Institute of Experimental Mineralogy Russian Academy of Sciences ------------------------------------------------- 142432, Chernogolovka, Moscow district A.V. Chichagov +7(496)52-22320 *** *** W W W - X R A Y P O L *** *********************** PRINGLEITE 1 Ca(9)B(26)O(34)(OH)(24)Cl(4).13H(2)O Triclinic P 1 Z = 1 R =0.045 NR =4918 27 .8 .1997 Ref.Str.: Grice J.D., Burns P.C., Hawthorne F.C. (1994) * Canad. Mineral., 32, 1-14 Reserv: D.T.N. Initial data from BDM-file Lattice parameters (cub. angs.,degr.): a = 12.746 alpha = 102.2 b = 13.019 beta = 102.1 c = 9.693 gamma = 85.6 Unit cell volume (cub. angs.) = 1536.32 Molar volume ( cub.cm/mol.) = 925.38 Co-ordinates, thermal parameters, occupation for atomic positions: NoP x/a y/b z/c B(j) atom / occupation 1 0.0 0.0 0.0 0.1 Ca = 1.00 2 0.6993 0.305 0.8019 0.11 Ca = 1.00 3 0.7648 0.877 0.3976 0.11 Ca = 1.00 4 0.1967 0.8075 0.798 0.1 Ca = 1.00 5 0.5658 0.0705 0.1942 0.09 Ca = 1.00 6 0.0641 0.5644 0.1807 0.11 Ca = 1.00 7 0.2679 0.3822 0.3988 0.12 Ca = 1.00 8 0.5001 0.4987 0.9941 0.11 Ca = 1.00 9 0.535 0.8586 0.7293 0.18 Ca = 1.00 10 0.0048 0.7343 0.4952 0.1 B = 1.00 11 0.9152 0.8006 0.1347 0.09 B = 1.00 12 0.286 0.0339 0.0667 0.09 B = 1.00 13 0.5141 0.7989 0.1497 0.07 B = 1.00 14 0.7864 0.5297 0.0606 0.08 B = 1.00 15 0.3571 0.5832 0.6933 0.1 B = 1.00 16 0.2613 0.6437 0.0342 0.08 B = 1.00 17 0.8506 0.0764 0.6984 0.11 B = 1.00 18 0.5026 0.2331 0.4974 0.14 B = 1.00 19 0.7683 0.1483 0.0546 0.09 B = 1.00 20 0.0154 0.2947 0.1535 0.15 B = 1.00 21 0.4141 0.2996 0.1322 0.11 B = 1.00 22 0.4174 0.9043 0.9719 0.11 B = 1.00 23 0.9042 0.2068 0.9322 0.11 B = 1.00 24 0.0802 0.7379 0.0132 0.06 B = 1.00 25 0.3634 0.1774 0.2743 0.11 B = 1.00 26 0.8665 0.6733 0.2718 0.12 B = 1.00 27 0.6805 0.1324 0.5343 0.14 B = 1.00 28 0.8234 0.9799 0.1643 0.11 B = 1.00 29 0.3177 0.4768 0.1459 0.11 B = 1.00 30 0.9207 0.3997 0.9744 0.09 B = 1.00 31 0.4043 0.7087 0.9286 0.09 B = 1.00 32 0.5859 0.2403 0.0278 0.17 B = 1.00 33 0.4526 0.4052 0.668 0.14 B = 1.00 34 0.1905 0.6433 0.5156 0.1 B = 1.00 35 0.9403 0.8947 0.6733 0.07 B = 1.00 36 0.9724 0.6688 0.3661 0.11 O = 1.00 37 0.9372 0.813 0.543 0.11 O = 1.00 38 0.1082 0.7206 0.5661 0.14 O = 1.00 39 0.9923 0.7301 0.0886 0.13 O = 1.00 40 0.8964 0.8968 0.0993 0.12 O = 1.00 41 0.8519 0.7717 0.2174 0.13 O = 1.00 42 0.3668 0.0842 0.1601 0.14 O = 1.00 43 0.4959 0.2323 0.0971 0.13 O = 1.00 44 0.3066 0.9416 0.9764 0.14 O = 1.00 45 0.4887 0.7066 0.0574 0.13 O = 1.00 46 0.3512 0.2744 0.219 0.11 O = 1.00 47 0.4809 0.8948 0.1174 0.1 O = 1.00 48 0.8061 0.4405 0.971 0.11 O = 1.00 49 0.8683 0.5824 0.1562 0.11 O = 1.00 50 0.4121 0.8049 0.8712 0.08 O = 1.00 51 0.2749 0.6496 0.6442 0.13 O = 1.00 52 0.3803 0.4882 0.6107 0.1 O = 1.00 53 0.4229 0.6133 0.8244 0.09 O = 1.00 54 0.2984 0.7109 0.9629 0.1 O = 1.00 55 0.3262 0.5593 0.0662 0.13 O = 1.00 56 0.1623 0.6618 0.0656 0.1 O = 1.00 57 0.9179 0.1077 0.8315 0.11 O = 1.00 58 0.8677 0.9791 0.6182 0.11 O = 1.00 59 0.7666 0.1402 0.6551 0.13 O = 1.00 60 0.5994 0.2087 0.5797 0.1 O = 1.00 61 0.4685 0.1679 0.3691 0.11 O = 1.00 62 0.8322 0.0659 0.0893 0.11 O = 1.00 63 0.7986 0.2107 0.9744 0.12 O = 1.00 64 0.6679 0.1683 0.0902 0.13 O = 1.00 65 0.4411 0.319 0.5408 0.14 O = 1.00 66 0.9918 0.2011 0.0608 0.1 O = 1.00 67 0.913 0.2966 0.8741 0.09 O = 1.00 68 0.9728 0.3884 0.124 0.14 O = 1.00 69 0.3931 0.3931 0.0909 0.1 O = 1.00 70 0.1789 0.0684 0.0502 0.23 OH = 1.00 71 0.5811 0.7988 0.2826 0.18 OH = 1.00 72 0.4738 0.9804 0.9255 0.15 OH = 1.00 73 0.6818 0.5692 0.055 0.19 OH = 1.00 74 0.0884 0.2956 0.28 0.19 OH = 1.00 75 0.0487 0.7129 0.8545 0.15 OH = 1.00 76 0.1175 0.8455 0.0338 0.12 OH = 1.00 77 0.2751 0.1812 0.3496 0.13 OH = 1.00 78 0.7747 0.6794 0.3414 0.16 OH = 1.00 79 0.7143 0.1635 0.4023 0.16 OH = 1.00 80 0.6439 0.0258 0.4606 0.15 OH = 1.00 81 0.7128 0.9458 0.1463 0.12 OH = 1.00 82 0.8641 0.0082 0.3189 0.16 OH = 1.00 83 0.3584 0.5126 0.3018 0.19 OH = 1.00 84 0.2079 0.4428 0.1318 0.18 OH = 1.00 85 0.9837 0.4758 0.9405 0.14 OH = 1.00 86 0.5631 0.201 0.8721 0.16 OH = 1.00 87 0.62 0.3492 0.0507 0.16 OH = 1.00 88 0.4171 0.3774 0.7902 0.15 OH = 1.00 89 0.5613 0.435 0.7344 0.13 OH = 1.00 90 0.1492 0.5356 0.4515 0.14 OH = 1.00 91 0.2247 0.668 0.3911 0.3 OH = 1.00 92 0.8919 0.864 0.7823 0.15 OH = 1.00 93 0.0481 0.9317 0.7473 0.16 OH = 1.00 94 0.2625 0.8958 0.3347 0.36 Cl = 1.00 95 0.6698 0.572 0.5622 0.33 Cl = 1.00 96 0.983 0.487 0.6205 0.38 Cl = 1.00 97 0.318 0.1373 0.7214 0.45 Cl = 1.00 98 0.6974 0.8161 0.6108 0.2 H(2)O = 1.00 99 0.1951 0.3378 0.5948 0.34 H(2)O = 1.00 100 0.064 0.0569 0.2731 0.3 H(2)O = 1.00 101 0.258 0.9088 0.6525 0.47 H(2)O = 1.00 102 0.7743 0.3614 0.6187 0.27 H(2)O = 1.00 103 0.6508 0.7708 0.9021 0.26 H(2)O = 1.00 104 0.4626 0.724 0.541 0.34 H(2)O = 1.00 105 0.6507 0.0049 0.7977 0.31 H(2)O = 1.00 106 0.4667 0.9714 0.5591 0.3 H(2)O = 1.00 107 0.5476 0.5654 0.257 0.24 H(2)O = 1.00 108 0.8207 0.6516 0.8498 0.32 H(2)O = 1.00 109 0.7978 0.4026 0.2941 0.54 H(2)O = 1.00 110 0.1485 0.2867 0.8894 0.63 H(2)O = 1.00 111 0.1756 0.0984 0.9947 0.3 H = 1.00 112 0.5896 0.7422 0.3025 0.3 H = 1.00 113 0.1238 0.8616 0.1142 0.3 H = 1.00 114 0.7774 0.6534 0.401 0.3 H = 1.00 115 0.7474 0.2086 0.4257 0.3 H = 1.00 116 0.6009 0.9996 0.513 0.3 H = 1.00 117 0.6946 0.9133 0.0691 0.3 H = 1.00 118 0.8439 0.072 0.3616 0.3 H = 1.00 119 0.3413 0.5801 0.3502 0.3 H = 1.00 120 0.1852 0.3944 0.0531 0.3 H = 1.00 121 0.9841 0.4716 0.8509 0.3 H = 1.00 122 0.5014 0.2285 0.8229 0.3 H = 1.00 123 0.3608 0.3638 0.7703 0.3 H = 1.00 124 0.5802 0.4831 0.6951 0.3 H = 1.00 125 0.1261 0.5147 0.5121 0.3 H = 1.00 126 0.2721 0.697 0.4234 0.3 H = 1.00 127 0.074 0.966 0.7111 0.3 H = 1.00 128 0.6928 0.7351 0.5906 0.3 H = 1.00 129 0.7409 0.8167 0.659 0.3 H = 1.00 130 0.1576 0.3375 0.6514 0.3 H = 1.00 131 0.0255 0.059 0.2779 0.3 H = 1.00 132 0.8301 0.3874 0.6123 0.3 H = 1.00 133 0.7539 0.408 0.5482 0.3 H = 1.00 134 0.4957 0.6571 0.5355 0.3 H = 1.00 135 0.433 0.9688 0.5004 0.3 H = 1.00 136 0.5923 0.5645 0.3039 0.3 H = 1.00 137 0.9723 0.0459 0.3289 0.3 H = 1.00 138 0.0938 0.2854 0.8609 0.3 H = 1.00 Co-ordinates for all atomic positions : No NoP x/a y/b z/c 1 1 0.0 0.0 0.0 2 2 0.6993 0.305 0.8019 3 3 0.7648 0.877 0.3976 4 4 0.1967 0.8075 0.798 5 5 0.5658 0.0705 0.1942 6 6 0.0641 0.5644 0.1807 7 7 0.2679 0.3822 0.3988 8 8 0.5001 0.4987 0.9941 9 9 0.535 0.8586 0.7293 10 10 0.0048 0.7343 0.4952 11 11 0.9152 0.8006 0.1347 12 12 0.286 0.0339 0.0667 13 13 0.5141 0.7989 0.1497 14 14 0.7864 0.5297 0.0606 15 15 0.3571 0.5832 0.6933 16 16 0.2613 0.6437 0.0342 17 17 0.8506 0.0764 0.6984 18 18 0.5026 0.2331 0.4974 19 19 0.7683 0.1483 0.0546 20 20 0.0154 0.2947 0.1535 21 21 0.4141 0.2996 0.1322 22 22 0.4174 0.9043 0.9719 23 23 0.9042 0.2068 0.9322 24 24 0.0802 0.7379 0.0132 25 25 0.3634 0.1774 0.2743 26 26 0.8665 0.6733 0.2718 27 27 0.6805 0.1324 0.5343 28 28 0.8234 0.9799 0.1643 29 29 0.3177 0.4768 0.1459 30 30 0.9207 0.3997 0.9744 31 31 0.4043 0.7087 0.9286 32 32 0.5859 0.2403 0.0278 33 33 0.4526 0.4052 0.668 34 34 0.1905 0.6433 0.5156 35 35 0.9403 0.8947 0.6733 36 36 0.9724 0.6688 0.3661 37 37 0.9372 0.813 0.543 38 38 0.1082 0.7206 0.5661 39 39 0.9923 0.7301 0.0886 40 40 0.8964 0.8968 0.0993 41 41 0.8519 0.7717 0.2174 42 42 0.3668 0.0842 0.1601 43 43 0.4959 0.2323 0.0971 44 44 0.3066 0.9416 0.9764 45 45 0.4887 0.7066 0.0574 46 46 0.3512 0.2744 0.219 47 47 0.4809 0.8948 0.1174 48 48 0.8061 0.4405 0.971 49 49 0.8683 0.5824 0.1562 50 50 0.4121 0.8049 0.8712 51 51 0.2749 0.6496 0.6442 52 52 0.3803 0.4882 0.6107 53 53 0.4229 0.6133 0.8244 54 54 0.2984 0.7109 0.9629 55 55 0.3262 0.5593 0.0662 56 56 0.1623 0.6618 0.0656 57 57 0.9179 0.1077 0.8315 58 58 0.8677 0.9791 0.6182 59 59 0.7666 0.1402 0.6551 60 60 0.5994 0.2087 0.5797 61 61 0.4685 0.1679 0.3691 62 62 0.8322 0.0659 0.0893 63 63 0.7986 0.2107 0.9744 64 64 0.6679 0.1683 0.0902 65 65 0.4411 0.319 0.5408 66 66 0.9918 0.2011 0.0608 67 67 0.913 0.2966 0.8741 68 68 0.9728 0.3884 0.124 69 69 0.3931 0.3931 0.0909 70 70 0.1789 0.0684 0.0502 71 71 0.5811 0.7988 0.2826 72 72 0.4738 0.9804 0.9255 73 73 0.6818 0.5692 0.055 74 74 0.0884 0.2956 0.28 75 75 0.0487 0.7129 0.8545 76 76 0.1175 0.8455 0.0338 77 77 0.2751 0.1812 0.3496 78 78 0.7747 0.6794 0.3414 79 79 0.7143 0.1635 0.4023 80 80 0.6439 0.0258 0.4606 81 81 0.7128 0.9458 0.1463 82 82 0.8641 0.0082 0.3189 83 83 0.3584 0.5126 0.3018 84 84 0.2079 0.4428 0.1318 85 85 0.9837 0.4758 0.9405 86 86 0.5631 0.201 0.8721 87 87 0.62 0.3492 0.0507 88 88 0.4171 0.3774 0.7902 89 89 0.5613 0.435 0.7344 90 90 0.1492 0.5356 0.4515 91 91 0.2247 0.668 0.3911 92 92 0.8919 0.864 0.7823 93 93 0.0481 0.9317 0.7473 94 94 0.2625 0.8958 0.3347 95 95 0.6698 0.572 0.5622 96 96 0.983 0.487 0.6205 97 97 0.318 0.1373 0.7214 98 98 0.6974 0.8161 0.6108 99 99 0.1951 0.3378 0.5948 100 100 0.064 0.0569 0.2731 101 101 0.258 0.9088 0.6525 102 102 0.7743 0.3614 0.6187 103 103 0.6508 0.7708 0.9021 104 104 0.4626 0.724 0.541 105 105 0.6507 0.0049 0.7977 106 106 0.4667 0.9714 0.5591 107 107 0.5476 0.5654 0.257 108 108 0.8207 0.6516 0.8498 109 109 0.7978 0.4026 0.2941 110 110 0.1485 0.2867 0.8894 111 111 0.1756 0.0984 0.9947 112 112 0.5896 0.7422 0.3025 113 113 0.1238 0.8616 0.1142 114 114 0.7774 0.6534 0.401 115 115 0.7474 0.2086 0.4257 116 116 0.6009 0.9996 0.513 117 117 0.6946 0.9133 0.0691 118 118 0.8439 0.072 0.3616 119 119 0.3413 0.5801 0.3502 120 120 0.1852 0.3944 0.0531 121 121 0.9841 0.4716 0.8509 122 122 0.5014 0.2285 0.8229 123 123 0.3608 0.3638 0.7703 124 124 0.5802 0.4831 0.6951 125 125 0.1261 0.5147 0.5121 126 126 0.2721 0.697 0.4234 127 127 0.074 0.966 0.7111 128 128 0.6928 0.7351 0.5906 129 129 0.7409 0.8167 0.659 130 130 0.1576 0.3375 0.6514 131 131 0.0255 0.059 0.2779 132 132 0.8301 0.3874 0.6123 133 133 0.7539 0.408 0.5482 134 134 0.4957 0.6571 0.5355 135 135 0.433 0.9688 0.5004 136 136 0.5923 0.5645 0.3039 137 137 0.9723 0.0459 0.3289 138 138 0.0938 0.2854 0.8609 X-ray density (g/cm cub.) = 2.16 MU (1/cm) = 94.863 Mass attenuation coefficient (cm**2/g) = 43.938 Selected interatomic distances (cation-anion,anion-anion): NoP Atom Rad.sph. C.N. Distance NoP N. (angs.) (angs.) 1 Ca 3.42 9 2.4139 40 2.3989 57 2.4981 62 2.5582 66 2.4275 70 2.4509 76 2.6575 92 2.6061 93 2.5652 100 2 Ca 3.42 9 2.4213 48 2.5106 59 2.4054 60 2.3763 63 2.6662 67 2.5603 86 2.7413 87 2.4321 89 2.4447 102 3 Ca 3.42 9 2.535 37 2.3938 41 2.4392 58 2.5599 71 2.5134 78 2.4366 80 2.7072 81 2.5276 82 2.6793 98 4 Ca 3.42 9 2.3797 38 2.4666 44 2.6873 50 2.5407 51 2.3553 54 2.5397 75 2.6269 76 2.4329 93 2.3969 101 5 Ca 3.42 9 2.4857 42 2.513 43 2.506 47 2.3983 61 2.3828 64 2.6784 72 2.6146 79 2.7324 80 2.4375 81 6 Ca 3.42 9 2.4592 36 2.541 39 2.4546 49 2.4179 56 2.5525 68 2.3858 84 2.4182 85 2.7142 90 2.7712 91 7 Ca 3.42 9 2.3765 46 2.4591 52 2.5241 65 2.564 74 2.5569 77 2.5547 83 2.801 84 2.4429 90 2.4678 99 8 Ca 3.42 9 2.6455 45 2.4563 53 2.4843 55 2.4495 69 2.4655 73 2.4634 87 2.3622 88 2.734 89 2.4724 107 9 Ca 3.42 7 2.5124 50 2.4284 72 2.5422 98 2.4092 103 2.3332 104 2.3936 105 2.4211 106 10 B 2.412 3 1.3602 36 1.3558 37 1.3701 38 11 B 2.412 3 1.3712 39 1.3583 40 1.3712 41 12 B 2.412 3 1.3308 42 1.372 44 1.3912 70 13 B 2.412 3 1.3539 45 1.3655 47 1.3886 71 14 B 2.412 3 1.3365 48 1.3619 49 1.3861 73 15 B 2.412 3 1.3775 51 1.3721 52 1.3656 53 16 B 2.412 3 1.3866 54 1.3729 55 1.3511 56 17 B 2.412 3 1.3906 57 1.3671 58 1.3546 59 18 B 2.412 3 1.3762 60 1.3564 61 1.359 65 19 B 2.412 3 1.3531 62 1.3618 63 1.3858 64 20 B 2.412 3 1.3649 66 1.3585 68 1.3736 74 21 B 2.412 3 1.3613 43 1.3777 46 1.3508 69 22 B 2.412 4 1.4642 44 1.4964 47 1.4436 50 1.4608 72 23 B 2.412 4 1.4671 57 1.4809 63 1.4996 66 1.4218 67 24 B 2.412 4 1.4805 39 1.4715 56 1.4775 75 1.4739 76 25 B 2.412 4 1.4642 42 1.4585 46 1.47 61 1.4569 77 26 B 2.412 4 1.4677 36 1.4702 41 1.4501 49 1.4576 78 27 B 2.412 4 1.4191 59 1.4482 60 1.5695 79 1.4814 80 28 B 2.412 4 1.4955 40 1.4806 62 1.4748 81 1.4562 82 29 B 2.412 4 1.4717 55 1.4845 69 1.4767 83 1.4706 84 30 B 2.412 4 1.5116 48 1.4782 67 1.4956 68 1.4507 85 31 B 2.412 4 1.4709 45 1.4916 50 1.4642 53 1.4531 54 32 B 2.412 4 1.4659 43 1.4701 64 1.4617 86 1.4729 87 33 B 2.412 4 1.4872 52 1.4716 65 1.473 88 1.4448 89 34 B 2.412 4 1.4825 38 1.4581 51 1.4957 90 1.4683 91 35 B 2.412 4 1.4649 37 1.4946 58 1.465 92 1.4754 93 36 O 3.804 9 2.3449 37 2.33 38 3.0267 39 2.409 41 2.3011 49 2.4767 78 2.8277 90 3.1733 91 3.7388 96 37 O 3.804 10 2.3449 36 2.3989 38 3.0603 41 2.3028 58 3.5234 75 2.9246 78 3.6285 82 2.4508 92 2.4851 93 3.2539 98 38 O 3.804 9 2.33 36 2.3989 37 2.2939 51 3.069 75 2.4955 90 2.4414 91 3.0701 93 3.7214 96 3.0872 101 39 O 3.804 10 3.0267 36 2.4012 40 2.3572 41 2.8386 49 2.3149 56 2.482 75 2.4792 76 3.3188 85 3.7072 92 2.8995 108 40 O 3.804 11 2.4012 39 2.3424 41 2.3035 62 3.7347 75 3.0122 76 2.4872 81 2.4031 82 3.0004 92 3.0719 100 3.6191 103 3.6334 108 41 O 3.804 12 2.409 36 3.0603 37 2.3572 39 2.3424 40 2.4134 49 3.6154 71 3.4382 73 2.2682 78 2.8788 81 3.0334 82 3.5519 103 3.5278 108 42 O 3.804 9 2.8643 43 2.3355 44 2.4232 46 2.7636 47 2.2704 61 2.4138 70 2.9284 72 2.4552 77 3.721 94 43 O 3.804 9 2.8643 42 2.3628 46 3.0235 61 2.294 64 2.3879 69 3.3527 72 2.4516 86 2.4449 87 3.776 88 44 O 3.804 9 2.3355 42 2.4589 47 2.3358 50 2.9875 54 2.3373 70 2.3983 72 3.0006 76 3.561 93 3.0136 101 45 O 3.804 9 2.395 47 2.4278 50 2.3414 53 2.4073 54 2.9542 55 2.3716 71 2.9307 73 3.0552 103 2.8928 107 46 O 3.804 11 2.4232 42 2.3628 43 2.4284 61 3.0361 65 2.3304 69 3.4979 70 3.5022 74 2.3152 77 3.0382 83 2.8946 84 3.6878 110 47 O 3.804 10 2.7636 42 2.4589 44 2.395 45 2.4359 50 3.3563 54 2.3454 71 2.3452 72 3.6797 80 3.0218 81 3.4037 103 48 O 3.804 11 2.3432 49 3.008 63 2.3769 67 2.4611 68 2.3532 73 2.4332 85 3.0373 87 3.4591 89 3.299 102 3.2408 108 3.2959 109 49 O 3.804 10 2.3011 36 2.8386 39 2.4134 41 2.3432 48 2.7524 68 2.3783 73 2.4391 78 2.8654 85 3.2081 108 3.1972 109 50 O 3.804 10 2.3358 44 2.4278 45 2.4359 47 3.0061 51 2.4377 53 2.379 54 2.3895 72 3.0398 101 3.0017 103 3.3321 104 51 O 3.804 10 2.2939 38 3.0061 50 2.4056 52 2.3798 53 2.9793 54 3.7439 83 2.4894 90 2.4601 91 3.3498 101 3.071 104 52 O 3.804 10 2.4056 51 2.3402 53 2.289 65 3.0302 83 2.4378 88 2.4871 89 3.1075 90 3.6834 91 3.1399 99 3.5565 104 53 O 3.804 11 2.3414 45 2.4377 50 2.3798 51 2.3402 52 2.4079 54 3.0898 55 3.6572 73 3.0235 88 2.9021 89 3.5431 103 3.4996 104 54 O 3.804 10 2.9875 44 2.4073 45 3.3563 47 2.379 50 2.9793 51 2.4079 53 2.367 55 2.3605 56 3.1354 75 2.8974 76 55 O 3.804 10 2.9542 45 3.0898 53 2.367 54 2.3907 56 2.3058 69 2.4308 83 2.4777 84 3.5083 88 3.6246 91 3.0289 107 56 O 3.804 10 2.3149 39 2.3605 54 2.3907 55 2.4314 75 2.4837 76 3.7414 83 3.04 84 3.3112 85 3.0731 91 3.6821 94 57 O 3.804 11 2.3736 58 2.3706 59 3.0893 62 2.4112 63 2.337 66 2.4043 67 3.6143 70 3.1399 92 2.8043 93 3.6802 105 3.7672 110 58 O 3.804 10 2.3028 37 2.3736 57 2.3767 59 3.6951 79 3.0232 80 2.9947 82 2.3667 92 2.4771 93 3.1301 98 3.5239 105 59 O 3.804 11 2.3706 57 2.3767 58 2.2808 60 2.9858 63 3.038 67 2.4777 79 2.4805 80 3.7577 82 3.6121 86 2.9858 102 3.079 105 60 O 3.804 11 2.2808 59 2.3415 61 2.396 65 2.438 79 2.496 80 2.989 86 3.7009 88 3.0632 89 3.0123 102 3.6683 105 3.5839 106 61 O 3.804 9 2.2704 42 3.0235 43 2.4284 46 2.3415 60 2.3486 65 2.428 77 3.0789 79 2.9043 80 3.4576 106 62 O 3.804 11 2.3035 40 3.0893 57 2.354 63 2.3953 64 2.8815 66 3.6148 79 2.4797 81 2.4419 82 3.6986 92 3.1217 100 3.2501 105 63 O 3.804 12 3.008 48 2.4112 57 2.9858 59 2.354 62 2.3509 64 2.4318 66 2.3719 67 3.2257 68 2.9609 86 2.9142 87 3.3388 105 3.5471 109 64 O 3.804 11 2.294 43 2.3953 62 2.3509 63 3.5037 72 2.9715 79 3.0488 81 3.787 82 2.3546 86 2.4756 87 3.1422 105 3.5787 109 65 O 3.804 9 3.0361 46 2.289 52 2.396 60 2.3486 61 2.9433 77 3.7239 83 2.4522 88 2.4701 89 3.2683 99 66 O 3.804 9 2.337 57 2.8815 62 2.4318 63 2.4139 67 2.3917 68 2.8422 70 2.3611 74 3.0298 100 3.2414 110 67 O 3.804 9 2.3769 48 2.4043 57 3.038 59 2.3719 63 2.4139 66 2.4534 68 2.4727 85 2.9639 102 2.9683 110 68 O 3.804 11 2.4611 48 2.7524 49 3.2257 63 2.3917 66 2.4534 67 2.3414 74 3.1137 84 2.3369 85 3.7286 90 3.0129 109 3.5138 110 69 O 3.804 10 2.3879 43 2.3304 46 2.3058 55 2.3925 83 2.4895 84 3.7817 86 2.9945 87 2.9569 88 3.0535 107 3.5242 110 70 OH 3.852 12 2.4138 42 2.3373 44 3.4979 46 3.6143 57 2.8422 66 3.5792 74 3.0266 76 3.0109 77 3.2805 93 3.8483 94 2.8866 100 3.4795 110 71 OH 3.852 11 3.6154 41 2.3716 45 2.3454 47 3.6415 73 2.8331 78 3.1592 80 3.2737 81 3.1843 98 3.5136 104 3.5984 106 3.0517 107 72 OH 3.852 13 2.9284 42 3.3527 43 2.3983 44 2.3452 47 2.3895 50 3.5037 64 3.3951 81 3.3449 86 3.3865 97 3.4258 101 3.4053 103 2.8581 105 3.5109 106 73 OH 3.852 13 3.4382 41 2.9307 45 2.3532 48 2.3783 49 3.6572 53 3.6415 71 2.8925 78 3.0179 87 3.3443 89 3.2374 103 2.8671 107 3.3032 108 3.5295 109 74 OH 3.852 9 3.5022 46 2.3611 66 2.3414 68 3.5792 70 2.7466 77 3.2534 84 3.2807 90 3.0213 99 3.1321 100 75 OH 3.852 13 3.5234 37 3.069 38 2.482 39 3.7347 40 3.8126 51 3.1354 54 2.4314 56 2.2572 76 3.5608 85 2.7832 92 3.2308 93 3.3552 96 3.0609 108 76 OH 3.852 11 2.4792 39 3.0122 40 3.0006 44 2.8974 54 2.4837 56 3.0266 70 2.2572 75 3.3871 92 3.1447 93 3.0773 94 3.3312 100 77 OH 3.852 10 2.4552 42 2.3152 46 2.428 61 2.9433 65 3.0109 70 2.7466 74 3.7024 94 3.6892 97 3.0813 99 3.1198 100 78 OH 3.852 10 2.4767 36 2.9246 37 2.2682 41 2.4391 49 2.8331 71 2.8925 73 3.3279 95 3.1309 98 3.2255 107 3.5325 109 79 OH 3.852 12 3.8194 43 3.6951 58 2.4777 59 2.438 60 3.0789 61 3.6148 62 2.9715 64 2.286 80 3.3476 81 2.7841 82 2.9947 102 3.7787 109 80 OH 3.852 12 3.6797 47 3.0232 58 2.4805 59 2.496 60 2.9043 61 3.1592 71 2.286 79 3.2829 81 3.3468 82 3.319 98 3.3184 105 2.8195 106 81 OH 3.852 12 2.4872 40 2.8788 41 3.0218 47 2.4797 62 3.0488 64 3.2737 71 3.3951 72 3.3476 79 3.2829 80 2.3433 82 2.9378 103 3.5384 105 82 OH 3.852 11 3.6285 37 2.4031 40 3.0334 41 2.9947 58 3.7577 59 2.4419 62 3.787 64 2.7841 79 3.3468 80 2.3433 81 2.8164 100 83 OH 3.852 12 3.0382 46 3.7439 51 3.0302 52 2.4308 55 3.7414 56 3.7239 65 2.3925 69 2.3516 84 3.259 90 2.6638 91 3.3597 104 2.7011 107 84 OH 3.852 11 2.8946 46 2.4777 55 3.04 56 3.1137 68 2.4895 69 3.2534 74 2.3516 83 3.117 85 3.2975 90 3.4227 91 2.7742 110 85 OH 3.852 12 3.3188 39 2.4332 48 2.8654 49 3.3112 56 2.4727 67 2.3369 68 3.5608 75 3.117 84 3.1339 96 3.7719 102 3.1117 108 3.1378 110 86 OH 3.852 14 2.4516 43 3.6121 59 2.989 60 2.9609 63 2.3546 64 3.8361 65 3.7817 69 3.3449 72 2.3499 87 2.977 88 3.5718 89 3.2486 97 2.7215 105 3.8493 106 87 OH 3.852 11 2.4449 43 3.0373 48 2.9142 63 2.4756 64 2.9945 69 3.0179 73 2.3499 86 3.2722 88 3.4007 89 3.2816 107 2.9142 109 88 OH 3.852 12 3.776 43 2.4378 52 3.0235 53 3.5083 55 3.7009 60 2.4522 65 2.9569 69 2.977 86 3.2722 87 2.2434 89 3.3441 97 3.0699 99 89 OH 3.852 11 3.4591 48 2.4871 52 2.9021 53 3.0632 60 2.4701 65 3.3443 73 3.5718 86 3.4007 87 2.2434 88 3.2379 95 3.1575 102 90 OH 3.852 11 2.8277 36 2.4955 38 2.4894 51 3.1075 52 3.7286 68 3.2807 74 3.259 83 3.2975 84 2.271 91 3.1096 96 3.1374 99 91 OH 3.852 12 3.1733 36 2.4414 38 2.4601 51 3.6834 52 3.6246 55 3.0731 56 2.6638 83 3.4227 84 2.271 90 3.2158 94 3.5811 101 3.1435 104 92 OH 3.852 12 2.4508 37 3.7072 39 3.0004 40 3.1399 57 2.3667 58 3.6986 62 2.7832 75 3.3871 76 2.3526 93 2.7147 98 3.4713 105 3.2089 108 93 OH 3.852 10 2.4851 37 3.0701 38 3.561 44 2.8043 57 2.4771 58 3.2805 70 3.2308 75 3.1447 76 2.3526 92 2.9805 101 94 Cl 4.344 17 4.3361 38 4.2102 39 3.721 42 3.805 44 3.8245 47 3.9809 54 3.6821 56 3.8483 70 4.2596 71 3.0773 76 3.7024 77 3.2158 91 4.3225 97 3.1998 100 3.0616 101 3.7925 104 3.0966 106 95 Cl 4.344 12 4.0729 52 3.3279 78 4.2625 83 3.2379 89 4.0151 96 3.1487 98 3.0594 102 3.7744 103 3.1742 104 3.0276 107 3.0629 108 3.6169 109 96 Cl 4.344 13 3.7388 36 3.7214 38 4.1009 67 4.0959 74 3.3552 75 3.1339 85 3.1096 90 4.0151 95 3.2273 99 3.2228 102 3.6119 108 3.5478 109 4.2151 110 97 Cl 4.344 15 3.8727 43 3.9358 44 4.328 60 3.8201 65 4.3411 69 4.234 70 3.3865 72 3.6892 77 3.2486 86 3.3441 88 4.3225 94 3.2702 99 3.0292 101 3.1493 106 3.2548 110 98 H(2)O 3.972 12 3.2539 37 3.1301 58 3.1843 71 3.1309 78 3.319 80 2.7147 92 3.1487 95 3.1834 103 3.1955 104 2.8326 105 3.4473 106 3.5323 108 99 H(2)O 3.972 9 3.1399 52 3.2683 65 3.0213 74 3.0813 77 3.0699 88 3.1374 90 3.2273 96 3.2702 97 3.2441 110 100 H(2)O 3.972 9 3.0719 40 3.1217 62 3.0298 66 2.8866 70 3.1321 74 3.3312 76 3.1198 77 2.8164 82 3.1998 94 101 H(2)O 3.972 11 3.0872 38 3.0136 44 3.0398 50 3.3498 51 3.4258 72 3.5811 91 2.9805 93 3.0616 94 3.0292 97 3.5885 104 3.1959 106 102 H(2)O 3.972 10 3.299 48 2.9858 59 3.0123 60 2.9639 67 2.9947 79 3.7719 85 3.1575 89 3.0594 95 3.2228 96 3.3779 109 103 H(2)O 3.972 16 3.6191 40 3.5519 41 3.0552 45 3.4037 47 3.0017 50 3.5431 53 3.909 71 3.4053 72 3.2374 73 2.9378 81 3.8637 92 3.7744 95 3.1834 98 3.7656 104 3.4081 105 2.6395 108 104 H(2)O 3.972 14 3.3321 50 3.071 51 3.5565 52 3.4996 53 3.5136 71 3.3597 83 3.1435 91 3.7925 94 3.1742 95 3.1955 98 3.5885 101 3.7656 103 3.1923 106 3.3941 107 105 H(2)O 3.972 15 3.6802 57 3.5239 58 3.079 59 3.6683 60 3.2501 62 3.3388 63 3.1422 64 2.8581 72 3.3184 80 3.5384 81 2.7215 86 3.4713 92 2.8326 98 3.4081 103 2.9148 106 106 H(2)O 3.972 12 3.5839 60 3.4576 61 3.5984 71 3.5109 72 2.8195 80 3.8493 86 3.0966 94 3.1493 97 3.4473 98 3.1959 101 3.1923 104 2.9148 105 107 H(2)O 3.972 11 2.8928 45 3.0289 55 3.0535 69 3.0517 71 2.8671 73 3.2255 78 2.7011 83 3.2816 87 3.0276 95 3.3941 104 3.6873 109 108 H(2)O 3.972 13 2.8995 39 3.6334 40 3.5278 41 3.2408 48 3.2081 49 3.3032 73 3.0609 75 3.1117 85 3.2089 92 3.0629 95 3.6119 96 3.5323 98 2.6395 103 109 H(2)O 3.972 14 3.2959 48 3.1972 49 3.5471 63 3.5787 64 3.0129 68 3.5295 73 3.8754 74 3.5325 78 3.7787 79 2.9142 87 3.6169 95 3.5478 96 3.3779 102 3.6873 107 110 H(2)O 3.972 11 3.6878 46 3.7672 57 3.2414 66 2.9683 67 3.5138 68 3.5242 69 3.4795 70 2.7742 84 3.1378 85 3.2548 97 3.2441 99 111 H 2.172 1 0.7215 70 112 H 2.172 1 0.7944 71 113 H 2.172 1 0.7517 76 114 H 2.172 1 0.7225 78 115 H 2.172 1 0.7182 79 116 H 2.172 2 0.9452 80 1.9356 106 117 H 2.172 1 0.7754 81 118 H 2.172 2 2.0189 79 0.8911 82 119 H 2.172 2 0.9376 83 1.8627 91 120 H 2.172 2 0.8916 84 1.8846 110 121 H 2.172 1 0.8597 85 122 H 2.172 1 0.9197 86 123 H 2.172 1 0.7284 88 124 H 2.172 1 0.8705 89 125 H 2.172 1 0.8112 90 126 H 2.172 1 0.7151 91 127 H 2.172 1 0.7543 93 128 H 2.172 2 2.1178 95 1.035 98 129 H 2.172 2 2.102 92 0.6452 98 130 H 2.172 1 0.8004 99 131 H 2.172 1 0.5007 100 132 H 2.172 1 0.8298 102 133 H 2.172 1 0.9895 102 134 H 2.172 1 0.9343 104 135 H 2.172 1 0.6333 106 136 H 2.172 1 0.6512 107 137 H 2.172 2 1.4765 82 1.4151 100 138 H 2.172 1 0.6941 110 X-ray diffraction powder data (II), X-Ray W.L. = 1.54056(angs.): No H K L Theta 2*Theta S LPG MF F I int. ( degree ) *100 1 0 1 0 3.472 6.945 0.039 542.2 2 31.1 44.3 2 1 0 0 3.546 7.091 0.04 519.97 2 34.5 52.6 3 0 0 1 4.758 9.517 0.054 287.66 2 101.1 249.0 4 1 1 0 4.881 9.761 0.055 273.31 2 110.3 282.0 5 -1 1 0 5.05 10.099 0.057 255.19 2 34.3 25.4 6 0 -1 1 5.302 10.603 0.06 231.29 2 28.2 15.6 7 -1 0 1 5.343 10.685 0.06 227.72 2 40.7 31.9 8 -1 -1 1 5.76 11.519 0.065 195.61 2 160.2 425.4 9 0 1 1 6.435 12.871 0.073 156.24 2 13.1 2.3 10 1 0 1 6.481 12.963 0.073 154.0 2 28.7 10.7 11 -1 1 1 6.941 13.882 0.078 133.98 2 44.9 22.8 12 1 -1 1 6.952 13.905 0.079 133.54 2 45.1 23.0 13 0 2 0 6.958 13.915 0.079 133.34 2 24.7 6.9 14 2 0 0 7.105 14.209 0.08 127.78 2 38.2 15.8 15 0 -2 1 7.608 15.217 0.086 111.14 2 75.9 54.2 16 1 2 0 7.708 15.416 0.087 108.22 2 21.5 4.2 17 -2 0 1 7.733 15.466 0.087 107.51 2 81.9 61.1 18 1 1 1 7.747 15.493 0.087 107.13 2 132.5 159.3 19 2 1 0 7.808 15.617 0.088 105.41 2 15.6 2.2 20 -1 -2 1 7.883 15.766 0.089 103.38 2 13.1 1.5 21 -1 2 0 7.924 15.849 0.089 102.28 2 5.1 0.2 22 -2 -1 1 7.976 15.952 0.09 100.93 2 28.8 7.1 23 -2 1 0 8.022 16.044 0.091 99.75 2 21.8 4.0 24 1 -2 1 8.893 17.786 0.1 80.75 2 25.2 4.4 25 -2 1 1 8.967 17.935 0.101 79.39 2 11.4 0.9 26 0 2 1 9.203 18.407 0.104 75.26 2 69.1 30.5 27 2 0 1 9.324 18.649 0.105 73.26 2 99.9 61.9 28 -1 -1 2 9.398 18.797 0.106 72.07 2 19.5 2.3 29 0 -1 2 9.487 18.975 0.107 70.69 2 36.7 8.1 30 -1 0 2 9.506 19.013 0.107 70.4 2 3.9 0.1 31 0 0 2 9.55 19.1 0.108 69.74 2 75.3 33.5 32 -2 -2 1 9.587 19.175 0.108 69.18 2 134.2 105.6 33 -1 2 1 9.611 19.223 0.108 68.82 2 18.3 1.9 34 2 -1 1 9.705 19.409 0.109 67.46 2 36.7 7.7 35 2 2 0 9.797 19.594 0.11 66.15 2 37.9 8.0 36 1 2 1 10.13 20.259 0.114 61.74 2 34.8 6.3 37 -2 2 0 10.139 20.278 0.114 61.63 2 54.2 15.4 38 2 1 1 10.211 20.421 0.115 60.73 2 25.0 3.2 39 0 3 0 10.469 20.938 0.118 57.67 2 22.5 2.5 40 -1 -2 2 10.529 21.059 0.119 56.99 2 10.7 0.6 41 -2 -1 2 10.596 21.192 0.119 56.24 2 28.7 3.9 42 0 -3 1 10.603 21.207 0.119 56.16 2 12.0 0.7 43 0 -2 2 10.649 21.298 0.12 55.66 2 59.2 16.5 44 3 0 0 10.692 21.384 0.12 55.2 2 20.5 2.0 45 -2 0 2 10.732 21.465 0.121 54.77 2 47.4 10.4 46 -1 -3 1 10.765 21.53 0.121 54.43 2 63.2 18.4 47 -3 0 1 10.813 21.625 0.122 53.93 2 17.7 1.4 48 0 1 2 10.817 21.633 0.122 53.89 2 56.4 14.5 49 -1 1 2 10.818 21.635 0.122 53.88 2 14.4 0.9 50 1 -1 2 10.832 21.665 0.122 53.72 2 30.6 4.3 51 1 0 2 10.848 21.696 0.122 53.56 2 24.9 2.8 52 1 3 0 10.949 21.899 0.123 52.54 2 56.6 14.3 53 -3 -1 1 10.951 21.901 0.123 52.52 2 76.4 26.0 54 3 1 0 11.14 22.279 0.125 50.69 2 30.1 3.9 55 -1 3 0 11.181 22.363 0.126 50.29 2 59.0 14.9 56 -2 2 1 11.214 22.428 0.126 49.99 2 38.0 6.1 57 2 -2 1 11.229 22.457 0.126 49.85 2 18.4 1.4 58 -3 1 0 11.368 22.735 0.128 48.59 2 84.5 29.4 59 -2 -2 2 11.579 23.157 0.13 46.76 2 162.9 105.1 60 1 -3 1 11.607 23.215 0.131 46.52 2 4.7 0.1 61 -3 1 1 11.774 23.548 0.132 45.15 2 30.2 3.5 62 1 -2 2 11.905 23.81 0.134 44.12 2 46.2 8.0 63 1 1 2 11.948 23.897 0.134 43.78 2 94.7 33.3 64 -2 1 2 11.951 23.902 0.134 43.76 2 26.2 2.5 65 -2 -3 1 12.047 24.094 0.135 43.04 2 25.3 2.3 66 2 2 1 12.099 24.198 0.136 42.65 2 145.8 76.8 67 -3 -2 1 12.153 24.305 0.137 42.25 2 32.4 3.8 68 0 3 1 12.376 24.752 0.139 40.67 2 28.1 2.7 69 2 3 0 12.492 24.984 0.14 39.88 2 7.1 0.2 70 3 0 1 12.576 25.152 0.141 39.32 2 15.8 0.8 71 -1 -3 2 12.582 25.165 0.141 39.28 2 151.1 76.0 72 3 2 0 12.598 25.195 0.142 39.18 2 33.3 3.7 73 0 -3 2 12.718 25.436 0.143 38.4 2 37.7 4.6 74 -1 3 1 12.72 25.441 0.143 38.39 2 36.3 4.3 75 -3 -1 2 12.737 25.474 0.143 38.28 2 83.8 22.8 76 -3 0 2 12.885 25.77 0.145 37.36 2 12.8 0.5 77 3 -1 1 12.898 25.797 0.145 37.28 2 7.0 0.2 78 -2 3 0 12.9 25.799 0.145 37.27 2 38.0 4.6 79 0 2 2 12.954 25.907 0.146 36.94 2 96.7 29.2 80 -1 2 2 12.988 25.975 0.146 36.74 2 21.1 1.4 81 -3 2 0 13.002 26.004 0.146 36.65 2 63.5 12.5 82 2 0 2 13.048 26.095 0.147 36.38 2 76.5 18.1 83 1 3 1 13.056 26.112 0.147 36.33 2 33.4 3.4 84 2 -1 2 13.067 26.135 0.147 36.27 2 42.2 5.5 85 3 1 1 13.224 26.447 0.148 35.37 2 11.1 0.4 86 -2 -3 2 13.449 26.898 0.151 34.12 2 5.3 0.1 87 2 -3 1 13.533 27.065 0.152 33.68 2 52.2 7.8 88 -3 -2 2 13.542 27.083 0.152 33.63 2 51.7 7.6 89 -3 2 1 13.616 27.231 0.153 33.25 2 45.5 5.8 90 -1 -1 3 13.816 27.631 0.155 32.23 2 42.4 4.9 91 1 -3 2 13.828 27.656 0.155 32.17 2 34.8 3.3 92 0 -4 1 13.878 27.755 0.156 31.93 2 73.1 14.4 93 1 2 2 13.891 27.782 0.156 31.86 2 21.8 1.3 94 2 1 2 13.954 27.909 0.157 31.56 2 37.1 3.7 95 -3 1 2 13.958 27.916 0.157 31.54 2 129.5 44.8 96 -1 -4 1 13.972 27.944 0.157 31.47 2 38.3 3.9 97 -2 2 2 13.987 27.974 0.157 31.4 2 89.7 21.4 98 2 -2 2 14.01 28.02 0.157 31.29 2 32.2 2.7 99 -2 3 1 14.019 28.039 0.157 31.25 2 16.5 0.7 100 0 4 0 14.021 28.041 0.157 31.24 2 22.9 1.4 101 0 -1 3 14.126 28.252 0.158 30.75 2 47.0 5.7 102 3 -2 1 14.128 28.257 0.158 30.73 2 52.8 7.3 103 -1 0 3 14.136 28.273 0.159 30.7 2 54.4 7.7 104 -3 -3 1 14.165 28.33 0.159 30.57 2 36.8 3.5 105 -4 0 1 14.17 28.34 0.159 30.54 2 60.2 9.4 106 -4 -1 1 14.247 28.494 0.16 30.19 2 24.0 1.5 107 4 0 0 14.322 28.644 0.161 29.86 2 69.0 12.0 108 1 4 0 14.359 28.718 0.161 29.69 2 45.4 5.2 109 -1 -2 3 14.387 28.774 0.161 29.57 2 46.0 5.3 110 0 0 3 14.41 28.82 0.162 29.47 2 54.9 7.5 111 -2 -1 3 14.434 28.869 0.162 29.36 2 21.1 1.1 112 -1 4 0 14.6 29.199 0.164 28.66 2 11.8 0.3 113 2 3 1 14.628 29.257 0.164 28.54 2 18.4 0.8 114 4 1 0 14.636 29.271 0.164 28.51 2 6.8 0.1 115 1 -4 1 14.701 29.403 0.165 28.24 2 17.2 0.7 116 0 -2 3 14.716 29.432 0.165 28.18 2 33.5 2.7 117 3 2 1 14.722 29.444 0.165 28.15 2 37.6 3.4 118 -2 0 3 14.772 29.544 0.166 27.95 2 43.6 4.5 119 3 3 0 14.788 29.576 0.166 27.88 2 33.1 2.6 120 -4 1 0 14.872 29.744 0.167 27.55 2 40.0 3.7 121 -2 -2 3 14.955 29.91 0.168 27.22 2 70.8 11.6 122 -4 1 1 14.958 29.917 0.168 27.21 2 49.6 5.7 123 -2 -4 1 14.969 29.938 0.168 27.17 2 12.7 0.4 124 -3 -3 2 15.159 30.318 0.17 26.44 2 54.0 6.5 125 -4 -2 1 15.177 30.355 0.17 26.37 2 53.5 6.4 126 -1 -4 2 15.213 30.426 0.17 26.24 2 17.7 0.7 127 -1 1 3 15.298 30.595 0.171 25.93 2 67.1 9.9 128 -3 3 0 15.311 30.621 0.171 25.88 2 39.7 3.5 129 1 -1 3 15.314 30.627 0.171 25.87 2 59.5 7.8 130 0 -4 2 15.355 30.711 0.172 25.72 2 142.6 44.3 131 -4 -1 2 15.46 30.919 0.173 25.35 2 30.9 2.0 132 0 1 3 15.525 31.049 0.174 25.12 2 42.7 3.9 133 1 0 3 15.55 31.1 0.174 25.03 2 23.2 1.1 134 2 4 0 15.56 31.121 0.174 25.0 2 65.4 9.1 135 -4 0 2 15.612 31.224 0.175 24.82 2 90.9 17.4 136 0 3 2 15.633 31.266 0.175 24.75 2 32.8 2.3 137 2 2 2 15.639 31.279 0.175 24.73 2 80.5 13.6 138 -1 3 2 15.69 31.379 0.176 24.56 2 73.3 11.2 139 2 -3 2 15.723 31.446 0.176 24.44 2 43.6 3.9 140 0 4 1 15.744 31.488 0.176 24.37 2 52.9 5.8 141 -1 -3 3 15.762 31.524 0.176 24.31 2 128.8 34.2 142 4 2 0 15.767 31.533 0.176 24.3 2 46.8 4.5 143 -3 2 2 15.782 31.565 0.177 24.25 2 33.3 2.3 144 3 0 2 15.803 31.606 0.177 24.18 2 41.5 3.5 145 3 -1 2 15.847 31.694 0.177 24.03 2 77.3 12.2 146 -3 -1 3 15.883 31.765 0.178 23.92 2 79.7 12.9 147 1 -2 3 15.891 31.782 0.178 23.89 2 54.7 6.1 148 -2 1 3 15.919 31.838 0.178 23.8 2 18.2 0.7 149 -2 -4 2 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28.665 57.33 0.311 6.4 2 17.8 0.2 763 0 -8 2 28.665 57.331 0.311 6.4 2 34.8 0.7 764 6 3 2 28.669 57.337 0.311 6.39 2 8.8 0.0 765 0 6 3 28.673 57.346 0.311 6.39 2 46.8 1.2 766 2 -7 3 28.692 57.384 0.312 6.38 2 20.7 0.2 767 2 4 4 28.696 57.391 0.312 6.38 2 1.8 0.0 768 -1 -1 6 28.704 57.408 0.312 6.38 2 49.9 1.3 769 3 -7 2 28.732 57.463 0.312 6.36 2 14.5 0.1 770 3 -1 5 28.751 57.502 0.312 6.35 2 20.4 0.2 771 -2 3 5 28.774 57.547 0.312 6.34 2 13.9 0.1 772 -5 1 5 28.776 57.553 0.312 6.34 2 82.0 3.6 773 4 2 4 28.836 57.671 0.313 6.31 2 11.9 0.1 774 -2 -8 1 28.843 57.686 0.313 6.31 2 94.8 4.8 775 -6 2 4 28.844 57.688 0.313 6.31 2 38.9 0.8 776 3 5 3 28.846 57.692 0.313 6.31 2 77.6 3.2 777 3 -2 5 28.867 57.733 0.313 6.3 2 19.7 0.2 778 -2 -8 2 28.875 57.75 0.313 6.29 2 32.9 0.6 779 1 -8 1 28.893 57.786 0.314 6.28 2 19.3 0.2 780 0 -7 4 28.896 57.793 0.314 6.28 2 40.4 0.9 781 -4 4 4 28.908 57.815 0.314 6.28 2 70.6 2.6 782 4 7 0 28.918 57.836 0.314 6.27 2 16.2 0.1 783 -2 -3 6 28.92 57.84 0.314 6.27 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6 30.744 61.487 0.332 5.47 2 77.8 2.8 956 -1 8 1 30.761 61.521 0.332 5.46 2 26.9 0.3 957 1 8 1 30.761 61.522 0.332 5.46 2 5.5 0.0 958 -3 1 6 30.788 61.576 0.332 5.45 2 61.5 1.7 959 7 2 2 30.826 61.653 0.333 5.43 2 30.8 0.4 960 4 7 1 30.849 61.698 0.333 5.43 2 25.8 0.3 961 -3 7 2 30.852 61.705 0.333 5.42 2 68.8 2.2 962 -7 3 3 30.855 61.71 0.333 5.42 2 41.7 0.8 963 3 8 0 30.859 61.719 0.333 5.42 2 10.1 0.0 964 0 1 6 30.884 61.767 0.333 5.41 2 20.9 0.2 965 -8 2 0 30.886 61.771 0.333 5.41 2 34.8 0.6 966 4 -7 2 30.898 61.797 0.333 5.41 2 33.7 0.5 967 1 0 6 30.903 61.806 0.333 5.4 2 22.2 0.2 968 -6 1 5 30.91 61.82 0.333 5.4 2 25.4 0.3 969 4 5 3 30.942 61.884 0.334 5.39 2 25.7 0.3 970 -1 4 5 31.024 62.048 0.335 5.36 2 15.1 0.1 971 5 4 3 31.038 62.076 0.335 5.35 2 13.0 0.1 972 7 -4 1 31.067 62.133 0.335 5.34 2 5.4 0.0 973 -4 -4 6 31.072 62.145 0.335 5.34 2 36.7 0.6 974 5 7 0 31.078 62.156 0.335 5.34 2 92.4 3.9 975 -8 2 2 31.08 62.16 0.335 5.34 2 24.6 0.3 976 -5 6 2 31.087 62.175 0.335 5.33 2 4.0 0.0 977 -8 -3 3 31.089 62.177 0.335 5.33 2 28.9 0.4 978 -4 -8 2 31.104 62.209 0.335 5.33 2 47.8 1.0 979 -2 -5 6 31.138 62.275 0.336 5.32 2 30.6 0.4 980 8 0 1 31.173 62.346 0.336 5.3 2 54.4 1.3 981 -2 4 5 31.174 62.348 0.336 5.3 2 94.9 4.0 982 7 4 1 31.188 62.375 0.336 5.3 2 33.8 0.5 983 -7 4 2 31.198 62.397 0.336 5.29 2 4.0 0.0 984 4 -1 5 31.214 62.428 0.336 5.29 2 28.0 0.4 985 2 -7 4 31.219 62.439 0.336 5.28 2 16.7 0.1 986 6 -5 2 31.232 62.464 0.337 5.28 2 23.1 0.2 987 2 3 5 31.266 62.532 0.337 5.27 2 25.9 0.3 988 -1 -5 6 31.268 62.536 0.337 5.27 2 60.1 1.6 989 -8 1 3 31.278 62.557 0.337 5.26 2 31.4 0.4 990 7 -3 2 31.287 62.575 0.337 5.26 2 55.4 1.4 991 7 5 0 31.32 62.64 0.337 5.25 2 43.8 0.9 992 -5 -2 6 31.322 62.643 0.337 5.25 2 32.0 0.5 993 3 2 5 31.324 62.648 0.337 5.25 2 59.2 1.6 994 -4 -8 1 31.337 62.674 0.338 5.24 2 55.2 1.4 995 4 -2 5 31.341 62.681 0.338 5.24 2 76.0 2.6 996 0 4 5 31.369 62.739 0.338 5.23 2 49.1 1.1 997 2 5 4 31.378 62.756 0.338 5.23 2 20.4 0.2 998 8 1 1 31.408 62.817 0.338 5.21 2 16.0 0.1 999 8 -1 1 31.411 62.822 0.338 5.21 2 23.2 0.2 1000 8 3 0 31.415 62.829 0.338 5.21 2 28.6 0.4 1001 3 -8 1 31.448 62.895 0.339 5.2 2 9.1 0.0 1002 -5 -1 6 31.472 62.945 0.339 5.19 2 61.3 1.7 1003 -2 -7 5 31.482 62.965 0.339 5.19 2 20.1 0.2 1004 -3 -5 6 31.501 63.002 0.339 5.18 2 38.0 0.6 1005 -2 8 1 31.503 63.006 0.339 5.18 2 65.7 1.9 1006 2 8 1 31.504 63.008 0.339 5.18 2 44.6 0.9 1007 -4 6 3 31.505 63.009 0.339 5.18 2 34.4 0.5 1008 -1 -7 5 31.514 63.027 0.339 5.18 2 115.8 5.9 1009 -6 -6 4 31.534 63.067 0.339 5.17 2 62.0 1.7 1010 4 0 5 31.561 63.121 0.34 5.16 2 59.6 1.6 1011 -1 -8 4 31.572 63.145 0.34 5.16 2 9.4 0.0 1012 -8 -4 2 31.575 63.15 0.34 5.15 2 48.1 1.0 1013 5 2 4 31.607 63.214 0.34 5.14 2 11.6 0.1 1014 -7 2 4 31.616 63.233 0.34 5.14 2 28.2 0.3 1015 1 -4 6 31.64 63.28 0.341 5.13 2 20.5 0.2 1016 -5 -3 6 31.643 63.286 0.341 5.13 2 48.6 1.0 1017 -3 8 0 31.647 63.295 0.341 5.13 2 20.8 0.2 1018 -2 -8 4 31.656 63.311 0.341 5.13 2 53.3 1.2 1019 -4 5 4 31.677 63.353 0.341 5.12 2 18.0 0.1 1020 3 7 2 31.741 63.481 0.341 5.1 2 55.8 1.3 1021 -4 1 6 31.744 63.488 0.342 5.09 2 43.7 0.8 1022 6 -4 3 31.75 63.501 0.342 5.09 2 46.6 0.9 1023 -4 -8 3 31.759 63.518 0.342 5.09 2 69.8 2.1 1024 -8 -4 1 31.812 63.624 0.342 5.07 2 63.6 1.7 1025 -3 4 5 31.814 63.628 0.342 5.07 2 33.1 0.5 1026 5 -4 4 31.821 63.642 0.342 5.07 2 11.0 0.1 1027 3 6 3 31.845 63.691 0.342 5.06 2 27.3 0.3 1028 -2 2 6 31.848 63.696 0.343 5.06 2 49.2 1.0 1029 -1 2 6 31.863 63.726 0.343 5.05 2 21.8 0.2 1030 -6 6 0 31.877 63.755 0.343 5.05 2 26.0 0.3 1031 2 -2 6 31.884 63.769 0.343 5.05 2 51.8 1.1 1032 0 -5 6 31.888 63.777 0.343 5.04 2 28.8 0.4 1033 -7 -2 5 31.894 63.788 0.343 5.04 2 41.0 0.7 1034 1 1 6 31.901 63.802 0.343 5.04 2 62.4 1.7 1035 -5 -7 4 31.916 63.832 0.343 5.03 2 67.7 2.0 1036 2 -1 6 31.92 63.84 0.343 5.03 2 9.3 0.0 1037 4 -3 5 31.937 63.874 0.343 5.03 2 12.8 0.1 1038 -3 -7 5 31.941 63.882 0.343 5.03 2 36.7 0.6 1039 -7 -1 5 31.947 63.895 0.343 5.02 2 73.3 2.3 1040 2 -8 3 31.948 63.896 0.343 5.02 2 40.3 0.7 1041 0 -8 4 31.979 63.958 0.344 5.01 2 5.9 0.0 1042 -8 3 1 31.98 63.961 0.344 5.01 2 17.4 0.1 1043 -5 -6 5 31.999 63.999 0.344 5.01 2 35.9 0.5 1044 0 -7 5 32.034 64.069 0.344 4.99 2 36.0 0.5 1045 -6 -7 2 32.055 64.11 0.345 4.99 2 17.6 0.1 1046 3 -5 5 32.089 64.178 0.345 4.98 2 6.9 0.0 1047 -5 0 6 32.092 64.183 0.345 4.98 2 41.8 0.7 1048 -6 -5 5 32.101 64.202 0.345 4.97 2 32.1 0.4 1049 2 -6 5 32.103 64.206 0.345 4.97 2 16.6 0.1 1050 8 2 1 32.112 64.223 0.345 4.97 2 77.9 2.6 1051 8 -2 1 32.117 64.234 0.345 4.97 2 82.8 2.9 1052 6 3 3 32.127 64.255 0.345 4.96 2 34.2 0.5 1053 3 -8 2 32.129 64.258 0.345 4.96 2 22.5 0.2 1054 -7 -5 4 32.142 64.285 0.345 4.96 2 15.2 0.1 1055 7 3 2 32.151 64.301 0.345 4.96 2 39.9 0.7 1056 -8 -1 4 32.158 64.315 0.345 4.95 2 12.3 0.1 1057 -1 7 3 32.167 64.335 0.346 4.95 2 52.5 1.2 1058 -7 -6 2 32.181 64.362 0.346 4.95 2 27.1 0.3 1059 -5 3 5 32.187 64.374 0.346 4.94 2 3.0 0.0 1060 -8 3 0 32.195 64.39 0.346 4.94 2 19.9 0.2 1061 0 7 3 32.199 64.399 0.346 4.94 2 38.4 0.6 1062 1 4 5 32.201 64.401 0.346 4.94 2 18.4 0.1 1063 -8 -2 4 32.216 64.433 0.346 4.93 2 88.9 3.3 1064 -8 -4 3 32.218 64.436 0.346 4.93 2 50.4 1.1 1065 -5 7 0 32.219 64.438 0.346 4.93 2 40.0 0.7 1066 -3 -8 4 32.226 64.453 0.346 4.93 2 25.2 0.3 1067 -1 -9 1 32.293 64.585 0.347 4.91 2 76.9 2.5 1068 -6 6 1 32.306 64.612 0.347 4.9 2 17.5 0.1 1069 -7 -3 5 32.308 64.616 0.347 4.9 2 42.2 0.7 1070 2 -3 6 32.316 64.631 0.347 4.9 2 22.1 0.2 1071 -3 2 6 32.32 64.64 0.347 4.9 2 12.7 0.1 1072 -1 -9 2 32.324 64.648 0.347 4.9 2 115.0 5.5 1073 0 -9 1 32.324 64.648 0.347 4.9 2 27.1 0.3 1074 6 -6 1 32.324 64.649 0.347 4.9 2 83.9 2.9 1075 -4 -5 6 32.349 64.698 0.347 4.89 2 3.3 0.0 1076 -6 2 5 32.36 64.719 0.347 4.89 2 4.0 0.0 1077 0 2 6 32.365 64.729 0.347 4.88 2 30.9 0.4 1078 4 1 5 32.372 64.743 0.348 4.88 2 9.4 0.0 1079 5 -7 1 32.408 64.816 0.348 4.87 2 77.8 2.5 1080 -6 -7 1 32.414 64.829 0.348 4.87 2 33.9 0.5 1081 2 0 6 32.422 64.844 0.348 4.87 2 13.6 0.1 1082 -4 7 2 32.423 64.846 0.348 4.87 2 7.9 0.0 1083 -5 -4 6 32.429 64.858 0.348 4.86 2 23.1 0.2 1084 -1 6 4 32.435 64.871 0.348 4.86 2 17.8 0.1 1085 4 8 0 32.446 64.892 0.348 4.86 2 56.8 1.3 1086 -7 5 0 32.456 64.913 0.348 4.85 2 20.6 0.2 1087 -7 0 5 32.467 64.933 0.348 4.85 2 18.5 0.1 1088 0 -9 2 32.485 64.969 0.349 4.85 2 26.6 0.3 1089 -8 2 3 32.497 64.994 0.349 4.84 2 60.5 1.5 1090 -7 -6 1 32.541 65.082 0.349 4.83 2 9.9 0.0 1091 -8 0 4 32.564 65.128 0.349 4.82 2 52.4 1.1 1092 -6 -7 3 32.569 65.137 0.349 4.82 2 8.1 0.0 1093 0 6 4 32.612 65.224 0.35 4.8 2 29.1 0.3 1094 -2 7 3 32.62 65.239 0.35 4.8 2 16.1 0.1 1095 -7 5 1 32.626 65.253 0.35 4.8 2 94.3 3.6 1096 4 4 4 32.627 65.254 0.35 4.8 2 102.9 4.3 1097 -8 3 2 32.639 65.279 0.35 4.8 2 11.9 0.1 1098 -2 -9 2 32.647 65.295 0.35 4.79 2 24.9 0.3 1099 7 -1 3 32.677 65.354 0.35 4.78 2 111.1 5.0 1100 5 -6 3 32.68 65.361 0.35 4.78 2 35.6 0.5 1101 -7 -6 3 32.692 65.384 0.351 4.78 2 14.8 0.1 1102 6 6 1 32.694 65.388 0.351 4.78 2 36.2 0.5 1103 5 6 2 32.714 65.429 0.351 4.77 2 29.6 0.4 1104 7 0 3 32.714 65.429 0.351 4.77 2 11.0 0.0 1105 1 7 3 32.715 65.431 0.351 4.77 2 28.7 0.3 1106 4 -7 3 32.719 65.439 0.351 4.77 2 28.3 0.3 1107 -3 8 1 32.72 65.439 0.351 4.77 2 26.6 0.3 1108 3 8 1 32.721 65.442 0.351 4.77 2 6.3 0.0 1109 -8 -3 4 32.739 65.477 0.351 4.77 2 18.2 0.1 1110 -6 5 3 32.739 65.478 0.351 4.76 2 3.9 0.0 1111 -2 6 4 32.742 65.483 0.351 4.76 2 12.3 0.1 1112 -2 -9 1 32.744 65.489 0.351 4.76 2 38.7 0.6 1113 7 -4 2 32.781 65.561 0.351 4.75 2 17.1 0.1 1114 4 -6 4 32.818 65.636 0.352 4.74 2 40.8 0.7 1115 6 -1 4 32.822 65.643 0.352 4.74 2 3.8 0.0 1116 6 5 2 32.825 65.651 0.352 4.74 2 9.0 0.0 1117 1 -9 1 32.839 65.677 0.352 4.73 2 18.2 0.1 1118 1 -8 4 32.865 65.731 0.352 4.73 2 25.8 0.3 1119 0 8 2 32.867 65.733 0.352 4.73 2 103.8 4.3 1120 -4 -7 5 32.879 65.758 0.352 4.72 2 24.9 0.2 1121 -5 7 1 32.901 65.801 0.353 4.71 2 81.7 2.7 1122 -2 -6 6 32.908 65.815 0.353 4.71 2 65.1 1.7 1123 -5 -8 2 32.91 65.819 0.353 4.71 2 16.9 0.1 1124 8 4 0 32.918 65.836 0.353 4.71 2 124.6 6.2 1125 -4 4 5 32.93 65.859 0.353 4.71 2 20.1 0.2 1126 -6 4 4 32.954 65.909 0.353 4.7 2 17.3 0.1 1127 -1 8 2 32.979 65.957 0.353 4.69 2 17.3 0.1 1128 1 -5 6 32.984 65.968 0.353 4.69 2 33.0 0.4 1129 4 -4 5 32.989 65.979 0.353 4.69 2 29.4 0.3 1130 -7 4 3 32.994 65.987 0.353 4.69 2 13.0 0.1 1131 6 0 4 33.001 66.002 0.354 4.68 2 65.6 1.7 1132 3 5 4 33.03 66.059 0.354 4.68 2 60.5 1.4 1133 1 -7 5 33.032 66.063 0.354 4.68 2 33.1 0.4 1134 0 9 0 33.032 66.064 0.354 4.67 2 4.8 0.0 1135 -1 -6 6 33.05 66.1 0.354 4.67 2 14.2 0.1 1136 5 7 1 33.062 66.124 0.354 4.67 2 17.8 0.1 1137 3 -7 4 33.067 66.134 0.354 4.66 2 81.5 2.6 1138 -9 -1 1 33.067 66.134 0.354 4.66 2 30.1 0.4 1139 3 3 5 33.08 66.16 0.354 4.66 2 146.3 8.4 1140 -9 -1 2 33.086 66.172 0.354 4.66 2 110.5 4.8 1141 7 -2 3 33.101 66.202 0.354 4.65 2 28.8 0.3 1142 6 -2 4 33.103 66.206 0.355 4.65 2 24.7 0.2 1143 -9 0 1 33.107 66.213 0.355 4.65 2 19.7 0.2 1144 1 -9 2 33.125 66.25 0.355 4.65 2 75.4 2.2 1145 1 9 0 33.128 66.257 0.355 4.65 2 37.8 0.6 1146 7 -5 1 33.153 66.306 0.355 4.64 2 14.3 0.1 1147 -5 1 6 33.165 66.33 0.355 4.64 2 53.7 1.1 1148 -7 -4 5 33.179 66.358 0.355 4.63 2 18.7 0.1 1149 -6 -2 6 33.185 66.369 0.355 4.63 2 60.9 1.5 1150 5 3 4 33.198 66.395 0.355 4.63 2 11.7 0.1 1151 2 -4 6 33.204 66.408 0.355 4.62 2 52.4 1.1 1152 7 1 3 33.212 66.424 0.356 4.62 2 33.9 0.4 1153 -1 -9 3 33.222 66.443 0.356 4.62 2 26.5 0.3 1154 1 8 2 33.234 66.468 0.356 4.61 2 10.0 0.0 1155 -3 -6 6 33.245 66.489 0.356 4.61 2 36.7 0.5 1156 -9 0 2 33.252 66.503 0.356 4.61 2 17.7 0.1 1157 -5 -8 1 33.263 66.525 0.356 4.61 2 17.3 0.1 1158 8 3 1 33.266 66.533 0.356 4.61 2 1.6 0.0 1159 -4 2 6 33.268 66.535 0.356 4.6 2 22.9 0.2 1160 1 6 4 33.268 66.535 0.356 4.6 2 15.2 0.1 1161 -4 -8 4 33.271 66.542 0.356 4.6 2 31.3 0.4 1162 8 -3 1 33.274 66.548 0.356 4.6 2 9.3 0.0 1163 -8 -5 2 33.282 66.563 0.356 4.6 2 20.2 0.2 1164 7 5 1 33.299 66.598 0.356 4.6 2 48.8 0.9 1165 1 2 6 33.341 66.682 0.357 4.58 2 13.4 0.1 1166 -6 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0 2 33.514 67.029 0.358 4.53 2 97.7 3.7 1188 -3 6 4 33.524 67.049 0.358 4.53 2 19.0 0.1 1189 -3 7 3 33.546 67.093 0.359 4.52 2 55.0 1.2 1190 6 -5 3 33.548 67.097 0.359 4.52 2 30.0 0.3 1191 -2 8 2 33.568 67.136 0.359 4.52 2 49.8 0.9 1192 4 7 2 33.574 67.147 0.359 4.52 2 23.6 0.2 1193 -6 6 2 33.593 67.186 0.359 4.51 2 86.2 2.8 1194 -9 1 1 33.604 67.207 0.359 4.51 2 90.9 3.2 1195 8 -1 2 33.619 67.237 0.359 4.5 2 38.9 0.6 1196 6 -6 2 33.629 67.257 0.359 4.5 2 42.3 0.7 1197 4 2 5 33.629 67.259 0.359 4.5 2 3.5 0.0 1198 6 7 0 33.632 67.264 0.36 4.5 2 19.9 0.2 1199 -8 -5 1 33.637 67.274 0.36 4.5 2 18.7 0.1 1200 6 1 4 33.637 67.275 0.36 4.5 2 40.3 0.6 1201 -7 5 2 33.656 67.312 0.36 4.49 2 19.3 0.1 1202 -5 -5 6 33.662 67.324 0.36 4.49 2 70.6 1.9 1203 3 -8 3 33.663 67.326 0.36 4.49 2 18.6 0.1 1204 0 -6 6 33.668 67.337 0.36 4.49 2 41.4 0.7 1205 -3 -9 1 33.67 67.339 0.36 4.49 2 26.0 0.3 1206 2 9 0 33.701 67.402 0.36 4.48 2 24.5 0.2 1207 2 7 3 33.703 67.406 0.36 4.48 2 12.2 0.1 1208 -8 -4 4 33.713 67.427 0.36 4.48 2 11.5 0.1 1209 7 6 0 33.758 67.516 0.361 4.46 2 22.4 0.2 1210 -1 5 5 33.769 67.539 0.361 4.46 2 71.1 1.9 1211 -8 -5 3 33.783 67.565 0.361 4.46 2 14.4 0.1 1212 -1 3 6 33.792 67.584 0.361 4.46 2 64.1 1.6 1213 -2 3 6 33.793 67.587 0.361 4.46 2 30.1 0.3 1214 -2 -2 7 33.8 67.599 0.361 4.45 2 42.2 0.7 1215 4 6 3 33.817 67.635 0.361 4.45 2 46.7 0.8 1216 9 0 0 33.819 67.639 0.361 4.45 2 23.5 0.2 1217 2 -9 1 33.824 67.649 0.361 4.45 2 32.7 0.4 1218 6 -3 4 33.839 67.677 0.361 4.44 2 27.7 0.3 1219 -8 4 1 33.847 67.695 0.362 4.44 2 43.7 0.7 1220 8 1 2 33.866 67.732 0.362 4.44 2 19.3 0.1 1221 -9 1 2 33.872 67.744 0.362 4.43 2 81.1 2.5 1222 3 -2 6 33.886 67.771 0.362 4.43 2 20.2 0.2 1223 7 4 2 33.902 67.803 0.362 4.43 2 41.2 0.6 1224 3 -1 6 33.905 67.809 0.362 4.42 2 96.5 3.5 1225 9 1 0 33.905 67.81 0.362 4.42 2 24.1 0.2 1226 -6 -6 5 33.905 67.811 0.362 4.42 2 135.2 6.9 1227 -2 5 5 33.928 67.856 0.362 4.42 2 24.8 0.2 1228 -8 4 0 33.932 67.863 0.362 4.42 2 39.5 0.6 1229 -6 -7 4 33.935 67.87 0.362 4.42 2 20.3 0.2 1230 -9 -1 3 33.962 67.923 0.363 4.41 2 63.8 1.5 1231 -6 0 6 33.963 67.927 0.363 4.41 2 42.3 0.7 1232 7 -3 3 33.977 67.955 0.363 4.4 2 75.9 2.1 1233 -1 -2 7 34.003 68.006 0.363 4.4 2 3.0 0.0 1234 6 4 3 34.019 68.038 0.363 4.39 2 69.6 1.8 1235 -2 -1 7 34.022 68.044 0.363 4.39 2 47.6 0.8 1236 -2 -3 7 34.031 68.063 0.363 4.39 2 15.9 0.1 1237 3 -6 5 34.035 68.07 0.363 4.39 2 21.9 0.2 1238 5 -1 5 34.045 68.09 0.363 4.39 2 55.6 1.1 1239 -4 -6 6 34.054 68.108 0.363 4.38 2 52.8 1.0 1240 -7 -6 4 34.054 68.109 0.363 4.38 2 18.1 0.1 1241 -3 -2 7 34.069 68.139 0.364 4.38 2 28.6 0.3 1242 2 8 2 34.073 68.146 0.364 4.38 2 86.6 2.8 1243 -3 -9 3 34.079 68.158 0.364 4.38 2 23.9 0.2 1244 0 5 5 34.084 68.168 0.364 4.38 2 4.2 0.0 1245 -9 -3 2 34.126 68.251 0.364 4.37 2 60.0 1.3 1246 -9 -2 3 34.127 68.254 0.364 4.36 2 27.6 0.3 1247 -8 3 3 34.145 68.291 0.364 4.36 2 9.0 0.0 1248 7 2 3 34.159 68.319 0.364 4.36 2 34.8 0.4 1249 8 -2 2 34.177 68.353 0.365 4.35 2 36.0 0.5 1250 5 -2 5 34.182 68.363 0.365 4.35 2 28.1 0.3 1251 4 -8 2 34.187 68.373 0.365 4.35 2 54.6 1.1 1252 -9 1 0 34.187 68.375 0.365 4.35 2 59.5 1.3 1253 -1 -1 7 34.209 68.418 0.365 4.34 2 68.6 1.7 1254 2 -8 4 34.212 68.425 0.365 4.34 2 32.3 0.4 1255 -6 -4 6 34.229 68.457 0.365 4.34 2 22.9 0.2 1256 -6 3 5 34.229 68.457 0.365 4.34 2 17.0 0.1 1257 2 -9 2 34.232 68.465 0.365 4.34 2 16.1 0.1 1258 -9 0 3 34.249 68.498 0.365 4.33 2 22.0 0.2 1259 -1 -3 7 34.25 68.5 0.365 4.33 2 48.8 0.9 1260 1 -9 3 34.263 68.526 0.365 4.33 2 48.7 0.9 1261 0 3 6 34.263 68.527 0.365 4.33 2 24.9 0.2 1262 -2 9 0 34.266 68.533 0.365 4.33 2 42.0 0.6 1263 -3 3 6 34.267 68.534 0.365 4.33 2 65.9 1.6 1264 -5 -7 5 34.275 68.551 0.366 4.33 2 33.8 0.4 1265 -2 -8 5 34.277 68.554 0.366 4.33 2 30.2 0.3 1266 -3 -3 7 34.285 68.569 0.366 4.32 2 70.6 1.8 1267 -3 -1 7 34.306 68.613 0.366 4.32 2 25.4 0.2 1268 3 -3 6 34.32 68.639 0.366 4.31 2 53.0 1.0 1269 -1 -8 5 34.323 68.645 0.366 4.31 2 41.7 0.6 1270 -9 -3 1 34.355 68.709 0.366 4.31 2 53.5 1.0 1271 5 0 5 34.361 68.721 0.366 4.3 2 47.6 0.8 1272 3 0 6 34.376 68.752 0.367 4.3 2 8.5 0.0 1273 -4 8 1 34.385 68.77 0.367 4.3 2 63.3 1.5 1274 4 8 1 34.386 68.773 0.367 4.3 2 67.5 1.7 1275 2 6 4 34.389 68.777 0.367 4.3 2 51.3 1.0 1276 -5 7 2 34.425 68.85 0.367 4.29 2 35.9 0.5 1277 9 2 0 34.442 68.885 0.367 4.28 2 3.5 0.0 1278 5 8 0 34.464 68.928 0.367 4.28 2 19.0 0.1 1279 4 -5 5 34.476 68.953 0.367 4.27 2 31.7 0.4 1280 2 -7 5 34.485 68.97 0.368 4.27 2 7.7 0.0 1281 -7 -5 5 34.491 68.982 0.368 4.27 2 16.1 0.1 1282 -5 4 5 34.497 68.994 0.368 4.27 2 11.2 0.0 1283 2 -5 6 34.532 69.064 0.368 4.26 2 33.1 0.4 1284 -9 2 1 34.548 69.097 0.368 4.26 2 31.3 0.4 1285 -3 5 5 34.557 69.114 0.368 4.25 2 77.6 2.2 1286 0 9 1 34.581 69.162 0.368 4.25 2 9.0 0.0 1287 -8 4 2 34.612 69.223 0.369 4.24 2 60.6 1.3 1288 -3 8 2 34.622 69.244 0.369 4.24 2 29.5 0.3 1289 8 2 2 34.666 69.332 0.369 4.23 2 70.8 1.8 1290 -5 2 6 34.672 69.343 0.369 4.22 2 20.2 0.1 1291 0 -2 7 34.676 69.352 0.369 4.22 2 62.7 1.4 1292 7 -5 2 34.69 69.379 0.369 4.22 2 65.3 1.5 1293 -2 0 7 34.694 69.387 0.369 4.22 2 83.1 2.5 1294 -3 -8 5 34.701 69.402 0.37 4.22 2 14.2 0.1 1295 -4 -9 2 34.707 69.415 0.37 4.22 2 6.3 0.0 1296 -2 -4 7 34.713 69.426 0.37 4.21 2 65.9 1.6 1297 6 2 4 34.718 69.436 0.37 4.21 2 28.9 0.3 1298 -8 2 4 34.728 69.457 0.37 4.21 2 45.0 0.7 1299 3 9 0 34.738 69.476 0.37 4.21 2 17.5 0.1 1300 -9 -3 3 34.743 69.485 0.37 4.21 2 21.3 0.2 1301 1 -6 6 34.751 69.502 0.37 4.21 2 34.6 0.4 1302 -4 6 4 34.767 69.534 0.37 4.2 2 21.6 0.2 1303 5 -3 5 34.768 69.536 0.37 4.2 2 58.2 1.2 1304 -5 -8 4 34.769 69.538 0.37 4.2 2 11.4 0.0 1305 2 2 6 34.773 69.545 0.37 4.2 2 20.8 0.2 1306 -7 -7 2 34.789 69.579 0.37 4.2 2 5.1 0.0 1307 1 9 1 34.8 69.6 0.37 4.19 2 40.4 0.6 1308 -4 -2 7 34.807 69.614 0.371 4.19 2 80.0 2.3 1309 -8 -2 5 34.807 69.614 0.371 4.19 2 74.6 2.0 1310 -1 9 1 34.831 69.661 0.371 4.19 2 64.8 1.5 1311 8 5 0 34.836 69.673 0.371 4.18 2 34.7 0.4 1312 0 -8 5 34.837 69.674 0.371 4.18 2 63.3 1.4 1313 -7 2 5 34.849 69.698 0.371 4.18 2 29.9 0.3 1314 8 4 1 34.851 69.702 0.371 4.18 2 42.8 0.6 1315 8 -4 1 34.861 69.722 0.371 4.18 2 37.7 0.5 1316 -1 0 7 34.864 69.727 0.371 4.18 2 16.3 0.1 1317 0 -1 7 34.864 69.729 0.371 4.18 2 11.8 0.0 1318 1 5 5 34.866 69.732 0.371 4.18 2 53.6 1.0 1319 -8 -1 5 34.874 69.747 0.371 4.18 2 12.2 0.1 1320 -4 7 3 34.929 69.857 0.372 4.16 2 17.6 0.1 1321 0 -3 7 34.936 69.872 0.372 4.16 2 24.2 0.2 1322 -9 2 2 34.936 69.873 0.372 4.16 2 12.3 0.1 1323 -1 -4 7 34.945 69.89 0.372 4.16 2 25.3 0.2 1324 -6 7 0 34.946 69.892 0.372 4.16 2 19.8 0.1 1325 -3 -4 7 34.948 69.897 0.372 4.16 2 13.2 0.1 1326 -1 -9 4 34.951 69.903 0.372 4.16 2 18.9 0.1 1327 -9 1 3 34.984 69.968 0.372 4.15 2 44.0 0.7 1328 -3 0 7 34.991 69.982 0.372 4.15 2 19.7 0.1 X-ray diffraction powder data (I)...X-Ray wave length = 1.54056 (angs.): No H K L Theta 2*Theta d I int I int.n. I p.h.n. H(Si) ( degree ) (angstrem) *100 *100 1 0 1 0 3.472 6.945 12.71766 44.3 10.4 10.4 5.5 2 1 0 0 3.546 7.091 12.45565 52.6 12.4 12.4 5.5 3 0 0 1 4.758 9.517 9.28565 249.0 58.5 58.6 5.6 4 1 1 0 4.881 9.761 9.05352 282.0 66.3 66.3 5.6 5 -1 1 0 5.05 10.099 8.75149 25.4 6.0 6.0 5.6 6 0 -1 1 5.302 10.603 8.33656 15.6 3.7 3.7 5.6 7 -1 0 1 5.343 10.685 8.27276 31.9 7.5 7.5 5.6 8 -1 -1 1 5.76 11.519 7.67544 425.4 100.0 100.0 5.6 9 1 0 1 6.481 12.963 6.82387 10.7 2.5 2.5 5.6 10 1 -1 1 6.952 13.905 6.36354 52.7 12.4 12.4 5.6 11 2 0 0 7.105 14.209 6.22783 15.8 3.7 3.7 5.6 12 0 -2 1 7.608 15.217 5.81774 54.2 12.7 12.7 5.6 13 1 1 1 7.747 15.493 5.71461 224.6 52.8 52.7 5.6 14 -2 -1 1 7.976 15.952 5.55117 7.1 1.7 1.7 5.6 15 1 -2 1 8.893 17.786 4.98261 4.4 1.0 1.0 5.6 16 0 2 1 9.203 18.407 4.81613 30.5 7.2 7.1 5.6 17 2 0 1 9.324 18.649 4.75415 61.9 14.6 14.5 5.6 18 0 -1 2 9.487 18.975 4.67318 8.2 1.9 1.9 5.6 19 0 0 2 9.55 19.1 4.64282 33.5 7.9 7.8 5.6 20 -2 -2 1 9.587 19.175 4.62491 107.5 25.3 25.2 5.6 21 2 -1 1 9.705 19.409 4.56951 7.7 1.8 1.8 5.6 22 2 2 0 9.797 19.594 4.52676 8.0 1.9 1.9 5.6 23 -2 2 0 10.139 20.278 4.37574 21.7 5.1 5.1 5.6 24 -2 -1 2 10.596 21.192 4.18894 4.6 1.1 1.1 5.6 25 0 -2 2 10.649 21.298 4.16828 16.5 3.9 3.9 5.6 26 -2 0 2 10.732 21.465 4.13638 10.4 2.4 2.4 5.6 27 -1 -3 1 10.765 21.53 4.12405 18.4 4.3 4.3 5.6 28 1 -1 2 10.832 21.665 4.09863 23.9 5.6 5.6 5.6 29 -3 -1 1 10.951 21.901 4.05489 40.2 9.5 9.4 5.6 30 -1 3 0 11.181 22.363 3.97226 14.9 3.5 3.5 5.6 31 -2 2 1 11.214 22.428 3.96075 7.5 1.8 1.8 5.6 32 -3 1 0 11.368 22.735 3.90796 29.4 6.9 6.9 5.6 33 -2 -2 2 11.579 23.157 3.83772 105.1 24.7 24.5 5.6 34 1 -2 2 11.905 23.81 3.73401 8.0 1.9 1.9 5.6 35 1 1 2 11.948 23.897 3.72062 35.8 8.4 8.4 5.6 36 2 2 1 12.099 24.198 3.67494 76.8 18.1 17.9 5.6 37 -1 -3 2 12.582 25.165 3.53591 79.7 18.7 18.6 5.6 38 -3 -1 2 12.737 25.474 3.49374 31.7 7.5 7.4 5.6 39 -2 3 0 12.9 25.799 3.45037 4.6 1.1 1.1 5.6 40 0 2 2 12.954 25.907 3.43625 29.2 6.9 6.8 5.6 41 -3 2 0 13.002 26.004 3.42369 13.9 3.3 3.2 5.6 42 2 0 2 13.048 26.095 3.41193 27.0 6.3 6.3 5.6 43 2 -3 1 13.533 27.065 3.29183 15.4 3.6 3.6 5.6 44 -3 2 1 13.616 27.231 3.27214 5.8 1.4 1.4 5.6 45 -1 -1 3 13.816 27.631 3.22564 8.2 1.9 1.9 5.6 46 0 -4 1 13.878 27.755 3.21154 15.7 3.7 3.7 5.6 47 -1 -4 1 13.972 27.944 3.19021 76.6 18.0 17.8 5.6 48 -1 0 3 14.136 28.273 3.15392 20.7 4.9 4.8 5.6 49 -4 0 1 14.17 28.34 3.14657 12.9 3.0 3.0 5.6 50 4 0 0 14.322 28.644 3.11391 12.0 2.8 2.8 5.6 51 -1 -2 3 14.387 28.774 3.10006 19.1 4.5 4.4 5.6 52 3 2 1 14.722 29.444 3.03101 6.1 1.4 1.4 5.6 53 -2 0 3 14.772 29.544 3.021 7.1 1.7 1.6 5.6 54 -2 -2 3 14.955 29.91 2.98488 17.6 4.1 4.1 5.6 55 -3 -3 2 15.159 30.318 2.94563 12.9 3.0 3.0 5.6 56 -1 1 3 15.298 30.595 2.91958 21.1 5.0 4.9 5.6 57 0 -4 2 15.355 30.711 2.90887 44.3 10.4 10.3 5.6 58 0 1 3 15.525 31.049 2.87791 5.0 1.2 1.2 5.6 59 2 4 0 15.56 31.121 2.87147 9.1 2.1 2.1 5.6 60 -4 0 2 15.612 31.224 2.8622 33.2 7.8 7.7 5.6 61 -1 3 2 15.69 31.379 2.84839 11.2 2.6 2.6 5.6 62 -1 -3 3 15.762 31.524 2.83564 50.7 11.9 11.7 5.6 63 3 -1 2 15.847 31.694 2.8208 12.2 2.9 2.8 5.6 64 -3 -1 3 15.883 31.765 2.81464 19.0 4.5 4.4 5.6 65 -2 -4 2 15.92 31.841 2.80816 13.7 3.2 3.2 5.6 66 -2 4 0 16.005 32.011 2.79362 100.7 23.7 23.3 5.6 67 3 -3 1 16.075 32.151 2.78176 22.5 5.3 5.2 5.6 68 -4 -2 2 16.112 32.224 2.77559 16.4 3.9 3.8 5.6 69 -4 2 0 16.207 32.413 2.75986 21.0 4.9 4.9 5.6 70 1 4 1 16.268 32.535 2.74976 4.7 1.1 1.1 5.6 71 2 -4 1 16.317 32.633 2.74175 24.5 5.8 5.7 5.6 72 1 3 2 16.404 32.807 2.72761 20.4 4.8 4.7 5.6 73 -4 2 1 16.499 32.999 2.71221 25.8 6.1 6.0 5.6 74 1 1 3 16.568 33.137 2.70121 87.0 20.4 20.1 5.6 75 3 3 1 16.866 33.732 2.65494 37.1 8.7 8.6 5.7 76 -2 4 1 17.143 34.287 2.61323 37.0 8.7 8.6 5.7 77 1 -3 3 17.209 34.418 2.60355 12.0 2.8 2.8 5.7 78 4 -2 1 17.347 34.694 2.58346 36.6 8.6 8.5 5.7 79 2 0 3 17.402 34.804 2.57553 20.8 4.9 4.8 5.7 80 -3 -3 3 17.522 35.044 2.55848 64.8 15.2 15.0 5.7 81 2 4 1 17.554 35.108 2.55397 12.3 2.9 2.8 5.7 82 -5 -1 1 17.726 35.451 2.52999 22.3 5.2 5.1 5.7 83 2 -2 3 17.762 35.524 2.525 18.2 4.3 4.2 5.7 84 1 -5 1 18.017 36.033 2.49046 36.6 8.6 8.4 5.7 85 -1 5 0 18.128 36.256 2.47569 5.6 1.3 1.3 5.7 86 3 -3 2 18.184 36.369 2.46825 57.3 13.5 13.2 5.7 87 -4 0 3 18.309 36.619 2.45198 9.0 2.1 2.1 5.7 88 -5 1 1 18.364 36.729 2.44488 31.8 7.5 7.3 5.7 89 -5 1 0 18.487 36.975 2.42918 6.3 1.5 1.5 5.7 90 -5 -1 2 18.544 37.088 2.422 44.4 10.4 10.3 5.7 91 0 4 2 18.655 37.311 2.40806 8.4 2.0 1.9 5.7 92 -1 -2 4 18.799 37.598 2.3903 6.5 1.5 1.5 5.7 93 -2 -1 4 18.834 37.668 2.38602 5.8 1.4 1.3 5.7 94 4 0 2 18.908 37.816 2.37707 18.4 4.3 4.2 5.7 95 -4 -4 1 19.048 38.095 2.36026 59.4 14.0 13.7 5.7 96 0 -2 4 19.248 38.496 2.33659 7.0 1.7 1.6 5.7 97 -2 0 4 19.288 38.576 2.33194 20.7 4.9 4.8 5.7 98 0 0 4 19.379 38.758 2.32141 11.2 2.6 2.6 5.7 99 -4 -4 2 19.457 38.914 2.31246 18.8 4.4 4.3 5.7 100 -5 1 2 19.528 39.057 2.30435 23.9 5.6 5.5 5.7 101 3 -1 3 19.649 39.298 2.29072 21.0 4.9 4.8 5.7 102 2 2 3 19.839 39.678 2.26967 22.9 5.4 5.3 5.7 103 4 4 0 19.897 39.793 2.26338 15.1 3.5 3.5 5.7 104 3 3 2 19.999 39.998 2.25226 14.3 3.4 3.3 5.7 105 -3 -5 2 20.047 40.094 2.24711 25.4 6.0 5.8 5.7 106 1 -1 4 20.086 40.172 2.24291 9.4 2.2 2.2 5.7 107 -5 -3 2 20.259 40.519 2.22451 30.4 7.1 7.0 5.7 108 3 5 0 20.471 40.943 2.20243 34.6 8.1 8.0 5.7 109 -5 -1 3 20.562 41.125 2.19312 37.6 8.8 8.6 5.7 110 2 4 2 20.595 41.189 2.18984 33.1 7.8 7.6 5.7 111 5 3 0 20.689 41.377 2.1803 36.5 8.6 8.4 5.7 112 4 2 2 20.765 41.53 2.17264 9.6 2.2 2.2 5.7 113 2 -4 3 20.794 41.587 2.16979 12.1 2.8 2.8 5.7 114 -3 -3 4 20.849 41.697 2.1643 22.4 5.3 5.1 5.7 115 -4 2 3 20.918 41.836 2.15747 4.3 1.0 1.0 5.7 116 -3 5 0 21.129 42.259 2.13684 5.1 1.2 1.2 5.7 117 -4 4 1 21.197 42.394 2.13033 59.4 14.0 13.6 5.7 118 1 -3 4 21.279 42.557 2.12254 18.7 4.4 4.3 5.7 119 -6 0 1 21.333 42.666 2.11738 11.4 2.7 2.6 5.7 120 3 -5 1 21.378 42.755 2.11317 17.8 4.2 4.1 5.7 121 1 1 4 21.434 42.867 2.10791 42.6 10.0 9.8 5.7 122 1 -5 3 21.528 43.057 2.09908 15.6 3.7 3.6 5.7 123 -4 -2 4 21.578 43.156 2.09447 49.0 11.5 11.2 5.7 124 0 -4 4 21.69 43.381 2.08414 9.0 2.1 2.1 5.7 125 -5 1 3 21.805 43.61 2.07371 11.6 2.7 2.7 5.7 126 4 4 1 21.881 43.763 2.06683 49.2 11.6 11.3 5.7 127 -2 -6 2 21.935 43.87 2.06202 13.6 3.2 3.1 5.7 128 -6 -2 1 21.968 43.936 2.05909 8.5 2.0 1.9 5.7 129 -1 5 2 22.004 44.009 2.05584 24.7 5.8 5.7 5.7 130 -6 0 2 22.036 44.072 2.05302 60.8 14.3 13.9 5.7 131 2 -2 4 22.078 44.156 2.04932 6.8 1.6 1.6 5.7 132 5 -3 1 22.257 44.514 2.03366 8.8 2.1 2.0 5.7 133 5 -1 2 22.335 44.669 2.02697 38.3 9.0 8.8 5.7 134 0 4 3 22.364 44.729 2.02441 42.5 10.0 9.7 5.7 135 1 5 2 22.463 44.926 2.016 8.0 1.9 1.8 5.7 136 4 0 3 22.59 45.18 2.00525 26.8 6.3 6.1 5.7 137 6 2 0 22.731 45.461 1.99349 10.7 2.5 2.5 5.7 138 -2 4 3 22.778 45.555 1.98958 36.2 8.5 8.3 5.7 139 0 6 1 22.868 45.736 1.98212 22.2 5.2 5.1 5.7 140 4 -4 2 22.92 45.84 1.97789 20.6 4.8 4.7 5.7 141 4 -2 3 22.962 45.923 1.9745 19.8 4.7 4.5 5.7 142 -6 2 0 23.217 46.434 1.95398 4.5 1.1 1.0 5.7 143 -1 -5 4 23.262 46.524 1.9504 21.2 5.0 4.8 5.7 144 6 0 1 23.325 46.651 1.94539 6.9 1.6 1.6 5.7 145 -2 -6 3 23.406 46.812 1.93906 43.7 10.3 10.0 5.7 146 -1 -1 5 23.502 47.004 1.93157 18.2 4.3 4.2 5.7 147 -2 -2 5 23.617 47.235 1.92269 14.5 3.4 3.3 5.7 148 -4 -4 4 23.667 47.335 1.91886 11.9 2.8 2.7 5.7 149 2 -6 2 23.729 47.458 1.91417 14.9 3.5 3.4 5.7 150 -6 -2 3 23.774 47.547 1.91078 9.6 2.3 2.2 5.7 151 -6 0 3 23.809 47.617 1.90814 9.3 2.2 2.1 5.7 152 -1 3 4 23.867 47.733 1.90376 14.4 3.4 3.3 5.7 153 3 -1 4 23.992 47.985 1.89437 32.0 7.5 7.3 5.7 154 -6 2 2 24.085 48.171 1.88749 18.1 4.3 4.1 5.7 155 2 6 1 24.147 48.293 1.88299 21.7 5.1 4.9 5.7 156 5 -3 2 24.216 48.433 1.87789 8.4 2.0 1.9 5.7 157 6 -2 1 24.386 48.773 1.86559 8.3 1.9 1.9 5.7 158 2 2 4 24.46 48.92 1.86031 7.1 1.7 1.6 5.7 159 6 2 1 24.535 49.069 1.85501 26.4 6.2 6.0 5.7 160 1 -5 4 24.714 49.429 1.84235 5.8 1.4 1.3 5.7 161 -3 -3 5 24.839 49.677 1.83373 4.3 1.0 1.0 5.7 162 -1 -7 2 24.886 49.771 1.83048 9.9 2.3 2.3 5.7 163 -5 1 4 24.953 49.906 1.82586 7.6 1.8 1.7 5.7 164 -3 3 4 25.07 50.139 1.8179 24.8 5.8 5.6 5.7 165 1 -7 1 25.118 50.236 1.81462 10.0 2.3 2.3 5.8 166 5 5 0 25.176 50.352 1.8107 17.2 4.0 3.9 5.8 167 3 5 2 25.267 50.533 1.80464 7.8 1.8 1.8 5.8 168 -1 5 3 25.313 50.627 1.80153 9.1 2.1 2.1 5.8 169 5 3 2 25.458 50.917 1.79195 4.7 1.1 1.1 5.8 170 -4 -6 3 25.727 51.454 1.77449 8.3 2.0 1.9 5.8 171 7 1 0 25.79 51.579 1.77048 8.4 2.0 1.9 5.8 172 -4 -3 5 26.008 52.016 1.75664 4.3 1.0 1.0 5.8 173 -6 -2 4 26.164 52.329 1.74687 5.1 1.2 1.2 5.8 174 -1 -7 3 26.231 52.463 1.74272 11.0 2.6 2.5 5.8 175 -4 6 0 26.519 53.038 1.72519 17.3 4.1 3.9 5.8 176 5 -5 1 26.613 53.227 1.7195 10.2 2.4 2.3 5.8 177 -7 -3 2 26.709 53.419 1.71377 12.7 3.0 2.9 5.8 178 -6 4 0 26.742 53.484 1.71185 31.1 7.3 7.0 5.8 179 2 -2 5 26.798 53.596 1.70853 12.4 2.9 2.8 5.8 180 -3 5 3 26.832 53.663 1.70653 12.2 2.9 2.8 5.8 181 1 7 1 26.908 53.815 1.70208 14.0 3.3 3.2 5.8 182 -1 -5 5 26.979 53.957 1.69793 9.7 2.3 2.2 5.8 183 5 -3 3 27.049 54.098 1.69384 7.4 1.7 1.7 5.8 184 2 0 5 27.112 54.224 1.6902 6.2 1.4 1.4 5.8 185 -5 -1 5 27.21 54.419 1.68461 11.8 2.8 2.7 5.8 186 -5 -5 4 27.282 54.563 1.6805 5.6 1.3 1.3 5.8 187 1 -7 3 27.355 54.709 1.67636 8.7 2.0 2.0 5.8 188 7 1 1 27.445 54.891 1.67124 7.8 1.8 1.8 5.8 189 -7 -3 3 27.704 55.408 1.65686 7.4 1.7 1.7 5.8 190 -7 1 3 27.837 55.674 1.64956 7.7 1.8 1.7 5.8 191 -2 -2 6 28.529 57.057 1.61282 6.7 1.6 1.5 5.8 192 -2 -8 1 28.843 57.686 1.59672 9.0 2.1 2.0 5.8 193 -4 6 2 28.98 57.959 1.58985 9.1 2.1 2.1 5.8 194 -1 -3 6 29.022 58.044 1.58773 9.0 2.1 2.0 5.8 195 -2 6 3 29.088 58.177 1.58442 15.7 3.7 3.5 5.8 196 0 -2 6 29.217 58.433 1.57808 13.3 3.1 3.0 5.8 197 2 2 5 29.433 58.865 1.56752 4.6 1.1 1.0 5.8 198 6 -2 3 29.462 58.924 1.5661 14.0 3.3 3.1 5.8 199 6 1 3 29.631 59.262 1.55797 8.4 2.0 1.9 5.8 200 -5 -7 2 29.699 59.397 1.55474 7.4 1.7 1.7 5.8 201 2 8 0 29.735 59.471 1.55299 12.5 2.9 2.8 5.8 202 0 -8 3 29.895 59.79 1.54547 9.6 2.3 2.2 5.8 203 2 -8 1 29.934 59.867 1.54365 7.8 1.8 1.8 5.8 204 -5 -5 5 30.118 60.236 1.53509 6.6 1.6 1.5 5.8 205 1 -1 6 30.37 60.741 1.52354 4.9 1.1 1.1 5.8 206 -8 0 3 30.515 61.03 1.517 13.2 3.1 3.0 5.8 207 6 4 2 30.548 61.097 1.51551 10.2 2.4 2.3 5.8 208 6 6 0 30.696 61.392 1.50892 5.4 1.3 1.2 5.8 209 5 7 0 31.078 62.156 1.49219 5.5 1.3 1.2 5.8 210 -2 4 5 31.174 62.348 1.48807 5.9 1.4 1.3 5.8 211 4 -2 5 31.341 62.681 1.48095 6.7 1.6 1.5 5.8 212 -1 -7 5 31.514 63.027 1.47365 12.4 2.9 2.8 5.9 213 -4 -8 3 31.759 63.518 1.46345 5.2 1.2 1.2 5.9 214 1 1 6 31.901 63.802 1.45762 6.5 1.5 1.5 5.9 215 8 -2 1 32.117 64.234 1.44886 6.1 1.4 1.4 5.9 216 -8 -2 4 32.216 64.433 1.44486 5.3 1.2 1.2 5.9 217 -1 -9 2 32.324 64.648 1.44057 8.7 2.1 1.9 5.9 218 4 4 4 32.627 65.254 1.42865 8.2 1.9 1.8 5.9 219 7 -1 3 32.677 65.354 1.42669 6.1 1.4 1.4 5.9 220 0 8 2 32.867 65.733 1.41939 4.6 1.1 1.0 5.9 221 8 4 0 32.918 65.836 1.41742 10.8 2.5 2.4 5.9 222 -9 -1 2 33.086 66.172 1.41103 16.3 3.8 3.6 5.9 223 -6 -2 6 33.185 66.369 1.40732 4.5 1.1 1.0 5.9 224 -7 3 4 33.397 66.795 1.39939 9.3 2.2 2.1 5.9 225 5 -5 4 33.476 66.952 1.39647 5.9 1.4 1.3 5.9 226 -9 1 1 33.604 67.207 1.39179 6.6 1.5 1.5 5.9 227 -6 -6 5 33.905 67.811 1.38086 11.4 2.7 2.5 5.9 228 7 -3 3 33.977 67.955 1.3783 4.3 1.0 1.0 5.9 229 2 8 2 34.073 68.146 1.37488 4.5 1.0 1.0 5.9 230 -1 -1 7 34.209 68.418 1.37008 4.5 1.1 1.0 5.9 231 -2 0 7 34.694 69.387 1.35329 10.0 2.4 2.2 5.9 232 -4 -2 7 34.807 69.614 1.34944 6.2 1.4 1.4 5.9 Reference: Chichagov A.V. et al. Information-Calculating System on Crystal Structure Data of Minerals (MINCRYST) - Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian) |