Institute of Experimental Mineralogy Russian Academy of Sciences ------------------------------------------------- 142432, Chernogolovka, Moscow district A.V. Chichagov +7(496)52-22320 *** *** W W W - X R A Y P O L *** *********************** ZOISITE 1, t-zoisite, f-epidote Ca(2)Al(3)[Si(3)O(12)]OH Orthorhombic P nma Z = 4 Pnma 31 .5 .1988 Ref.Str.: Dollase W.A. (1968) * Amer. Mineral., 53, 1882-1898 Initial data from BDM-file Lattice parameters (cub. angs.,degr.): a = 16.212 alpha = 90.0 b = 5.559 beta = 90.0 c = 10.036 gamma = 90.0 Unit cell volume (cub. angs.) = 904.47 Molar volume ( cub.cm/mol.) = 136.2 Co-ordinates, thermal parameters, occupation for atomic positions: NoP x/a y/b z/c B(j) atom / occupation 1 0.3667 0.25 0.4376 0.0 Ca = 1.00 2 0.4518 0.25 0.115 0.0 Ca = 1.00 3 0.0816 0.25 0.1064 0.0 Si = 1.00 4 0.4104 0.75 0.2821 0.0 Si = 1.00 5 0.1601 0.25 0.4356 0.0 Si = 1.00 6 0.2496 0.9971 0.1899 0.0 Al = 1.00 7 0.1054 0.75 0.3006 0.0 Al = 1.00 8 0.1317 0.0 0.1451 0.0 O = 1.00 9 0.1012 0.015 0.43 0.0 O = 1.00 10 0.3584 0.99 0.2452 0.0 O = 1.00 11 0.2178 0.75 0.301 0.0 O = 1.00 12 0.2273 0.25 0.312 0.0 O = 1.00 13 0.2713 0.75 0.06 0.0 O = 1.00 14 0.9905 0.25 0.164 0.0 O = 1.00 15 0.9954 0.75 0.295 0.0 O = 1.00 16 0.4209 0.75 0.443 0.0 O = 1.00 17 0.268 0.25 0.074 0.0 O = 1.00 18 0.26 0.25 0.95 0.0 H = 1.00 Co-ordinates for all atomic positions : No NoP x/a y/b z/c 1 1 0.3667 0.25 0.4376 2 2 0.4518 0.25 0.115 3 3 0.0816 0.25 0.1064 4 4 0.4104 0.75 0.2821 5 5 0.1601 0.25 0.4356 6 6 0.2496 0.9971 0.1899 7 7 0.1054 0.75 0.3006 8 8 0.1317 0.0 0.1451 9 9 0.1012 0.015 0.43 10 10 0.3584 0.99 0.2452 11 11 0.2178 0.75 0.301 12 12 0.2273 0.25 0.312 13 13 0.2713 0.75 0.06 14 14 0.9905 0.25 0.164 15 15 0.9954 0.75 0.295 16 16 0.4209 0.75 0.443 17 17 0.268 0.25 0.074 18 18 0.26 0.25 0.95 19 1 0.1333 0.75 0.9376 20 2 0.0482 0.75 0.615 21 3 0.4184 0.75 0.6064 22 4 0.0896 0.25 0.7821 23 5 0.3399 0.75 0.9356 24 6 0.2504 0.0029 0.6899 25 7 0.3946 0.25 0.8006 26 8 0.3683 0.0 0.6451 27 9 0.3988 0.985 0.93 28 10 0.1416 0.01 0.7452 29 11 0.2822 0.25 0.801 30 12 0.2727 0.75 0.812 31 13 0.2287 0.25 0.56 32 14 0.5095 0.75 0.664 33 15 0.5046 0.25 0.795 34 16 0.0791 0.25 0.943 35 17 0.232 0.75 0.574 36 18 0.24 0.75 0.45 37 6 0.2504 0.4971 0.6899 38 8 0.3683 0.5 0.6451 39 9 0.3988 0.515 0.93 40 10 0.1416 0.49 0.7452 41 6 0.2496 0.5029 0.1899 42 8 0.1317 0.5 0.1451 43 9 0.1012 0.485 0.43 44 10 0.3584 0.51 0.2452 45 1 0.8667 0.25 0.0624 46 2 0.9518 0.25 0.385 47 3 0.5816 0.25 0.3936 48 4 0.9104 0.75 0.2179 49 5 0.6601 0.25 0.0644 50 6 0.7496 0.9971 0.3101 51 7 0.6054 0.75 0.1994 52 8 0.6317 0.0 0.3549 53 9 0.6012 0.015 0.07 54 10 0.8584 0.99 0.2548 55 11 0.7178 0.75 0.199 56 12 0.7273 0.25 0.188 57 13 0.7713 0.75 0.44 58 14 0.4905 0.25 0.336 59 15 0.4954 0.75 0.205 60 16 0.9209 0.75 0.057 61 17 0.768 0.25 0.426 62 18 0.76 0.25 0.55 63 1 0.6333 0.75 0.5624 64 2 0.5482 0.75 0.885 65 3 0.9184 0.75 0.8936 66 4 0.5896 0.25 0.7179 67 5 0.8399 0.75 0.5644 68 6 0.7504 0.0029 0.8101 69 7 0.8946 0.25 0.6994 70 8 0.8683 0.0 0.8549 71 9 0.8988 0.985 0.57 72 10 0.6416 0.01 0.7548 73 11 0.7822 0.25 0.699 74 12 0.7727 0.75 0.688 75 13 0.7287 0.25 0.94 76 14 0.0095 0.75 0.836 77 15 0.0046 0.25 0.705 78 16 0.5791 0.25 0.557 79 17 0.732 0.75 0.926 80 18 0.74 0.75 0.05 81 6 0.7504 0.4971 0.8101 82 8 0.8683 0.5 0.8549 83 9 0.8988 0.515 0.57 84 10 0.6416 0.49 0.7548 85 6 0.7496 0.5029 0.3101 86 8 0.6317 0.5 0.3549 87 9 0.6012 0.485 0.07 88 10 0.8584 0.51 0.2548 X-ray density (g/cm cub.) = 3.34 MU (1/cm) = 179.261 Mass attenuation coefficient (cm**2/g) = 53.742 Selected interatomic distances (cation-anion,anion-anion): NoP Atom Rad.sph. C.N. Distance NoP N. (angs.) (angs.) 1 Ca 2.88 7 2.4157 10 2.5877 12 2.5037 8 2.5523 13 2.5037 8 2.4157 10 2.2512 14 2 Ca 2.88 7 2.4676 10 2.521 9 2.521 9 2.4676 10 2.7887 9 2.305 14 2.7887 9 3 Si 2.1 4 1.6559 8 1.586 14 1.6404 16 1.6559 8 4 Si 2.1 4 1.6211 10 1.6237 16 1.6211 10 1.5804 15 5 Si 2.1 4 1.6191 9 1.6509 12 1.672 13 1.6191 9 6 Al 2.316 6 1.9636 8 1.8495 10 1.8428 11 1.8997 12 1.9262 13 1.8489 17 7 Al 2.316 6 2.1328 8 1.965 9 1.8222 11 1.7842 15 2.1328 8 1.965 9 8 O 3.264 10 2.9029 9 2.5155 11 2.6719 12 2.7898 13 2.6847 14 3.0129 15 2.7062 17 2.6024 16 2.7795 8 2.7795 8 9 O 3.264 9 2.9029 8 2.7239 11 2.6997 12 2.6359 15 3.2306 10 2.7715 13 2.9589 17 2.6127 9 2.9463 9 10 O 3.264 10 2.6999 11 2.6563 12 2.6886 13 2.5976 16 2.6812 17 3.2306 9 2.8907 10 2.6683 10 2.7397 14 2.6222 15 11 O 3.264 10 2.5155 8 2.7239 9 2.6999 10 2.786 12 2.786 12 2.5695 13 2.7495 17 2.5155 8 2.7239 9 2.6999 10 12 O 3.264 10 2.6719 8 2.6997 9 2.6563 10 2.786 11 2.786 11 2.478 17 2.489 13 2.6719 8 2.6997 9 2.6563 10 13 O 3.264 10 2.7898 8 2.6886 10 2.5695 11 2.7836 17 2.7836 17 2.7715 9 2.489 12 2.7715 9 2.7898 8 2.6886 10 14 O 3.264 9 2.6847 8 3.0758 15 3.0758 15 2.6424 16 2.6847 8 2.7397 10 3.1862 16 3.1862 16 2.7397 10 15 O 3.264 9 3.0129 8 2.6359 9 3.0758 14 3.0758 14 3.0129 8 2.6359 9 2.6222 10 2.6766 16 2.6222 10 16 O 3.264 8 2.5976 10 2.6024 8 2.6424 14 2.6024 8 2.5976 10 3.1862 14 3.1862 14 2.6766 15 17 O 3.264 10 2.7062 8 2.6812 10 2.478 12 2.7836 13 2.7836 13 2.9589 9 2.7495 11 2.9589 9 2.7062 8 2.6812 10 18 H 1.632 2 1.2512 17 1.5381 11 X-ray diffraction powder data (II), X-Ray W.L. = 1.54056(angs.): No H K L Theta 2*Theta S LPG MF F I int. ( degree ) *100 1 1 0 1 5.179 10.358 0.059 242.47 4 1.2 0.2 2 2 0 0 5.453 10.906 0.062 218.51 2 47.5 120.7 3 2 0 1 7.016 14.032 0.079 131.08 4 1.6 0.2 4 0 0 2 8.83 17.66 0.1 81.94 2 99.1 196.9 5 0 1 1 9.114 18.228 0.103 76.78 4 16.5 10.2 6 1 0 2 9.247 18.494 0.104 74.53 4 23.6 20.4 7 3 0 1 9.317 18.633 0.105 73.39 4 5.5 1.1 8 1 1 1 9.519 19.038 0.107 70.21 8 29.1 58.2 9 2 1 0 9.673 19.345 0.109 67.93 4 5.3 0.9 10 2 0 2 10.401 20.802 0.117 58.45 4 29.6 25.1 11 2 1 1 10.645 21.289 0.12 55.71 8 4.3 1.0 12 4 0 0 10.956 21.912 0.123 52.47 2 88.5 100.5 13 4 0 1 11.827 23.655 0.133 44.72 4 52.7 60.6 14 3 0 2 12.092 24.183 0.136 42.7 4 65.8 90.4 15 1 1 2 12.25 24.5 0.138 41.55 8 14.5 8.6 16 3 1 1 12.304 24.607 0.138 41.17 8 72.6 212.4 17 2 1 2 13.155 26.309 0.148 35.76 8 2.5 0.2 18 1 0 3 13.598 27.196 0.153 33.34 4 2.0 0.1 19 4 1 0 13.604 27.207 0.153 33.31 4 1.4 0.0 20 4 0 2 14.141 28.281 0.159 30.68 4 76.0 86.6 21 4 1 1 14.324 28.648 0.161 29.85 8 33.1 32.1 22 2 0 3 14.424 28.848 0.162 29.41 4 69.7 69.9 23 5 0 1 14.457 28.914 0.162 29.26 4 92.3 122.0 24 3 1 2 14.546 29.092 0.163 28.88 8 16.3 7.5 25 0 1 3 15.589 31.178 0.174 24.9 4 250.3 762.7 26 3 0 3 15.712 31.424 0.176 24.48 4 22.2 5.9 27 1 1 3 15.837 31.674 0.177 24.07 8 74.4 130.4 28 0 2 0 16.089 32.178 0.18 23.26 2 235.0 314.1 29 4 1 2 16.312 32.623 0.182 22.58 8 13.6 4.1 30 5 0 2 16.43 32.86 0.184 22.23 4 152.0 251.0 31 2 1 3 16.561 33.122 0.185 21.85 8 59.9 76.7 32 6 0 0 16.563 33.127 0.185 21.84 2 176.2 165.8 33 5 1 1 16.591 33.181 0.185 21.76 8 156.0 518.2 34 1 2 1 16.945 33.891 0.189 20.79 8 30.9 19.4 35 2 2 0 17.036 34.071 0.19 20.55 4 117.3 138.3 36 6 0 1 17.171 34.343 0.192 20.2 4 33.1 10.8 37 4 0 3 17.371 34.742 0.194 19.69 4 5.3 0.3 38 2 2 1 17.629 35.258 0.197 19.07 8 20.5 7.8 39 3 1 3 17.71 35.42 0.197 18.88 8 94.3 164.3 40 0 0 4 17.879 35.758 0.199 18.49 2 51.7 12.1 41 1 0 4 18.099 36.198 0.202 18.0 4 72.8 46.7 42 5 1 2 18.358 36.717 0.204 17.45 8 25.1 10.8 43 0 2 2 18.47 36.939 0.206 17.22 4 85.2 61.2 44 6 1 0 18.48 36.959 0.206 17.2 4 2.0 0.0 45 1 2 2 18.684 37.368 0.208 16.78 8 109.4 196.6 46 3 2 1 18.72 37.441 0.208 16.71 8 7.2 0.8 47 2 0 4 18.746 37.492 0.209 16.66 4 64.9 34.3 48 6 0 2 18.892 37.783 0.21 16.38 4 35.1 9.9 49 6 1 1 19.034 38.068 0.212 16.11 8 44.1 30.7 50 4 1 3 19.217 38.434 0.214 15.77 8 93.1 133.8 51 2 2 2 19.314 38.628 0.215 15.6 8 117.0 208.9 52 5 0 3 19.32 38.639 0.215 15.59 4 29.4 6.6 53 4 2 0 19.636 39.271 0.218 15.04 4 15.4 1.7 54 3 0 4 19.784 39.569 0.22 14.79 4 25.3 4.6 55 1 1 4 19.887 39.774 0.221 14.62 8 44.3 28.0 56 7 0 1 19.958 39.916 0.222 14.5 4 72.9 37.6 57 4 2 1 20.163 40.326 0.224 14.18 8 84.8 99.8 58 3 2 2 20.328 40.656 0.225 13.92 8 52.7 37.9 59 2 1 4 20.486 40.972 0.227 13.68 8 19.0 4.8 60 6 1 2 20.621 41.242 0.229 13.48 8 22.1 6.5 61 5 1 3 21.019 42.039 0.233 12.92 8 7.1 0.6 62 4 0 4 21.166 42.332 0.234 12.72 4 22.0 3.0 63 1 2 3 21.31 42.621 0.236 12.53 8 66.7 54.6 64 3 1 4 21.454 42.907 0.237 12.34 8 38.6 18.0 65 7 0 2 21.488 42.976 0.238 12.3 4 12.6 1.0 66 6 0 3 21.497 42.994 0.238 12.29 4 109.9 72.5 67 7 1 1 21.616 43.232 0.239 12.13 8 4.7 0.3 68 4 2 2 21.681 43.362 0.24 12.05 8 13.6 2.2 69 2 2 3 21.877 43.755 0.242 11.81 8 127.8 188.6 70 5 2 1 21.901 43.801 0.242 11.78 8 123.5 175.9 71 8 0 0 22.34 44.68 0.247 11.27 2 193.7 103.3 72 1 0 5 22.749 45.497 0.251 10.81 4 0.1 0.0 73 4 1 4 22.752 45.504 0.251 10.81 8 41.1 17.9 74 3 2 3 22.797 45.595 0.252 10.76 8 39.3 16.3 75 8 0 1 22.816 45.632 0.252 10.74 4 92.2 44.6 76 5 0 4 22.842 45.684 0.252 10.72 4 102.1 54.7 77 7 1 2 23.056 46.113 0.254 10.49 8 57.3 33.7 78 6 1 3 23.065 46.13 0.254 10.48 8 10.1 1.0 79 2 0 5 23.288 46.575 0.257 10.26 4 98.2 48.4 80 5 2 2 23.327 46.654 0.257 10.22 8 107.1 114.6 81 6 2 0 23.427 46.854 0.258 10.12 4 20.4 2.1 82 7 0 3 23.861 47.722 0.263 9.71 4 35.9 6.1 83 8 1 0 23.864 47.729 0.263 9.7 4 75.1 26.7 84 6 2 1 23.886 47.772 0.263 9.68 8 15.0 2.1 85 4 2 3 24.039 48.077 0.264 9.54 8 2.6 0.1 86 0 1 5 24.08 48.16 0.265 9.51 4 17.8 1.5 87 3 0 5 24.166 48.331 0.266 9.43 4 40.1 7.4 88 8 0 2 24.2 48.401 0.266 9.4 4 86.0 34.0 89 1 1 5 24.253 48.506 0.267 9.35 8 24.9 5.7 90 8 1 1 24.317 48.634 0.267 9.3 8 25.3 5.8 91 5 1 4 24.342 48.683 0.268 9.28 8 57.1 29.6 92 0 2 4 24.43 48.861 0.268 9.2 4 48.0 10.4 93 1 2 4 24.602 49.203 0.27 9.06 8 142.5 179.9 94 2 1 5 24.767 49.534 0.272 8.92 8 65.9 37.9 95 6 0 4 24.769 49.537 0.272 8.92 4 22.4 2.2 96 0 3 1 25.006 50.013 0.274 8.73 4 20.7 1.8 97 2 2 4 25.11 50.221 0.275 8.64 8 34.9 10.3 98 1 3 1 25.175 50.35 0.276 8.59 8 13.3 1.5 99 6 2 2 25.226 50.451 0.277 8.55 8 24.9 5.2 100 2 3 0 25.24 50.481 0.277 8.54 4 22.0 2.0 101 7 1 3 25.315 50.63 0.278 8.49 8 24.8 5.1 102 4 0 5 25.356 50.712 0.278 8.45 4 27.8 3.2 103 5 2 3 25.567 51.135 0.28 8.3 8 26.3 5.6 104 3 1 5 25.607 51.213 0.281 8.27 8 6.3 0.3 105 8 1 2 25.64 51.28 0.281 8.24 8 10.7 0.9 106 2 3 1 25.675 51.35 0.281 8.22 8 4.2 0.1 107 9 0 1 25.75 51.501 0.282 8.16 4 8.9 0.3 108 3 2 4 25.942 51.884 0.284 8.03 8 52.5 21.6 109 7 2 1 26.083 52.165 0.285 7.93 8 8.2 0.5 110 6 1 4 26.185 52.37 0.286 7.86 8 49.7 19.0 111 8 0 3 26.385 52.771 0.288 7.72 4 3.9 0.1 112 1 3 2 26.466 52.932 0.289 7.67 8 16.8 2.1 113 3 3 1 26.494 52.988 0.29 7.65 8 63.0 29.7 114 4 1 5 26.75 53.5 0.292 7.48 8 77.5 44.0 115 5 0 5 26.83 53.659 0.293 7.43 4 12.5 0.6 116 7 0 4 26.912 53.825 0.294 7.38 4 32.8 3.9 117 2 3 2 26.949 53.899 0.294 7.36 8 1.2 0.0 118 9 0 2 27.022 54.044 0.295 7.31 4 69.0 17.0 119 4 2 4 27.075 54.151 0.295 7.28 8 35.2 8.8 120 9 1 1 27.13 54.26 0.296 7.25 8 95.4 64.5 121 4 3 0 27.199 54.397 0.297 7.21 4 7.8 0.2 122 7 2 2 27.344 54.687 0.298 7.12 8 79.9 44.5 123 6 2 3 27.351 54.702 0.298 7.11 8 29.5 6.1 124 0 0 6 27.42 54.84 0.299 7.07 2 98.3 16.7 125 1 0 6 27.578 55.156 0.301 6.98 4 95.0 30.8 126 4 3 1 27.612 55.223 0.301 6.96 8 27.3 5.1 127 3 3 2 27.742 55.484 0.302 6.89 8 18.5 2.3 128 8 1 3 27.743 55.486 0.302 6.89 8 14.3 1.4 129 2 0 6 28.048 56.096 0.305 6.72 4 36.1 4.3 130 8 2 0 28.06 56.121 0.305 6.71 4 91.3 27.3 131 5 1 5 28.173 56.345 0.306 6.65 8 102.1 67.9 132 7 1 4 28.253 56.505 0.307 6.61 8 14.7 1.4 133 9 1 2 28.359 56.718 0.308 6.55 8 105.8 71.8 134 10 0 0 28.368 56.736 0.308 6.55 2 74.5 8.9 135 0 3 3 28.373 56.745 0.308 6.55 4 175.7 98.8 136 1 2 5 28.408 56.815 0.309 6.53 8 18.0 2.1 137 8 2 1 28.465 56.93 0.309 6.5 8 20.1 2.6 138 5 2 4 28.487 56.974 0.31 6.49 8 178.3 201.6 139 1 3 3 28.527 57.054 0.31 6.47 8 63.3 25.4 140 6 0 5 28.559 57.117 0.31 6.45 4 78.7 19.5 141 10 0 1 28.77 57.539 0.312 6.34 4 3.1 0.0 142 3 0 6 28.82 57.641 0.313 6.32 4 220.0 149.5 143 4 3 2 28.827 57.654 0.313 6.32 8 20.3 2.6 144 2 2 5 28.869 57.738 0.313 6.29 8 8.4 0.4 145 1 1 6 28.898 57.795 0.314 6.28 8 31.5 6.1 146 2 3 3 28.987 57.974 0.315 6.24 8 47.1 13.5 147 5 3 1 29.006 58.012 0.315 6.23 8 123.1 92.3 148 9 0 3 29.056 58.112 0.315 6.2 4 5.3 0.1 149 8 0 4 29.249 58.497 0.317 6.11 4 43.8 5.7 150 2 1 6 29.354 58.708 0.318 6.06 8 30.7 5.6 151 7 2 3 29.363 58.726 0.318 6.06 8 10.7 0.7 152 3 2 5 29.627 59.255 0.321 5.94 8 32.6 6.2 153 8 2 2 29.658 59.315 0.321 5.92 8 56.7 18.6 154 10 1 0 29.665 59.329 0.321 5.92 4 142.2 58.5 155 3 3 3 29.744 59.487 0.322 5.89 8 72.1 29.9 156 6 1 5 29.85 59.701 0.323 5.84 8 72.5 30.0 157 4 0 6 29.88 59.76 0.323 5.83 4 130.0 48.1 158 10 0 2 29.954 59.909 0.324 5.79 4 16.9 0.8 159 10 1 1 30.055 60.111 0.325 5.75 8 105.2 62.2 160 3 1 6 30.105 60.21 0.326 5.73 8 18.2 1.9 161 6 2 4 30.153 60.307 0.326 5.71 8 4.1 0.1 162 5 3 2 30.185 60.37 0.326 5.69 8 35.8 7.1 163 6 3 0 30.269 60.537 0.327 5.66 4 16.5 0.8 164 9 1 3 30.335 60.669 0.328 5.63 8 19.8 2.2 165 7 0 5 30.519 61.038 0.33 5.56 4 19.0 1.0 166 8 1 4 30.522 61.044 0.33 5.56 8 42.7 9.9 167 6 3 1 30.655 61.31 0.331 5.5 8 41.9 9.5 168 4 2 5 30.67 61.34 0.331 5.5 8 40.0 8.6 169 4 3 3 30.784 61.567 0.332 5.45 8 65.5 22.9 170 9 2 1 31.018 62.037 0.334 5.36 8 41.6 9.1 171 4 1 6 31.138 62.275 0.336 5.32 8 18.8 1.8 172 5 0 6 31.21 62.42 0.336 5.29 4 40.1 4.2 173 10 1 2 31.21 62.421 0.336 5.29 8 31.1 5.0 174 1 3 4 31.262 62.524 0.337 5.27 8 20.3 2.1 175 8 2 3 31.583 63.166 0.34 5.15 8 0.9 0.0 176 2 3 4 31.698 63.395 0.341 5.11 8 8.7 0.4 177 7 1 5 31.762 63.524 0.342 5.09 8 62.9 19.7 178 9 0 4 31.763 63.527 0.342 5.09 4 128.0 40.8 179 6 3 2 31.797 63.594 0.342 5.08 8 14.2 1.0 180 10 0 3 31.869 63.738 0.343 5.05 4 103.4 26.4 181 11 0 1 31.887 63.774 0.343 5.04 4 22.2 1.2 182 5 2 5 31.98 63.961 0.344 5.01 8 39.4 7.6 183 7 2 4 32.055 64.109 0.345 4.99 8 160.7 126.0 184 5 3 3 32.092 64.184 0.345 4.97 8 0.4 0.0 185 9 2 2 32.153 64.306 0.345 4.95 8 101.2 49.7 186 3 3 4 32.417 64.833 0.348 4.87 8 29.4 4.1 187 5 1 6 32.438 64.876 0.348 4.86 8 33.1 5.2 188 0 2 6 32.511 65.023 0.349 4.84 4 98.9 23.2 189 7 3 1 32.539 65.078 0.349 4.83 8 16.2 1.2 190 1 0 7 32.64 65.28 0.35 4.8 4 29.4 2.0 191 1 2 6 32.654 65.308 0.35 4.79 8 138.9 90.3 192 8 0 5 32.693 65.386 0.351 4.78 4 36.4 3.1 193 6 0 6 32.793 65.586 0.352 4.75 4 3.6 0.0 194 9 1 4 32.98 65.96 0.353 4.69 8 13.9 0.9 195 11 0 2 33.005 66.011 0.354 4.68 4 79.0 14.3 196 2 0 7 33.066 66.131 0.354 4.66 4 39.0 3.5 197 2 2 6 33.079 66.159 0.354 4.66 8 47.9 10.5 198 10 1 3 33.084 66.167 0.354 4.66 8 22.4 2.3 199 11 1 1 33.101 66.202 0.354 4.65 8 10.2 0.5 200 10 2 0 33.37 66.74 0.357 4.57 4 65.7 9.7 201 4 3 4 33.409 66.818 0.357 4.56 8 36.1 5.8 202 6 2 5 33.544 67.088 0.359 4.53 8 1.9 0.0 203 7 3 2 33.646 67.292 0.36 4.5 8 38.3 6.5 204 6 3 3 33.653 67.305 0.36 4.49 8 7.7 0.3 205 0 4 0 33.66 67.319 0.36 4.49 2 446.5 218.9 206 0 1 7 33.7 67.4 0.36 4.48 4 65.4 9.4 207 10 2 1 33.736 67.473 0.361 4.47 8 14.7 0.9 208 3 0 7 33.769 67.538 0.361 4.46 4 45.9 4.6 209 3 2 6 33.783 67.566 0.361 4.46 8 66.9 19.5 210 1 1 7 33.84 67.68 0.361 4.44 8 17.3 1.3 211 8 1 5 33.892 67.784 0.362 4.43 8 45.8 9.1 212 6 1 6 33.99 67.981 0.363 4.4 8 2.6 0.0 213 9 2 3 33.999 67.997 0.363 4.4 8 40.1 6.9 214 1 4 1 34.164 68.328 0.365 4.36 8 1.9 0.0 215 8 2 4 34.175 68.35 0.365 4.35 8 46.4 9.2 216 11 1 2 34.199 68.398 0.365 4.35 8 44.6 8.5 217 2 4 0 34.218 68.436 0.365 4.34 4 23.1 1.1 218 2 1 7 34.258 68.516 0.365 4.33 8 51.2 11.1 219 8 3 0 34.283 68.565 0.366 4.32 4 55.9 6.6 220 10 0 4 34.45 68.9 0.367 4.28 4 36.8 2.8 221 0 3 5 34.454 68.909 0.367 4.28 4 12.1 0.3 222 2 4 1 34.58 69.16 0.368 4.25 8 0.9 0.0 223 1 3 5 34.593 69.186 0.369 4.24 8 24.0 2.4 224 7 0 6 34.615 69.229 0.369 4.24 4 5.2 0.1 225 8 3 1 34.644 69.289 0.369 4.23 8 15.9 1.0 226 5 3 4 34.664 69.328 0.369 4.23 8 57.0 13.4 227 4 0 7 34.742 69.485 0.37 4.21 4 13.0 0.3 228 4 2 6 34.756 69.511 0.37 4.2 8 6.2 0.2 229 12 0 0 34.761 69.522 0.37 4.2 2 70.3 5.1 230 10 2 2 34.824 69.649 0.371 4.19 8 186.8 142.9 231 11 0 3 34.828 69.656 0.371 4.19 4 47.2 4.6 232 3 1 7 34.95 69.9 0.372 4.16 8 17.8 1.3 233 2 3 5 35.007 70.014 0.372 4.14 8 56.8 13.1 234 9 0 5 35.069 70.139 0.373 4.13 4 74.2 11.1 235 0 4 2 35.108 70.216 0.373 4.12 4 56.2 6.4 236 12 0 1 35.121 70.241 0.373 4.12 4 32.2 2.1 237 1 4 2 35.246 70.491 0.375 4.09 8 15.1 0.9 238 3 4 1 35.269 70.538 0.375 4.08 8 6.5 0.2 239 7 2 5 35.347 70.693 0.376 4.06 8 8.0 0.3 240 7 3 3 35.453 70.905 0.377 4.04 8 23.5 2.2 241 10 1 4 35.62 71.24 0.378 4.0 8 20.2 1.6 242 2 4 2 35.656 71.312 0.378 3.99 8 19.7 1.5 243 3 3 5 35.692 71.384 0.379 3.99 8 2.8 0.0 244 8 3 2 35.72 71.439 0.379 3.98 8 4.9 0.1 245 7 1 6 35.783 71.565 0.38 3.97 8 44.1 7.6 246 4 4 0 35.869 71.738 0.38 3.95 4 51.7 5.2 247 4 1 7 35.908 71.817 0.381 3.94 8 6.2 0.1 248 12 1 0 35.927 71.854 0.381 3.93 4 0.6 0.0 249 5 0 7 35.976 71.951 0.381 3.92 4 46.3 4.1 250 5 2 6 35.989 71.978 0.381 3.92 8 74.3 21.1 251 11 1 3 35.993 71.986 0.381 3.92 8 0.7 0.0 252 6 3 4 36.17 72.341 0.383 3.88 8 45.1 7.7 253 12 0 2 36.19 72.379 0.383 3.88 4 44.8 3.8 254 4 4 1 36.224 72.448 0.384 3.87 8 31.8 3.8 255 9 1 5 36.231 72.461 0.384 3.87 8 13.7 0.7 256 12 1 1 36.281 72.563 0.384 3.86 8 30.7 3.6 257 3 4 2 36.336 72.672 0.385 3.85 8 38.5 5.6 258 9 2 4 36.506 73.011 0.386 3.82 8 5.1 0.1 259 10 2 3 36.605 73.21 0.387 3.8 8 143.2 76.1 260 11 2 1 36.622 73.243 0.387 3.79 8 84.1 26.2 261 4 3 5 36.642 73.285 0.387 3.79 8 63.7 15.0 262 8 0 6 36.664 73.327 0.388 3.78 4 45.4 3.8 263 9 3 1 36.962 73.924 0.39 3.73 8 83.5 25.4 264 1 4 3 37.018 74.035 0.391 3.72 8 5.2 0.1 265 5 1 7 37.125 74.251 0.392 3.7 8 62.7 14.2 266 4 4 2 37.28 74.56 0.393 3.67 8 49.6 8.8 267 11 0 4 37.311 74.622 0.393 3.66 4 84.3 12.7 268 1 2 7 37.329 74.658 0.394 3.66 8 55.2 10.9 269 12 1 2 37.337 74.674 0.394 3.66 8 19.6 1.4 270 8 2 5 37.379 74.758 0.394 3.65 8 124.2 55.1 271 2 4 3 37.42 74.841 0.394 3.64 8 34.9 4.3 272 5 4 1 37.437 74.874 0.395 3.64 8 59.1 12.5 273 6 0 7 37.46 74.92 0.395 3.64 4 18.8 0.6 274 6 2 6 37.473 74.946 0.395 3.63 8 52.9 9.9 275 8 3 3 37.483 74.965 0.395 3.63 8 0.1 0.0 276 10 0 5 37.644 75.288 0.396 3.6 4 71.5 9.0 277 11 2 2 37.674 75.347 0.397 3.6 8 14.4 0.7 278 2 2 7 37.731 75.461 0.397 3.59 8 20.5 1.5 279 8 1 6 37.806 75.611 0.398 3.58 8 27.6 2.7 280 5 3 5 37.85 75.701 0.398 3.57 8 83.0 24.0 281 0 0 8 37.88 75.761 0.399 3.56 2 152.9 20.4 282 7 3 4 37.919 75.838 0.399 3.56 8 15.2 0.8 283 12 0 3 37.944 75.888 0.399 3.55 4 49.3 4.2 284 9 3 2 38.011 76.021 0.4 3.54 8 94.9 31.2 285 1 0 8 38.014 76.027 0.4 3.54 4 18.4 0.6 286 3 4 3 38.088 76.177 0.4 3.53 8 12.3 0.5 287 3 2 7 38.397 76.793 0.403 3.48 8 20.9 1.5 288 2 0 8 38.413 76.826 0.403 3.48 4 115.6 22.7 289 11 1 4 38.446 76.892 0.404 3.47 8 46.1 7.2 290 1 3 6 38.477 76.953 0.404 3.47 8 27.2 2.5 291 5 4 2 38.481 76.962 0.404 3.47 8 113.8 43.9 292 13 0 1 38.493 76.986 0.404 3.47 4 13.2 0.3 293 6 4 0 38.556 77.111 0.405 3.46 4 118.3 23.6 294 6 1 7 38.594 77.188 0.405 3.45 8 73.1 18.0 295 10 1 5 38.776 77.551 0.407 3.42 8 47.0 7.4 296 2 3 6 38.874 77.749 0.407 3.41 8 14.3 0.7 297 6 4 1 38.901 77.803 0.408 3.4 8 23.7 1.9 298 9 0 6 38.934 77.869 0.408 3.4 4 63.4 6.7 299 4 4 3 39.017 78.035 0.409 3.39 8 1.2 0.0 300 10 2 4 39.044 78.089 0.409 3.38 8 74.3 18.3 301 12 1 3 39.073 78.146 0.409 3.38 8 8.8 0.3 302 3 0 8 39.075 78.151 0.409 3.38 4 23.2 0.9 303 1 1 8 39.142 78.284 0.41 3.37 8 11.0 0.4 304 10 3 0 39.147 78.293 0.41 3.37 4 126.3 26.3 305 7 0 7 39.189 78.377 0.41 3.36 4 29.8 1.5 306 7 2 6 39.201 78.403 0.41 3.36 8 50.4 8.4 307 6 3 5 39.31 78.62 0.411 3.35 8 73.8 17.8 308 0 4 4 39.317 78.633 0.411 3.34 4 34.9 2.0 309 4 2 7 39.323 78.647 0.411 3.34 8 7.6 0.2 310 12 2 0 39.341 78.683 0.411 3.34 4 3.5 0.0 311 11 2 3 39.405 78.811 0.412 3.33 8 75.8 18.7 312 1 4 4 39.448 78.897 0.412 3.33 8 55.3 10.0 313 10 3 1 39.491 78.982 0.413 3.32 8 103.2 34.6 314 13 0 2 39.528 79.056 0.413 3.32 4 22.9 0.8 315 3 3 6 39.535 79.069 0.413 3.32 8 15.3 0.8 316 2 1 8 39.538 79.076 0.413 3.31 8 18.6 1.1 317 13 1 1 39.617 79.235 0.414 3.3 8 17.4 1.0 318 9 2 5 39.636 79.272 0.414 3.3 8 92.8 27.8 319 12 2 1 39.685 79.37 0.415 3.3 8 13.1 0.6 320 9 3 3 39.738 79.476 0.415 3.29 8 12.0 0.5 321 2 4 4 39.843 79.687 0.416 3.27 8 42.4 5.8 322 8 3 4 39.904 79.809 0.416 3.27 8 30.4 3.0 323 6 4 2 39.934 79.867 0.417 3.26 8 48.3 7.4 324 4 0 8 39.997 79.995 0.417 3.26 4 30.7 1.5 325 9 1 6 40.055 80.11 0.418 3.25 8 29.6 2.8 326 3 1 8 40.195 80.39 0.419 3.23 8 12.8 0.5 327 5 4 3 40.202 80.405 0.419 3.23 8 14.5 0.7 328 7 1 7 40.308 80.615 0.42 3.22 8 59.2 11.0 329 12 0 4 40.358 80.715 0.42 3.21 4 34.3 1.8 330 11 0 5 40.421 80.843 0.421 3.2 4 15.9 0.4 331 4 3 6 40.454 80.908 0.421 3.2 8 13.5 0.6 332 3 4 4 40.499 80.999 0.422 3.19 8 13.9 0.6 333 5 2 7 40.506 81.012 0.422 3.19 8 116.9 42.7 334 10 3 2 40.519 81.038 0.422 3.19 8 23.4 1.7 335 7 4 1 40.612 81.223 0.423 3.18 8 36.5 4.2 336 13 1 2 40.645 81.289 0.423 3.18 8 15.8 0.8 337 12 2 2 40.712 81.424 0.423 3.17 8 4.5 0.1 338 7 3 5 41.016 82.032 0.426 3.14 8 53.8 8.9 339 4 1 8 41.111 82.222 0.427 3.13 8 3.5 0.0 340 8 0 7 41.157 82.314 0.427 3.12 4 33.7 1.7 341 8 2 6 41.17 82.34 0.427 3.12 8 10.7 0.4 342 5 0 8 41.176 82.351 0.427 3.12 4 51.8 4.1 343 13 0 3 41.238 82.476 0.428 3.11 4 40.6 2.5 344 4 4 4 41.414 82.828 0.429 3.09 8 15.5 0.7 345 10 0 6 41.428 82.856 0.43 3.09 4 12.7 0.2 346 12 1 4 41.469 82.938 0.43 3.09 8 10.5 0.3 347 11 1 5 41.532 83.065 0.43 3.08 8 40.3 4.9 348 5 3 6 41.629 83.259 0.431 3.07 8 23.3 1.6 349 7 4 2 41.634 83.267 0.431 3.07 8 4.1 0.1 350 6 4 3 41.64 83.28 0.431 3.07 8 59.2 10.5 351 14 0 0 41.696 83.392 0.432 3.07 2 7.8 0.0 352 11 2 4 41.797 83.593 0.433 3.06 8 7.2 0.2 353 6 2 7 41.941 83.883 0.434 3.04 8 58.0 10.0 354 14 0 1 42.036 84.072 0.435 3.03 4 18.5 0.5 355 10 2 5 42.12 84.24 0.435 3.03 8 5.3 0.1 356 9 3 4 42.125 84.25 0.435 3.03 8 20.8 1.3 357 10 3 3 42.221 84.441 0.436 3.02 8 21.4 1.4 358 8 4 0 42.227 84.454 0.436 3.02 4 118.6 20.7 359 11 3 1 42.237 84.474 0.436 3.02 8 3.5 0.0 360 8 1 7 42.265 84.529 0.437 3.01 8 54.0 8.6 361 5 1 8 42.283 84.566 0.437 3.01 8 11.0 0.4 362 13 1 3 42.345 84.69 0.437 3.01 8 9.1 0.2 363 0 2 8 42.35 84.7 0.437 3.01 4 62.7 5.8 364 12 2 3 42.412 84.824 0.438 3.0 8 52.4 8.1 365 1 2 8 42.48 84.96 0.438 3.0 8 0.5 0.0 366 1 4 5 42.518 85.035 0.439 2.99 8 0.6 0.0 367 10 1 6 42.534 85.069 0.439 2.99 8 63.3 11.7 368 8 4 1 42.566 85.132 0.439 2.99 8 54.7 8.8 369 5 4 4 42.585 85.169 0.439 2.99 8 63.8 11.9 370 6 0 8 42.607 85.214 0.439 2.99 4 60.7 5.4 371 0 3 7 42.789 85.578 0.441 2.97 4 59.7 5.2 372 14 1 0 42.801 85.603 0.441 2.97 4 145.8 30.9 373 2 2 8 42.869 85.738 0.442 2.96 8 27.3 2.2 374 2 4 5 42.907 85.814 0.442 2.96 8 60.8 10.7 375 1 3 7 42.919 85.838 0.442 2.96 8 8.6 0.2 376 13 2 1 42.947 85.895 0.442 2.96 8 2.9 0.0 377 8 3 5 42.967 85.934 0.442 2.96 8 40.8 4.8 378 14 0 2 43.052 86.104 0.443 2.95 4 28.5 1.2 379 6 3 6 43.058 86.117 0.443 2.95 8 6.4 0.1 380 14 1 1 43.14 86.28 0.444 2.94 8 20.7 1.2 381 11 3 2 43.253 86.505 0.445 2.94 8 43.5 5.4 382 2 3 7 43.308 86.615 0.445 2.93 8 48.2 6.7 383 7 4 3 43.328 86.656 0.445 2.93 8 17.1 0.8 384 9 0 7 43.367 86.733 0.446 2.93 4 59.4 5.0 385 9 2 6 43.379 86.758 0.446 2.93 8 9.9 0.3 386 12 0 5 43.415 86.83 0.446 2.92 4 72.9 7.6 387 3 2 8 43.517 87.034 0.447 2.92 8 23.7 1.6 388 3 4 5 43.555 87.11 0.447 2.91 8 27.9 2.2 389 8 4 2 43.581 87.162 0.447 2.91 8 58.5 9.7 390 13 0 4 43.611 87.222 0.448 2.91 4 14.2 0.3 391 7 2 7 43.628 87.256 0.448 2.91 8 8.8 0.2 392 6 1 8 43.709 87.419 0.449 2.9 8 77.5 17.0 393 1 0 9 43.82 87.64 0.449 2.9 4 24.6 0.9 394 3 3 7 43.955 87.91 0.451 2.89 8 22.5 1.4 395 13 2 2 43.961 87.923 0.451 2.89 8 18.4 1.0 396 6 4 4 44.01 88.02 0.451 2.88 8 13.7 0.5 397 11 0 6 44.153 88.307 0.452 2.87 4 35.8 1.8 398 14 1 2 44.154 88.307 0.452 2.87 8 27.9 2.2 399 0 5 1 44.192 88.383 0.452 2.87 4 4.0 0.0 400 2 0 9 44.208 88.417 0.453 2.87 4 45.2 2.9 401 7 0 8 44.291 88.582 0.453 2.87 4 49.7 3.5 402 1 5 1 44.321 88.642 0.454 2.86 8 23.4 1.5 403 2 5 0 44.372 88.743 0.454 2.86 4 14.4 0.3 404 4 2 8 44.423 88.846 0.454 2.86 8 102.4 29.3 405 4 4 5 44.461 88.922 0.455 2.86 8 11.1 0.3 406 9 1 7 44.467 88.935 0.455 2.86 8 88.1 21.7 407 12 1 5 44.516 89.031 0.455 2.85 8 25.3 1.8 408 10 3 4 44.588 89.175 0.456 2.85 8 15.2 0.6 409 2 5 1 44.709 89.418 0.457 2.84 8 8.1 0.2 410 13 1 4 44.712 89.423 0.457 2.84 8 2.0 0.0 411 14 0 3 44.741 89.482 0.457 2.84 4 90.4 11.4 412 7 3 6 44.741 89.483 0.457 2.84 8 36.7 3.7 413 9 4 1 44.768 89.536 0.457 2.84 8 17.3 0.8 414 12 2 4 44.778 89.557 0.457 2.84 8 8.5 0.2 415 0 1 9 44.791 89.583 0.457 2.84 4 7.8 0.1 416 11 2 5 44.841 89.682 0.458 2.84 8 43.5 5.2 417 3 0 9 44.855 89.711 0.458 2.84 4 34.8 1.7 418 4 3 7 44.861 89.722 0.458 2.84 8 2.8 0.0 419 12 3 0 44.878 89.757 0.458 2.83 4 2.7 0.0 420 1 1 9 44.921 89.841 0.458 2.83 8 95.0 25.0 421 11 3 3 44.941 89.882 0.459 2.83 8 4.7 0.1 X-ray diffraction powder data (I)...X-Ray wave length = 1.54056 (angs.): No H K L Theta 2*Theta d I int I int.n. I p.h.n. H(Si) ( degree ) (angstrem) *100 *100 1 2 0 0 5.453 10.906 8.106 120.7 15.8 16.0 5.6 2 0 0 2 8.83 17.66 5.018 196.9 25.8 26.1 5.6 3 0 1 1 9.114 18.228 4.86284 10.2 1.3 1.4 5.6 4 1 0 2 9.247 18.494 4.79362 20.4 2.7 2.7 5.6 5 1 1 1 9.519 19.038 4.65782 58.2 7.6 7.7 5.6 6 2 0 2 10.401 20.802 4.26663 25.1 3.3 3.3 5.6 7 4 0 0 10.956 21.912 4.053 100.5 13.2 13.3 5.6 8 4 0 1 11.827 23.655 3.75811 60.6 7.9 8.0 5.6 9 3 0 2 12.092 24.183 3.67716 90.4 11.9 11.9 5.6 10 1 1 2 12.25 24.5 3.63029 8.6 1.1 1.1 5.6 11 3 1 1 12.304 24.607 3.61477 212.4 27.9 28.0 5.6 12 4 0 2 14.141 28.281 3.153 86.6 11.4 11.4 5.6 13 4 1 1 14.324 28.648 3.1134 32.1 4.2 4.2 5.6 14 2 0 3 14.424 28.848 3.09234 69.9 9.2 9.2 5.6 15 5 0 1 14.457 28.914 3.08537 122.0 16.0 16.0 5.6 16 0 1 3 15.589 31.178 2.86634 762.7 100.0 100.0 5.6 17 1 1 3 15.837 31.674 2.82256 130.4 17.1 17.1 5.6 18 0 2 0 16.089 32.178 2.7795 314.1 41.2 41.1 5.6 19 5 0 2 16.43 32.86 2.72335 251.0 32.9 32.9 5.6 20 5 1 1 16.591 33.181 2.69771 760.7 99.7 99.6 5.6 21 1 2 1 16.945 33.891 2.64283 19.4 2.5 2.5 5.7 22 2 2 0 17.036 34.071 2.62923 138.3 18.1 18.1 5.7 23 6 0 1 17.171 34.343 2.60909 10.8 1.4 1.4 5.7 24 2 2 1 17.629 35.258 2.54339 7.8 1.0 1.0 5.7 25 3 1 3 17.71 35.42 2.53219 164.3 21.5 21.5 5.7 26 0 0 4 17.879 35.758 2.509 12.1 1.6 1.6 5.7 27 1 0 4 18.099 36.198 2.47948 46.7 6.1 6.1 5.7 28 5 1 2 18.358 36.717 2.44564 10.8 1.4 1.4 5.7 29 0 2 2 18.47 36.939 2.43142 61.2 8.0 8.0 5.7 30 1 2 2 18.684 37.368 2.40453 196.6 25.8 25.6 5.7 31 2 0 4 18.746 37.492 2.39681 34.3 4.5 4.5 5.7 32 6 0 2 18.892 37.783 2.37903 9.9 1.3 1.3 5.7 33 6 1 1 19.034 38.068 2.36189 30.7 4.0 4.0 5.7 34 4 1 3 19.217 38.434 2.34024 133.8 17.5 17.4 5.7 35 2 2 2 19.314 38.628 2.32891 215.5 28.3 28.1 5.7 36 1 1 4 19.887 39.774 2.26445 28.0 3.7 3.6 5.7 37 7 0 1 19.958 39.916 2.25669 37.6 4.9 4.9 5.7 38 4 2 1 20.163 40.326 2.23471 99.8 13.1 13.0 5.7 39 3 2 2 20.328 40.656 2.21732 37.9 5.0 4.9 5.7 40 1 2 3 21.31 42.621 2.11952 54.6 7.2 7.1 5.7 41 3 1 4 21.454 42.907 2.10605 18.0 2.4 2.3 5.7 42 6 0 3 21.497 42.994 2.102 72.5 9.5 9.4 5.7 43 2 2 3 21.877 43.755 2.06718 364.5 47.8 47.2 5.7 44 8 0 0 22.34 44.68 2.0265 103.3 13.5 13.4 5.7 45 4 1 4 22.752 45.504 1.99169 17.9 2.3 2.3 5.7 46 8 0 1 22.816 45.632 1.98641 115.5 15.2 14.9 5.7 47 7 1 2 23.056 46.113 1.96682 34.7 4.6 4.5 5.7 48 2 0 5 23.288 46.575 1.94836 48.4 6.3 6.2 5.7 49 5 2 2 23.327 46.654 1.94525 114.6 15.0 14.8 5.7 50 8 1 0 23.864 47.729 1.90394 35.0 4.6 4.5 5.7 51 8 0 2 24.2 48.401 1.87906 34.0 4.5 4.4 5.7 52 5 1 4 24.342 48.683 1.86881 35.4 4.6 4.6 5.7 53 0 2 4 24.43 48.861 1.86244 10.4 1.4 1.3 5.7 54 1 2 4 24.602 49.203 1.85027 179.9 23.6 23.2 5.7 55 2 1 5 24.767 49.534 1.83869 40.0 5.3 5.2 5.7 56 2 2 4 25.11 50.221 1.81515 10.3 1.4 1.3 5.8 57 3 2 4 25.942 51.884 1.7608 21.6 2.8 2.8 5.8 58 6 1 4 26.185 52.37 1.74558 19.0 2.5 2.4 5.8 59 3 3 1 26.494 52.988 1.72668 31.9 4.2 4.1 5.8 60 4 1 5 26.75 53.5 1.71135 44.0 5.8 5.6 5.8 61 9 0 2 27.022 54.044 1.69541 17.0 2.2 2.2 5.8 62 4 2 4 27.075 54.151 1.69232 8.8 1.2 1.1 5.8 63 9 1 1 27.13 54.26 1.68917 64.5 8.5 8.2 5.8 64 7 2 2 27.344 54.687 1.67698 50.5 6.6 6.5 5.8 65 0 0 6 27.42 54.84 1.67267 16.7 2.2 2.1 5.8 66 1 0 6 27.578 55.156 1.66383 30.8 4.0 3.9 5.8 67 8 2 0 28.06 56.121 1.63749 31.6 4.1 4.0 5.8 68 5 1 5 28.173 56.345 1.6315 67.9 8.9 8.7 5.8 69 0 3 3 28.373 56.745 1.62095 179.4 23.5 22.9 5.8 70 5 2 4 28.487 56.974 1.61498 204.1 26.8 26.0 5.8 71 1 3 3 28.527 57.054 1.61291 25.4 3.3 3.2 5.8 72 6 0 5 28.559 57.117 1.61127 19.5 2.6 2.5 5.8 73 3 0 6 28.82 57.641 1.59787 152.1 19.9 19.4 5.8 74 5 3 1 29.006 58.012 1.58853 105.8 13.9 13.5 5.8 75 10 1 0 29.665 59.329 1.55637 77.1 10.1 9.8 5.8 76 3 3 3 29.744 59.487 1.55261 29.9 3.9 3.8 5.8 77 6 1 5 29.85 59.701 1.54757 30.0 3.9 3.8 5.8 78 4 0 6 29.88 59.76 1.54617 48.1 6.3 6.1 5.8 79 10 1 1 30.055 60.111 1.53798 62.2 8.2 7.9 5.8 80 8 1 4 30.522 61.044 1.51669 9.9 1.3 1.3 5.8 81 6 3 1 30.655 61.31 1.51076 18.1 2.4 2.3 5.8 82 4 3 3 30.784 61.567 1.50504 22.9 3.0 2.9 5.8 83 9 2 1 31.018 62.037 1.49478 9.1 1.2 1.1 5.8 84 10 1 2 31.21 62.421 1.48651 9.1 1.2 1.2 5.8 85 9 0 4 31.763 63.527 1.46327 60.4 7.9 7.6 5.9 86 10 0 3 31.869 63.738 1.45891 27.6 3.6 3.5 5.9 87 7 2 4 32.055 64.109 1.45137 126.0 16.5 15.9 5.9 88 9 2 2 32.153 64.306 1.44739 49.7 6.5 6.3 5.9 89 5 1 6 32.438 64.876 1.43606 9.3 1.2 1.2 5.9 90 0 2 6 32.511 65.023 1.43317 24.4 3.2 3.1 5.9 91 1 2 6 32.654 65.308 1.4276 92.4 12.1 11.6 5.9 92 11 0 2 33.005 66.011 1.41409 14.3 1.9 1.8 5.9 93 2 2 6 33.079 66.159 1.41128 16.2 2.1 2.0 5.9 94 10 2 0 33.37 66.74 1.4004 9.7 1.3 1.2 5.9 95 0 4 0 33.66 67.319 1.38975 225.6 29.6 28.3 5.9 96 0 1 7 33.7 67.4 1.38829 9.4 1.2 1.2 5.9 97 3 2 6 33.783 67.566 1.38528 24.1 3.2 3.0 5.9 98 8 1 5 33.892 67.784 1.38135 9.1 1.2 1.1 5.9 99 8 2 4 34.175 68.35 1.37128 17.6 2.3 2.2 5.9 100 2 1 7 34.258 68.516 1.36836 17.7 2.3 2.2 5.9 101 5 3 4 34.664 69.328 1.35431 14.5 1.9 1.8 5.9 102 10 2 2 34.824 69.649 1.34886 147.5 19.3 18.4 5.9 103 2 3 5 35.007 70.014 1.34271 13.1 1.7 1.6 5.9 104 9 0 5 35.069 70.139 1.34063 11.1 1.5 1.4 5.9 105 0 4 2 35.108 70.216 1.33933 8.4 1.1 1.1 5.9 106 5 2 6 35.989 71.978 1.31083 25.3 3.3 3.1 5.9 107 6 3 4 36.17 72.341 1.30514 11.5 1.5 1.4 5.9 108 10 2 3 36.605 73.21 1.29178 102.4 13.4 12.7 6.0 109 4 3 5 36.642 73.285 1.29065 18.8 2.5 2.3 6.0 110 9 3 1 36.962 73.924 1.28105 25.4 3.3 3.1 6.0 111 5 1 7 37.125 74.251 1.27622 14.2 1.9 1.8 6.0 112 4 4 2 37.28 74.56 1.2717 8.8 1.2 1.1 6.0 113 11 0 4 37.311 74.622 1.27079 25.0 3.3 3.1 6.0 114 8 2 5 37.379 74.758 1.26882 55.1 7.2 6.8 6.0 115 5 4 1 37.437 74.874 1.26714 16.8 2.2 2.1 6.0 116 6 2 6 37.473 74.946 1.26609 9.9 1.3 1.2 6.0 117 10 0 5 37.644 75.288 1.2612 9.7 1.3 1.2 6.0 118 5 3 5 37.85 75.701 1.25534 44.4 5.8 5.5 6.0 119 9 3 2 38.011 76.021 1.25084 31.8 4.2 3.9 6.0 120 2 0 8 38.413 76.826 1.23974 24.2 3.2 3.0 6.0 121 5 4 2 38.481 76.962 1.23788 46.7 6.1 5.8 6.0 122 6 4 0 38.556 77.111 1.23586 23.6 3.1 2.9 6.0 123 6 1 7 38.594 77.188 1.23483 18.0 2.4 2.2 6.0 124 10 2 4 39.044 78.089 1.22282 18.5 2.4 2.3 6.0 125 10 3 0 39.147 78.293 1.22013 26.3 3.4 3.2 6.0 126 7 2 6 39.201 78.403 1.2187 9.8 1.3 1.2 6.0 127 6 3 5 39.31 78.62 1.21588 20.0 2.6 2.5 6.0 128 11 2 3 39.405 78.811 1.21342 18.7 2.5 2.3 6.0 129 1 4 4 39.448 78.897 1.21231 10.0 1.3 1.2 6.0 130 10 3 1 39.491 78.982 1.21122 34.6 4.5 4.2 6.0 131 9 2 5 39.636 79.272 1.20751 27.8 3.6 3.4 6.0 132 6 4 2 39.934 79.867 1.2 10.4 1.4 1.3 6.0 133 7 1 7 40.308 80.615 1.19074 11.0 1.4 1.3 6.1 134 5 2 7 40.506 81.012 1.18591 44.4 5.8 5.4 6.1 135 7 3 5 41.016 82.032 1.17373 8.9 1.2 1.1 6.1 136 6 4 3 41.64 83.28 1.15928 12.2 1.6 1.5 6.1 137 6 2 7 41.941 83.883 1.15247 10.0 1.3 1.2 6.1 138 8 4 0 42.227 84.454 1.14613 22.1 2.9 2.7 6.1 139 8 1 7 42.265 84.529 1.14531 9.0 1.2 1.1 6.1 140 12 2 3 42.412 84.824 1.14207 8.1 1.1 1.0 6.1 141 10 1 6 42.534 85.069 1.13942 11.7 1.5 1.4 6.1 142 5 4 4 42.585 85.169 1.13833 26.0 3.4 3.1 6.1 143 14 1 0 42.801 85.603 1.13366 36.0 4.7 4.3 6.1 144 2 4 5 42.907 85.814 1.13142 10.9 1.4 1.3 6.1 145 8 4 2 43.581 87.162 1.11735 12.0 1.6 1.4 6.2 146 6 1 8 43.709 87.419 1.11473 17.0 2.2 2.0 6.2 147 4 2 8 44.423 88.846 1.10048 29.3 3.8 3.5 6.2 148 9 1 7 44.467 88.935 1.09961 21.7 2.8 2.6 6.2 149 14 0 3 44.741 89.482 1.09429 15.9 2.1 1.9 6.2 150 1 1 9 44.921 89.841 1.09085 25.1 3.3 3.0 6.2 Reference: Chichagov A.V. et al. Information-Calculating System on Crystal Structure Data of Minerals (MINCRYST) - Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian) |