Institute of Experimental Mineralogy Russian Academy of Sciences ------------------------------------------------- 142432, Chernogolovka, Moscow district A.V. Chichagov +7(496)52-22320 *** *** W W W - X R A Y P O L *** *********************** VLASOVITE 1 Na(2)ZrSi(4)O(11) Monoclinic C 2/c Z = 4 C2/c 28 .3 .1988 Ref.Str.: 1. Tikhonenkova R.P., Kazakova M.E. (1961) * Dokl. Akad. Nauk SSSR, 137, 944-946 2. Pjatenko Ju.A., Voronkov A.A. (1961) * Ibid., 141, 958-961 3. Voronkov A.A., Pjatenko Ju.A. (1961) * Kristallogr., SSSR, 6, 937-943 Initial data from BDM-file Lattice parameters (cub. angs.,degr.): a = 10.98 alpha = 90.0 b = 10.0 beta = 100.4 c = 8.52 gamma = 90.0 Unit cell volume (cub. angs.) = 920.13 Molar volume ( cub.cm/mol.) = 138.56 Co-ordinates, thermal parameters, occupation for atomic positions: NoP x/a y/b z/c B(j) atom / occupation 1 0.0 0.081 0.75 0.0 Na = 1.00 2 0.0 0.412 0.75 0.0 Na = 1.00 3 0.25 0.25 0.0 0.0 Zr = 1.00 4 0.265 0.072 0.638 0.0 Si = 1.00 5 0.049 0.216 0.431 0.0 Si = 1.00 6 0.0 0.166 0.25 0.0 O = 1.00 7 0.147 0.103 0.504 0.0 O = 1.00 8 0.111 0.358 0.418 0.0 O = 1.00 9 0.054 0.239 0.965 0.0 O = 1.00 10 0.243 0.137 0.8 0.0 O = 1.00 11 0.296 0.088 0.158 0.0 O = 1.00 Co-ordinates for all atomic positions : No NoP x/a y/b z/c 1 1 0.0 0.081 0.75 2 2 0.0 0.412 0.75 3 3 0.25 0.25 0.0 4 4 0.265 0.072 0.638 5 5 0.049 0.216 0.431 6 6 0.0 0.166 0.25 7 7 0.147 0.103 0.504 8 8 0.111 0.358 0.418 9 9 0.054 0.239 0.965 10 10 0.243 0.137 0.8 11 11 0.296 0.088 0.158 12 1 0.0 0.919 0.25 13 2 0.0 0.588 0.25 14 3 0.75 0.75 0.0 15 4 0.735 0.928 0.362 16 5 0.951 0.784 0.569 17 6 0.0 0.834 0.75 18 7 0.853 0.897 0.496 19 8 0.889 0.642 0.582 20 9 0.946 0.761 0.035 21 10 0.757 0.863 0.2 22 11 0.704 0.912 0.842 23 3 0.25 0.75 0.5 24 4 0.265 0.928 0.138 25 5 0.049 0.784 0.931 26 7 0.147 0.897 0.004 27 8 0.111 0.642 0.918 28 9 0.054 0.761 0.465 29 10 0.243 0.863 0.3 30 11 0.296 0.912 0.658 31 3 0.75 0.25 0.5 32 4 0.735 0.072 0.862 33 5 0.951 0.216 0.069 34 7 0.853 0.103 0.996 35 8 0.889 0.358 0.082 36 9 0.946 0.239 0.535 37 10 0.757 0.137 0.7 38 11 0.704 0.088 0.342 39 1 0.5 0.419 0.25 40 2 0.5 0.088 0.25 41 4 0.765 0.428 0.138 42 5 0.549 0.284 0.931 43 6 0.5 0.334 0.75 44 7 0.647 0.397 0.004 45 8 0.611 0.142 0.918 46 9 0.554 0.261 0.465 47 10 0.743 0.363 0.3 48 11 0.796 0.412 0.658 49 1 0.5 0.581 0.75 50 2 0.5 0.912 0.75 51 4 0.235 0.572 0.862 52 5 0.451 0.716 0.069 53 6 0.5 0.666 0.25 54 7 0.353 0.603 0.996 55 8 0.389 0.858 0.082 56 9 0.446 0.739 0.535 57 10 0.257 0.637 0.7 58 11 0.204 0.588 0.342 59 4 0.765 0.572 0.638 60 5 0.549 0.716 0.431 61 7 0.647 0.603 0.504 62 8 0.611 0.858 0.418 63 9 0.554 0.739 0.965 64 10 0.743 0.637 0.8 65 11 0.796 0.588 0.158 66 4 0.235 0.428 0.362 67 5 0.451 0.284 0.569 68 7 0.353 0.397 0.496 69 8 0.389 0.142 0.582 70 9 0.446 0.261 0.035 71 10 0.257 0.363 0.2 72 11 0.204 0.412 0.842 X-ray density (g/cm cub.) = 3.07 MU (1/cm) = 167.856 Mass attenuation coefficient (cm**2/g) = 54.662 Selected interatomic distances (cation-anion,anion-anion): NoP Atom Rad.sph. C.N. Distance NoP N. (angs.) (angs.) 1 Na 2.808 5 2.4107 9 2.684 10 2.47 6 2.4107 9 2.684 10 2 Na 2.808 4 2.5115 9 2.5115 9 2.2356 11 2.2356 11 3 Zr 2.616 6 2.1215 9 2.0345 10 2.1086 11 2.1215 9 2.0345 10 2.1086 11 4 Si 2.1 4 1.595 7 1.5831 10 1.6383 11 1.6751 8 5 Si 2.1 4 1.618 6 1.6062 7 1.5872 8 1.5744 9 6 O 3.264 6 2.5346 7 2.5673 8 2.7019 9 2.5346 7 2.5673 8 2.7019 9 7 O 3.264 7 2.5346 6 2.6629 8 2.5743 10 3.2486 10 2.6965 11 2.6459 9 2.6489 8 8 O 3.264 6 2.5673 6 2.6629 7 2.5187 9 2.644 11 2.6489 7 2.664 10 9 O 3.264 7 2.7019 6 2.8942 10 3.2353 11 2.6459 7 2.5187 8 2.9838 10 2.7252 11 10 O 3.264 8 2.5743 7 2.8942 9 3.04 11 3.2486 7 2.6682 11 2.664 8 2.9838 9 2.8159 11 11 O 3.264 7 3.2353 9 3.04 10 2.6965 7 2.6682 10 2.644 8 2.7252 9 2.8159 10 X-ray diffraction powder data (II), X-Ray W.L. = 1.54056(angs.): No H K L Theta 2*Theta S LPG MF F I int. ( degree ) *100 1 1 1 0 6.026 12.052 0.068 178.51 4 19.7 32.8 2 1 1 -1 7.514 15.029 0.085 113.99 4 62.7 211.8 3 2 0 0 8.201 16.402 0.093 95.34 2 121.2 330.9 4 1 1 1 8.498 16.996 0.096 88.65 4 108.1 489.5 5 0 2 0 8.862 17.724 0.1 81.34 2 186.0 664.8 6 0 2 1 10.334 20.669 0.116 59.24 4 55.4 86.0 7 0 0 2 10.593 21.187 0.119 56.27 2 148.9 294.8 8 1 1 -2 11.549 23.098 0.13 47.01 4 136.0 410.6 9 2 2 0 12.12 24.24 0.136 42.49 4 23.0 10.7 10 2 0 -2 12.203 24.405 0.137 41.89 2 229.6 521.6 11 2 2 -1 12.628 25.257 0.142 38.98 4 125.5 289.8 12 1 1 2 12.862 25.724 0.144 37.5 4 95.1 160.3 13 3 1 0 13.145 26.29 0.148 35.82 4 56.5 54.0 14 3 1 -1 13.318 26.637 0.15 34.84 4 199.4 654.3 15 2 2 1 13.845 27.691 0.155 32.09 4 75.2 85.8 16 0 2 2 13.878 27.756 0.156 31.93 4 256.1 989.1 17 1 3 0 13.995 27.99 0.157 31.36 4 58.7 51.1 18 2 0 2 14.609 29.217 0.164 28.62 2 49.4 16.5 19 1 3 -1 14.721 29.441 0.165 28.16 4 109.5 159.5 20 3 1 1 15.032 30.064 0.168 26.92 4 181.3 418.3 21 2 2 -2 15.162 30.325 0.17 26.43 4 73.7 67.8 22 1 3 1 15.263 30.527 0.171 26.06 4 281.9 978.5 23 3 1 -2 15.488 30.977 0.173 25.25 4 111.9 149.4 24 1 1 -3 16.426 32.852 0.184 22.24 4 1.8 0.0 25 4 0 0 16.577 33.153 0.185 21.8 2 314.4 509.1 26 2 2 2 17.19 34.38 0.192 20.15 4 3.3 0.1 27 1 3 -2 17.211 34.421 0.192 20.09 4 13.5 1.7 28 1 1 3 17.87 35.74 0.199 18.51 4 174.2 265.5 29 0 4 0 17.945 35.891 0.2 18.34 2 3.8 0.1 30 4 0 -2 18.074 36.149 0.201 18.05 2 75.0 24.0 31 1 3 2 18.148 36.296 0.202 17.89 4 36.7 11.4 32 3 3 0 18.357 36.714 0.204 17.45 4 49.4 20.1 33 3 1 2 18.408 36.816 0.205 17.34 4 20.6 3.5 34 0 2 3 18.413 36.827 0.205 17.33 4 39.5 12.8 35 3 3 -1 18.486 36.972 0.206 17.18 4 193.9 305.3 36 0 4 1 18.756 37.511 0.209 16.64 4 51.5 20.9 37 4 2 -1 18.824 37.648 0.209 16.51 4 41.4 13.4 38 4 2 0 18.919 37.839 0.21 16.33 4 88.9 61.0 39 2 2 -3 18.993 37.986 0.211 16.19 4 28.7 6.3 40 3 1 -3 19.043 38.086 0.212 16.09 4 131.1 130.7 41 3 3 1 19.799 39.598 0.22 14.76 4 60.6 25.6 42 2 4 0 19.848 39.697 0.22 14.68 4 10.1 0.7 43 3 3 -2 20.16 40.32 0.224 14.18 4 35.4 8.4 44 2 4 -1 20.179 40.359 0.224 14.15 4 2.7 0.0 45 4 2 -2 20.267 40.534 0.225 14.02 4 73.0 35.3 46 4 2 1 20.535 41.07 0.228 13.61 4 10.7 0.7 47 1 3 -3 20.914 41.828 0.232 13.07 4 195.4 235.7 48 2 4 1 21.003 42.006 0.233 12.94 4 30.3 5.6 49 0 4 2 21.026 42.052 0.233 12.91 4 220.5 296.7 50 5 1 -1 21.111 42.222 0.234 12.79 4 157.7 150.2 51 5 1 0 21.398 42.796 0.237 12.41 4 26.9 4.3 52 4 0 2 21.484 42.967 0.238 12.3 2 27.8 2.3 53 2 2 3 21.5 43.0 0.238 12.28 4 33.2 6.4 54 0 0 4 21.572 43.144 0.239 12.19 2 150.6 65.3 55 2 0 -4 21.69 43.381 0.24 12.04 2 27.4 2.1 56 1 1 -4 21.702 43.404 0.24 12.03 4 42.0 10.0 57 2 4 -2 21.941 43.881 0.243 11.73 4 42.1 9.8 58 1 3 3 22.107 44.214 0.244 11.54 4 99.7 54.2 59 5 1 -2 22.239 44.478 0.246 11.38 4 37.6 7.6 60 3 3 2 22.56 45.119 0.249 11.02 4 24.2 3.0 61 3 1 3 22.711 45.422 0.251 10.86 4 77.5 30.8 62 4 2 -3 23.008 46.015 0.254 10.54 4 16.9 1.4 63 5 1 1 23.058 46.116 0.254 10.49 4 73.1 26.5 64 1 5 0 23.06 46.119 0.254 10.49 4 83.3 34.4 65 3 3 -3 23.1 46.199 0.255 10.45 4 44.6 9.8 66 1 1 4 23.238 46.476 0.256 10.31 4 58.1 16.4 67 4 2 2 23.411 46.821 0.258 10.14 4 260.6 325.2 68 3 1 -4 23.461 46.921 0.258 10.09 4 41.1 8.0 69 2 4 2 23.464 46.929 0.258 10.08 4 68.9 22.6 70 0 2 4 23.493 46.987 0.259 10.05 4 148.2 104.3 71 1 5 -1 23.539 47.078 0.259 10.01 4 150.1 106.5 72 2 2 -4 23.604 47.208 0.26 9.95 4 247.2 287.2 73 1 5 1 23.907 47.815 0.263 9.66 4 50.0 11.4 74 0 4 3 24.424 48.849 0.268 9.21 4 50.4 11.0 75 5 1 -3 24.627 49.255 0.27 9.03 4 143.1 87.4 76 2 0 4 24.689 49.378 0.271 8.98 2 100.7 21.5 77 4 4 -1 24.753 49.505 0.272 8.93 4 101.0 43.1 78 4 4 0 24.829 49.658 0.273 8.87 4 93.1 36.3 79 2 4 -3 24.889 49.777 0.273 8.82 4 30.9 4.0 80 5 3 -1 24.894 49.788 0.273 8.81 4 9.8 0.4 81 4 0 -4 25.008 50.015 0.274 8.72 2 29.6 1.8 82 5 3 0 25.147 50.295 0.276 8.61 4 53.5 11.7 83 1 5 -2 25.289 50.577 0.277 8.5 4 72.1 20.9 84 6 0 0 25.337 50.675 0.278 8.47 2 148.8 44.3 85 1 3 -4 25.416 50.832 0.279 8.41 4 66.3 17.5 86 6 0 -2 25.735 51.469 0.282 8.17 2 274.8 145.8 87 5 1 2 25.884 51.769 0.283 8.07 4 14.2 0.8 88 5 3 -2 25.893 51.787 0.283 8.06 4 78.7 23.6 89 4 4 -2 25.929 51.857 0.284 8.03 4 175.1 116.3 90 1 5 2 25.984 51.968 0.284 8.0 4 100.5 38.1 91 3 5 0 26.141 52.283 0.286 7.89 4 46.9 8.2 92 4 4 1 26.151 52.301 0.286 7.88 4 20.0 1.5 93 3 5 -1 26.239 52.478 0.287 7.82 4 5.5 0.1 94 3 3 3 26.316 52.631 0.288 7.77 4 91.1 30.5 95 2 2 4 26.436 52.872 0.289 7.69 4 100.3 36.6 96 5 3 1 26.627 53.254 0.291 7.56 4 160.2 91.7 97 6 2 -1 26.645 53.29 0.291 7.55 4 109.4 42.7 98 4 2 -4 26.739 53.479 0.292 7.49 4 73.7 19.2 99 1 3 4 26.789 53.578 0.293 7.46 4 5.0 0.1 100 2 4 3 26.959 53.917 0.294 7.35 4 10.1 0.4 101 3 3 -4 26.99 53.98 0.295 7.33 4 49.1 8.3 102 6 2 0 27.054 54.108 0.295 7.29 4 141.4 68.9 103 4 2 3 27.245 54.489 0.297 7.18 4 29.1 2.9 104 3 5 1 27.251 54.503 0.297 7.17 4 77.7 20.5 105 1 1 -5 27.304 54.607 0.298 7.14 4 140.9 67.0 106 6 2 -2 27.434 54.868 0.299 7.07 4 139.5 65.0 107 0 6 0 27.527 55.054 0.3 7.01 2 280.7 130.5 108 3 5 -2 27.535 55.07 0.3 7.01 4 60.9 12.3 109 3 1 4 27.646 55.293 0.301 6.94 4 68.4 15.3 110 5 1 -4 28.038 56.077 0.305 6.72 4 18.4 1.1 111 5 3 -3 28.049 56.099 0.305 6.72 4 104.1 34.4 112 0 6 1 28.114 56.227 0.306 6.68 4 31.7 3.2 113 1 5 -3 28.135 56.27 0.306 6.67 4 142.5 64.0 114 4 4 -3 28.245 56.491 0.307 6.61 4 55.9 9.8 115 3 1 -5 28.483 56.967 0.31 6.49 4 84.4 21.8 116 4 4 2 28.594 57.188 0.311 6.43 4 285.2 247.1 117 6 2 1 28.626 57.252 0.311 6.42 4 68.6 14.3 118 0 4 4 28.666 57.332 0.311 6.4 4 86.2 22.5 119 2 4 -4 28.762 57.524 0.312 6.35 4 167.7 84.3 120 2 2 -5 28.77 57.539 0.312 6.34 4 53.5 8.6 121 2 6 0 28.926 57.852 0.314 6.27 4 110.6 36.2 122 1 1 5 28.935 57.87 0.314 6.26 4 179.6 95.4 123 0 2 5 28.994 57.989 0.315 6.23 4 34.9 3.6 124 1 5 3 29.103 58.205 0.316 6.18 4 198.5 115.1 125 2 6 -1 29.177 58.354 0.316 6.15 4 34.5 3.5 126 5 3 2 29.203 58.405 0.317 6.13 4 64.9 12.2 127 6 2 -3 29.355 58.709 0.318 6.06 4 13.5 0.5 128 3 5 2 29.476 58.951 0.319 6.01 4 49.3 6.9 129 5 1 3 29.645 59.291 0.321 5.93 4 134.1 50.4 130 6 0 2 29.691 59.381 0.322 5.91 2 45.4 2.9 131 7 1 -1 29.807 59.614 0.323 5.86 4 86.0 20.5 132 2 6 1 29.81 59.62 0.323 5.86 4 10.4 0.3 133 0 6 2 29.827 59.655 0.323 5.85 4 106.1 31.1 134 3 5 -3 29.924 59.849 0.324 5.81 4 204.8 115.1 135 4 0 4 30.294 60.587 0.327 5.65 2 230.8 71.1 136 7 1 0 30.343 60.687 0.328 5.63 4 73.0 14.2 137 7 1 -2 30.387 60.773 0.328 5.61 4 52.7 7.3 138 1 3 -5 30.518 61.037 0.33 5.56 4 21.8 1.3 139 2 6 -2 30.545 61.089 0.33 5.55 4 133.8 46.9 140 6 0 -4 30.756 61.512 0.332 5.46 2 6.9 0.1 141 3 3 4 30.838 61.676 0.333 5.43 4 35.4 3.2 142 5 3 -4 31.205 62.409 0.336 5.29 4 29.4 2.2 143 4 2 -5 31.243 62.486 0.337 5.28 4 41.6 4.3 144 6 2 2 31.247 62.493 0.337 5.27 4 97.8 23.8 145 2 4 4 31.268 62.536 0.337 5.27 4 107.1 28.6 146 5 5 -1 31.444 62.887 0.339 5.2 4 61.5 9.3 147 6 4 -1 31.456 62.912 0.339 5.2 4 41.3 4.2 148 4 4 -4 31.541 63.082 0.34 5.17 4 54.5 7.2 149 3 3 -5 31.622 63.244 0.34 5.14 4 93.6 21.2 150 5 5 0 31.661 63.322 0.341 5.12 4 49.1 5.8 151 2 6 2 31.77 63.54 0.342 5.09 4 83.6 16.8 152 6 4 0 31.825 63.65 0.342 5.07 4 127.4 38.9 153 4 2 4 31.832 63.664 0.342 5.06 4 198.0 93.8 154 2 2 5 31.883 63.766 0.343 5.05 4 42.8 4.4 155 1 5 -4 31.893 63.786 0.343 5.04 4 26.7 1.7 156 7 1 1 31.962 63.925 0.344 5.02 4 118.5 33.3 157 4 4 3 31.997 63.995 0.344 5.01 4 31.8 2.4 158 7 1 -3 32.046 64.093 0.344 4.99 4 94.9 21.2 159 1 3 5 32.047 64.093 0.344 4.99 4 144.7 49.3 160 6 4 -2 32.169 64.337 0.346 4.95 4 150.9 53.3 161 5 1 -5 32.277 64.553 0.347 4.91 4 206.7 99.2 162 6 2 -4 32.282 64.564 0.347 4.91 4 244.0 138.1 163 5 5 -2 32.307 64.614 0.347 4.9 4 97.5 22.0 164 0 6 3 32.56 65.12 0.349 4.82 4 53.6 6.6 165 3 5 3 32.675 65.35 0.35 4.79 4 86.7 17.0 166 5 3 3 32.717 65.434 0.351 4.77 4 2.9 0.0 167 4 6 -1 32.833 65.666 0.352 4.74 4 59.0 7.8 168 7 3 -1 32.87 65.739 0.352 4.72 4 205.1 93.9 169 4 6 0 32.897 65.795 0.353 4.72 4 197.4 86.9 170 2 6 -3 32.947 65.894 0.353 4.7 4 72.9 11.8 171 5 5 1 32.948 65.895 0.353 4.7 4 43.3 4.2 172 1 7 0 32.949 65.898 0.353 4.7 4 80.8 14.5 173 2 0 -6 32.967 65.934 0.353 4.69 2 295.3 96.7 174 1 5 4 33.09 66.181 0.354 4.66 4 17.1 0.6 175 3 1 5 33.114 66.228 0.355 4.65 4 86.8 16.6 176 6 4 1 33.256 66.512 0.356 4.61 4 84.5 15.5 177 3 5 -4 33.267 66.534 0.356 4.61 4 11.7 0.3 178 1 1 -6 33.272 66.545 0.356 4.6 4 74.0 11.9 179 1 7 -1 33.33 66.659 0.357 4.59 4 140.3 42.7 180 7 3 0 33.378 66.756 0.357 4.57 4 21.8 1.0 181 2 4 -5 33.388 66.776 0.357 4.57 4 47.5 4.9 182 7 3 -2 33.419 66.838 0.358 4.56 4 35.8 2.8 183 0 0 6 33.471 66.941 0.358 4.55 2 52.4 3.0 184 0 4 5 33.595 67.19 0.359 4.51 4 6.9 0.1 185 1 7 1 33.624 67.249 0.359 4.5 4 47.9 4.9 186 4 6 -2 33.824 67.648 0.361 4.45 4 82.4 14.3 187 6 4 -3 33.927 67.853 0.362 4.42 4 37.7 3.0 188 4 6 1 34.013 68.027 0.363 4.4 4 70.8 10.4 189 3 1 -6 34.036 68.072 0.363 4.39 4 45.1 4.2 190 5 1 4 34.182 68.363 0.365 4.35 4 62.0 7.9 191 5 5 -3 34.207 68.414 0.365 4.34 4 93.7 18.0 192 2 2 -6 34.44 68.881 0.367 4.28 4 131.2 34.9 193 8 0 -2 34.542 69.085 0.368 4.26 2 31.5 1.0 194 7 1 2 34.581 69.163 0.368 4.25 4 44.5 4.0 195 7 1 -4 34.702 69.404 0.37 4.22 4 53.0 5.6 196 2 6 3 34.707 69.414 0.37 4.22 4 87.4 15.2 197 1 7 -2 34.749 69.498 0.37 4.21 4 132.4 34.8 198 6 2 3 34.788 69.576 0.37 4.2 4 8.1 0.1 199 8 0 0 34.792 69.584 0.37 4.2 2 170.4 28.8 200 7 3 1 34.921 69.842 0.372 4.16 4 111.6 24.5 201 0 2 6 34.933 69.867 0.372 4.16 4 31.1 1.9 202 4 0 -6 34.986 69.971 0.372 4.15 2 13.9 0.2 203 7 3 -3 35.001 70.002 0.372 4.14 4 3.0 0.0 204 1 1 6 35.024 70.048 0.373 4.14 4 71.3 9.9 205 5 3 -5 35.222 70.443 0.374 4.09 4 23.4 1.1 206 5 5 2 35.243 70.486 0.375 4.09 4 52.9 5.4 207 1 7 2 35.326 70.652 0.375 4.07 4 6.1 0.1 208 3 7 0 35.458 70.915 0.377 4.04 4 58.4 6.5 209 3 7 -1 35.539 71.079 0.377 4.02 4 71.6 9.7 210 8 2 -1 35.598 71.195 0.378 4.01 4 3.6 0.0 211 4 4 -5 35.681 71.363 0.379 3.99 4 18.0 0.6 212 6 4 2 35.685 71.37 0.379 3.99 4 82.1 12.7 213 4 6 -3 35.828 71.655 0.38 3.96 4 15.3 0.4 214 8 2 -2 35.985 71.97 0.381 3.92 4 0.6 0.0 215 3 3 5 36.026 72.051 0.382 3.91 4 38.0 2.7 216 6 2 -5 36.096 72.192 0.382 3.9 4 70.5 9.2 217 4 6 2 36.135 72.269 0.383 3.89 4 36.1 2.4 218 1 3 -6 36.178 72.356 0.383 3.88 4 30.5 1.7 219 0 6 4 36.198 72.396 0.383 3.88 4 93.8 16.1 220 8 2 0 36.23 72.46 0.384 3.87 4 2.5 0.0 221 4 4 4 36.234 72.468 0.384 3.87 4 114.6 24.0 222 2 4 5 36.282 72.564 0.384 3.86 4 103.8 19.7 223 2 6 -4 36.283 72.566 0.384 3.86 4 19.2 0.7 224 3 7 1 36.395 72.791 0.385 3.84 4 122.1 27.0 225 4 2 -6 36.42 72.841 0.385 3.83 4 54.1 5.3 226 1 5 -5 36.44 72.88 0.386 3.83 4 129.5 30.4 227 2 0 6 36.446 72.893 0.386 3.83 2 240.7 52.4 228 3 7 -2 36.638 73.275 0.387 3.79 4 132.8 31.6 229 6 4 -4 36.658 73.316 0.388 3.79 4 244.9 107.2 230 3 5 4 36.733 73.466 0.388 3.77 4 120.5 25.9 231 3 3 -6 36.914 73.829 0.39 3.74 4 56.1 5.6 232 5 3 4 37.055 74.11 0.391 3.71 4 19.5 0.7 233 5 5 -4 37.07 74.14 0.391 3.71 4 70.7 8.8 234 4 2 5 37.09 74.18 0.391 3.7 4 92.8 15.1 235 1 7 -3 37.154 74.307 0.392 3.69 4 34.9 2.1 236 5 1 -6 37.243 74.487 0.393 3.67 4 124.3 26.8 237 8 2 -3 37.379 74.758 0.394 3.65 4 48.2 4.0 238 7 3 2 37.442 74.883 0.395 3.64 4 7.4 0.1 239 3 5 -5 37.455 74.911 0.395 3.64 4 66.9 7.7 240 7 3 -4 37.559 75.118 0.396 3.62 4 49.4 4.2 241 6 0 4 37.769 75.538 0.398 3.58 2 43.7 1.6 242 1 5 5 37.849 75.698 0.398 3.57 4 47.8 3.8 243 2 2 6 37.859 75.718 0.398 3.57 4 44.9 3.4 244 8 2 1 37.862 75.724 0.398 3.57 4 127.3 27.3 245 1 3 6 37.871 75.742 0.398 3.57 4 0.3 0.0 246 1 7 3 37.995 75.991 0.4 3.54 4 85.5 12.3 247 0 8 0 38.041 76.082 0.4 3.54 2 67.5 3.8 248 7 1 3 38.113 76.226 0.401 3.53 4 119.6 23.8 249 7 1 -5 38.268 76.537 0.402 3.5 4 80.8 10.8 250 3 7 2 38.323 76.646 0.403 3.49 4 149.1 36.7 251 8 0 -4 38.353 76.706 0.403 3.49 2 59.4 2.9 252 5 5 3 38.473 76.945 0.404 3.47 4 214.4 75.3 253 2 6 4 38.532 77.064 0.404 3.46 4 5.3 0.0 254 0 8 1 38.539 77.077 0.404 3.46 4 34.8 2.0 255 7 5 -1 38.615 77.231 0.405 3.45 4 29.4 1.4 256 6 6 -1 38.703 77.407 0.406 3.43 4 7.8 0.1 257 2 4 -6 38.707 77.413 0.406 3.43 4 82.1 10.9 258 3 7 -3 38.719 77.438 0.406 3.43 4 106.1 18.2 259 4 6 -4 38.781 77.562 0.407 3.42 4 1.6 0.0 260 6 4 3 39.04 78.079 0.409 3.38 4 55.2 4.9 261 6 6 0 39.041 78.081 0.409 3.38 4 86.3 11.9 262 8 0 2 39.071 78.141 0.409 3.38 2 54.3 2.4 263 7 5 0 39.091 78.183 0.409 3.38 4 88.8 12.6 264 7 5 -2 39.13 78.26 0.41 3.37 4 60.3 5.8 265 3 1 6 39.143 78.286 0.41 3.37 4 75.7 9.1 266 6 2 4 39.165 78.33 0.41 3.37 4 68.5 7.5 267 0 4 6 39.179 78.357 0.41 3.36 4 68.2 7.4 268 4 6 3 39.199 78.398 0.41 3.36 4 27.3 1.2 269 2 8 0 39.236 78.473 0.411 3.36 4 70.4 7.9 270 6 0 -6 39.354 78.708 0.412 3.34 2 155.4 19.1 271 6 6 -2 39.356 78.712 0.412 3.34 4 200.2 63.2 272 5 1 5 39.437 78.874 0.412 3.33 4 154.1 37.3 273 2 8 -1 39.453 78.907 0.412 3.33 4 66.5 7.0 274 9 1 -1 39.532 79.064 0.413 3.32 4 67.7 7.2 275 1 1 -7 39.725 79.45 0.415 3.29 4 93.8 13.7 276 8 2 -4 39.743 79.485 0.415 3.29 4 60.3 5.7 277 9 1 -2 39.768 79.536 0.415 3.28 4 17.7 0.5 278 8 4 -1 39.817 79.634 0.416 3.28 4 31.5 1.5 279 2 8 1 40.005 80.01 0.417 3.25 4 57.4 5.1 280 0 8 2 40.02 80.041 0.417 3.25 4 142.3 31.1 281 5 3 -6 40.033 80.065 0.418 3.25 4 61.1 5.7 282 5 7 -1 40.079 80.157 0.418 3.24 4 178.6 48.9 283 3 1 -7 40.165 80.33 0.419 3.23 4 22.5 0.8 284 8 4 -2 40.19 80.38 0.419 3.23 4 21.3 0.7 285 5 7 0 40.275 80.551 0.42 3.22 4 72.7 8.0 286 9 1 0 40.28 80.561 0.42 3.22 4 73.1 8.1 287 6 4 -5 40.297 80.594 0.42 3.22 4 12.9 0.3 288 6 6 1 40.361 80.722 0.42 3.21 4 48.1 3.5 289 8 4 0 40.426 80.853 0.421 3.2 4 33.7 1.7 290 8 2 2 40.454 80.907 0.421 3.2 4 115.7 20.2 291 2 6 -5 40.484 80.968 0.421 3.2 4 46.9 3.3 292 1 7 -4 40.486 80.971 0.421 3.2 4 87.4 11.5 293 7 5 1 40.549 81.098 0.422 3.19 4 140.2 29.6 294 4 4 -6 40.61 81.221 0.423 3.18 4 55.3 4.6 295 7 5 -3 40.625 81.25 0.423 3.18 4 147.2 32.5 296 2 8 -2 40.652 81.305 0.423 3.18 4 55.6 4.6 297 0 6 5 40.676 81.353 0.423 3.17 4 69.9 7.3 298 2 2 -7 40.683 81.367 0.423 3.17 4 13.7 0.3 299 6 2 -6 40.734 81.469 0.424 3.17 4 122.1 22.3 300 5 5 -5 40.835 81.67 0.424 3.16 4 140.5 29.4 301 5 7 -2 40.863 81.725 0.425 3.15 4 29.5 1.3 302 7 3 3 40.885 81.769 0.425 3.15 4 86.4 11.1 303 9 1 -3 40.984 81.967 0.426 3.14 4 80.0 9.5 304 6 6 -3 40.986 81.972 0.426 3.14 4 35.6 1.9 305 7 3 -5 41.037 82.074 0.426 3.13 4 48.2 3.4 306 3 7 3 41.199 82.399 0.428 3.12 4 41.7 2.6 307 4 4 5 41.259 82.518 0.428 3.11 4 11.4 0.2 308 0 2 7 41.423 82.846 0.429 3.09 4 3.7 0.0 309 5 7 1 41.45 82.9 0.43 3.09 4 84.5 10.4 310 8 4 -3 41.539 83.079 0.43 3.08 4 8.2 0.1 311 1 7 4 41.581 83.162 0.431 3.08 4 80.5 9.4 312 3 5 5 41.603 83.206 0.431 3.08 4 95.2 13.2 313 1 1 7 41.646 83.292 0.431 3.07 4 62.3 5.6 314 4 0 6 41.691 83.381 0.432 3.07 2 136.8 13.6 315 3 7 -4 41.744 83.488 0.432 3.06 4 48.6 3.4 316 2 8 2 41.747 83.494 0.432 3.06 4 51.4 3.8 317 1 5 -6 41.749 83.498 0.432 3.06 4 23.4 0.8 318 3 3 6 41.897 83.795 0.433 3.05 4 35.4 1.8 319 9 1 1 42.001 84.002 0.434 3.04 4 32.9 1.6 320 2 4 6 42.007 84.013 0.434 3.04 4 23.2 0.8 321 8 4 1 42.009 84.019 0.434 3.04 4 30.1 1.3 322 5 3 5 42.187 84.374 0.436 3.02 4 128.1 23.4 323 9 3 -1 42.281 84.561 0.437 3.01 4 120.5 20.7 324 4 2 -7 42.295 84.59 0.437 3.01 4 43.0 2.6 325 3 5 -6 42.457 84.914 0.438 3.0 4 99.7 14.1 326 0 8 3 42.463 84.925 0.438 3.0 4 51.4 3.7 327 1 3 -7 42.471 84.942 0.438 3.0 4 205.8 59.9 328 9 3 -2 42.513 85.027 0.439 2.99 4 82.3 9.6 329 7 1 4 42.514 85.028 0.439 2.99 4 10.9 0.2 330 5 5 4 42.593 85.186 0.439 2.99 4 28.0 1.1 331 5 7 -3 42.617 85.233 0.44 2.98 4 88.1 11.0 332 4 6 -5 42.641 85.283 0.44 2.98 4 16.9 0.4 333 6 6 2 42.645 85.289 0.44 2.98 4 40.4 2.3 334 7 1 -6 42.703 85.407 0.44 2.98 4 87.6 10.8 335 4 8 -1 42.712 85.424 0.44 2.98 4 20.5 0.6 336 4 8 0 42.771 85.541 0.441 2.97 4 13.4 0.3 337 2 8 -3 42.816 85.632 0.441 2.97 4 80.0 9.0 338 3 3 -7 42.906 85.811 0.442 2.96 4 33.6 1.6 339 5 1 -7 42.951 85.902 0.442 2.96 4 108.3 16.4 340 7 5 2 42.967 85.933 0.442 2.96 4 27.7 1.1 341 9 3 0 43.02 86.039 0.443 2.95 4 35.6 1.8 342 8 2 -5 43.042 86.085 0.443 2.95 4 21.5 0.6 343 4 2 6 43.056 86.113 0.443 2.95 4 110.7 17.1 344 7 5 -4 43.08 86.16 0.443 2.95 4 14.3 0.3 345 9 1 -4 43.164 86.327 0.444 2.94 4 60.2 5.0 346 4 6 4 43.168 86.336 0.444 2.94 4 91.7 11.7 347 2 6 5 43.214 86.427 0.444 2.94 4 47.2 3.1 348 6 4 4 43.284 86.568 0.445 2.93 4 60.2 5.0 349 1 5 6 43.383 86.765 0.446 2.93 4 88.9 10.9 350 6 6 -4 43.574 87.147 0.447 2.91 4 31.7 1.4 351 5 7 2 43.589 87.177 0.448 2.91 4 16.5 0.4 352 4 8 -2 43.624 87.247 0.448 2.91 4 63.8 5.6 353 9 3 -3 43.716 87.432 0.449 2.9 4 161.6 35.8 354 4 8 1 43.799 87.598 0.449 2.9 4 32.7 1.5 355 8 4 -4 43.851 87.702 0.45 2.89 4 24.5 0.8 356 8 2 3 43.978 87.956 0.451 2.89 4 53.3 3.9 357 1 9 0 44.18 88.359 0.452 2.87 4 59.2 4.8 358 1 3 7 44.373 88.746 0.454 2.86 4 113.0 17.3 359 6 2 5 44.376 88.752 0.454 2.86 4 7.1 0.1 360 2 8 3 44.446 88.891 0.455 2.86 4 50.8 3.5 361 2 2 7 44.497 88.994 0.455 2.85 4 40.3 2.2 362 1 9 -1 44.528 89.057 0.455 2.85 4 81.5 9.0 363 8 4 2 44.552 89.104 0.455 2.85 4 129.7 22.7 364 9 1 2 44.679 89.358 0.456 2.84 4 31.2 1.3 365 10 0 -2 44.724 89.447 0.457 2.84 2 256.7 44.3 366 1 7 -5 44.726 89.451 0.457 2.84 4 123.5 20.5 367 9 3 1 44.726 89.452 0.457 2.84 4 124.8 20.9 368 2 4 -7 44.779 89.558 0.457 2.84 4 11.8 0.2 369 1 9 1 44.8 89.599 0.457 2.84 4 154.1 31.9 370 6 4 -6 44.83 89.659 0.458 2.84 4 107.7 15.6 X-ray diffraction powder data (I)...X-Ray wave length = 1.54056 (angs.): No H K L Theta 2*Theta d I int I int.n. I p.h.n. H(Si) ( degree ) (angstrem) *100 *100 1 1 1 0 6.026 12.052 7.33749 32.8 3.3 3.3 5.6 2 1 1 -1 7.514 15.029 5.89004 211.8 21.4 21.6 5.6 3 2 0 0 8.201 16.402 5.39981 330.9 33.5 33.7 5.6 4 1 1 1 8.498 16.996 5.21263 489.5 49.5 49.9 5.6 5 0 2 0 8.862 17.724 5.0 664.8 67.2 67.7 5.6 6 0 2 1 10.334 20.669 4.29379 86.0 8.7 8.7 5.6 7 0 0 2 10.593 21.187 4.19001 294.8 29.8 30.0 5.6 8 1 1 -2 11.549 23.098 3.84743 410.6 41.5 41.7 5.6 9 2 2 0 12.12 24.24 3.66874 10.7 1.1 1.1 5.6 10 2 0 -2 12.203 24.405 3.64424 521.6 52.7 52.9 5.6 11 2 2 -1 12.628 25.257 3.52328 289.8 29.3 29.4 5.6 12 1 1 2 12.862 25.724 3.46038 160.3 16.2 16.2 5.6 13 3 1 0 13.145 26.29 3.38709 54.0 5.5 5.5 5.6 14 3 1 -1 13.318 26.637 3.34379 654.3 66.1 66.2 5.6 15 2 2 1 13.845 27.691 3.21887 85.8 8.7 8.7 5.6 16 0 2 2 13.878 27.756 3.21147 989.1 100.0 100.0 5.6 17 1 3 0 13.995 27.99 3.18507 51.1 5.2 5.2 5.6 18 2 0 2 14.609 29.217 3.05405 16.5 1.7 1.7 5.6 19 1 3 -1 14.721 29.441 3.03135 159.5 16.1 16.1 5.6 20 3 1 1 15.032 30.064 2.96991 418.3 42.3 42.2 5.6 21 2 2 -2 15.162 30.325 2.94502 67.8 6.9 6.8 5.6 22 1 3 1 15.263 30.527 2.92599 978.5 98.9 98.7 5.6 23 3 1 -2 15.488 30.977 2.88447 149.4 15.1 15.1 5.6 24 4 0 0 16.577 33.153 2.6999 509.1 51.5 51.2 5.6 25 1 1 3 17.87 35.74 2.51021 265.5 26.8 26.7 5.7 26 4 0 -2 18.074 36.149 2.48276 24.0 2.4 2.4 5.7 27 1 3 2 18.148 36.296 2.473 11.4 1.1 1.1 5.7 28 3 3 0 18.357 36.714 2.44583 20.1 2.0 2.0 5.7 29 0 2 3 18.413 36.827 2.43859 16.3 1.6 1.6 5.7 30 3 3 -1 18.486 36.972 2.42938 305.3 30.9 30.6 5.7 31 0 4 1 18.756 37.511 2.39567 20.9 2.1 2.1 5.7 32 4 2 -1 18.824 37.648 2.38728 13.4 1.4 1.3 5.7 33 4 2 0 18.919 37.839 2.37568 61.0 6.2 6.1 5.7 34 3 1 -3 19.043 38.086 2.36082 130.7 13.2 13.1 5.7 35 3 3 1 19.799 39.598 2.27406 25.6 2.6 2.6 5.7 36 4 2 -2 20.267 40.534 2.22371 35.3 3.6 3.5 5.7 37 1 3 -3 20.914 41.828 2.15783 235.7 23.8 23.5 5.7 38 0 4 2 21.026 42.052 2.14689 302.3 30.6 30.2 5.7 39 5 1 -1 21.111 42.222 2.13861 150.2 15.2 15.0 5.7 40 0 0 4 21.572 43.144 2.09501 65.3 6.6 6.5 5.7 41 1 1 -4 21.702 43.404 2.08308 12.2 1.2 1.2 5.7 42 1 3 3 22.107 44.214 2.04679 54.2 5.5 5.4 5.7 43 3 1 3 22.711 45.422 1.9951 30.8 3.1 3.1 5.7 44 1 5 0 23.06 46.119 1.96656 60.9 6.2 6.0 5.7 45 1 1 4 23.238 46.476 1.95228 16.4 1.7 1.6 5.7 46 4 2 2 23.411 46.821 1.9387 325.2 32.9 32.3 5.7 47 2 4 2 23.464 46.929 1.93451 30.6 3.1 3.0 5.7 48 0 2 4 23.493 46.987 1.93225 104.3 10.5 10.4 5.7 49 1 5 -1 23.539 47.078 1.9287 106.5 10.8 10.6 5.7 50 2 2 -4 23.604 47.208 1.92371 287.2 29.0 28.5 5.7 51 1 5 1 23.907 47.815 1.9007 11.4 1.2 1.1 5.7 52 0 4 3 24.424 48.849 1.86287 11.0 1.1 1.1 5.7 53 5 1 -3 24.627 49.255 1.84846 87.4 8.8 8.7 5.7 54 2 0 4 24.689 49.378 1.84412 21.5 2.2 2.1 5.7 55 4 4 -1 24.753 49.505 1.83969 43.1 4.4 4.3 5.7 56 4 4 0 24.829 49.658 1.83437 36.3 3.7 3.6 5.7 57 5 3 0 25.147 50.295 1.81265 11.7 1.2 1.2 5.8 58 1 5 -2 25.289 50.577 1.80318 20.9 2.1 2.1 5.8 59 6 0 0 25.337 50.675 1.79994 44.3 4.5 4.4 5.8 60 1 3 -4 25.416 50.832 1.79473 17.5 1.8 1.7 5.8 61 6 0 -2 25.735 51.469 1.77401 145.8 14.7 14.4 5.8 62 5 3 -2 25.893 51.787 1.76387 23.6 2.4 2.3 5.8 63 4 4 -2 25.929 51.857 1.76164 116.3 11.8 11.5 5.8 64 1 5 2 25.984 51.968 1.75814 38.1 3.9 3.8 5.8 65 3 3 3 26.316 52.631 1.73754 30.5 3.1 3.0 5.8 66 2 2 4 26.436 52.872 1.73019 36.6 3.7 3.6 5.8 67 5 3 1 26.627 53.254 1.71869 134.4 13.6 13.2 5.8 68 4 2 -4 26.739 53.479 1.71198 19.2 1.9 1.9 5.8 69 6 2 0 27.054 54.108 1.69354 68.9 7.0 6.8 5.8 70 3 5 1 27.251 54.503 1.68222 23.3 2.4 2.3 5.8 71 1 1 -5 27.304 54.607 1.67925 67.0 6.8 6.6 5.8 72 6 2 -2 27.434 54.868 1.6719 65.0 6.6 6.4 5.8 73 0 6 0 27.527 55.054 1.66667 142.8 14.4 14.0 5.8 74 3 1 4 27.646 55.293 1.66005 15.3 1.5 1.5 5.8 75 5 3 -3 28.049 56.099 1.63809 35.5 3.6 3.5 5.8 76 1 5 -3 28.135 56.27 1.6335 67.2 6.8 6.6 5.8 77 3 1 -5 28.483 56.967 1.61516 21.8 2.2 2.1 5.8 78 4 4 2 28.594 57.188 1.60943 247.1 25.0 24.2 5.8 79 6 2 1 28.626 57.252 1.60781 14.3 1.4 1.4 5.8 80 0 4 4 28.666 57.332 1.60574 22.5 2.3 2.2 5.8 81 2 4 -4 28.762 57.524 1.60083 92.9 9.4 9.1 5.8 82 1 1 5 28.935 57.87 1.59208 131.6 13.3 12.9 5.8 83 1 5 3 29.103 58.205 1.58371 115.1 11.6 11.3 5.8 84 5 3 2 29.203 58.405 1.57877 15.7 1.6 1.5 5.8 85 5 1 3 29.645 59.291 1.55728 50.4 5.1 4.9 5.8 86 0 6 2 29.827 59.655 1.54865 51.9 5.2 5.1 5.8 87 3 5 -3 29.924 59.849 1.5441 115.1 11.6 11.2 5.8 88 4 0 4 30.294 60.587 1.52702 71.1 7.2 6.9 5.8 89 7 1 0 30.343 60.687 1.52476 14.2 1.4 1.4 5.8 90 2 6 -2 30.545 61.089 1.51568 48.2 4.9 4.7 5.8 91 2 4 4 31.268 62.536 1.48405 56.7 5.7 5.5 5.8 92 5 5 -1 31.444 62.887 1.4766 13.5 1.4 1.3 5.9 93 3 3 -5 31.622 63.244 1.46912 21.2 2.1 2.1 5.9 94 2 6 2 31.77 63.54 1.46299 16.8 1.7 1.6 5.9 95 4 2 4 31.832 63.664 1.46043 132.6 13.4 12.9 5.9 96 7 1 1 31.962 63.925 1.45511 33.3 3.4 3.2 5.9 97 1 3 5 32.047 64.093 1.45169 70.6 7.1 6.8 5.9 98 6 4 -2 32.169 64.337 1.44677 53.3 5.4 5.2 5.9 99 6 2 -4 32.282 64.564 1.44223 259.3 26.2 25.1 5.9 100 3 5 3 32.675 65.35 1.42678 17.0 1.7 1.6 5.9 101 7 3 -1 32.87 65.739 1.41927 180.7 18.3 17.5 5.9 102 2 0 -6 32.967 65.934 1.41554 127.1 12.9 12.3 5.9 103 3 1 5 33.114 66.228 1.40998 16.6 1.7 1.6 5.9 104 6 4 1 33.256 66.512 1.40464 27.8 2.8 2.7 5.9 105 1 7 -1 33.33 66.659 1.4019 42.7 4.3 4.1 5.9 106 4 6 -2 33.824 67.648 1.38379 14.3 1.4 1.4 5.9 107 4 6 1 34.013 68.027 1.37701 14.6 1.5 1.4 5.9 108 5 5 -3 34.207 68.414 1.37016 25.9 2.6 2.5 5.9 109 2 2 -6 34.44 68.881 1.36201 34.9 3.5 3.4 5.9 110 2 6 3 34.707 69.414 1.35284 20.8 2.1 2.0 5.9 111 1 7 -2 34.749 69.498 1.35141 34.8 3.5 3.3 5.9 112 8 0 0 34.792 69.584 1.34995 28.8 2.9 2.8 5.9 113 7 3 1 34.921 69.842 1.3456 26.4 2.7 2.5 5.9 114 1 1 6 35.024 70.048 1.34213 9.9 1.0 1.0 5.9 115 6 4 2 35.685 71.37 1.32049 12.7 1.3 1.2 5.9 116 0 6 4 36.198 72.396 1.30428 17.8 1.8 1.7 5.9 117 4 4 4 36.234 72.468 1.30316 24.0 2.4 2.3 5.9 118 2 4 5 36.282 72.564 1.30168 20.3 2.1 1.9 6.0 119 3 7 1 36.395 72.791 1.29818 32.3 3.3 3.1 6.0 120 2 0 6 36.446 72.893 1.29662 82.7 8.4 7.9 6.0 121 6 4 -4 36.658 73.316 1.29018 138.8 14.0 13.2 6.0 122 3 5 4 36.733 73.466 1.28791 25.9 2.6 2.5 6.0 123 4 2 5 37.09 74.18 1.27726 23.8 2.4 2.3 6.0 124 5 1 -6 37.243 74.487 1.27277 26.8 2.7 2.6 6.0 125 8 2 1 37.862 75.724 1.25502 34.6 3.5 3.3 6.0 126 1 7 3 37.995 75.991 1.25127 12.3 1.2 1.2 6.0 127 7 1 3 38.113 76.226 1.24799 23.8 2.4 2.3 6.0 128 7 1 -5 38.268 76.537 1.2437 10.8 1.1 1.0 6.0 129 3 7 2 38.323 76.646 1.2422 39.6 4.0 3.8 6.0 130 5 5 3 38.473 76.945 1.23811 75.3 7.6 7.1 6.0 131 3 7 -3 38.719 77.438 1.23145 29.2 2.9 2.8 6.0 132 6 6 0 39.041 78.081 1.22291 16.8 1.7 1.6 6.0 133 7 5 0 39.091 78.183 1.22158 14.9 1.5 1.4 6.0 134 3 1 6 39.143 78.286 1.22023 29.8 3.0 2.8 6.0 135 6 6 -2 39.356 78.712 1.21469 82.3 8.3 7.8 6.0 136 5 1 5 39.437 78.874 1.2126 44.3 4.5 4.2 6.0 137 1 1 -7 39.725 79.45 1.20525 19.3 2.0 1.8 6.0 138 5 3 -6 40.033 80.065 1.19753 41.9 4.2 3.9 6.0 139 5 7 -1 40.079 80.157 1.19639 48.9 4.9 4.6 6.0 140 9 1 0 40.28 80.561 1.19141 16.4 1.7 1.5 6.1 141 8 2 2 40.454 80.907 1.18718 22.0 2.2 2.1 6.1 142 1 7 -4 40.486 80.971 1.1864 14.8 1.5 1.4 6.1 143 7 5 1 40.549 81.098 1.18487 29.6 3.0 2.8 6.1 144 7 5 -3 40.625 81.25 1.18303 37.1 3.8 3.5 6.1 145 0 6 5 40.676 81.353 1.1818 12.0 1.2 1.1 6.1 146 6 2 -6 40.734 81.469 1.18041 22.3 2.3 2.1 6.1 147 5 5 -5 40.835 81.67 1.17801 30.7 3.1 2.9 6.1 148 7 3 3 40.885 81.769 1.17683 11.1 1.1 1.0 6.1 149 9 1 -3 40.984 81.967 1.17449 11.4 1.2 1.1 6.1 150 5 7 1 41.45 82.9 1.16363 10.4 1.1 1.0 6.1 151 3 5 5 41.603 83.206 1.16012 22.6 2.3 2.1 6.1 152 4 0 6 41.691 83.381 1.15813 13.6 1.4 1.3 6.1 153 5 3 5 42.187 84.374 1.14702 23.4 2.4 2.2 6.1 154 9 3 -1 42.281 84.561 1.14495 23.3 2.4 2.2 6.1 155 1 3 -7 42.471 84.942 1.14079 77.8 7.9 7.2 6.1 156 5 7 -3 42.617 85.233 1.13764 14.4 1.5 1.3 6.1 157 7 1 -6 42.703 85.407 1.13577 11.4 1.2 1.1 6.1 158 5 1 -7 42.951 85.902 1.13048 17.5 1.8 1.6 6.1 159 4 2 6 43.056 86.113 1.12826 17.4 1.8 1.6 6.1 160 4 6 4 43.168 86.336 1.12591 16.7 1.7 1.5 6.1 161 1 5 6 43.383 86.765 1.12144 10.9 1.1 1.0 6.1 162 9 3 -3 43.716 87.432 1.1146 35.8 3.6 3.3 6.2 163 1 3 7 44.373 88.746 1.10146 17.3 1.8 1.6 6.2 164 8 4 2 44.552 89.104 1.09796 31.6 3.2 2.9 6.2 165 10 0 -2 44.724 89.447 1.09463 85.7 8.7 7.9 6.2 166 1 9 1 44.8 89.599 1.09317 47.4 4.8 4.4 6.2 Reference: Chichagov A.V. et al. Information-Calculating System on Crystal Structure Data of Minerals (MINCRYST) - Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian) |