Institute of Experimental Mineralogy Russian Academy of Sciences ------------------------------------------------- 142432, Chernogolovka, Moscow district A.V. Chichagov +7(496)52-22320 *** *** W W W - X R A Y P O L *** *********************** WICKSITE 1, DN NaCa(2)(Fe,Mg)(2)(Fe,Al,Mg)(2)(Fe,Mn)(2)[PO(4)](6).H(2)O Orthorhombic P cab Z = 4 R =0.024 NR =2413 24 .11 .1997 Ref.Str.: Cooper M.A., Hawthorne F.C., (1997) * Canad. Mineral., 35, 777-784 Reserv: There are U(ij) in the article. D.T.N. Initial data from BDM-file Lattice parameters (cub. angs.,degr.): a = 12.524 alpha = 90.0 b = 12.907 beta = 90.0 c = 11.646 gamma = 90.0 Unit cell volume (cub. angs.) = 1882.54 Molar volume ( cub.cm/mol.) = 283.48 Co-ordinates, thermal parameters, occupation for atomic positions: NoP x/a y/b z/c B(j) atom / occupation 1 0.3914 0.3014 0.2249 0.01 P = 1.00 2 0.101 0.443 0.2536 0.01 P = 1.00 3 0.2675 0.1241 0.4759 0.01 P = 1.00 4 0.1544 0.2067 0.2267 0.01 Fe = 0.79, Mg = 0.21 5 0.3329 0.0431 0.2259 0.01 Fe = 0.64, Mg = 0.27, Al = 0.09 6 0.0257 0.2687 0.4551 0.01 Fe = 0.7 , Mn = 0.3 7 0.264 0.374 0.4935 0.01 Ca = 1.00 8 0.0 0.0 0.0 0.02 Na = 1.00 9 0.4989 0.2754 0.282 0.01 O = 1.00 10 0.4092 0.338 0.1008 0.01 O = 1.00 11 0.3216 0.2027 0.2215 0.01 O = 1.00 12 0.3358 0.385 0.2973 0.01 O = 1.00 13 0.166 0.5444 0.2551 0.01 O = 1.00 14 0.155 0.3625 0.1765 0.01 O = 1.00 15 0.0938 0.4034 0.3784 0.01 O = 1.00 16 0.9903 0.466 0.2013 0.02 O = 1.00 17 0.1923 0.2033 0.4165 0.01 O = 1.00 18 0.3527 0.1897 0.54 0.01 O = 1.00 19 0.2009 0.0519 0.5539 0.01 O = 1.00 20 0.3297 0.0509 0.3959 0.02 O = 1.00 21 0.9724 0.1165 0.4864 0.02 O = 0.5 , O = 0.0 22 0.013 0.085 0.549 0.07 H = 0.5 , H = 0.0 23 0.993 0.074 0.421 0.07 H = 0.5 , H = 0.0 Co-ordinates for all atomic positions : No NoP x/a y/b z/c 1 1 0.3914 0.3014 0.2249 2 2 0.101 0.443 0.2536 3 3 0.2675 0.1241 0.4759 4 4 0.1544 0.2067 0.2267 5 5 0.3329 0.0431 0.2259 6 6 0.0257 0.2687 0.4551 7 7 0.264 0.374 0.4935 8 8 0.0 0.0 0.0 9 9 0.4989 0.2754 0.282 10 10 0.4092 0.338 0.1008 11 11 0.3216 0.2027 0.2215 12 12 0.3358 0.385 0.2973 13 13 0.166 0.5444 0.2551 14 14 0.155 0.3625 0.1765 15 15 0.0938 0.4034 0.3784 16 16 0.9903 0.466 0.2013 17 17 0.1923 0.2033 0.4165 18 18 0.3527 0.1897 0.54 19 19 0.2009 0.0519 0.5539 20 20 0.3297 0.0509 0.3959 21 21 0.9724 0.1165 0.4864 22 22 0.013 0.085 0.549 23 23 0.993 0.074 0.421 24 1 0.6086 0.6986 0.7751 25 2 0.899 0.557 0.7464 26 3 0.7325 0.8759 0.5241 27 4 0.8456 0.7933 0.7733 28 5 0.6671 0.9569 0.7741 29 6 0.9743 0.7313 0.5449 30 7 0.736 0.626 0.5065 31 9 0.5011 0.7246 0.718 32 10 0.5908 0.662 0.8992 33 11 0.6784 0.7973 0.7785 34 12 0.6642 0.615 0.7027 35 13 0.834 0.4556 0.7449 36 14 0.845 0.6375 0.8235 37 15 0.9062 0.5966 0.6216 38 16 0.0097 0.534 0.7987 39 17 0.8077 0.7967 0.5835 40 18 0.6473 0.8103 0.46 41 19 0.7991 0.9481 0.4461 42 20 0.6703 0.9491 0.6041 43 21 0.0276 0.8835 0.5136 44 22 0.987 0.915 0.451 45 23 0.007 0.926 0.579 46 1 0.8914 0.1986 0.2249 47 2 0.601 0.057 0.2536 48 3 0.7675 0.3759 0.4759 49 4 0.6544 0.2933 0.2267 50 5 0.8329 0.4569 0.2259 51 6 0.5257 0.2313 0.4551 52 7 0.764 0.126 0.4935 53 8 0.5 0.5 0.0 54 9 0.9989 0.2246 0.282 55 10 0.9092 0.162 0.1008 56 11 0.8216 0.2973 0.2215 57 12 0.8358 0.115 0.2973 58 13 0.666 0.9556 0.2551 59 14 0.655 0.1375 0.1765 60 15 0.5938 0.0966 0.3784 61 16 0.4903 0.034 0.2013 62 17 0.6923 0.2967 0.4165 63 18 0.8527 0.3103 0.54 64 19 0.7009 0.4481 0.5539 65 20 0.8297 0.4491 0.3959 66 21 0.4724 0.3835 0.4864 67 22 0.513 0.415 0.549 68 23 0.493 0.426 0.421 69 1 0.1086 0.8014 0.7751 70 2 0.399 0.943 0.7464 71 3 0.2325 0.6241 0.5241 72 4 0.3456 0.7067 0.7733 73 5 0.1671 0.5431 0.7741 74 6 0.4743 0.7687 0.5449 75 7 0.236 0.874 0.5065 76 9 0.0011 0.7754 0.718 77 10 0.0908 0.838 0.8992 78 11 0.1784 0.7027 0.7785 79 12 0.1642 0.885 0.7027 80 13 0.334 0.0444 0.7449 81 14 0.345 0.8625 0.8235 82 15 0.4062 0.9034 0.6216 83 16 0.5097 0.966 0.7987 84 17 0.3077 0.7033 0.5835 85 18 0.1473 0.6897 0.46 86 19 0.2991 0.5519 0.4461 87 20 0.1703 0.5509 0.6041 88 21 0.5276 0.6165 0.5136 89 22 0.487 0.585 0.451 90 23 0.507 0.574 0.579 91 1 0.3914 0.8014 0.2751 92 2 0.101 0.943 0.2464 93 3 0.2675 0.6241 0.0241 94 4 0.1544 0.7067 0.2733 95 5 0.3329 0.5431 0.2741 96 6 0.0257 0.7687 0.0449 97 7 0.264 0.874 0.0065 98 8 0.0 0.5 0.5 99 9 0.4989 0.7754 0.218 100 10 0.4092 0.838 0.3992 101 11 0.3216 0.7027 0.2785 102 12 0.3358 0.885 0.2027 103 13 0.166 0.0444 0.2449 104 14 0.155 0.8625 0.3235 105 15 0.0938 0.9034 0.1216 106 16 0.9903 0.966 0.2987 107 17 0.1923 0.7033 0.0835 108 18 0.3527 0.6897 0.96 109 19 0.2009 0.5519 0.9461 110 20 0.3297 0.5509 0.1041 111 21 0.9724 0.6165 0.0136 112 22 0.013 0.585 0.951 113 23 0.993 0.574 0.079 114 1 0.6086 0.1986 0.7249 115 2 0.899 0.057 0.7536 116 3 0.7325 0.3759 0.9759 117 4 0.8456 0.2933 0.7267 118 5 0.6671 0.4569 0.7259 119 6 0.9743 0.2313 0.9551 120 7 0.736 0.126 0.9935 121 9 0.5011 0.2246 0.782 122 10 0.5908 0.162 0.6008 123 11 0.6784 0.2973 0.7215 124 12 0.6642 0.115 0.7973 125 13 0.834 0.9556 0.7551 126 14 0.845 0.1375 0.6765 127 15 0.9062 0.0966 0.8784 128 16 0.0097 0.034 0.7013 129 17 0.8077 0.2967 0.9165 130 18 0.6473 0.3103 0.04 131 19 0.7991 0.4481 0.0539 132 20 0.6703 0.4491 0.8959 133 21 0.0276 0.3835 0.9864 134 22 0.987 0.415 0.049 135 23 0.007 0.426 0.921 136 1 0.8914 0.6986 0.2751 137 2 0.601 0.557 0.2464 138 3 0.7675 0.8759 0.0241 139 4 0.6544 0.7933 0.2733 140 5 0.8329 0.9569 0.2741 141 6 0.5257 0.7313 0.0449 142 7 0.764 0.626 0.0065 143 8 0.5 0.0 0.5 144 9 0.9989 0.7246 0.218 145 10 0.9092 0.662 0.3992 146 11 0.8216 0.7973 0.2785 147 12 0.8358 0.615 0.2027 148 13 0.666 0.4556 0.2449 149 14 0.655 0.6375 0.3235 150 15 0.5938 0.5966 0.1216 151 16 0.4903 0.534 0.2987 152 17 0.6923 0.7967 0.0835 153 18 0.8527 0.8103 0.96 154 19 0.7009 0.9481 0.9461 155 20 0.8297 0.9491 0.1041 156 21 0.4724 0.8835 0.0136 157 22 0.513 0.915 0.951 158 23 0.493 0.926 0.079 159 1 0.1086 0.3014 0.7249 160 2 0.399 0.443 0.7536 161 3 0.2325 0.1241 0.9759 162 4 0.3456 0.2067 0.7267 163 5 0.1671 0.0431 0.7259 164 6 0.4743 0.2687 0.9551 165 7 0.236 0.374 0.9935 166 9 0.0011 0.2754 0.782 167 10 0.0908 0.338 0.6008 168 11 0.1784 0.2027 0.7215 169 12 0.1642 0.385 0.7973 170 13 0.334 0.5444 0.7551 171 14 0.345 0.3625 0.6765 172 15 0.4062 0.4034 0.8784 173 16 0.5097 0.466 0.7013 174 17 0.3077 0.2033 0.9165 175 18 0.1473 0.1897 0.04 176 19 0.2991 0.0519 0.0539 177 20 0.1703 0.0509 0.8959 178 21 0.5276 0.1165 0.9864 179 22 0.487 0.085 0.049 180 23 0.507 0.074 0.921 X-ray density (g/cm cub.) = 3.49 MU (1/cm) = 222.802 Mass attenuation coefficient (cm**2/g) = 63.803 Selected interatomic distances (cation-anion,anion-anion): NoP Atom Rad.sph. C.N. Distance NoP N. (angs.) (angs.) 1 P 2.232 4 1.5386 9 1.5368 10 1.5455 11 1.5363 12 2 P 2.232 4 1.5414 13 1.5307 14 1.5433 15 1.5431 16 3 P 2.232 4 1.5526 17 1.5533 18 1.5457 19 1.5387 20 4 Fe ,Mg 2.592 6 2.0955 11 2.0942 14 2.2612 17 2.0642 9 2.1105 13 2.1872 18 5 Fe ,Mg ,Al 2.592 6 2.0654 11 1.9828 20 1.9954 16 2.0587 12 2.102 13 2.0505 19 6 Fe ,Mn 2.724 6 2.1326 15 2.2952 17 2.1065 21 2.1215 9 2.4414 18 2.0842 10 7 Ca 2.88 9 2.4596 12 2.5465 15 2.5426 17 2.6806 18 2.6142 21 2.4021 19 2.8722 20 2.5461 10 2.365 14 8 Na 2.808 6 2.6539 10 2.6539 10 2.2226 15 2.2226 15 2.5398 20 2.5398 20 9 O 3.264 9 2.5235 10 2.5115 11 2.4911 12 2.9154 14 2.8282 15 3.2562 16 2.8976 17 2.7791 21 3.1585 13 10 O 3.264 7 2.5235 9 2.4958 11 2.5397 12 2.923 20 3.0857 18 2.7244 15 3.0406 17 11 O 3.264 10 2.5115 9 2.4958 10 2.5194 12 2.9803 14 2.7892 17 2.8239 20 3.0431 16 2.8366 13 3.0432 18 2.7708 19 12 O 3.264 10 2.4911 9 2.5397 10 2.5194 11 2.9994 13 2.6816 14 3.1834 15 2.7887 21 2.8026 19 3.107 20 2.7282 16 13 O 3.264 10 2.9994 12 2.5237 14 2.4883 15 2.5017 16 3.044 18 2.7814 19 2.8366 11 2.8825 17 2.7024 20 3.1585 9 14 O 3.264 8 2.9803 11 2.6816 12 2.5237 13 2.5288 15 2.4744 16 2.9154 9 2.7424 21 2.7406 18 15 O 3.264 7 3.1834 12 2.4883 13 2.5288 14 2.5665 16 2.8964 17 2.8282 9 2.7244 10 16 O 3.264 10 2.5017 13 2.4744 14 2.5665 15 3.2562 9 3.0431 11 3.038 20 2.9329 21 2.9554 19 2.7597 21 2.7282 12 17 O 3.264 9 2.7892 11 2.8964 15 2.4769 18 2.528 19 2.6245 20 3.0826 21 2.8976 9 2.8825 13 3.0406 10 18 O 3.264 8 2.4769 17 2.6084 19 2.4716 20 2.9823 21 3.044 13 3.0857 10 3.0432 11 2.7406 14 19 O 3.264 9 2.528 17 2.6084 18 2.4471 20 3.0826 21 3.1073 21 2.8026 12 2.7814 13 2.9554 16 2.7708 11 20 O 3.264 8 2.8239 11 2.6245 17 2.4716 18 2.4471 19 3.038 16 2.923 10 3.107 12 2.7024 13 21 O ,O 3.264 10 3.0826 17 3.0826 19 3.1073 19 3.102 21 2.7791 9 2.7887 12 2.9823 18 2.9329 16 2.7424 14 2.7597 16 22 H ,H 1.632 1 0.9774 21 23 H ,H 1.632 1 0.9734 21 X-ray diffraction powder data (II), X-Ray W.L. = 1.78892(angs.): No H K L Theta 2*Theta S LPG MF F I int. ( degree ) *100 1 1 1 1 7.222 14.443 0.07 123.61 8 60.6 102.5 2 0 2 0 7.967 15.934 0.077 101.16 2 165.7 156.8 3 2 0 0 8.212 16.424 0.08 95.08 2 170.0 155.1 4 0 0 2 8.836 17.672 0.086 81.83 2 182.1 153.1 5 1 2 0 8.97 17.94 0.087 79.34 4 41.4 15.3 6 2 0 1 9.333 18.667 0.091 73.11 4 30.4 7.6 7 0 1 2 9.702 19.403 0.094 67.51 4 40.7 12.6 8 1 2 1 10.009 20.019 0.097 63.29 8 19.2 5.2 9 2 1 1 10.158 20.316 0.099 61.39 8 33.8 15.9 10 1 1 2 10.546 21.092 0.102 56.8 8 31.2 12.5 11 2 2 0 11.48 22.961 0.111 47.6 4 146.3 115.0 12 0 2 2 11.94 23.881 0.116 43.84 4 110.4 60.3 13 2 0 2 12.108 24.216 0.117 42.58 4 6.3 0.2 14 2 2 1 12.318 24.636 0.119 41.07 8 73.7 50.4 15 1 2 2 12.643 25.286 0.122 38.88 8 23.0 4.7 16 2 1 2 12.762 25.525 0.123 38.12 8 77.6 51.8 17 1 3 1 13.465 26.931 0.13 34.04 8 76.4 44.8 18 3 1 1 13.764 27.528 0.133 32.49 8 39.3 11.4 19 1 1 3 14.536 29.072 0.14 28.93 8 74.1 35.9 20 2 2 2 14.561 29.122 0.141 28.82 8 93.7 57.1 21 3 2 0 14.784 29.569 0.143 27.9 4 223.1 156.8 22 0 3 2 14.981 29.961 0.144 27.12 4 17.3 0.9 23 2 3 1 15.288 30.577 0.147 25.96 8 58.2 19.9 24 3 2 1 15.455 30.911 0.149 25.36 8 14.7 1.2 25 1 3 2 15.556 31.112 0.15 25.01 8 52.1 15.4 26 2 0 3 15.729 31.459 0.152 24.42 4 5.4 0.1 27 3 1 2 15.818 31.637 0.152 24.13 8 26.3 3.8 28 0 4 0 16.093 32.187 0.155 23.25 2 117.2 18.0 29 1 2 3 16.153 32.307 0.156 23.06 8 29.0 4.4 30 2 1 3 16.249 32.498 0.156 22.77 8 8.7 0.4 31 4 0 0 16.599 33.199 0.16 21.74 2 56.2 3.9 32 1 4 0 16.634 33.268 0.16 21.64 4 23.0 1.3 33 2 3 2 17.177 34.355 0.165 20.18 8 101.8 47.2 34 4 0 1 17.207 34.414 0.165 20.1 4 81.3 15.0 35 1 4 1 17.24 34.48 0.166 20.02 8 330.1 492.6 36 3 2 2 17.328 34.657 0.166 19.8 8 79.5 28.2 37 4 1 1 17.688 35.376 0.17 18.93 8 188.2 151.3 38 2 2 3 17.726 35.453 0.17 18.84 8 92.7 36.5 39 0 0 4 17.892 35.783 0.172 18.46 2 734.9 562.6 40 3 3 1 17.955 35.91 0.172 18.32 8 5.4 0.1 41 2 4 0 18.17 36.34 0.174 17.85 4 334.9 226.0 42 0 1 4 18.357 36.714 0.176 17.45 4 332.8 218.1 43 0 4 2 18.477 36.953 0.177 17.2 4 246.2 117.7 44 4 2 0 18.513 37.027 0.177 17.13 4 31.8 2.0 45 1 3 3 18.569 37.139 0.178 17.01 8 46.9 8.5 46 2 4 1 18.733 37.466 0.18 16.69 8 6.5 0.2 47 3 1 3 18.795 37.589 0.18 16.57 8 11.8 0.5 48 1 1 4 18.84 37.681 0.181 16.48 8 95.0 33.6 49 4 0 2 18.927 37.853 0.181 16.31 4 621.6 711.5 50 1 4 2 18.957 37.915 0.182 16.25 8 16.0 0.9 51 4 2 1 19.068 38.135 0.183 16.05 8 220.4 176.0 52 4 1 2 19.371 38.741 0.185 15.5 8 197.4 136.3 53 3 3 2 19.618 39.236 0.188 15.07 8 4.4 0.1 54 0 2 4 19.696 39.393 0.188 14.94 4 57.4 5.6 55 2 0 4 19.804 39.607 0.189 14.76 4 129.6 28.0 56 2 3 3 19.977 39.953 0.191 14.47 8 53.0 9.2 57 3 2 3 20.109 40.219 0.192 14.26 8 21.7 1.5 58 1 2 4 20.152 40.305 0.193 14.19 8 51.5 8.5 59 2 1 4 20.232 40.463 0.193 14.07 8 5.6 0.1 60 2 4 2 20.342 40.684 0.194 13.9 8 274.9 237.1 61 3 4 0 20.509 41.018 0.196 13.65 4 10.0 0.2 62 4 2 2 20.654 41.309 0.197 13.44 8 59.2 10.6 63 3 4 1 21.019 42.037 0.2 12.92 8 225.6 148.4 64 4 3 1 21.197 42.393 0.202 12.68 8 11.4 0.4 65 1 5 1 21.225 42.449 0.202 12.64 8 147.3 61.9 66 2 2 4 21.472 42.945 0.205 12.32 8 44.0 5.4 67 4 0 3 21.532 43.064 0.205 12.24 4 49.9 3.4 68 1 4 3 21.559 43.119 0.205 12.21 8 179.7 88.9 69 0 3 4 21.774 43.549 0.207 11.94 4 112.0 16.9 70 5 1 1 21.825 43.651 0.208 11.87 8 82.8 18.4 71 4 1 3 21.932 43.864 0.209 11.74 8 22.3 1.3 72 3 3 3 22.155 44.311 0.211 11.48 8 48.2 6.0 73 1 3 4 22.195 44.39 0.211 11.43 8 16.5 0.7 74 0 5 2 22.273 44.546 0.212 11.34 4 79.6 8.1 75 3 1 4 22.39 44.78 0.213 11.21 8 8.4 0.2 76 3 4 2 22.492 44.983 0.214 11.1 8 27.8 1.9 77 2 5 1 22.493 44.987 0.214 11.09 8 87.8 19.3 78 5 2 0 22.523 45.046 0.214 11.06 4 209.4 54.7 79 4 3 2 22.66 45.321 0.215 10.91 8 146.8 53.0 80 1 5 2 22.687 45.374 0.216 10.88 8 3.5 0.0 81 2 4 3 22.813 45.626 0.217 10.75 8 22.5 1.2 82 5 2 1 22.997 45.993 0.218 10.55 8 26.1 1.6 83 4 2 3 23.099 46.197 0.219 10.45 8 94.0 20.8 84 5 1 2 23.257 46.515 0.221 10.29 8 2.7 0.0 85 1 1 5 23.372 46.745 0.222 10.17 8 113.1 29.4 86 2 3 4 23.422 46.844 0.222 10.12 8 76.2 13.3 87 4 4 0 23.457 46.914 0.223 10.09 4 18.6 0.4 88 3 2 4 23.539 47.078 0.223 10.01 8 33.8 2.6 89 2 5 2 23.894 47.788 0.226 9.68 8 105.3 24.2 90 4 4 1 23.916 47.833 0.227 9.66 8 4.2 0.0 91 2 0 5 24.188 48.375 0.229 9.41 4 60.0 3.8 92 5 2 2 24.375 48.75 0.231 9.25 8 27.5 1.6 93 0 4 4 24.443 48.886 0.231 9.19 4 119.4 14.8 94 1 2 5 24.486 48.971 0.232 9.15 8 22.0 1.0 95 3 5 1 24.492 48.985 0.232 9.15 8 75.6 11.8 96 2 1 5 24.554 49.107 0.232 9.1 8 119.8 29.5 97 0 6 0 24.57 49.14 0.232 9.08 2 98.3 5.0 98 3 4 3 24.792 49.585 0.234 8.9 8 34.9 2.4 99 4 0 4 24.804 49.608 0.235 8.89 4 62.6 3.9 100 1 4 4 24.829 49.658 0.235 8.87 8 24.7 1.2 101 5 3 1 24.853 49.705 0.235 8.85 8 71.7 10.3 102 4 3 3 24.949 49.898 0.236 8.77 8 63.6 8.0 103 1 6 0 24.954 49.908 0.236 8.77 4 426.8 180.2 104 1 5 3 24.974 49.947 0.236 8.75 8 104.6 21.6 105 4 1 4 25.163 50.327 0.238 8.6 8 50.4 4.9 106 4 4 2 25.257 50.513 0.239 8.53 8 30.5 1.8 107 3 3 4 25.365 50.73 0.239 8.45 8 92.9 16.5 108 6 0 0 25.374 50.747 0.24 8.44 2 365.8 63.7 109 1 6 1 25.393 50.786 0.24 8.43 8 5.7 0.1 110 5 1 3 25.505 51.011 0.241 8.34 8 109.9 22.7 111 2 2 5 25.628 51.257 0.242 8.25 8 103.0 19.8 112 6 0 1 25.807 51.615 0.243 8.12 4 77.3 5.5 113 3 5 2 25.81 51.62 0.243 8.12 8 32.6 1.9 114 2 4 4 25.96 51.921 0.245 8.01 8 240.1 104.3 115 2 6 0 26.082 52.163 0.246 7.93 4 96.0 8.3 116 2 5 3 26.101 52.201 0.246 7.91 8 10.7 0.2 117 6 1 1 26.157 52.313 0.246 7.88 8 88.7 14.0 118 5 3 2 26.157 52.315 0.246 7.88 8 20.4 0.7 119 4 2 4 26.22 52.44 0.247 7.83 8 9.9 0.2 120 1 3 5 26.263 52.525 0.247 7.8 8 24.4 1.1 121 0 6 2 26.313 52.625 0.248 7.77 4 26.1 0.6 122 3 1 5 26.435 52.869 0.249 7.69 8 108.8 20.6 123 2 6 1 26.507 53.014 0.249 7.64 8 69.7 8.4 124 5 2 3 26.552 53.104 0.25 7.61 8 39.9 2.7 125 1 6 2 26.679 53.357 0.251 7.53 8 132.3 29.7 126 6 2 0 26.768 53.536 0.252 7.47 4 50.4 2.1 127 5 4 0 26.876 53.752 0.253 7.4 4 76.0 4.8 128 6 0 2 27.079 54.158 0.254 7.28 4 301.0 74.4 129 4 5 1 27.104 54.208 0.255 7.26 8 31.4 1.6 130 6 2 1 27.186 54.372 0.255 7.21 8 89.5 13.0 131 5 4 1 27.293 54.586 0.256 7.15 8 79.4 10.2 132 2 3 5 27.352 54.704 0.257 7.11 8 7.5 0.1 133 4 4 3 27.383 54.766 0.257 7.1 8 61.7 6.1 134 6 1 2 27.417 54.834 0.257 7.08 8 12.7 0.3 135 0 0 6 27.44 54.881 0.258 7.06 2 225.9 20.3 136 3 2 5 27.456 54.913 0.258 7.05 8 64.6 6.6 137 0 5 4 27.586 55.172 0.259 6.98 4 151.2 18.0 138 2 6 2 27.756 55.513 0.26 6.88 8 40.8 2.6 139 3 4 4 27.773 55.546 0.26 6.87 8 43.3 2.9 140 0 1 6 27.775 55.551 0.26 6.87 4 16.3 0.2 141 3 6 0 27.889 55.778 0.261 6.81 4 151.9 17.7 142 3 5 3 27.907 55.814 0.262 6.8 8 164.0 41.3 143 4 3 4 27.918 55.836 0.262 6.79 8 2.0 0.0 144 1 5 4 27.941 55.881 0.262 6.78 8 33.9 1.8 145 1 1 6 28.128 56.257 0.264 6.68 8 155.8 36.6 146 5 3 3 28.236 56.473 0.264 6.62 8 22.3 0.7 147 3 6 1 28.296 56.591 0.265 6.59 8 41.0 2.5 148 4 5 2 28.335 56.67 0.265 6.57 8 23.0 0.8 149 6 2 2 28.415 56.829 0.266 6.52 8 30.7 1.4 150 5 1 4 28.433 56.866 0.266 6.51 8 70.9 7.4 151 5 4 2 28.519 57.038 0.267 6.47 8 64.9 6.2 152 4 0 5 28.596 57.192 0.268 6.43 4 123.3 11.0 153 1 4 5 28.618 57.236 0.268 6.42 8 129.0 24.1 154 1 6 3 28.732 57.464 0.269 6.36 8 73.9 7.8 155 0 2 6 28.765 57.53 0.269 6.35 4 41.0 1.2 156 6 3 1 28.845 57.69 0.27 6.31 8 190.3 51.6 157 2 0 6 28.846 57.692 0.27 6.31 4 29.9 0.6 158 4 1 5 28.922 57.844 0.27 6.27 8 104.7 15.5 159 2 5 4 28.987 57.974 0.271 6.24 8 130.8 24.1 160 3 3 5 29.105 58.211 0.272 6.18 8 116.1 18.8 161 1 2 6 29.11 58.22 0.272 6.18 8 157.1 34.4 162 6 0 3 29.113 58.226 0.272 6.18 4 101.6 7.2 163 2 1 6 29.17 58.34 0.272 6.15 8 173.8 41.9 164 5 2 4 29.408 58.817 0.274 6.04 8 147.5 29.7 165 6 1 3 29.436 58.871 0.275 6.02 8 14.2 0.3 166 3 6 2 29.494 58.988 0.275 6.0 8 13.2 0.2 167 2 4 5 29.649 59.298 0.277 5.93 8 104.8 14.7 168 1 7 1 29.756 59.512 0.277 5.88 8 84.8 9.5 169 2 6 3 29.76 59.52 0.277 5.88 8 7.0 0.1 170 4 2 5 29.887 59.774 0.279 5.82 8 79.2 8.2 171 6 3 2 30.03 60.059 0.28 5.76 8 92.7 11.2 172 2 2 6 30.13 60.261 0.281 5.72 8 72.7 6.8 173 4 4 4 30.187 60.374 0.281 5.69 8 173.2 38.6 174 5 5 1 30.23 60.46 0.281 5.68 8 57.2 4.2 175 4 6 0 30.297 60.594 0.282 5.65 4 86.8 4.8 176 4 5 3 30.314 60.629 0.282 5.64 8 37.6 1.8 177 0 3 6 30.368 60.736 0.283 5.62 4 98.3 6.1 178 6 2 3 30.391 60.781 0.283 5.61 8 100.2 12.7 179 5 4 3 30.49 60.981 0.284 5.57 8 77.4 7.5 180 0 7 2 30.587 61.173 0.284 5.53 4 218.6 29.8 181 3 5 4 30.68 61.361 0.285 5.49 8 49.7 3.1 182 4 6 1 30.684 61.367 0.285 5.49 8 116.5 16.8 183 6 4 0 30.688 61.376 0.285 5.49 4 386.7 92.6 184 7 1 1 30.699 61.398 0.285 5.48 8 37.4 1.7 185 1 3 6 30.702 61.404 0.285 5.48 8 14.9 0.3 186 2 7 1 30.763 61.527 0.286 5.46 8 5.5 0.0 187 3 1 6 30.857 61.715 0.287 5.42 8 2.1 0.0 188 1 7 2 30.919 61.839 0.287 5.4 8 67.7 5.6 189 5 3 4 30.991 61.982 0.288 5.37 8 8.7 0.1 190 6 4 1 31.072 62.143 0.289 5.34 8 21.2 0.5 191 0 6 4 31.13 62.26 0.289 5.32 4 34.6 0.7 192 7 2 0 31.251 62.503 0.29 5.27 4 244.5 35.6 193 3 4 5 31.321 62.641 0.291 5.25 8 253.6 76.2 194 5 5 2 31.382 62.765 0.291 5.22 8 18.0 0.4 195 3 6 3 31.428 62.856 0.291 5.21 8 60.9 4.4 196 4 3 5 31.455 62.91 0.292 5.2 8 79.2 7.4 197 1 6 4 31.459 62.919 0.292 5.2 8 146.9 25.3 198 1 5 5 31.476 62.953 0.292 5.19 8 127.9 19.2 199 7 2 1 31.631 63.262 0.293 5.13 8 46.4 2.5 200 2 3 6 31.691 63.383 0.294 5.11 8 200.2 46.3 201 3 2 6 31.787 63.574 0.294 5.08 8 136.6 21.4 202 6 0 4 31.821 63.642 0.295 5.07 4 161.1 14.9 203 4 6 2 31.827 63.653 0.295 5.07 8 64.2 4.7 204 7 1 2 31.842 63.684 0.295 5.06 8 34.1 1.3 205 2 7 2 31.905 63.81 0.295 5.04 8 52.7 3.2 206 5 1 5 31.935 63.87 0.296 5.03 8 63.3 4.6 207 6 3 3 31.944 63.889 0.296 5.03 8 130.1 19.2 208 6 1 4 32.127 64.254 0.297 4.96 8 106.9 12.8 209 6 4 2 32.207 64.414 0.298 4.94 8 124.1 17.2 210 3 7 1 32.401 64.803 0.3 4.87 8 31.1 1.1 211 2 6 4 32.436 64.872 0.3 4.86 8 37.9 1.6 212 2 5 5 32.452 64.905 0.3 4.86 8 164.7 29.7 213 0 4 6 32.532 65.064 0.301 4.83 4 282.9 43.6 214 7 2 2 32.756 65.511 0.302 4.76 8 138.2 20.5 215 1 7 3 32.804 65.608 0.303 4.74 8 2.6 0.0 216 4 0 6 32.833 65.666 0.303 4.74 4 336.4 60.5 217 5 2 5 32.847 65.695 0.303 4.73 8 51.4 2.8 218 1 4 6 32.854 65.707 0.303 4.73 8 0.7 0.0 219 4 5 4 32.964 65.928 0.304 4.7 8 5.4 0.0 220 6 2 4 33.037 66.074 0.305 4.67 8 40.5 1.7 221 5 4 4 33.132 66.264 0.306 4.64 8 56.9 3.4 222 4 1 6 33.134 66.268 0.306 4.64 8 328.0 112.8 223 1 1 7 33.145 66.29 0.306 4.64 8 73.3 5.6 224 7 3 1 33.152 66.304 0.306 4.64 8 1.5 0.0 225 5 6 0 33.237 66.473 0.306 4.61 4 356.7 66.3 226 5 5 3 33.253 66.506 0.307 4.61 8 108.4 12.2 227 3 3 6 33.304 66.608 0.307 4.59 8 35.6 1.3 228 3 7 2 33.512 67.024 0.309 4.53 8 55.1 3.1 229 4 4 5 33.58 67.161 0.309 4.51 8 39.8 1.6 230 5 6 1 33.604 67.208 0.309 4.51 8 86.1 7.5 231 0 8 0 33.67 67.339 0.31 4.49 2 68.7 1.2 232 4 6 3 33.684 67.368 0.31 4.49 8 73.4 5.5 233 7 1 3 33.699 67.397 0.31 4.48 8 126.3 16.1 234 2 7 3 33.76 67.52 0.311 4.46 8 65.8 4.4 235 2 0 7 33.799 67.598 0.311 4.45 4 2.9 0.0 236 6 5 1 33.808 67.616 0.311 4.45 8 178.4 32.0 237 2 4 6 33.809 67.617 0.311 4.45 8 195.0 38.2 238 1 8 0 33.986 67.971 0.312 4.4 4 28.1 0.4 239 3 6 4 34.03 68.06 0.313 4.39 8 134.7 18.0 240 4 2 6 34.03 68.06 0.313 4.39 8 64.9 4.2 241 1 2 7 34.041 68.081 0.313 4.39 8 19.7 0.4 242 3 5 5 34.046 68.092 0.313 4.39 8 120.5 14.4 243 6 4 3 34.053 68.106 0.313 4.38 8 125.3 15.5 244 2 1 7 34.096 68.192 0.313 4.37 8 45.6 2.0 245 7 3 2 34.25 68.501 0.315 4.33 8 50.3 2.5 246 5 3 5 34.34 68.68 0.315 4.31 8 10.2 0.1 247 1 8 1 34.349 68.699 0.315 4.31 8 141.4 19.4 248 6 3 4 34.526 69.051 0.317 4.26 8 47.0 2.1 249 7 2 3 34.587 69.174 0.317 4.25 8 40.7 1.6 250 4 7 1 34.624 69.248 0.318 4.24 8 99.5 9.5 251 5 6 2 34.696 69.391 0.318 4.22 8 209.9 42.0 252 1 6 5 34.785 69.569 0.319 4.2 8 70.5 4.7 253 8 0 0 34.845 69.69 0.319 4.18 2 144.2 4.9 254 7 4 0 34.865 69.73 0.32 4.18 4 93.8 4.2 255 6 5 2 34.896 69.792 0.32 4.17 8 11.8 0.1 256 2 8 0 34.925 69.851 0.32 4.16 4 41.1 0.8 257 2 2 7 34.98 69.959 0.32 4.15 8 80.6 6.1 258 0 7 4 35.044 70.087 0.321 4.13 4 13.2 0.1 259 0 8 2 35.12 70.24 0.322 4.12 4 420.4 82.1 260 6 0 5 35.129 70.257 0.322 4.11 4 11.5 0.1 261 8 0 1 35.204 70.409 0.322 4.1 4 43.8 0.9 262 0 5 6 35.209 70.418 0.322 4.1 4 114.9 6.1 263 7 4 1 35.225 70.449 0.322 4.09 8 101.5 9.5 264 2 8 1 35.285 70.569 0.323 4.08 8 3.1 0.0 265 3 7 3 35.324 70.649 0.323 4.07 8 114.6 12.1 266 1 7 4 35.354 70.708 0.323 4.06 8 47.9 2.1 267 3 4 6 35.372 70.744 0.324 4.06 8 14.6 0.2 268 6 1 5 35.42 70.841 0.324 4.05 8 31.1 0.9 269 1 8 2 35.43 70.86 0.324 4.04 8 7.1 0.0 270 8 1 1 35.496 70.992 0.325 4.03 8 74.1 5.0 271 4 3 6 35.499 70.997 0.325 4.03 8 135.3 16.7 272 1 3 7 35.509 71.018 0.325 4.03 8 147.5 19.8 273 1 5 6 35.519 71.037 0.325 4.02 8 130.8 15.6 274 3 1 7 35.654 71.307 0.326 3.99 8 36.8 1.2 275 4 7 2 35.701 71.401 0.326 3.98 8 7.2 0.0 276 2 6 5 35.715 71.43 0.326 3.98 8 43.6 1.7 277 5 5 4 35.787 71.575 0.327 3.97 8 92.7 7.7 278 5 1 6 35.951 71.902 0.328 3.93 8 130.3 15.1 279 8 2 0 36.01 72.02 0.329 3.92 4 92.0 3.7 280 7 3 3 36.046 72.091 0.329 3.91 8 12.0 0.1 281 4 6 4 36.204 72.408 0.33 3.88 8 18.4 0.3 282 7 1 4 36.218 72.437 0.33 3.87 8 61.4 3.3 283 4 5 5 36.22 72.44 0.33 3.87 8 87.1 6.6 284 8 0 2 36.274 72.548 0.331 3.86 4 111.0 5.4 285 2 7 4 36.278 72.556 0.331 3.86 8 48.6 2.1 286 6 2 5 36.29 72.58 0.331 3.86 8 140.3 17.1 287 7 4 2 36.294 72.587 0.331 3.86 8 1.1 0.0 288 2 8 2 36.353 72.706 0.331 3.85 8 48.1 2.0 289 8 2 1 36.365 72.729 0.331 3.84 8 292.2 74.1 290 5 4 5 36.381 72.762 0.332 3.84 8 68.0 4.0 291 2 3 7 36.431 72.863 0.332 3.83 8 47.0 1.9 292 2 5 6 36.441 72.882 0.332 3.83 8 215.2 40.0 293 3 8 0 36.467 72.935 0.332 3.82 4 55.4 1.3 294 5 6 3 36.481 72.962 0.332 3.82 8 11.5 0.1 295 3 2 7 36.521 73.042 0.333 3.81 8 10.6 0.1 296 8 1 2 36.562 73.124 0.333 3.8 8 4.6 0.0 297 6 4 4 36.562 73.124 0.333 3.8 8 219.8 41.5 298 6 6 0 36.662 73.324 0.334 3.78 4 22.7 0.2 299 6 5 3 36.678 73.355 0.334 3.78 8 130.4 14.5 300 5 2 6 36.815 73.631 0.335 3.75 8 77.1 5.0 301 3 8 1 36.82 73.641 0.335 3.75 8 164.3 22.9 302 6 6 1 37.014 74.028 0.337 3.72 8 21.6 0.4 303 7 2 4 37.08 74.161 0.337 3.7 8 107.8 9.7 304 1 8 3 37.201 74.402 0.338 3.68 8 241.4 48.4 305 3 6 5 37.243 74.487 0.338 3.67 8 85.6 6.1 306 5 7 1 37.39 74.781 0.339 3.65 8 0.6 0.0 307 8 2 2 37.421 74.841 0.34 3.64 8 50.2 2.1 308 4 7 3 37.467 74.933 0.34 3.63 8 27.3 0.6 309 4 0 7 37.504 75.008 0.34 3.63 4 66.6 1.8 310 4 4 6 37.513 75.026 0.34 3.63 8 39.1 1.3 311 1 4 7 37.523 75.047 0.34 3.62 8 181.2 26.9 312 6 3 5 37.721 75.442 0.342 3.59 8 50.4 2.1 313 4 1 7 37.788 75.577 0.343 3.58 8 29.7 0.7 314 8 3 1 37.795 75.59 0.343 3.58 8 67.1 3.6 315 3 7 4 37.798 75.595 0.343 3.58 8 45.7 1.7 316 7 5 1 37.814 75.629 0.343 3.57 8 114.0 10.5 317 3 8 2 37.872 75.743 0.343 3.57 8 38.4 1.2 318 0 0 8 37.911 75.821 0.343 3.56 2 186.1 7.0 319 3 3 7 37.949 75.898 0.344 3.55 8 60.9 3.0 320 3 5 6 37.958 75.916 0.344 3.55 8 18.0 0.3 321 8 0 3 38.03 76.059 0.344 3.54 4 124.7 6.2 322 7 4 3 38.049 76.098 0.345 3.54 8 155.6 19.3 323 6 6 2 38.063 76.127 0.345 3.53 8 29.4 0.7 324 2 8 3 38.107 76.214 0.345 3.53 8 48.0 1.8 325 0 1 8 38.194 76.388 0.346 3.51 4 276.5 30.3 326 5 3 6 38.24 76.479 0.346 3.51 8 20.0 0.3 327 8 1 3 38.313 76.625 0.347 3.49 8 222.1 38.9 328 0 6 6 38.366 76.732 0.347 3.48 4 61.6 1.5 329 2 4 7 38.427 76.855 0.347 3.48 8 25.5 0.5 330 5 7 2 38.436 76.872 0.347 3.47 8 4.4 0.0 331 1 1 8 38.494 76.989 0.348 3.46 8 98.1 7.5 332 7 3 4 38.501 77.002 0.348 3.46 8 20.5 0.3 333 1 7 5 38.522 77.044 0.348 3.46 8 56.4 2.5 334 4 8 0 38.585 77.171 0.349 3.45 4 413.7 66.7 335 4 2 7 38.638 77.275 0.349 3.44 8 162.8 20.6 336 1 6 6 38.666 77.332 0.349 3.44 8 74.8 4.3 337 8 3 2 38.837 77.675 0.351 3.41 8 4.2 0.0 338 7 5 2 38.857 77.713 0.351 3.41 8 84.1 5.4 339 5 6 4 38.927 77.853 0.351 3.4 8 156.8 18.9 340 4 8 1 38.931 77.863 0.351 3.4 8 3.2 0.0 341 5 5 5 38.942 77.884 0.351 3.4 8 17.6 0.2 342 6 0 6 38.997 77.993 0.352 3.39 4 156.2 9.3 343 0 2 8 39.041 78.081 0.352 3.38 4 141.7 7.7 344 2 0 8 39.11 78.221 0.353 3.37 4 127.1 6.2 345 6 5 4 39.119 78.238 0.353 3.37 8 149.1 16.9 346 8 2 3 39.158 78.317 0.353 3.37 8 90.8 6.3 347 1 9 1 39.232 78.464 0.354 3.36 8 95.9 7.0 348 6 1 6 39.278 78.555 0.354 3.35 8 55.7 2.3 349 0 8 4 39.334 78.667 0.354 3.34 4 11.1 0.0 350 1 2 8 39.339 78.678 0.354 3.34 8 44.6 1.5 351 4 6 5 39.347 78.694 0.354 3.34 8 83.0 5.2 352 7 1 5 39.361 78.722 0.355 3.34 8 25.0 0.5 353 2 1 8 39.391 78.782 0.355 3.33 8 3.7 0.0 354 2 7 5 39.418 78.837 0.355 3.33 8 118.1 10.5 355 8 4 0 39.424 78.848 0.355 3.33 4 44.4 0.7 356 2 6 6 39.562 79.123 0.356 3.31 8 31.1 0.7 357 3 8 3 39.603 79.206 0.356 3.31 8 7.8 0.0 358 1 8 4 39.631 79.263 0.357 3.3 8 15.0 0.2 359 6 4 5 39.695 79.39 0.357 3.29 8 94.0 6.6 360 8 4 1 39.768 79.536 0.358 3.28 8 33.3 0.8 361 6 6 3 39.792 79.585 0.358 3.28 8 64.4 3.1 362 4 7 4 39.892 79.784 0.359 3.27 8 114.5 9.7 363 3 4 7 39.919 79.839 0.359 3.26 8 68.9 3.5 364 4 8 2 39.965 79.93 0.359 3.26 8 67.2 3.3 365 0 9 2 39.967 79.933 0.359 3.26 4 17.7 0.1 366 4 3 7 40.041 80.082 0.36 3.25 8 121.8 10.9 367 4 5 6 40.05 80.1 0.36 3.25 8 73.0 3.9 368 1 5 7 40.06 80.12 0.36 3.25 8 53.6 2.1 369 6 2 6 40.118 80.235 0.36 3.24 8 38.8 1.1 370 2 9 1 40.124 80.248 0.36 3.24 8 8.9 0.1 371 5 7 3 40.16 80.321 0.361 3.23 8 52.4 2.0 372 7 2 5 40.2 80.4 0.361 3.23 8 88.7 5.7 373 5 4 6 40.206 80.412 0.361 3.23 8 3.4 0.0 374 2 2 8 40.23 80.461 0.361 3.23 8 76.7 4.3 375 1 9 2 40.263 80.526 0.361 3.22 8 22.5 0.4 376 0 3 8 40.44 80.88 0.363 3.2 4 69.4 1.7 377 8 0 4 40.445 80.89 0.363 3.2 4 184.1 12.2 378 7 4 4 40.464 80.928 0.363 3.2 8 40.1 1.2 379 5 1 7 40.476 80.952 0.363 3.2 8 117.3 9.9 380 2 8 4 40.521 81.042 0.363 3.19 8 43.6 1.4 381 8 3 3 40.557 81.114 0.363 3.19 8 23.7 0.4 382 7 6 0 40.561 81.121 0.363 3.19 4 304.5 33.3 383 7 5 3 40.576 81.152 0.364 3.19 8 17.2 0.2 384 9 1 1 40.621 81.241 0.364 3.18 8 21.2 0.3 385 6 7 1 40.678 81.356 0.364 3.17 8 44.8 1.4 386 8 1 4 40.723 81.447 0.365 3.17 8 26.6 0.5 387 1 3 8 40.736 81.472 0.365 3.17 8 10.5 0.1 388 8 4 2 40.796 81.592 0.365 3.16 8 87.2 5.4 389 3 1 8 40.874 81.748 0.366 3.15 8 28.9 0.6 390 3 7 5 40.901 81.802 0.366 3.15 8 110.6 8.7 391 7 6 1 40.902 81.805 0.366 3.15 8 61.7 2.7 392 2 5 7 40.948 81.896 0.366 3.14 8 64.1 2.9 393 3 6 6 41.043 82.086 0.367 3.13 8 58.4 2.4 394 9 2 0 41.113 82.227 0.368 3.13 4 0.7 0.0 395 2 9 2 41.15 82.3 0.368 3.12 8 6.4 0.0 396 5 8 0 41.258 82.517 0.369 3.11 4 73.9 1.9 397 5 2 7 41.31 82.62 0.369 3.11 8 64.6 2.9 398 9 2 1 41.454 82.908 0.37 3.09 8 5.6 0.0 399 6 3 6 41.508 83.017 0.37 3.09 8 126.0 11.1 400 8 2 4 41.556 83.113 0.371 3.08 8 56.3 2.2 401 7 3 5 41.59 83.181 0.371 3.08 8 65.0 2.9 402 5 8 1 41.599 83.198 0.371 3.08 8 66.5 3.1 403 3 9 1 41.601 83.202 0.371 3.08 8 101.9 7.2 404 2 3 8 41.62 83.241 0.371 3.07 8 97.7 6.6 405 9 1 2 41.644 83.288 0.371 3.07 8 3.8 0.0 406 4 8 3 41.673 83.346 0.372 3.07 8 55.4 2.1 407 6 7 2 41.701 83.402 0.372 3.07 8 19.3 0.3 408 3 2 8 41.707 83.413 0.372 3.07 8 6.5 0.0 409 7 6 2 41.924 83.849 0.373 3.05 8 347.3 82.9 410 1 9 3 41.969 83.938 0.374 3.04 8 68.4 3.2 411 4 4 7 41.986 83.973 0.374 3.04 8 39.3 1.1 412 3 8 4 41.995 83.99 0.374 3.04 8 13.6 0.1 413 0 7 6 41.997 83.994 0.374 3.04 4 347.5 41.4 414 5 6 5 42.008 84.017 0.374 3.04 8 46.9 1.5 415 6 6 4 42.182 84.365 0.375 3.02 8 13.9 0.1 416 6 5 5 42.197 84.395 0.375 3.02 8 61.0 2.5 417 8 5 1 42.269 84.539 0.376 3.01 8 40.1 1.1 418 1 7 6 42.291 84.581 0.376 3.01 8 134.4 12.3 419 0 4 8 42.382 84.764 0.377 3.0 4 96.0 3.1 420 3 5 7 42.419 84.838 0.377 3.0 8 105.5 7.5 421 9 2 2 42.474 84.948 0.377 3.0 8 98.7 6.6 422 8 4 3 42.498 84.995 0.378 2.99 8 23.1 0.4 423 5 7 4 42.546 85.092 0.378 2.99 8 155.9 16.4 424 5 8 2 42.618 85.236 0.379 2.98 8 45.6 1.4 425 3 9 2 42.62 85.24 0.379 2.98 8 82.8 4.6 426 4 0 8 42.656 85.313 0.379 2.98 4 85.9 2.5 427 1 4 8 42.675 85.35 0.379 2.98 8 14.3 0.1 428 5 3 7 42.693 85.387 0.379 2.98 8 20.5 0.3 429 1 8 5 42.702 85.404 0.379 2.98 8 22.5 0.3 430 5 5 6 42.702 85.405 0.379 2.98 8 28.5 0.5 431 9 3 1 42.837 85.674 0.38 2.97 8 2.4 0.0 432 2 9 3 42.849 85.699 0.38 2.97 8 30.8 0.6 433 4 1 8 42.932 85.864 0.381 2.96 8 7.6 0.0 434 8 3 4 42.939 85.877 0.381 2.96 8 30.7 0.6 435 7 5 4 42.958 85.915 0.381 2.96 8 57.0 2.2 436 4 7 5 42.959 85.918 0.381 2.96 8 83.1 4.6 437 3 3 8 43.088 86.176 0.382 2.95 8 98.3 6.4 438 4 6 6 43.1 86.2 0.382 2.95 8 24.6 0.4 439 1 6 7 43.11 86.22 0.382 2.95 8 65.1 2.8 440 7 1 6 43.114 86.227 0.382 2.95 8 183.1 22.3 441 2 7 6 43.17 86.341 0.382 2.94 8 35.4 0.8 442 8 5 2 43.286 86.573 0.383 2.93 8 10.6 0.1 443 9 1 3 43.341 86.681 0.384 2.93 8 42.3 1.2 444 6 7 3 43.397 86.795 0.384 2.92 8 40.1 1.1 445 6 0 7 43.433 86.867 0.384 2.92 4 23.8 0.2 446 6 4 6 43.442 86.885 0.384 2.92 8 2.1 0.0 447 8 0 5 43.505 87.01 0.385 2.92 4 182.1 10.9 448 7 4 5 43.524 87.048 0.385 2.92 8 53.3 1.9 449 2 4 8 43.554 87.108 0.385 2.91 8 0.8 0.0 450 2 8 5 43.581 87.161 0.385 2.91 8 59.8 2.3 451 7 6 3 43.62 87.239 0.386 2.91 8 99.7 6.5 452 4 9 1 43.654 87.308 0.386 2.91 8 63.7 2.7 453 6 1 7 43.709 87.418 0.386 2.9 8 112.5 8.3 454 4 2 8 43.759 87.518 0.387 2.9 8 18.2 0.2 455 8 1 5 43.781 87.561 0.387 2.9 8 3.4 0.0 456 9 3 2 43.853 87.705 0.387 2.89 8 63.5 2.6 457 0 10 0 43.868 87.737 0.387 2.89 2 14.5 0.0 458 7 2 6 43.94 87.88 0.388 2.89 8 145.6 13.8 459 2 6 7 43.988 87.976 0.388 2.89 8 77.7 3.9 460 4 8 4 44.046 88.092 0.389 2.88 8 329.6 70.7 461 0 9 4 44.048 88.096 0.389 2.88 4 59.9 1.2 462 1 10 0 44.161 88.322 0.389 2.87 4 31.2 0.3 463 9 2 3 44.167 88.334 0.389 2.87 8 7.5 0.0 464 1 1 9 44.296 88.592 0.39 2.87 8 26.5 0.5 465 5 8 3 44.311 88.622 0.39 2.87 8 11.3 0.1 466 3 9 3 44.313 88.625 0.39 2.87 8 93.0 5.6 467 1 9 4 44.34 88.681 0.391 2.86 8 28.3 0.5 468 9 4 0 44.427 88.854 0.391 2.86 4 13.8 0.1 469 4 5 7 44.468 88.937 0.392 2.86 8 27.4 0.5 470 6 8 0 44.484 88.968 0.392 2.86 4 115.4 4.3 471 7 7 1 44.494 88.987 0.392 2.86 8 66.3 2.8 472 1 10 1 44.499 88.998 0.392 2.85 8 5.3 0.0 473 6 2 7 44.535 89.07 0.392 2.85 8 44.9 1.3 474 8 2 5 44.606 89.213 0.393 2.85 8 247.7 39.5 475 5 4 7 44.622 89.244 0.393 2.85 8 68.4 3.0 476 3 7 6 44.633 89.266 0.393 2.85 8 20.6 0.3 477 4 9 2 44.668 89.337 0.393 2.85 8 15.5 0.2 478 9 4 1 44.765 89.53 0.394 2.84 8 36.4 0.8 479 6 8 1 44.822 89.644 0.394 2.84 8 33.6 0.7 480 0 5 8 44.862 89.724 0.394 2.84 4 73.1 1.7 481 8 4 4 44.867 89.733 0.394 2.84 8 43.9 1.2 482 2 0 9 44.897 89.795 0.395 2.83 4 118.3 4.5 483 8 6 0 44.962 89.924 0.395 2.83 4 8.3 0.0 484 8 5 3 44.977 89.954 0.395 2.83 8 59.8 2.3 X-ray diffraction powder data (I)...X-Ray wave length = 1.78892 (angs.): No H K L Theta 2*Theta d I int I int.n. I p.h.n. H(Si) ( degree ) (angstrem) *100 *100 1 1 1 1 7.222 14.443 7.11545 102.5 14.4 14.7 5.6 2 0 2 0 7.967 15.934 6.4535 156.8 22.0 22.4 5.6 3 2 0 0 8.212 16.424 6.262 155.1 21.8 22.2 5.6 4 0 0 2 8.836 17.672 5.823 153.1 21.5 21.9 5.6 5 1 2 0 8.97 17.94 5.73667 15.3 2.2 2.2 5.6 6 2 0 1 9.333 18.667 5.51527 7.6 1.1 1.1 5.6 7 0 1 2 9.702 19.403 5.30783 12.6 1.8 1.8 5.6 8 2 1 1 10.158 20.316 5.07165 15.9 2.2 2.3 5.6 9 1 1 2 10.546 21.092 4.88705 12.5 1.8 1.8 5.6 10 2 2 0 11.48 22.961 4.49408 115.0 16.2 16.4 5.6 11 0 2 2 11.94 23.881 4.32325 60.3 8.5 8.6 5.6 12 2 2 1 12.318 24.636 4.19274 50.4 7.1 7.2 5.6 13 2 1 2 12.762 25.525 4.04899 51.8 7.3 7.4 5.6 14 1 3 1 13.465 26.931 3.84124 44.8 6.3 6.4 5.6 15 3 1 1 13.764 27.528 3.75942 11.4 1.6 1.6 5.6 16 2 2 2 14.561 29.122 3.55773 93.0 13.1 13.2 5.6 17 3 2 0 14.784 29.569 3.5052 156.8 22.0 22.2 5.6 18 2 3 1 15.288 30.577 3.39227 19.9 2.8 2.8 5.6 19 1 3 2 15.556 31.112 3.33533 15.4 2.2 2.2 5.6 20 0 4 0 16.093 32.187 3.22675 18.0 2.5 2.5 5.6 21 2 3 2 17.177 34.355 3.02865 47.2 6.6 6.7 5.7 22 4 0 1 17.207 34.414 3.02363 15.0 2.1 2.1 5.7 23 1 4 1 17.24 34.48 3.01796 492.6 69.2 69.4 5.7 24 3 2 2 17.328 34.657 3.00309 28.2 4.0 4.0 5.7 25 4 1 1 17.688 35.376 2.94393 151.3 21.3 21.3 5.7 26 2 2 3 17.726 35.453 2.93774 36.5 5.1 5.1 5.7 27 0 0 4 17.892 35.783 2.9115 562.6 79.1 79.2 5.7 28 2 4 0 18.17 36.34 2.86834 226.0 31.8 31.8 5.7 29 0 1 4 18.357 36.714 2.84014 218.1 30.7 30.7 5.7 30 0 4 2 18.477 36.953 2.82238 117.7 16.5 16.6 5.7 31 1 3 3 18.569 37.139 2.80875 8.5 1.2 1.2 5.7 32 1 1 4 18.84 37.681 2.76981 33.6 4.7 4.7 5.7 33 4 0 2 18.927 37.853 2.75764 711.5 100.0 100.0 5.7 34 4 2 1 19.068 38.135 2.73801 176.0 24.7 24.7 5.7 35 4 1 2 19.371 38.741 2.69677 136.3 19.2 19.1 5.7 36 2 0 4 19.804 39.607 2.64009 28.0 3.9 3.9 5.7 37 2 3 3 19.977 39.953 2.61816 9.2 1.3 1.3 5.7 38 1 2 4 20.152 40.305 2.59626 8.5 1.2 1.2 5.7 39 2 4 2 20.342 40.684 2.5731 237.1 33.3 33.2 5.7 40 4 2 2 20.654 41.309 2.53583 10.6 1.5 1.5 5.7 41 3 4 1 21.019 42.037 2.4938 148.4 20.9 20.8 5.7 42 1 5 1 21.225 42.449 2.4707 61.9 8.7 8.7 5.7 43 1 4 3 21.559 43.119 2.43413 92.4 13.0 12.9 5.7 44 0 3 4 21.774 43.549 2.41126 16.9 2.4 2.4 5.7 45 5 1 1 21.825 43.651 2.40588 18.4 2.6 2.6 5.7 46 0 5 2 22.273 44.546 2.3599 8.1 1.1 1.1 5.7 47 2 5 1 22.493 44.987 2.33798 21.2 3.0 3.0 5.7 48 5 2 0 22.523 45.046 2.33508 54.7 7.7 7.6 5.7 49 4 3 2 22.66 45.321 2.32166 53.1 7.5 7.4 5.7 50 4 2 3 23.099 46.197 2.27994 20.8 2.9 2.9 5.7 51 1 1 5 23.372 46.745 2.25472 29.4 4.1 4.1 5.7 52 2 3 4 23.422 46.844 2.2502 13.3 1.9 1.8 5.7 53 2 5 2 23.894 47.788 2.20829 24.2 3.4 3.4 5.7 54 0 4 4 24.443 48.886 2.16163 14.8 2.1 2.1 5.7 55 3 5 1 24.492 48.985 2.15755 11.8 1.7 1.6 5.7 56 2 1 5 24.554 49.107 2.1525 34.4 4.8 4.8 5.7 57 5 3 1 24.853 49.705 2.12821 11.5 1.6 1.6 5.7 58 1 5 3 24.974 49.947 2.11856 209.8 29.5 29.1 5.7 59 6 0 0 25.374 50.747 2.08733 80.3 11.3 11.1 5.8 60 5 1 3 25.505 51.011 2.07727 22.7 3.2 3.1 5.8 61 2 2 5 25.628 51.257 2.06796 19.8 2.8 2.7 5.8 62 6 0 1 25.807 51.615 2.05459 7.4 1.0 1.0 5.8 63 2 4 4 25.96 51.921 2.04331 104.3 14.7 14.4 5.8 64 2 6 0 26.082 52.163 2.03447 8.5 1.2 1.2 5.8 65 6 1 1 26.157 52.313 2.02905 14.7 2.1 2.0 5.8 66 3 1 5 26.435 52.869 2.00923 20.6 2.9 2.8 5.8 67 2 6 1 26.507 53.014 2.00412 8.4 1.2 1.2 5.8 68 1 6 2 26.679 53.357 1.99218 29.7 4.2 4.1 5.8 69 6 0 2 27.079 54.158 1.96491 76.1 10.7 10.5 5.8 70 6 2 1 27.186 54.372 1.95777 13.0 1.8 1.8 5.8 71 5 4 1 27.293 54.586 1.95067 10.2 1.4 1.4 5.8 72 0 0 6 27.44 54.881 1.941 27.0 3.8 3.7 5.8 73 0 5 4 27.586 55.172 1.93154 18.0 2.5 2.5 5.8 74 3 5 3 27.907 55.814 1.91108 59.0 8.3 8.1 5.8 75 1 1 6 28.128 56.257 1.89726 36.6 5.1 5.0 5.8 76 5 1 4 28.433 56.866 1.87859 8.8 1.2 1.2 5.8 77 1 4 5 28.618 57.236 1.86746 35.2 4.9 4.8 5.8 78 1 6 3 28.732 57.464 1.86071 7.8 1.1 1.1 5.8 79 6 3 1 28.845 57.69 1.85403 52.2 7.3 7.2 5.8 80 4 1 5 28.922 57.844 1.84952 15.5 2.2 2.1 5.8 81 2 5 4 28.987 57.974 1.84573 24.1 3.4 3.3 5.8 82 1 2 6 29.11 58.22 1.83861 60.4 8.5 8.3 5.8 83 2 1 6 29.17 58.34 1.83514 41.9 5.9 5.8 5.8 84 5 2 4 29.408 58.817 1.8216 29.9 4.2 4.1 5.8 85 2 4 5 29.649 59.298 1.80813 14.7 2.1 2.0 5.8 86 1 7 1 29.756 59.512 1.80222 9.6 1.3 1.3 5.8 87 4 2 5 29.887 59.774 1.79505 8.2 1.2 1.1 5.8 88 6 3 2 30.03 60.059 1.78733 11.2 1.6 1.5 5.8 89 4 4 4 30.187 60.374 1.77886 38.6 5.4 5.3 5.8 90 6 2 3 30.391 60.781 1.76808 18.8 2.6 2.6 5.8 91 5 4 3 30.49 60.981 1.76285 7.5 1.1 1.0 5.8 92 0 7 2 30.587 61.173 1.75783 29.8 4.2 4.1 5.8 93 6 4 0 30.688 61.376 1.7526 114.5 16.1 15.6 5.8 94 7 2 0 31.251 62.503 1.72411 35.6 5.0 4.9 5.8 95 3 4 5 31.321 62.641 1.72069 76.2 10.7 10.4 5.8 96 1 6 4 31.459 62.919 1.71387 56.2 7.9 7.7 5.9 97 2 3 6 31.691 63.383 1.70262 46.3 6.5 6.3 5.9 98 3 2 6 31.787 63.574 1.69804 21.4 3.0 2.9 5.9 99 6 0 4 31.821 63.642 1.69641 20.9 2.9 2.8 5.9 100 6 3 3 31.944 63.889 1.69055 23.7 3.3 3.2 5.9 101 6 1 4 32.127 64.254 1.68195 12.8 1.8 1.7 5.9 102 6 4 2 32.207 64.414 1.67824 17.2 2.4 2.3 5.9 103 2 5 5 32.452 64.905 1.66691 31.3 4.4 4.3 5.9 104 0 4 6 32.532 65.064 1.66327 43.6 6.1 5.9 5.9 105 7 2 2 32.756 65.511 1.65317 20.5 2.9 2.8 5.9 106 4 0 6 32.833 65.666 1.64971 63.3 8.9 8.6 5.9 107 1 1 7 33.145 66.29 1.63592 121.8 17.1 16.5 5.9 108 5 6 0 33.237 66.473 1.63194 78.5 11.0 10.6 5.9 109 5 6 1 33.604 67.208 1.61615 9.2 1.3 1.2 5.9 110 7 1 3 33.699 67.397 1.61215 22.8 3.2 3.1 5.9 111 2 4 6 33.809 67.617 1.60753 70.2 9.9 9.5 5.9 112 3 6 4 34.03 68.06 1.59832 52.5 7.4 7.1 5.9 113 1 8 1 34.349 68.699 1.58526 19.4 2.7 2.6 5.9 114 4 7 1 34.624 69.248 1.57424 9.5 1.3 1.3 5.9 115 5 6 2 34.696 69.391 1.57139 42.0 5.9 5.7 5.9 116 8 0 0 34.845 69.69 1.5655 9.1 1.3 1.2 5.9 117 0 8 2 35.12 70.24 1.5548 82.2 11.5 11.1 5.9 118 7 4 1 35.225 70.449 1.55078 15.6 2.2 2.1 5.9 119 3 7 3 35.324 70.649 1.54696 14.2 2.0 1.9 5.9 120 1 5 6 35.519 71.037 1.5396 57.0 8.0 7.7 5.9 121 5 5 4 35.787 71.575 1.52957 7.7 1.1 1.0 5.9 122 5 1 6 35.951 71.902 1.52353 15.1 2.1 2.0 5.9 123 4 5 5 36.22 72.44 1.51376 9.9 1.4 1.3 5.9 124 6 2 5 36.29 72.58 1.51125 24.6 3.5 3.3 6.0 125 5 4 5 36.381 72.762 1.50797 80.1 11.3 10.7 6.0 126 2 5 6 36.441 72.882 1.50585 43.4 6.1 5.8 6.0 127 6 4 4 36.562 73.124 1.50155 41.5 5.8 5.6 6.0 128 6 5 3 36.678 73.355 1.49748 14.5 2.0 1.9 6.0 129 3 8 1 36.82 73.641 1.49249 27.9 3.9 3.7 6.0 130 7 2 4 37.08 74.161 1.48351 9.7 1.4 1.3 6.0 131 1 8 3 37.201 74.402 1.4794 48.4 6.8 6.5 6.0 132 1 4 7 37.523 75.047 1.46853 29.9 4.2 4.0 6.0 133 7 5 1 37.814 75.629 1.4589 15.8 2.2 2.1 6.0 134 7 4 3 38.049 76.098 1.45126 25.5 3.6 3.4 6.0 135 0 1 8 38.194 76.388 1.44658 30.3 4.3 4.0 6.0 136 8 1 3 38.313 76.625 1.44279 38.9 5.5 5.2 6.0 137 1 1 8 38.494 76.989 1.43702 10.3 1.5 1.4 6.0 138 4 8 0 38.585 77.171 1.43417 66.7 9.4 8.9 6.0 139 4 2 7 38.638 77.275 1.43253 25.0 3.5 3.3 6.0 140 5 6 4 38.927 77.853 1.42356 19.1 2.7 2.5 6.0 141 6 0 6 38.997 77.993 1.42141 9.3 1.3 1.2 6.0 142 0 2 8 39.041 78.081 1.42007 7.7 1.1 1.0 6.0 143 6 5 4 39.119 78.238 1.41768 23.1 3.2 3.1 6.0 144 4 6 5 39.347 78.694 1.41079 7.2 1.0 0.9 6.0 145 2 7 5 39.418 78.837 1.40864 11.2 1.6 1.5 6.0 146 4 7 4 39.892 79.784 1.39467 13.2 1.9 1.7 6.0 147 4 3 7 40.041 80.082 1.39035 16.9 2.4 2.2 6.0 148 8 0 4 40.445 80.89 1.37882 15.1 2.1 2.0 6.1 149 5 1 7 40.476 80.952 1.37794 9.9 1.4 1.3 6.1 150 7 6 0 40.561 81.121 1.37556 33.6 4.7 4.4 6.1 151 3 7 5 40.901 81.802 1.3661 11.4 1.6 1.5 6.1 152 6 3 6 41.508 83.017 1.34966 11.1 1.6 1.4 6.1 153 2 3 8 41.62 83.241 1.34669 19.8 2.8 2.6 6.1 154 7 6 2 41.924 83.849 1.33871 82.9 11.7 10.8 6.1 155 0 7 6 41.997 83.994 1.33683 47.3 6.6 6.2 6.1 156 1 7 6 42.291 84.581 1.32928 13.4 1.9 1.7 6.1 157 3 5 7 42.419 84.838 1.32601 7.5 1.1 1.0 6.1 158 5 7 4 42.546 85.092 1.3228 16.4 2.3 2.1 6.1 159 7 1 6 43.114 86.227 1.30875 31.9 4.5 4.2 6.1 160 8 0 5 43.505 87.01 1.2993 12.8 1.8 1.7 6.1 161 6 1 7 43.709 87.418 1.29445 8.3 1.2 1.1 6.2 162 7 2 6 43.94 87.88 1.28902 13.8 1.9 1.8 6.2 163 4 8 4 44.046 88.092 1.28655 71.8 10.1 9.3 6.2 164 6 8 0 44.484 88.968 1.27651 7.1 1.0 0.9 6.2 165 8 2 5 44.606 89.213 1.27374 42.7 6.0 5.5 6.2 Reference: Chichagov A.V. et al. Information-Calculating System on Crystal Structure Data of Minerals (MINCRYST) - Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian) |