 1 9.449 18.898 0.107 71.28 4 13.3 6.9 7 1 0 2 9.451 18.902 0.107 71.25 4 25.4 25.0 8 1 1 1 9.714 19.428 0.11 67.33 8 32.8 78.9 9 2 1 0 9.845 19.69 0.111 65.49 4 4.6 0.8 10 2 0 2 10.608 21.217 0.119 56.11 4 28.6 25.0 11 2 1 1 10.844 21.689 0.122 53.6 8 3.2 0.6 12 4 0 0 11.084 22.168 0.125 51.22 2 81.4 92.5 13 4 0 1 11.985 23.97 0.135 43.5 4 49.9 59.2 14 3 0 2 12.308 24.616 0.138 41.14 4 62.8 88.6 15 3 1 1 12.514 25.027 0.141 39.73 8 72.8 229.4 16 1 1 2 12.515 25.03 0.141 39.72 8 17.7 13.6 17 2 1 2 13.423 26.846 0.151 34.27 8 4.4 0.7 18 4 1 0 13.807 27.614 0.155 32.28 4 0.0 0.0 19 1 0 3 13.908 27.817 0.156 31.78 4 0.1 0.0 20 4 0 2 14.372 28.744 0.161 29.64 4 67.1 72.7 21 4 1 1 14.55 29.101 0.163 28.87 8 38.5 46.7 22 5 0 1 14.643 29.287 0.164 28.47 4 90.1 126.0 23 2 0 3 14.737 29.473 0.165 28.09 4 69.7 74.4 24 3 1 2 14.821 29.643 0.166 27.75 8 19.0 10.9 25 0 1 3 15.944 31.889 0.178 23.72 4 244.1 770.3 26 3 0 3 16.03 32.06 0.179 23.44 4 19.2 4.7 27 1 1 3 16.193 32.386 0.181 22.94 8 66.0 109.0 28 0 2 0 16.428 32.856 0.184 22.23 2 230.2 321.2 29 4 1 2 16.599 33.197 0.185 21.74 8 16.8 6.7 30 5 0 2 16.682 33.363 0.186 21.51 4 158.4 294.2 31 6 0 0 16.76 33.52 0.187 21.29 2 174.6 176.8 32 5 1 1 16.838 33.676 0.188 21.08 8 158.9 580.1 33 2 1 3 16.92 33.84 0.189 20.85 8 57.2 74.3 34 1 2 1 17.302 34.605 0.193 19.86 8 28.3 17.4 35 2 2 0 17.38 34.759 0.194 19.67 4 117.1 146.9 36 6 0 1 17.389 34.778 0.194 19.65 4 26.7 7.6 37 4 0 3 17.699 35.398 0.197 18.9 4 5.3 0.3 38 2 2 1 17.99 35.979 0.2 18.24 8 19.2 7.4 39 3 1 3 18.074 36.148 0.201 18.05 8 81.6 131.0 40 0 0 4 18.302 36.603 0.204 17.57 2 50.1 12.0 41 1 0 4 18.522 37.045 0.206 17.11 4 74.8 52.2 42 5 1 2 18.662 37.325 0.208 16.83 8 25.2 11.7 43 6 1 0 18.734 37.468 0.208 16.69 4 10.2 1.0 44 0 2 2 18.873 37.746 0.21 16.42 4 85.1 64.8 45 3 2 1 19.087 38.175 0.212 16.01 8 4.8 0.4 46 1 2 2 19.088 38.176 0.212 16.01 8 116.3 236.0 47 6 0 2 19.168 38.336 0.213 15.86 4 34.5 10.3 48 2 0 4 19.172 38.344 0.213 15.86 4 63.1 34.4 49 6 1 1 19.307 38.614 0.215 15.61 8 53.1 48.0 50 4 1 3 19.59 39.181 0.218 15.11 8 89.7 132.6 51 5 0 3 19.662 39.324 0.218 14.99 4 36.3 10.7 52 2 2 2 19.722 39.443 0.219 14.89 8 111.8 202.9 53 4 2 0 19.997 39.993 0.222 14.44 4 22.1 3.9 54 7 0 1 20.21 40.42 0.224 14.1 4 52.8 21.4 55 3 0 4 20.215 40.429 0.224 14.1 4 28.4 6.2 56 1 1 4 20.348 40.697 0.226 13.89 8 53.4 43.2 57 4 2 1 20.54 41.08 0.228 13.6 8 83.5 103.4 58 3 2 2 20.741 41.483 0.23 13.31 8 49.9 36.1 59 6 1 2 20.946 41.893 0.232 13.02 8 17.1 4.2 60 2 1 4 20.95 41.9 0.232 13.02 8 19.9 5.6 61 5 1 3 21.406 42.812 0.237 12.4 8 10.6 1.5 62 4 0 4 21.604 43.208 0.239 12.15 4 30.3 6.1 63 1 2 3 21.787 43.574 0.241 11.92 8 64.0 53.3 64 7 0 2 21.793 43.587 0.241 11.91 4 4.8 0.1 65 6 0 3 21.859 43.718 0.242 11.83 4 102.8 68.1 66 7 1 1 21.918 43.837 0.242 11.76 8 3.5 0.2 67 3 1 4 21.923 43.845 0.242 11.76 8 49.0 30.7 68 4 2 2 22.104 44.208 0.244 11.54 8 9.2 1.1 69 5 2 1 22.292 44.585 0.246 11.32 8 120.1 178.0 70 2 2 3 22.357 44.714 0.247 11.25 8 120.7 178.5 71 8 0 0 22.612 45.224 0.25 10.96 2 203.8 124.1 72 8 0 1 23.105 46.211 0.255 10.44 4 107.3 65.6 73 4 1 4 23.229 46.459 0.256 10.32 8 37.0 15.4 74 3 2 3 23.283 46.566 0.257 10.26 8 34.1 13.0 75 5 0 4 23.292 46.584 0.257 10.25 4 121.3 82.3 76 1 0 5 23.294 46.589 0.257 10.25 4 3.8 0.1 77 7 1 2 23.408 46.816 0.258 10.14 8 44.8 22.2 78 6 1 3 23.47 46.94 0.259 10.08 8 10.6 1.2 79 5 2 2 23.764 47.527 0.262 9.8 8 107.3 122.9 80 6 2 0 23.822 47.645 0.262 9.74 4 8.1 0.3 81 2 0 5 23.836 47.672 0.262 9.73 4 97.4 50.3 82 8 1 0 24.184 48.368 0.266 9.41 4 88.2 39.9 83 7 0 3 24.247 48.494 0.267 9.36 4 19.7 2.0 84 6 2 1 24.297 48.593 0.267 9.32 8 13.4 1.8 85 4 2 3 24.533 49.066 0.27 9.11 8 6.3 0.4 86 8 0 2 24.539 49.078 0.27 9.11 4 84.0 35.0 87 8 1 1 24.653 49.306 0.271 9.01 8 20.2 4.0 88 0 1 5 24.659 49.318 0.271 9.01 4 3.9 0.1 89 3 0 5 24.719 49.438 0.271 8.96 4 56.5 15.6 90 5 1 4 24.831 49.662 0.273 8.87 8 57.2 31.6 91 1 1 5 24.833 49.666 0.273 8.86 8 29.2 8.3 92 0 2 4 24.999 49.998 0.274 8.73 4 39.8 7.5 93 1 2 4 25.171 50.342 0.276 8.6 8 148.8 207.4 94 6 0 4 25.235 50.471 0.277 8.55 4 13.6 0.9 95 2 1 5 25.35 50.7 0.278 8.46 8 58.5 31.6 96 0 3 1 25.558 51.115 0.28 8.3 4 19.0 1.6 97 6 2 2 25.68 51.36 0.281 8.21 8 26.1 6.1 98 2 2 4 25.683 51.366 0.281 8.21 8 43.1 16.7 99 1 3 1 25.727 51.455 0.282 8.18 8 14.9 2.0 100 7 1 3 25.743 51.486 0.282 8.17 8 22.2 4.4 101 2 3 0 25.783 51.567 0.282 8.14 4 8.0 0.3 102 4 0 5 25.917 51.835 0.284 8.04 4 17.1 1.3 103 8 1 2 26.023 52.045 0.285 7.97 8 15.7 2.2 104 5 2 3 26.075 52.149 0.285 7.93 8 24.2 5.1 105 9 0 1 26.079 52.159 0.285 7.93 4 8.9 0.3 106 3 1 5 26.195 52.39 0.287 7.85 8 0.1 0.0 107 2 3 1 26.231 52.463 0.287 7.82 8 1.4 0.0 108 7 2 1 26.517 53.034 0.29 7.63 8 1.9 0.0 109 3 2 4 26.521 53.041 0.29 7.63 8 45.8 17.5 110 6 1 4 26.691 53.382 0.292 7.52 8 41.2 13.9 111 8 0 3 26.801 53.601 0.293 7.45 4 13.5 0.7 112 3 3 1 27.057 54.114 0.295 7.29 8 62.8 31.4 113 1 3 2 27.058 54.115 0.295 7.29 8 20.8 3.4 114 4 1 5 27.347 54.694 0.298 7.12 8 61.1 29.0 115 9 0 2 27.398 54.795 0.299 7.09 4 79.1 24.2 116 7 0 4 27.401 54.801 0.299 7.09 4 35.5 4.9 117 5 0 5 27.403 54.805 0.299 7.08 4 24.9 2.4 118 9 1 1 27.503 55.006 0.3 7.03 8 86.8 57.7 119 2 3 2 27.545 55.09 0.3 7.0 8 2.4 0.0 120 4 2 4 27.663 55.326 0.301 6.93 8 28.7 6.2 121 4 3 0 27.758 55.517 0.302 6.88 4 6.8 0.2 122 7 2 2 27.821 55.642 0.303 6.84 8 87.3 56.9 123 6 2 3 27.875 55.751 0.303 6.81 8 34.0 8.6 124 0 0 6 28.101 56.202 0.306 6.69 2 92.7 15.7 125 4 3 1 28.185 56.369 0.307 6.65 8 27.8 5.6 126 8 1 3 28.199 56.399 0.307 6.64 8 11.3 0.9 127 1 0 6 28.26 56.52 0.307 6.61 4 80.5 23.3 128 3 3 2 28.344 56.688 0.308 6.56 8 23.6 4.0 129 8 2 0 28.509 57.018 0.31 6.48 4 84.9 25.5 130 10 0 0 28.725 57.451 0.312 6.37 2 79.7 11.0 131 2 0 6 28.733 57.467 0.312 6.36 4 50.5 8.8 132 9 1 2 28.777 57.554 0.312 6.34 8 98.1 66.5 133 7 1 4 28.78 57.559 0.313 6.34 8 16.7 1.9 134 5 1 5 28.782 57.563 0.313 6.34 8 108.2 80.9 135 8 2 1 28.928 57.856 0.314 6.27 8 19.3 2.5 136 0 3 3 29.026 58.052 0.315 6.22 4 182.0 112.3 137 5 2 4 29.088 58.175 0.316 6.19 8 184.8 230.3 138 1 2 5 29.09 58.179 0.316 6.19 8 12.3 1.0 139 10 0 1 29.142 58.285 0.316 6.16 4 4.3 0.1 140 6 0 5 29.148 58.295 0.316 6.16 4 67.7 15.4 141 1 3 3 29.182 58.364 0.316 6.14 8 58.3 22.8 142 4 3 2 29.439 58.878 0.319 6.02 8 19.6 2.5 143 9 0 3 29.506 59.011 0.32 5.99 4 1.8 0.0 144 3 0 6 29.512 59.023 0.32 5.99 4 208.5 142.0 145 2 2 5 29.554 59.109 0.32 5.97 8 13.9 1.3 146 5 3 1 29.593 59.186 0.321 5.95 8 121.9 96.5 147 1 1 6 29.613 59.226 0.321 5.94 8 30.3 6.0 148 2 3 3 29.646 59.292 0.321 5.93 8 44.8 13.0 149 8 0 4 29.764 59.528 0.322 5.88 4 31.3 3.1 150 7 2 3 29.909 59.819 0.324 5.81 8 6.1 0.2 151 10 1 0 30.065 60.13 0.325 5.75 4 147.5 68.1 152 2 1 6 30.073 60.146 0.325 5.74 8 28.9 5.2 153 8 2 2 30.163 60.326 0.326 5.7 8 54.3 18.3 154 3 2 5 30.32 60.639 0.328 5.64 8 39.9 9.8 155 10 0 2 30.372 60.743 0.328 5.62 4 29.6 2.7 156 3 3 3 30.41 60.819 0.329 5.6 8 67.4 27.8 157 10 1 1 30.471 60.941 0.329 5.58 8 107.8 70.6 158 6 1 5 30.476 60.952 0.329 5.57 8 74.5 33.7 159 4 0 6 30.581 61.161 0.33 5.53 4 138.6 57.9 160 6 2 4 30.771 61.542 0.332 5.46 8 25.0 3.7 161 5 3 2 30.811 61.622 0.332 5.44 8 37.1 8.2 162 9 1 3 30.824 61.649 0.333 5.44 8 18.9 2.1 163 3 1 6 30.83 61.66 0.333 5.43 8 20.8 2.6 164 6 3 0 30.86 61.721 0.333 5.42 4 11.9 0.4 165 8 1 4 31.076 62.152 0.335 5.34 8 42.4 10.5 166 7 0 5 31.129 62.258 0.336 5.32 4 12.2 0.4 167 6 3 1 31.26 62.52 0.337 5.27 8 47.6 13.0 168 4 2 5 31.372 62.744 0.338 5.23 8 44.2 11.1 169 4 3 3 31.46 62.92 0.339 5.2 8 69.7 27.6 170 9 2 1 31.515 63.031 0.339 5.18 8 31.8 5.7 171 10 1 2 31.669 63.338 0.341 5.12 8 27.2 4.1 172 4 1 6 31.873 63.746 0.343 5.05 8 14.1 1.1 173 5 0 6 31.923 63.847 0.343 5.03 4 34.4 3.2 174 1 3 4 32.004 64.008 0.344 5.0 8 31.1 5.3 175 8 2 3 32.157 64.314 0.345 4.95 8 12.0 0.8 176 11 0 1 32.308 64.616 0.347 4.9 4 17.7 0.8 177 9 0 4 32.311 64.622 0.347 4.9 4 117.4 36.8 178 10 0 3 32.358 64.717 0.347 4.89 4 107.0 30.5 179 7 1 5 32.409 64.818 0.348 4.87 8 71.2 26.9 180 6 3 2 32.442 64.883 0.348 4.86 8 13.9 1.0 181 2 3 4 32.444 64.888 0.348 4.86 8 8.6 0.4 182 9 2 2 32.692 65.384 0.351 4.78 8 90.9 43.1 183 7 2 4 32.695 65.389 0.351 4.78 8 162.3 137.2 184 5 2 5 32.696 65.393 0.351 4.78 8 40.3 8.4 185 5 3 3 32.783 65.566 0.351 4.75 8 8.6 0.4 186 7 3 1 33.168 66.335 0.355 4.63 8 14.1 1.0 187 3 3 4 33.171 66.341 0.355 4.63 8 34.4 6.0 188 5 1 6 33.187 66.373 0.355 4.63 8 35.0 6.2 189 0 2 6 33.326 66.653 0.357 4.59 4 115.2 33.2 190 8 0 5 33.33 66.66 0.357 4.59 4 37.8 3.6 191 11 0 2 33.47 66.939 0.358 4.55 4 67.1 11.2 192 1 2 6 33.47 66.941 0.358 4.55 8 124.7 77.1 193 1 0 7 33.479 66.958 0.358 4.54 4 32.5 2.6 194 6 0 6 33.524 67.048 0.358 4.53 4 7.5 0.1 195 11 1 1 33.563 67.127 0.359 4.52 8 3.1 0.0 196 9 1 4 33.566 67.133 0.359 4.52 8 12.1 0.7 197 10 1 3 33.613 67.226 0.359 4.51 8 35.6 6.2 198 10 2 0 33.893 67.786 0.362 4.43 4 46.3 5.2 199 2 2 6 33.901 67.801 0.362 4.43 8 42.8 8.8 200 2 0 7 33.909 67.818 0.362 4.42 4 47.5 5.4 201 4 3 4 34.175 68.349 0.365 4.35 8 30.8 4.5 202 10 2 1 34.274 68.547 0.366 4.33 8 23.7 2.7 203 6 2 5 34.279 68.557 0.366 4.32 8 2.4 0.0 204 7 3 2 34.314 68.629 0.366 4.32 8 32.2 4.9 205 6 3 3 34.363 68.726 0.366 4.3 8 7.7 0.3 206 0 4 0 34.446 68.891 0.367 4.28 2 439.9 225.8 207 8 1 5 34.567 69.133 0.368 4.25 8 46.5 10.0 208 0 1 7 34.572 69.143 0.368 4.25 4 65.3 9.9 209 9 2 3 34.606 69.213 0.369 4.24 8 56.1 14.5 210 3 2 6 34.612 69.224 0.369 4.24 8 68.2 21.5 211 3 0 7 34.62 69.24 0.369 4.24 4 45.7 4.8 212 11 1 2 34.704 69.408 0.37 4.22 8 39.6 7.2 213 1 1 7 34.713 69.426 0.37 4.21 8 14.9 1.0 214 6 1 6 34.757 69.515 0.37 4.2 8 4.2 0.1 215 8 2 4 34.843 69.687 0.371 4.18 8 45.2 9.3 216 8 3 0 34.927 69.854 0.372 4.16 4 64.4 9.4 217 1 4 1 34.964 69.928 0.372 4.15 8 1.6 0.0 218 2 4 0 35.011 70.022 0.372 4.14 4 20.2 0.9 219 10 0 4 35.037 70.074 0.373 4.14 4 38.2 3.3 220 2 1 7 35.136 70.272 0.374 4.11 8 57.7 14.9 221 12 0 0 35.221 70.442 0.374 4.09 2 73.4 6.0 222 8 3 1 35.302 70.604 0.375 4.07 8 12.5 0.7 223 0 3 5 35.307 70.614 0.375 4.07 4 2.7 0.0 224 11 0 3 35.363 70.726 0.376 4.06 4 39.6 3.5 225 7 0 6 35.369 70.737 0.376 4.06 4 2.4 0.0 226 2 4 1 35.386 70.772 0.376 4.05 8 1.7 0.0 227 10 2 2 35.403 70.807 0.376 4.05 8 190.7 160.5 228 5 3 4 35.445 70.891 0.376 4.04 8 53.0 12.4 229 1 3 5 35.447 70.894 0.376 4.04 8 26.0 3.0 230 12 0 1 35.595 71.19 0.378 4.01 4 20.8 0.9 231 4 2 6 35.596 71.193 0.378 4.01 8 0.3 0.0 232 4 0 7 35.605 71.209 0.378 4.01 4 7.3 0.1 233 9 0 5 35.74 71.479 0.379 3.98 4 70.2 10.7 234 3 1 7 35.836 71.672 0.38 3.95 8 29.4 3.7 235 2 3 5 35.866 71.733 0.38 3.95 8 49.5 10.5 236 0 4 2 35.945 71.89 0.381 3.93 4 50.7 5.5 237 3 4 1 36.084 72.167 0.382 3.9 8 10.0 0.4 238 1 4 2 36.084 72.169 0.382 3.9 8 14.9 0.9 239 7 2 5 36.105 72.211 0.383 3.9 8 24.2 2.5 240 7 3 3 36.188 72.375 0.383 3.88 8 22.0 2.0 241 10 1 4 36.247 72.493 0.384 3.87 8 27.5 3.2 242 8 3 2 36.418 72.836 0.385 3.83 8 3.3 0.0 243 12 1 0 36.428 72.856 0.385 3.83 4 12.9 0.3 244 2 4 2 36.5 73.001 0.386 3.82 8 18.9 1.5 245 3 3 5 36.56 73.121 0.387 3.8 8 4.4 0.1 246 11 1 3 36.568 73.137 0.387 3.8 8 1.9 0.0 247 7 1 6 36.574 73.148 0.387 3.8 8 50.9 10.8 248 4 4 0 36.684 73.368 0.388 3.78 4 46.8 4.5 249 12 0 2 36.707 73.414 0.388 3.78 4 37.0 2.8 250 12 1 1 36.797 73.594 0.389 3.76 8 30.0 3.7 251 4 1 7 36.807 73.613 0.389 3.76 8 8.9 0.3 252 5 2 6 36.846 73.692 0.389 3.75 8 53.3 11.6 253 5 0 7 36.854 73.708 0.389 3.75 4 29.5 1.8 254 9 1 5 36.94 73.879 0.39 3.73 8 17.0 1.2 255 6 3 4 36.973 73.945 0.39 3.72 8 39.1 6.2 256 4 4 1 37.052 74.104 0.391 3.71 8 29.5 3.5 257 3 4 2 37.19 74.38 0.392 3.68 8 37.8 5.7 258 11 2 1 37.206 74.412 0.393 3.68 8 76.2 23.3 259 9 2 4 37.209 74.418 0.393 3.68 8 9.8 0.4 260 10 2 3 37.253 74.507 0.393 3.67 8 144.4 83.5 261 8 0 6 37.447 74.894 0.395 3.64 4 60.6 7.3 262 4 3 5 37.524 75.048 0.395 3.62 8 44.2 7.7 263 9 3 1 37.656 75.312 0.397 3.6 8 73.4 21.2 264 12 1 2 37.895 75.791 0.399 3.56 8 17.4 1.2 265 1 4 3 37.921 75.843 0.399 3.56 8 3.7 0.1 266 11 0 4 37.945 75.889 0.399 3.55 4 77.2 11.5 267 5 1 7 38.041 76.081 0.4 3.54 8 73.6 20.9 268 4 4 2 38.148 76.295 0.401 3.52 8 43.0 7.1 269 8 2 5 38.168 76.336 0.401 3.52 8 111.8 48.0 270 8 3 3 38.249 76.498 0.402 3.5 8 3.1 0.0 271 5 4 1 38.283 76.566 0.402 3.5 8 56.8 12.3 272 11 2 2 38.3 76.6 0.402 3.5 8 17.6 1.2 273 1 2 7 38.309 76.618 0.402 3.49 8 58.0 12.8 274 2 4 3 38.33 76.66 0.403 3.49 8 35.9 4.9 275 6 2 6 38.352 76.704 0.403 3.49 8 63.8 15.5 276 10 0 5 38.355 76.71 0.403 3.49 4 66.7 8.4 277 6 0 7 38.36 76.72 0.403 3.49 4 12.2 0.3 278 12 0 3 38.533 77.066 0.404 3.46 4 42.8 3.5 279 8 1 6 38.628 77.255 0.405 3.44 8 46.7 8.2 280 2 2 7 38.716 77.433 0.406 3.43 8 17.3 1.1 281 9 3 2 38.746 77.492 0.406 3.43 8 88.6 29.3 282 7 3 4 38.748 77.497 0.406 3.43 8 17.7 1.2 283 5 3 5 38.75 77.5 0.406 3.43 8 89.6 30.0 284 0 0 8 38.905 77.811 0.408 3.4 2 167.9 26.2 285 3 4 3 39.008 78.017 0.409 3.39 8 10.6 0.4 286 13 0 1 39.029 78.057 0.409 3.39 4 23.5 1.0 287 1 0 8 39.041 78.082 0.409 3.38 4 28.8 1.5 288 11 1 4 39.12 78.24 0.41 3.37 8 45.5 7.6 289 5 4 2 39.368 78.735 0.412 3.34 8 117.3 50.0 290 3 2 7 39.393 78.785 0.412 3.33 8 27.6 2.8 291 6 4 0 39.412 78.824 0.412 3.33 4 115.3 24.2 292 2 0 8 39.446 78.892 0.412 3.33 4 107.8 21.1 293 1 3 6 39.473 78.947 0.413 3.32 8 23.9 2.1 294 10 1 5 39.527 79.054 0.413 3.32 8 57.2 11.8 295 6 1 7 39.532 79.063 0.413 3.32 8 54.9 10.9 296 12 1 3 39.703 79.407 0.415 3.29 8 8.5 0.3 297 9 0 6 39.755 79.51 0.415 3.29 4 64.6 7.5 298 6 4 1 39.771 79.543 0.415 3.28 8 18.5 1.2 299 10 2 4 39.79 79.581 0.415 3.28 8 71.1 18.1 300 10 3 0 39.87 79.741 0.416 3.27 4 125.1 27.9 301 2 3 6 39.877 79.755 0.416 3.27 8 15.5 0.9 302 4 4 3 39.952 79.904 0.417 3.26 8 2.0 0.0 303 12 2 0 39.967 79.933 0.417 3.26 4 13.3 0.3 304 11 2 3 40.103 80.206 0.418 3.24 8 63.9 14.4 305 13 0 2 40.107 80.214 0.418 3.24 4 4.9 0.0 306 7 2 6 40.108 80.216 0.418 3.24 8 31.0 3.4 307 7 0 7 40.116 80.232 0.418 3.24 4 27.3 1.3 308 3 0 8 40.119 80.238 0.418 3.24 4 0.8 0.0 309 13 1 1 40.195 80.39 0.419 3.23 8 25.0 2.2 310 1 1 8 40.207 80.414 0.419 3.23 8 16.4 0.9 311 10 3 1 40.229 80.457 0.419 3.23 8 99.7 35.0 312 6 3 5 40.233 80.467 0.419 3.23 8 71.3 17.9 313 0 4 4 40.312 80.623 0.42 3.22 4 33.7 2.0 314 12 2 1 40.325 80.65 0.42 3.21 8 24.6 2.1 315 4 2 7 40.334 80.668 0.42 3.21 8 9.9 0.3 316 1 4 4 40.446 80.891 0.421 3.2 8 56.8 11.3 317 9 2 5 40.464 80.927 0.421 3.2 8 92.7 30.0 318 9 3 3 40.543 81.086 0.422 3.19 8 9.8 0.3 319 3 3 6 40.548 81.097 0.422 3.19 8 19.2 1.3 320 2 1 8 40.609 81.218 0.423 3.18 8 23.7 1.9 321 8 3 4 40.768 81.535 0.424 3.16 8 33.0 3.8 322 6 4 2 40.845 81.69 0.425 3.16 8 46.7 7.5 323 2 4 4 40.847 81.695 0.425 3.15 8 39.8 5.4 324 9 1 6 40.916 81.832 0.425 3.15 8 35.1 4.2 325 12 0 4 41.047 82.094 0.426 3.13 4 37.0 2.3 326 4 0 8 41.056 82.113 0.426 3.13 4 37.0 2.3 327 5 4 3 41.158 82.316 0.427 3.12 8 17.4 1.0 328 11 0 5 41.182 82.365 0.427 3.12 4 11.3 0.2 329 13 1 2 41.266 82.532 0.428 3.11 8 31.1 3.3 330 7 1 7 41.275 82.55 0.428 3.11 8 56.9 11.0 331 3 1 8 41.278 82.555 0.428 3.11 8 25.6 2.2 332 10 3 2 41.3 82.6 0.428 3.11 8 23.2 1.8 333 12 2 2 41.396 82.791 0.429 3.1 8 5.7 0.1 334 4 3 6 41.484 82.968 0.43 3.09 8 9.9 0.3 335 7 4 1 41.512 83.024 0.43 3.08 8 24.5 2.0 336 3 4 4 41.515 83.03 0.43 3.08 8 12.9 0.6 337 5 2 7 41.538 83.075 0.43 3.08 8 107.9 39.1 338 13 0 3 41.89 83.781 0.433 3.05 4 33.3 1.8 339 7 3 5 41.97 83.94 0.434 3.04 8 60.2 12.0 340 8 2 6 42.112 84.224 0.435 3.03 8 11.1 0.4 341 8 0 7 42.12 84.24 0.435 3.03 4 27.7 1.3 342 12 1 4 42.201 84.402 0.436 3.02 8 1.8 0.0 343 4 1 8 42.21 84.42 0.436 3.02 8 5.4 0.1 344 5 0 8 42.256 84.512 0.436 3.02 4 42.7 3.0 345 14 0 0 42.288 84.576 0.437 3.01 2 12.2 0.1 346 10 0 6 42.295 84.589 0.437 3.01 4 25.0 1.0 347 11 1 5 42.336 84.671 0.437 3.01 8 30.0 3.0 348 4 4 4 42.447 84.893 0.438 3.0 8 22.4 1.6 349 7 4 2 42.577 85.154 0.439 2.99 8 0.7 0.0 350 11 2 4 42.596 85.191 0.439 2.99 8 6.5 0.1 351 6 4 3 42.622 85.245 0.44 2.98 8 55.8 10.1 352 14 0 1 42.642 85.285 0.44 2.98 4 13.3 0.3 353 5 3 6 42.681 85.363 0.44 2.98 8 27.1 2.4 354 10 2 5 42.996 85.991 0.443 2.95 8 3.2 0.0 355 6 2 7 43.0 86.0 0.443 2.95 8 50.5 8.2 356 11 3 1 43.028 86.057 0.443 2.95 8 3.6 0.0 357 9 3 4 43.031 86.063 0.443 2.95 8 16.5 0.9 358 13 1 3 43.041 86.081 0.443 2.95 8 5.5 0.1 359 10 3 3 43.074 86.148 0.443 2.95 8 34.3 3.8 360 8 4 0 43.152 86.303 0.444 2.94 4 123.9 24.6 361 12 2 3 43.169 86.339 0.444 2.94 8 37.8 4.6 362 8 1 7 43.269 86.539 0.445 2.93 8 47.2 7.1 363 5 1 8 43.405 86.81 0.446 2.92 8 19.6 1.2 364 14 1 0 43.437 86.874 0.446 2.92 4 133.9 28.6 365 10 1 6 43.444 86.887 0.446 2.92 8 69.0 15.2 366 8 4 1 43.505 87.011 0.447 2.92 8 64.6 13.3 367 0 2 8 43.533 87.067 0.447 2.92 4 66.8 7.1 368 5 4 4 43.641 87.281 0.448 2.91 8 75.2 17.9 369 1 4 5 43.642 87.285 0.448 2.91 8 2.5 0.0 370 13 2 1 43.654 87.308 0.448 2.91 8 16.6 0.9 371 1 2 8 43.666 87.332 0.448 2.91 8 5.5 0.1 372 14 0 2 43.704 87.408 0.448 2.9 4 23.3 0.9 373 6 0 8 43.715 87.431 0.449 2.9 4 54.6 4.7 374 14 1 1 43.79 87.581 0.449 2.9 8 17.6 1.0 375 8 3 5 43.961 87.922 0.451 2.89 8 35.5 4.0 376 0 3 7 43.965 87.931 0.451 2.89 4 57.8 5.2 377 2 4 5 44.04 88.08 0.451 2.88 8 60.5 11.5 378 2 2 8 44.063 88.126 0.451 2.88 8 18.7 1.1 379 11 3 2 44.089 88.178 0.452 2.88 8 34.9 3.8 380 1 3 7 44.098 88.196 0.452 2.88 8 11.3 0.4 381 6 3 6 44.139 88.279 0.452 2.88 8 3.4 0.0 382 12 0 5 44.238 88.475 0.453 2.87 4 76.1 9.1 383 7 4 3 44.346 88.691 0.454 2.86 8 6.4 0.1 384 9 2 6 44.367 88.734 0.454 2.86 8 15.2 0.7 385 13 0 4 44.368 88.737 0.454 2.86 4 5.7 0.1 386 9 0 7 44.375 88.749 0.454 2.86 4 45.2 3.2 387 2 3 7 44.495 88.99 0.455 2.86 8 52.7 8.6 388 8 4 2 44.565 89.131 0.455 2.85 8 56.9 10.1 389 3 4 5 44.702 89.403 0.457 2.84 8 37.8 4.4 390 13 2 2 44.714 89.427 0.457 2.84 8 8.4 0.2 391 7 2 7 44.722 89.444 0.457 2.84 8 19.1 1.1 392 3 2 8 44.725 89.45 0.457 2.84 8 18.3 1.0 393 14 1 2 44.85 89.7 0.458 2.84 8 27.3 2.3 394 6 1 8 44.861 89.723 0.458 2.84 8 68.6 14.5 X-ray diffraction powder data (I)...X-Ray wave length = 1.54056 (angs.): No H K L Theta 2*Theta d I int I int.n. I p.h.n. H(Si) ( degree ) (angstrem) *100 *100 1 2 0 0 5.516 11.032 8.01355 95.3 12.4 12.6 5.6 2 0 0 2 9.033 18.067 4.90595 177.0 23.0 23.2 5.6 3 0 1 1 9.308 18.615 4.76257 10.8 1.4 1.4 5.6 4 1 0 2 9.451 18.902 4.69109 31.8 4.1 4.2 5.6 5 1 1 1 9.714 19.428 4.56527 78.9 10.2 10.3 5.6 6 2 0 2 10.608 21.217 4.18412 25.0 3.2 3.3 5.6 7 4 0 0 11.084 22.168 4.00677 92.5 12.0 12.1 5.6 8 4 0 1 11.985 23.97 3.70941 59.2 7.7 7.7 5.6 9 3 0 2 12.308 24.616 3.61348 88.6 11.5 11.6 5.6 10 3 1 1 12.514 25.027 3.55503 243.0 31.5 31.7 5.6 11 4 0 2 14.372 28.744 3.1033 72.7 9.4 9.5 5.6 12 4 1 1 14.55 29.101 3.06604 46.7 6.1 6.1 5.6 13 5 0 1 14.643 29.287 3.04695 126.0 16.4 16.4 5.6 14 2 0 3 14.737 29.473 3.02814 74.4 9.7 9.7 5.6 15 3 1 2 14.821 29.643 3.0112 10.9 1.4 1.4 5.6 16 0 1 3 15.944 31.889 2.80403 770.3 100.0 100.0 5.6 17 1 1 3 16.193 32.386 2.76208 109.0 14.1 14.1 5.6 18 0 2 0 16.428 32.856 2.72365 321.2 41.7 41.7 5.6 19 5 0 2 16.682 33.363 2.68342 294.2 38.2 38.2 5.7 20 6 0 0 16.76 33.52 2.67118 176.8 23.0 22.9 5.7 21 5 1 1 16.838 33.676 2.65922 580.1 75.3 75.2 5.7 22 2 1 3 16.92 33.84 2.64668 74.3 9.7 9.6 5.7 23 1 2 1 17.302 34.605 2.58992 17.4 2.3 2.3 5.7 24 2 2 0 17.38 34.759 2.57877 154.6 20.1 20.0 5.7 25 3 1 3 18.074 36.148 2.48282 131.0 17.0 16.9 5.7 26 0 0 4 18.302 36.603 2.45298 12.0 1.6 1.6 5.7 27 1 0 4 18.522 37.045 2.42474 52.2 6.8 6.7 5.7 28 5 1 2 18.662 37.325 2.40719 11.7 1.5 1.5 5.7 29 0 2 2 18.873 37.746 2.38129 64.8 8.4 8.4 5.7 30 1 2 2 19.088 38.176 2.35543 236.0 30.6 30.5 5.7 31 2 0 4 19.172 38.344 2.34555 44.6 5.8 5.8 5.7 32 6 1 1 19.307 38.614 2.32976 48.0 6.2 6.2 5.7 33 4 1 3 19.59 39.181 2.29734 132.6 17.2 17.1 5.7 34 5 0 3 19.662 39.324 2.28928 10.7 1.4 1.4 5.7 35 2 2 2 19.722 39.443 2.28264 202.9 26.3 26.2 5.7 36 7 0 1 20.21 40.42 2.22969 27.6 3.6 3.6 5.7 37 1 1 4 20.348 40.697 2.21519 43.2 5.6 5.6 5.7 38 4 2 1 20.54 41.08 2.1954 103.4 13.4 13.3 5.7 39 3 2 2 20.741 41.483 2.175 36.1 4.7 4.6 5.7 40 2 1 4 20.95 41.9 2.15432 9.8 1.3 1.3 5.7 41 1 2 3 21.787 43.574 2.07534 53.4 6.9 6.9 5.7 42 6 0 3 21.859 43.718 2.06887 68.1 8.8 8.7 5.7 43 3 1 4 21.923 43.845 2.06314 30.7 4.0 3.9 5.7 44 5 2 1 22.292 44.585 2.03063 178.0 23.1 22.8 5.7 45 2 2 3 22.357 44.714 2.02503 178.5 23.2 22.9 5.7 46 8 0 0 22.612 45.224 2.00339 124.1 16.1 15.9 5.7 47 8 0 1 23.105 46.211 1.96289 65.6 8.5 8.4 5.7 48 4 1 4 23.229 46.459 1.95298 15.4 2.0 2.0 5.7 49 5 0 4 23.292 46.584 1.94802 95.4 12.4 12.2 5.7 50 7 1 2 23.408 46.816 1.93889 22.2 2.9 2.8 5.7 51 5 2 2 23.764 47.527 1.91153 122.9 16.0 15.7 5.7 52 2 0 5 23.836 47.672 1.90606 50.3 6.5 6.4 5.7 53 8 1 0 24.184 48.368 1.88026 39.9 5.2 5.1 5.7 54 8 0 2 24.539 49.078 1.8547 35.0 4.5 4.5 5.7 55 3 0 5 24.719 49.438 1.84204 15.6 2.0 2.0 5.7 56 5 1 4 24.831 49.662 1.83426 39.9 5.2 5.1 5.7 57 1 2 4 25.171 50.342 1.81105 207.4 26.9 26.4 5.8 58 2 1 5 25.35 50.7 1.7991 31.6 4.1 4.0 5.8 59 2 2 4 25.683 51.366 1.77732 22.8 3.0 2.9 5.8 60 3 2 4 26.521 53.041 1.72508 17.5 2.3 2.2 5.8 61 6 1 4 26.691 53.382 1.71488 13.9 1.8 1.8 5.8 62 3 3 1 27.057 54.114 1.69338 34.8 4.5 4.4 5.8 63 4 1 5 27.347 54.694 1.67679 29.0 3.8 3.7 5.8 64 9 0 2 27.398 54.795 1.67392 31.4 4.1 4.0 5.8 65 9 1 1 27.503 55.006 1.668 57.7 7.5 7.3 5.8 66 7 2 2 27.821 55.642 1.65045 56.9 7.4 7.2 5.8 67 6 2 3 27.875 55.751 1.64748 8.6 1.1 1.1 5.8 68 0 0 6 28.101 56.202 1.63532 15.7 2.0 2.0 5.8 69 1 0 6 28.26 56.52 1.62687 23.3 3.0 2.9 5.8 70 8 2 0 28.509 57.018 1.61383 25.5 3.3 3.2 5.8 71 10 0 0 28.725 57.451 1.60271 19.9 2.6 2.5 5.8 72 5 1 5 28.782 57.563 1.59984 149.3 19.4 18.8 5.8 73 0 3 3 29.026 58.052 1.58752 112.3 14.6 14.2 5.8 74 5 2 4 29.088 58.175 1.58447 231.3 30.0 29.2 5.8 75 6 0 5 29.148 58.295 1.58148 15.4 2.0 1.9 5.8 76 1 3 3 29.182 58.364 1.57979 22.8 3.0 2.9 5.8 77 3 0 6 29.512 59.023 1.5637 142.0 18.4 17.9 5.8 78 5 3 1 29.593 59.186 1.5598 102.4 13.3 12.9 5.8 79 2 3 3 29.646 59.292 1.55726 13.0 1.7 1.6 5.8 80 10 1 0 30.065 60.13 1.53754 73.4 9.5 9.2 5.8 81 8 2 2 30.163 60.326 1.53302 18.3 2.4 2.3 5.8 82 3 2 5 30.32 60.639 1.52584 9.8 1.3 1.2 5.8 83 3 3 3 30.41 60.819 1.52176 27.8 3.6 3.5 5.8 84 10 1 1 30.471 60.941 1.519 104.3 13.5 13.1 5.8 85 4 0 6 30.581 61.161 1.51407 57.9 7.5 7.3 5.8 86 5 3 2 30.811 61.622 1.50384 12.9 1.7 1.6 5.8 87 8 1 4 31.076 62.152 1.49229 10.5 1.4 1.3 5.8 88 6 3 1 31.26 62.52 1.48439 13.0 1.7 1.6 5.8 89 4 2 5 31.372 62.744 1.47963 11.1 1.4 1.4 5.9 90 4 3 3 31.46 62.92 1.4759 27.6 3.6 3.4 5.9 91 9 0 4 32.311 64.622 1.44108 36.8 4.8 4.6 5.9 92 10 0 3 32.358 64.717 1.4392 30.5 4.0 3.8 5.9 93 7 1 5 32.409 64.818 1.4372 26.9 3.5 3.4 5.9 94 7 2 4 32.695 65.389 1.42602 188.7 24.5 23.5 5.9 95 5 1 6 33.187 66.373 1.40725 13.2 1.7 1.6 5.9 96 0 2 6 33.326 66.653 1.40202 36.8 4.8 4.6 5.9 97 1 2 6 33.47 66.941 1.39668 90.9 11.8 11.3 5.9 98 2 0 7 33.909 67.818 1.38074 19.5 2.5 2.4 5.9 99 0 4 0 34.446 68.891 1.36182 225.8 29.3 28.0 5.9 100 8 1 5 34.567 69.133 1.35765 19.9 2.6 2.5 5.9 101 3 2 6 34.612 69.224 1.3561 40.9 5.3 5.1 5.9 102 11 1 2 34.704 69.408 1.35295 8.2 1.1 1.0 5.9 103 8 2 4 34.843 69.687 1.34821 9.3 1.2 1.2 5.9 104 8 3 0 34.927 69.854 1.34539 9.4 1.2 1.2 5.9 105 2 1 7 35.136 70.272 1.33841 14.9 1.9 1.8 5.9 106 10 2 2 35.403 70.807 1.32961 160.5 20.8 19.8 5.9 107 5 3 4 35.445 70.891 1.32824 15.3 2.0 1.9 5.9 108 9 0 5 35.74 71.479 1.31874 10.7 1.4 1.3 5.9 109 2 3 5 35.866 71.733 1.3147 10.5 1.4 1.3 5.9 110 7 1 6 36.574 73.148 1.29272 10.8 1.4 1.3 6.0 111 5 2 6 36.846 73.692 1.28452 13.4 1.7 1.6 6.0 112 11 2 1 37.206 74.412 1.27386 29.4 3.8 3.6 6.0 113 10 2 3 37.253 74.507 1.27248 83.5 10.8 10.2 6.0 114 4 3 5 37.524 75.048 1.26464 7.7 1.0 0.9 6.0 115 9 3 1 37.656 75.312 1.26085 21.2 2.7 2.6 6.0 116 11 0 4 37.945 75.889 1.25269 11.5 1.5 1.4 6.0 117 5 1 7 38.041 76.081 1.25001 20.9 2.7 2.6 6.0 118 8 2 5 38.168 76.336 1.24647 55.1 7.1 6.7 6.0 119 1 2 7 38.309 76.618 1.24258 26.3 3.4 3.2 6.0 120 10 0 5 38.355 76.71 1.24132 29.1 3.8 3.6 6.0 121 8 1 6 38.628 77.255 1.23392 8.2 1.1 1.0 6.0 122 5 3 5 38.75 77.5 1.23063 61.6 8.0 7.5 6.0 123 0 0 8 38.905 77.811 1.22649 26.2 3.4 3.2 6.0 124 5 4 2 39.368 78.735 1.21439 52.8 6.9 6.4 6.0 125 6 4 0 39.412 78.824 1.21325 24.2 3.1 2.9 6.0 126 2 0 8 39.446 78.892 1.21237 23.1 3.0 2.8 6.0 127 10 1 5 39.527 79.054 1.21029 22.7 2.9 2.8 6.0 128 9 0 6 39.755 79.51 1.20449 8.7 1.1 1.1 6.0 129 10 2 4 39.79 79.581 1.2036 18.1 2.3 2.2 6.0 130 10 3 0 39.87 79.741 1.20159 28.8 3.7 3.5 6.0 131 11 2 3 40.103 80.206 1.19579 19.2 2.5 2.3 6.0 132 10 3 1 40.229 80.457 1.19268 52.9 6.9 6.4 6.0 133 9 2 5 40.464 80.927 1.18693 41.2 5.4 5.0 6.1 134 6 4 2 40.845 81.69 1.17777 12.9 1.7 1.6 6.1 135 7 1 7 41.275 82.55 1.16767 18.3 2.4 2.2 6.1 136 5 2 7 41.538 83.075 1.16162 41.7 5.4 5.0 6.1 137 7 3 5 41.97 83.94 1.15183 12.0 1.6 1.4 6.1 138 6 4 3 42.622 85.245 1.13751 10.4 1.4 1.2 6.1 139 6 2 7 43.0 86.0 1.12944 8.3 1.1 1.0 6.1 140 8 4 0 43.152 86.303 1.12625 29.2 3.8 3.5 6.1 141 14 1 0 43.437 86.874 1.12032 43.7 5.7 5.2 6.1 142 8 4 1 43.505 87.011 1.11891 20.4 2.6 2.4 6.1 143 5 4 4 43.641 87.281 1.11613 18.9 2.5 2.3 6.2 144 0 3 7 43.965 87.931 1.10956 9.2 1.2 1.1 6.2 145 2 4 5 44.04 88.08 1.10807 12.6 1.6 1.5 6.2 146 12 0 5 44.238 88.475 1.10413 9.1 1.2 1.1 6.2 147 2 3 7 44.495 88.99 1.09907 8.6 1.1 1.0 6.2 148 8 4 2 44.565 89.131 1.0977 10.1 1.3 1.2 6.2 149 6 1 8 44.861 89.723 1.09198 16.8 2.2 2.0 6.2 Reference: Chichagov A.V. et al. Information-Calculating System on Crystal Structure Data of Minerals (MINCRYST) - Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian) |