Institute of Experimental Mineralogy Russian Academy of Sciences ------------------------------------------------- 142432, Chernogolovka, Moscow district A.V. Chichagov +7(496)52-22320 *** *** W W W - X R A Y P O L *** *********************** MOYDITE_Y 1 (Y,TR)[B(OH)(4)][CO(3)] Orthorhombic P bca Z = 8 R =0.051 19 .4 .1990 Ref.Str.: J.D. Grice, T.S. Ercit (1986) * Canad. Mineral., 24, 665-773, 675-678 Reserv: Some O - O dist. are short (2.16, 2.2) Initial data from BDM-file Lattice parameters (cub. angs.,degr.): a = 9.089 alpha = 90.0 b = 12.244 beta = 90.0 c = 8.926 gamma = 90.0 Unit cell volume (cub. angs.) = 993.34 Molar volume ( cub.cm/mol.) = 74.79 Co-ordinates, thermal parameters, occupation for atomic positions: NoP x/a y/b z/c B(j) atom / occupation 1 0.0146 0.4991 0.2272 0.0 Y = 1.00 2 0.0032 0.249 0.2415 0.0 B = 1.00 3 0.2622 0.5454 0.0268 0.0 C = 1.00 4 0.7208 0.4688 0.8308 0.0 O = 1.00 5 0.8733 0.455 0.0164 0.0 O = 1.00 6 0.368 0.5565 0.9383 0.0 O = 1.00 7 0.1019 0.3172 0.1534 0.0 O = 1.00 8 0.9056 0.3256 0.3258 0.0 O = 1.00 9 0.0879 0.1796 0.3505 0.0 O = 1.00 10 0.9156 0.17 0.1538 0.0 O = 1.00 Co-ordinates for all atomic positions : No NoP x/a y/b z/c 1 1 0.0146 0.4991 0.2272 2 2 0.0032 0.249 0.2415 3 3 0.2622 0.5454 0.0268 4 4 0.7208 0.4688 0.8308 5 5 0.8733 0.455 0.0164 6 6 0.368 0.5565 0.9383 7 7 0.1019 0.3172 0.1534 8 8 0.9056 0.3256 0.3258 9 9 0.0879 0.1796 0.3505 10 10 0.9156 0.17 0.1538 11 1 0.4854 0.5009 0.7272 12 2 0.4968 0.751 0.7415 13 3 0.2378 0.4546 0.5268 14 4 0.7792 0.5312 0.3308 15 5 0.6267 0.545 0.5164 16 6 0.132 0.4435 0.4383 17 7 0.3981 0.6828 0.6534 18 8 0.5944 0.6744 0.8258 19 9 0.4121 0.8204 0.8505 20 10 0.5844 0.83 0.6538 21 1 0.4854 0.9991 0.2272 22 2 0.4968 0.749 0.2415 23 3 0.2378 0.0454 0.0268 24 4 0.7792 0.9688 0.8308 25 5 0.6267 0.955 0.0164 26 6 0.132 0.0565 0.9383 27 7 0.3981 0.8172 0.1534 28 8 0.5944 0.8256 0.3258 29 9 0.4121 0.6796 0.3505 30 10 0.5844 0.67 0.1538 31 1 0.0146 0.0009 0.7272 32 2 0.0032 0.251 0.7415 33 3 0.2622 0.9546 0.5268 34 4 0.7208 0.0312 0.3308 35 5 0.8733 0.045 0.5164 36 6 0.368 0.9435 0.4383 37 7 0.1019 0.1828 0.6534 38 8 0.9056 0.1744 0.8258 39 9 0.0879 0.3204 0.8505 40 10 0.9156 0.33 0.6538 41 1 0.5146 0.4991 0.2728 42 2 0.5032 0.249 0.2585 43 3 0.7622 0.5454 0.4732 44 4 0.2208 0.4688 0.6692 45 5 0.3733 0.455 0.4836 46 6 0.868 0.5565 0.5617 47 7 0.6019 0.3172 0.3466 48 8 0.4056 0.3256 0.1742 49 9 0.5879 0.1796 0.1495 50 10 0.4156 0.17 0.3462 51 1 0.9854 0.5009 0.7728 52 2 0.9968 0.751 0.7585 53 3 0.7378 0.4546 0.9732 54 4 0.2792 0.5312 0.1692 55 5 0.1267 0.545 0.9836 56 6 0.632 0.4435 0.0617 57 7 0.8981 0.6828 0.8466 58 8 0.0944 0.6744 0.6742 59 9 0.9121 0.8204 0.6495 60 10 0.0844 0.83 0.8462 61 1 0.9854 0.9991 0.2728 62 2 0.9968 0.749 0.2585 63 3 0.7378 0.0454 0.4732 64 4 0.2792 0.9688 0.6692 65 5 0.1267 0.955 0.4836 66 6 0.632 0.0565 0.5617 67 7 0.8981 0.8172 0.3466 68 8 0.0944 0.8256 0.1742 69 9 0.9121 0.6796 0.1495 70 10 0.0844 0.67 0.3462 71 1 0.5146 0.0009 0.7728 72 2 0.5032 0.251 0.7585 73 3 0.7622 0.9546 0.9732 74 4 0.2208 0.0312 0.1692 75 5 0.3733 0.045 0.9836 76 6 0.868 0.9435 0.0617 77 7 0.6019 0.1828 0.8466 78 8 0.4056 0.1744 0.6742 79 9 0.5879 0.3204 0.6495 80 10 0.4156 0.33 0.8462 X-ray density (g/cm cub.) = 2.99 MU (1/cm) = 177.574 Mass attenuation coefficient (cm**2/g) = 59.371 Selected interatomic distances (cation-anion,anion-anion): NoP Atom Rad.sph. C.N. Distance NoP N. (angs.) (angs.) 1 Y 2.796 9 2.3412 5 2.4544 7 2.5038 8 2.3637 4 2.2699 6 2.4912 4 2.4661 5 2.4966 9 2.4309 10 2 B 1.872 4 1.4562 7 1.4942 8 1.5038 9 1.4773 10 3 C 1.872 3 1.2519 6 1.2922 4 1.2905 5 4 O 3.264 9 2.1666 5 3.0786 5 2.7675 8 2.9187 10 2.9517 6 2.235 6 3.0793 7 2.7165 9 3.2561 10 5 O 3.264 9 2.1666 4 2.9426 7 3.1974 8 3.0786 4 2.9518 9 2.5699 5 2.2346 6 3.1824 7 3.0163 9 6 O 3.264 8 2.9888 7 2.7068 8 3.0822 10 2.9517 4 2.235 4 2.2346 5 2.9808 6 2.9247 10 7 O 3.264 9 2.9426 5 2.3584 8 2.4392 9 2.473 10 2.9888 6 2.707 9 2.7685 8 3.0793 4 3.1824 5 8 O 3.264 8 3.1974 5 2.3584 7 2.4474 9 2.4485 10 2.7675 4 2.7068 6 2.9296 10 2.7685 7 9 O 3.264 8 2.4392 7 2.4474 8 2.3556 10 2.9518 5 2.707 7 2.981 10 3.0163 5 2.7165 4 10 O 3.264 9 2.473 7 2.4485 8 2.3556 9 3.0822 6 2.9187 4 2.9296 8 2.981 9 3.2561 4 2.9247 6 X-ray diffraction powder data (II), X-Ray W.L. = 1.54056(angs.): No H K L Theta 2*Theta S LPG MF F I int. ( degree ) *100 1 0 2 0 7.228 14.456 0.082 123.38 2 296.0 2191.6 2 1 1 1 7.836 15.672 0.088 104.65 8 36.7 114.1 3 0 2 1 8.776 17.552 0.099 82.98 4 1.8 0.1 4 2 0 0 9.759 19.517 0.11 66.7 2 295.1 1177.7 5 0 0 2 9.939 19.877 0.112 64.22 2 281.5 1031.2 6 1 2 1 10.051 20.103 0.113 62.74 8 24.4 30.4 7 2 1 0 10.416 20.832 0.117 58.28 4 16.1 6.1 8 1 0 2 11.086 22.171 0.125 51.2 4 31.5 20.5 9 2 1 1 11.557 23.113 0.13 46.95 8 43.6 72.4 10 1 1 2 11.672 23.344 0.131 45.98 8 1.8 0.1 11 2 2 0 12.186 24.373 0.137 42.01 4 99.9 170.0 12 0 2 2 12.333 24.665 0.139 40.97 4 99.0 162.8 13 1 3 1 12.954 25.907 0.146 36.94 8 36.8 40.6 14 2 2 1 13.182 26.365 0.148 35.6 8 11.7 4.0 15 1 2 2 13.284 26.569 0.149 35.03 8 26.3 19.6 16 2 0 2 13.999 27.998 0.157 31.34 4 311.2 1230.4 17 2 1 2 14.475 28.949 0.162 29.19 8 7.0 1.1 18 0 4 0 14.575 29.15 0.163 28.76 2 305.1 542.7 19 2 3 0 14.695 29.39 0.165 28.26 4 3.9 0.2 20 0 4 1 15.428 30.856 0.173 25.46 4 11.9 1.5 21 2 3 1 15.542 31.084 0.174 25.06 8 40.0 32.6 22 1 3 2 15.63 31.26 0.175 24.76 8 10.6 2.3 23 2 2 2 15.823 31.646 0.177 24.11 8 200.1 782.8 24 3 1 1 16.008 32.015 0.179 23.52 8 50.1 47.8 25 1 4 1 16.213 32.425 0.181 22.88 8 161.7 484.7 26 1 1 3 16.235 32.47 0.181 22.81 8 72.5 97.1 27 0 2 3 16.729 33.458 0.187 21.37 4 8.8 0.7 28 3 2 1 17.248 34.496 0.192 20.0 8 67.7 74.3 29 1 2 3 17.461 34.923 0.195 19.47 8 99.7 156.9 30 2 4 0 17.662 35.324 0.197 18.99 4 197.2 299.3 31 0 4 2 17.767 35.534 0.198 18.75 4 216.4 355.9 32 2 3 2 17.868 35.735 0.199 18.52 8 3.5 0.2 33 3 0 2 17.896 35.792 0.199 18.45 4 58.5 25.6 34 3 1 2 18.28 36.561 0.204 17.61 8 1.1 0.0 35 2 4 1 18.387 36.774 0.205 17.39 8 41.9 24.7 36 2 1 3 18.407 36.815 0.205 17.34 8 9.7 1.3 37 1 4 2 18.463 36.926 0.206 17.23 8 34.1 16.3 38 3 3 1 19.159 38.318 0.213 15.88 8 46.2 27.5 39 1 3 3 19.354 38.707 0.215 15.53 8 84.9 90.7 40 3 2 2 19.394 38.787 0.216 15.46 8 35.0 15.3 41 2 2 3 19.514 39.029 0.217 15.25 8 7.0 0.6 42 1 5 1 19.695 39.389 0.219 14.94 8 51.6 32.2 43 4 0 0 19.816 39.631 0.22 14.74 2 97.9 28.6 44 4 1 0 20.169 40.337 0.224 14.17 4 13.6 1.1 45 0 0 4 20.193 40.386 0.224 14.13 2 145.4 60.6 46 2 4 2 20.43 40.859 0.227 13.77 8 227.9 580.0 47 4 1 1 20.819 41.638 0.231 13.2 8 103.3 114.2 48 1 0 4 20.82 41.64 0.231 13.2 4 86.0 39.6 49 2 5 0 20.935 41.871 0.232 13.04 4 31.8 5.4 50 3 3 2 21.138 42.277 0.234 12.76 8 5.0 0.3 51 1 1 4 21.159 42.318 0.234 12.73 8 5.5 0.3 52 0 4 3 21.164 42.328 0.234 12.72 4 50.4 13.1 53 4 2 0 21.198 42.396 0.235 12.68 4 245.8 310.5 54 2 3 3 21.251 42.502 0.235 12.61 8 40.8 17.0 55 0 2 4 21.555 43.111 0.238 12.21 4 270.6 362.4 56 2 5 1 21.567 43.134 0.239 12.2 8 28.4 8.0 57 3 4 1 21.591 43.183 0.239 12.16 8 96.1 91.0 58 3 1 3 21.609 43.218 0.239 12.14 8 119.9 141.5 59 1 5 2 21.633 43.267 0.239 12.11 8 6.0 0.4 60 1 4 3 21.768 43.536 0.241 11.94 8 53.1 27.3 61 4 2 1 21.823 43.647 0.241 11.88 8 33.6 10.9 62 1 2 4 22.151 44.302 0.245 11.48 8 54.6 27.8 63 0 6 0 22.177 44.353 0.245 11.45 2 338.5 266.0 64 4 0 2 22.359 44.717 0.247 11.25 4 238.4 259.1 65 3 2 3 22.585 45.17 0.249 10.99 8 139.3 173.0 66 2 0 4 22.616 45.232 0.25 10.96 4 159.2 112.6 67 4 1 2 22.679 45.358 0.25 10.89 8 6.5 0.4 68 0 6 1 22.781 45.561 0.251 10.78 4 2.5 0.0 69 4 3 0 22.83 45.659 0.252 10.73 4 32.4 4.6 70 2 1 4 22.934 45.867 0.253 10.62 8 27.4 6.5 71 1 6 1 23.351 46.703 0.257 10.19 8 70.9 41.5 72 2 5 2 23.379 46.758 0.258 10.17 8 26.2 5.7 73 3 4 2 23.402 46.804 0.258 10.14 8 1.5 0.0 74 4 3 1 23.42 46.84 0.258 10.13 8 101.4 84.4 75 2 4 3 23.506 47.012 0.259 10.04 8 9.2 0.7 76 4 2 2 23.62 47.24 0.26 9.93 8 253.1 515.8 77 1 3 4 23.731 47.461 0.261 9.83 8 16.6 2.2 78 2 2 4 23.867 47.734 0.263 9.7 8 188.4 279.3 79 3 3 3 24.142 48.285 0.265 9.45 8 119.2 108.9 80 3 5 1 24.429 48.857 0.268 9.2 8 21.4 3.4 81 2 6 0 24.442 48.884 0.269 9.19 4 244.0 221.7 82 0 6 2 24.523 49.045 0.269 9.12 4 274.8 279.2 83 1 5 3 24.589 49.179 0.27 9.07 8 90.5 60.2 84 4 4 0 24.973 49.945 0.274 8.75 4 250.9 223.3 85 2 6 1 25.004 50.007 0.274 8.73 8 36.5 9.4 86 1 6 2 25.063 50.126 0.275 8.68 8 26.0 4.8 87 4 3 2 25.128 50.257 0.276 8.63 8 1.0 0.0 88 0 4 4 25.288 50.577 0.277 8.51 4 232.1 185.7 89 2 3 4 25.364 50.728 0.278 8.45 8 14.2 1.4 90 3 0 4 25.386 50.772 0.278 8.43 4 60.0 12.3 91 4 4 1 25.526 51.051 0.28 8.33 8 15.6 1.7 92 4 1 3 25.541 51.082 0.28 8.31 8 70.1 33.1 93 3 1 4 25.677 51.355 0.281 8.21 8 5.0 0.2 94 1 4 4 25.817 51.634 0.283 8.11 8 34.7 7.9 95 5 1 1 25.912 51.824 0.284 8.05 8 0.0 0.0 96 3 5 2 26.087 52.175 0.285 7.92 8 3.1 0.1 97 2 5 3 26.183 52.367 0.286 7.86 8 36.7 8.6 98 3 4 3 26.204 52.409 0.287 7.84 8 91.6 53.3 99 1 1 5 26.372 52.745 0.288 7.73 8 152.8 146.4 100 4 2 3 26.405 52.81 0.289 7.71 8 26.2 4.3 101 3 2 4 26.538 53.076 0.29 7.62 8 33.5 6.9 102 2 6 2 26.636 53.273 0.291 7.56 8 193.1 228.5 103 0 2 5 26.709 53.417 0.292 7.51 4 43.2 5.7 104 5 2 1 26.768 53.535 0.292 7.47 8 31.7 6.1 105 4 4 2 27.136 54.272 0.296 7.24 8 232.9 318.6 106 1 7 1 27.173 54.347 0.296 7.22 8 25.3 3.8 107 1 2 5 27.218 54.435 0.297 7.19 8 6.1 0.2 108 5 0 2 27.229 54.457 0.297 7.19 4 51.2 7.6 109 0 6 3 27.24 54.48 0.297 7.18 4 19.4 1.1 110 2 4 4 27.359 54.719 0.298 7.11 8 201.5 234.1 111 5 1 2 27.506 55.013 0.3 7.02 8 8.0 0.4 112 4 5 0 27.545 55.091 0.3 7.0 4 11.1 0.4 113 3 6 1 27.595 55.189 0.301 6.97 8 19.7 2.2 114 1 6 3 27.742 55.484 0.302 6.89 8 43.9 10.7 115 4 3 3 27.803 55.606 0.303 6.85 8 75.2 31.4 116 2 1 5 27.893 55.787 0.304 6.8 8 45.1 11.2 117 3 3 4 27.932 55.863 0.304 6.78 8 22.5 2.8 118 4 5 1 28.062 56.125 0.305 6.71 8 80.0 34.8 119 5 3 1 28.153 56.307 0.306 6.66 8 9.0 0.4 120 2 7 0 28.156 56.311 0.306 6.66 4 8.6 0.2 121 5 2 2 28.329 56.657 0.308 6.57 8 78.2 32.5 122 1 5 4 28.336 56.671 0.308 6.57 8 26.4 3.7 123 1 3 5 28.589 57.177 0.311 6.43 8 167.1 145.8 124 2 7 1 28.665 57.331 0.311 6.4 8 27.2 3.8 125 3 5 3 28.7 57.399 0.312 6.38 8 90.3 42.2 126 2 2 5 28.708 57.417 0.312 6.37 8 8.3 0.4 127 1 7 2 28.719 57.439 0.312 6.37 8 1.4 0.0 128 4 0 4 28.934 57.869 0.314 6.26 4 205.4 107.1 129 3 6 2 29.126 58.252 0.316 6.17 8 6.5 0.2 130 4 1 4 29.201 58.403 0.317 6.13 8 4.1 0.1 131 2 6 3 29.215 58.43 0.317 6.13 8 2.0 0.0 132 4 5 2 29.578 59.156 0.32 5.96 8 11.0 0.6 133 5 3 2 29.666 59.332 0.321 5.92 8 19.6 1.9 134 4 4 3 29.686 59.371 0.321 5.91 8 53.5 13.7 135 2 5 4 29.79 59.579 0.322 5.87 8 25.8 3.2 136 3 4 4 29.809 59.618 0.323 5.86 8 25.2 3.0 137 0 4 5 29.967 59.934 0.324 5.79 4 44.6 4.7 138 4 2 4 29.993 59.987 0.324 5.78 8 88.9 37.0 139 5 4 1 30.022 60.044 0.325 5.76 8 7.2 0.2 140 2 3 5 30.035 60.069 0.325 5.76 8 45.1 9.5 141 5 1 3 30.036 60.071 0.325 5.76 8 72.6 24.6 142 2 7 2 30.162 60.323 0.326 5.7 8 11.6 0.6 143 0 8 0 30.218 60.435 0.327 5.68 2 54.3 3.4 144 3 1 5 30.315 60.63 0.328 5.64 8 113.4 58.8 145 1 4 5 30.44 60.88 0.329 5.59 8 46.2 9.7 146 4 6 0 30.487 60.974 0.329 5.57 4 124.7 35.1 147 6 0 0 30.563 61.127 0.33 5.54 2 54.7 3.4 148 0 8 1 30.706 61.412 0.331 5.48 4 19.4 0.8 149 0 6 4 30.764 61.528 0.332 5.46 4 70.4 11.0 150 5 2 3 30.815 61.629 0.333 5.44 8 6.2 0.2 151 6 1 0 30.822 61.643 0.333 5.44 4 2.2 0.0 152 4 6 1 30.973 61.945 0.334 5.38 8 36.3 5.7 153 3 7 1 31.049 62.098 0.335 5.35 8 20.2 1.8 154 3 2 5 31.09 62.179 0.335 5.33 8 28.1 3.4 155 1 8 1 31.172 62.345 0.336 5.3 8 32.6 4.6 156 0 0 6 31.183 62.367 0.336 5.3 2 3.4 0.0 157 1 7 3 31.186 62.372 0.336 5.3 8 63.5 17.3 158 1 6 4 31.23 62.46 0.337 5.28 8 15.4 1.0 159 4 3 4 31.286 62.573 0.337 5.26 8 8.4 0.3 160 6 1 1 31.304 62.609 0.337 5.25 8 71.3 21.7 161 5 4 2 31.479 62.957 0.339 5.19 8 48.8 10.0 162 3 6 3 31.573 63.146 0.34 5.16 8 73.2 22.4 163 6 2 0 31.589 63.179 0.34 5.15 4 199.4 83.0 164 1 0 6 31.646 63.292 0.341 5.13 4 16.2 0.5 165 2 4 5 31.835 63.67 0.342 5.06 8 12.6 0.7 166 1 1 6 31.899 63.798 0.343 5.04 8 8.7 0.3 167 4 5 3 32.004 64.009 0.344 5.0 8 60.2 14.7 168 6 2 1 32.065 64.131 0.345 4.98 8 14.6 0.9 169 2 8 0 32.077 64.154 0.345 4.98 4 183.8 68.2 170 5 3 3 32.088 64.177 0.345 4.98 8 66.0 17.6 171 3 5 4 32.122 64.245 0.345 4.96 8 18.1 1.3 172 0 8 2 32.145 64.289 0.345 4.96 4 213.2 91.3 173 0 2 6 32.198 64.396 0.346 4.94 4 135.6 36.8 174 5 5 1 32.326 64.653 0.347 4.9 8 2.9 0.0 175 3 3 5 32.357 64.715 0.347 4.89 8 113.2 50.8 176 4 6 2 32.405 64.809 0.348 4.87 8 124.7 61.4 177 6 0 2 32.479 64.957 0.349 4.85 4 133.5 35.0 178 3 7 2 32.479 64.958 0.349 4.85 8 9.7 0.4 179 2 8 1 32.549 65.099 0.349 4.82 8 28.9 3.3 180 2 7 3 32.563 65.125 0.349 4.82 8 46.8 8.6 181 1 8 2 32.6 65.199 0.35 4.81 8 13.9 0.8 182 2 6 4 32.606 65.211 0.35 4.81 8 125.3 61.1 183 1 2 6 32.653 65.305 0.35 4.79 8 0.4 0.0 184 1 5 5 32.728 65.456 0.351 4.77 8 115.3 51.4 185 6 1 2 32.728 65.457 0.351 4.77 8 1.0 0.0 186 6 3 0 32.846 65.693 0.352 4.73 4 21.9 0.9 187 2 0 6 33.012 66.024 0.354 4.68 4 132.6 33.3 188 4 4 4 33.048 66.096 0.354 4.67 8 142.0 76.3 189 5 0 4 33.13 66.261 0.355 4.65 4 8.8 0.1 190 2 1 6 33.26 66.519 0.356 4.61 8 12.9 0.6 191 6 3 1 33.313 66.626 0.356 4.59 8 79.3 23.4 192 5 1 4 33.378 66.755 0.357 4.57 8 8.8 0.3 193 6 2 2 33.472 66.944 0.358 4.55 8 167.9 103.8 194 4 1 5 33.526 67.052 0.359 4.53 8 35.5 4.6 195 5 5 2 33.727 67.454 0.36 4.47 8 27.9 2.8 196 4 7 0 33.762 67.524 0.361 4.46 4 26.7 1.3 197 5 4 3 33.827 67.655 0.361 4.45 8 48.6 8.5 198 1 3 6 33.889 67.777 0.362 4.43 8 3.0 0.0 199 2 8 2 33.945 67.891 0.362 4.41 8 168.1 101.1 200 2 2 6 33.997 67.995 0.363 4.4 8 162.0 93.6 201 2 5 5 34.071 68.142 0.364 4.38 8 19.3 1.3 202 3 4 5 34.089 68.178 0.364 4.37 8 11.3 0.4 203 5 2 4 34.114 68.228 0.364 4.37 8 33.0 3.9 204 4 7 1 34.222 68.444 0.365 4.34 8 74.3 19.4 205 4 2 5 34.261 68.522 0.365 4.33 8 18.2 1.2 206 1 7 4 34.466 68.932 0.367 4.28 8 3.1 0.0 207 0 8 3 34.47 68.939 0.367 4.28 4 8.8 0.1 208 6 4 0 34.566 69.132 0.368 4.25 4 189.4 61.9 209 6 3 2 34.693 69.387 0.369 4.22 8 0.7 0.0 210 4 6 3 34.721 69.442 0.37 4.21 8 39.8 5.4 211 3 8 1 34.78 69.56 0.37 4.2 8 33.5 3.8 212 3 7 3 34.793 69.585 0.37 4.19 8 82.2 23.0 213 3 6 4 34.834 69.668 0.371 4.18 8 14.9 0.8 214 1 8 3 34.909 69.819 0.371 4.17 8 29.2 2.9 215 0 6 5 34.98 69.959 0.372 4.15 4 41.2 2.9 216 6 4 1 35.021 70.042 0.373 4.14 8 12.9 0.6 217 5 6 1 35.03 70.06 0.373 4.14 8 18.8 1.2 218 6 1 3 35.034 70.068 0.373 4.14 8 108.2 39.2 219 0 4 6 35.148 70.296 0.374 4.11 4 132.4 29.2 220 2 3 6 35.21 70.42 0.374 4.1 8 31.9 3.4 221 3 0 6 35.228 70.456 0.374 4.09 4 24.5 1.0 222 4 5 4 35.245 70.49 0.375 4.09 8 4.3 0.1 223 5 3 4 35.325 70.65 0.375 4.07 8 1.8 0.0 224 1 9 1 35.378 70.757 0.376 4.06 8 33.9 3.8 225 1 6 5 35.416 70.833 0.376 4.05 8 30.3 3.0 226 3 1 6 35.468 70.936 0.377 4.04 8 10.4 0.4 227 4 3 5 35.47 70.939 0.377 4.04 8 41.7 5.7 228 1 4 6 35.584 71.168 0.378 4.01 8 9.2 0.3 229 4 7 2 35.586 71.172 0.378 4.01 8 8.7 0.2 230 6 2 3 35.754 71.509 0.379 3.97 8 17.1 0.9 231 2 7 4 35.778 71.556 0.38 3.97 8 37.0 4.4 232 5 5 3 36.002 72.004 0.382 3.92 8 53.4 9.1 233 3 8 2 36.135 72.269 0.383 3.89 8 30.1 2.9 234 3 2 6 36.185 72.37 0.383 3.88 8 5.0 0.1 235 2 8 3 36.214 72.428 0.383 3.87 8 8.3 0.2 236 2 9 0 36.23 72.459 0.384 3.87 4 23.6 0.9 237 3 5 5 36.257 72.514 0.384 3.87 8 122.5 47.0 238 6 4 2 36.372 72.744 0.385 3.84 8 175.6 96.1 239 5 6 2 36.381 72.762 0.385 3.84 8 2.1 0.0 240 2 9 1 36.676 73.352 0.388 3.78 8 30.2 2.8 241 2 6 5 36.714 73.427 0.388 3.77 8 3.3 0.0 242 6 5 0 36.721 73.442 0.388 3.77 4 34.0 1.8 243 1 9 2 36.724 73.447 0.388 3.77 8 12.9 0.5 244 2 4 6 36.879 73.757 0.39 3.74 8 161.3 79.0 245 6 3 3 36.942 73.884 0.39 3.73 8 90.5 24.8 246 5 4 4 36.991 73.983 0.391 3.72 8 47.1 6.7 247 7 1 1 37.069 74.138 0.391 3.71 8 41.5 5.2 248 4 4 5 37.133 74.266 0.392 3.7 8 36.8 4.1 249 6 5 1 37.165 74.33 0.392 3.69 8 83.4 20.8 250 4 8 0 37.359 74.718 0.394 3.65 4 270.1 108.1 251 3 3 6 37.367 74.735 0.394 3.65 8 1.5 0.0 252 5 1 5 37.447 74.893 0.395 3.64 8 82.6 20.1 253 0 8 4 37.61 75.22 0.396 3.61 4 198.5 57.7 254 1 5 6 37.715 75.43 0.397 3.59 8 17.0 0.8 255 7 2 1 37.774 75.548 0.398 3.58 8 7.7 0.2 256 4 8 1 37.8 75.601 0.398 3.58 8 15.1 0.7 257 4 7 3 37.813 75.626 0.398 3.58 8 55.6 8.9 258 1 1 7 37.823 75.646 0.398 3.57 8 123.5 44.2 259 4 6 4 37.853 75.706 0.398 3.57 8 166.3 80.0 260 6 0 4 37.922 75.844 0.399 3.56 4 198.6 56.8 261 3 7 4 37.922 75.845 0.399 3.56 8 13.4 0.5 262 2 9 2 38.003 76.007 0.4 3.54 8 16.0 0.7 263 1 8 4 38.035 76.07 0.4 3.54 8 13.6 0.5 264 0 2 7 38.1 76.2 0.401 3.53 4 10.6 0.2 265 5 7 1 38.112 76.224 0.401 3.53 8 30.3 2.6 266 5 2 5 38.149 76.298 0.401 3.52 8 0.9 0.0 267 6 1 4 38.155 76.311 0.401 3.52 8 18.1 0.9 268 7 0 2 38.158 76.317 0.401 3.52 4 20.3 0.6 269 4 0 6 38.234 76.469 0.402 3.51 4 158.2 35.6 270 3 8 3 38.349 76.698 0.403 3.49 8 72.0 14.7 271 7 1 2 38.391 76.783 0.403 3.48 8 3.6 0.0 272 4 1 6 38.467 76.935 0.404 3.47 8 9.6 0.3 273 1 7 5 38.486 76.972 0.404 3.47 8 103.8 30.3 274 6 5 2 38.487 76.973 0.404 3.47 8 0.7 0.0 275 1 2 7 38.523 77.046 0.404 3.46 8 26.9 2.0 276 6 4 3 38.582 77.163 0.405 3.45 8 2.6 0.0 277 5 6 3 38.59 77.181 0.405 3.45 8 17.9 0.9 278 3 9 1 38.802 77.604 0.407 3.42 8 18.8 1.0 279 3 6 5 38.839 77.678 0.407 3.41 8 18.2 0.9 280 6 2 4 38.854 77.707 0.407 3.41 8 77.2 16.5 281 1 9 3 38.926 77.852 0.408 3.4 8 92.9 23.8 282 7 3 1 38.939 77.878 0.408 3.4 8 33.4 3.1 283 2 5 6 38.984 77.968 0.408 3.39 8 18.3 0.9 284 0 10 0 38.984 77.969 0.408 3.39 2 107.2 7.9 285 3 4 6 39.001 78.002 0.409 3.39 8 16.5 0.7 286 7 2 2 39.088 78.177 0.409 3.38 8 37.7 3.9 287 2 1 7 39.091 78.181 0.409 3.38 8 37.0 3.7 288 5 5 4 39.094 78.189 0.409 3.38 8 5.3 0.1 289 4 8 2 39.115 78.229 0.41 3.37 8 173.4 82.2 290 4 2 6 39.164 78.328 0.41 3.37 8 43.7 5.2 291 4 5 5 39.234 78.467 0.411 3.36 8 43.2 5.1 292 6 6 0 39.293 78.585 0.411 3.35 4 53.8 3.9 293 2 8 4 39.3 78.601 0.411 3.35 8 189.8 97.8 294 5 3 5 39.311 78.621 0.411 3.35 8 66.4 12.0 295 0 10 1 39.42 78.84 0.412 3.33 4 14.8 0.3 296 5 7 2 39.423 78.846 0.412 3.33 8 19.9 1.1 297 1 3 7 39.682 79.363 0.414 3.3 8 149.4 59.6 298 6 6 1 39.727 79.454 0.415 3.29 8 14.8 0.6 299 2 7 5 39.747 79.495 0.415 3.29 8 12.5 0.4 300 2 2 7 39.784 79.568 0.415 3.28 8 16.0 0.7 301 1 10 1 39.839 79.678 0.416 3.28 8 39.7 4.2 302 0 6 6 39.848 79.697 0.416 3.27 4 14.1 0.3 303 6 3 4 40.009 80.019 0.417 3.25 8 10.6 0.3 304 3 9 2 40.107 80.213 0.418 3.24 8 6.5 0.1 305 2 9 3 40.184 80.367 0.419 3.23 8 49.8 6.5 306 7 3 2 40.242 80.484 0.419 3.22 8 25.9 1.8 307 1 6 6 40.266 80.532 0.42 3.22 8 29.0 2.2 308 4 3 6 40.317 80.634 0.42 3.22 8 10.6 0.3 309 7 4 1 40.554 81.107 0.422 3.19 8 73.9 14.1 310 7 1 3 40.566 81.131 0.422 3.19 8 71.2 13.1 311 2 10 0 40.658 81.316 0.423 3.18 4 187.0 45.0 312 6 5 3 40.659 81.319 0.423 3.18 8 81.7 17.2 313 0 10 2 40.719 81.439 0.423 3.17 4 203.9 53.4 314 4 7 4 40.86 81.721 0.425 3.15 8 0.3 0.0 315 0 4 7 40.874 81.747 0.425 3.15 4 22.2 0.6 316 5 4 5 40.922 81.843 0.425 3.15 8 9.8 0.2 317 2 3 7 40.933 81.866 0.425 3.15 8 22.6 1.3 318 6 6 2 41.024 82.048 0.426 3.14 8 98.5 24.7 319 3 5 6 41.073 82.146 0.426 3.13 8 5.0 0.1 320 2 10 1 41.089 82.178 0.427 3.13 8 31.3 2.5 321 1 10 2 41.135 82.27 0.427 3.12 8 12.2 0.4 322 3 1 7 41.179 82.357 0.427 3.12 8 166.7 70.3 323 7 2 3 41.253 82.506 0.428 3.11 8 65.9 11.0 324 4 8 3 41.279 82.558 0.428 3.11 8 19.0 0.9 325 1 4 7 41.289 82.578 0.428 3.11 8 42.4 4.5 326 4 9 0 41.294 82.588 0.428 3.11 4 24.0 0.7 327 3 8 4 41.386 82.772 0.429 3.1 8 5.6 0.1 328 2 6 6 41.514 83.027 0.43 3.08 8 78.1 15.2 329 0 8 5 41.524 83.047 0.43 3.08 4 42.2 2.2 330 5 8 1 41.571 83.143 0.431 3.08 8 9.1 0.2 331 5 7 3 41.584 83.167 0.431 3.08 8 73.8 13.6 332 6 4 4 41.614 83.228 0.431 3.07 8 122.6 37.5 333 5 6 4 41.623 83.245 0.431 3.07 8 50.1 6.2 334 4 9 1 41.724 83.448 0.432 3.06 8 61.8 9.5 335 4 6 5 41.76 83.52 0.432 3.06 8 16.3 0.7 336 3 7 5 41.828 83.656 0.433 3.05 8 121.9 36.8 337 7 4 2 41.845 83.69 0.433 3.05 8 26.2 1.7 338 3 2 7 41.864 83.728 0.433 3.05 8 58.1 8.3 339 4 4 6 41.919 83.839 0.434 3.05 8 95.5 22.5 340 1 8 5 41.938 83.876 0.434 3.04 8 21.8 1.2 341 1 9 4 41.953 83.905 0.434 3.04 8 9.5 0.2 342 5 0 6 41.995 83.99 0.434 3.04 4 106.6 14.0 343 6 1 5 42.055 84.111 0.435 3.03 8 73.2 13.2 344 5 1 6 42.223 84.446 0.436 3.02 8 18.9 0.9 345 3 9 3 42.26 84.519 0.437 3.01 8 65.1 10.4 346 6 7 0 42.274 84.548 0.437 3.01 4 26.5 0.9 347 2 10 2 42.378 84.755 0.438 3.0 8 139.9 47.7 348 7 3 3 42.394 84.788 0.438 3.0 8 54.7 7.3 349 2 4 7 42.531 85.062 0.439 2.99 8 18.9 0.9 350 7 5 1 42.609 85.219 0.439 2.99 8 32.4 2.5 351 8 0 0 42.687 85.373 0.44 2.98 2 190.9 22.0 352 6 7 1 42.702 85.405 0.44 2.98 8 95.0 21.8 353 6 2 5 42.739 85.477 0.441 2.97 8 3.7 0.0 354 5 8 2 42.858 85.715 0.442 2.97 8 16.3 0.6 355 0 10 3 42.867 85.733 0.442 2.96 4 5.0 0.0 356 5 2 6 42.906 85.812 0.442 2.96 8 79.7 15.2 357 8 1 0 42.914 85.828 0.442 2.96 4 2.5 0.0 358 5 5 5 42.975 85.949 0.442 2.96 8 103.9 25.9 359 3 3 7 43.003 86.005 0.443 2.95 8 143.6 49.4 360 4 9 2 43.009 86.019 0.443 2.95 8 3.8 0.0 361 3 10 1 43.158 86.315 0.444 2.94 8 31.1 2.3 362 6 6 3 43.169 86.338 0.444 2.94 8 9.0 0.2 363 2 8 5 43.177 86.354 0.444 2.94 8 4.0 0.0 364 2 9 4 43.192 86.384 0.444 2.94 8 5.8 0.1 365 1 7 6 43.235 86.469 0.445 2.94 8 6.3 0.1 366 1 10 3 43.279 86.558 0.445 2.93 8 57.3 7.8 367 1 5 7 43.339 86.679 0.445 2.93 8 130.2 40.2 368 8 1 1 43.342 86.683 0.446 2.93 8 137.5 44.9 369 7 0 4 43.342 86.685 0.446 2.93 4 27.6 0.9 370 7 1 4 43.57 87.139 0.447 2.91 8 10.2 0.2 371 3 6 6 43.579 87.159 0.447 2.91 8 61.2 8.8 372 8 2 0 43.596 87.191 0.448 2.91 4 162.9 31.3 373 0 0 8 43.659 87.319 0.448 2.91 2 61.4 2.2 374 6 5 4 43.662 87.325 0.448 2.91 8 16.0 0.6 375 6 3 5 43.874 87.749 0.45 2.89 8 70.7 11.7 376 7 5 2 43.892 87.784 0.45 2.89 8 24.1 1.4 377 4 5 6 43.966 87.932 0.451 2.89 8 3.2 0.0 378 7 4 3 43.985 87.969 0.451 2.89 8 39.8 3.7 379 6 7 2 43.985 87.969 0.451 2.89 8 4.6 0.0 380 8 2 1 44.023 88.045 0.451 2.88 8 21.9 1.1 381 5 3 6 44.041 88.083 0.451 2.88 8 1.8 0.0 382 4 1 7 44.07 88.141 0.451 2.88 8 19.5 0.9 383 1 0 8 44.071 88.142 0.451 2.88 4 3.4 0.0 384 7 2 4 44.25 88.501 0.453 2.87 8 53.9 6.7 385 4 8 4 44.276 88.552 0.453 2.87 8 119.4 33.1 386 1 1 8 44.298 88.596 0.453 2.87 8 3.8 0.0 387 8 0 2 44.396 88.792 0.454 2.86 4 86.5 8.7 388 3 10 2 44.439 88.878 0.454 2.86 8 42.8 4.3 389 2 7 6 44.47 88.94 0.455 2.86 8 17.7 0.7 390 2 10 3 44.515 89.029 0.455 2.85 8 1.0 0.0 391 0 2 8 44.567 89.134 0.456 2.85 4 46.9 2.5 392 2 5 7 44.575 89.15 0.456 2.85 8 29.6 2.0 393 5 7 4 44.578 89.157 0.456 2.85 8 16.1 0.6 394 3 4 7 44.591 89.183 0.456 2.85 8 47.3 5.2 395 8 1 2 44.623 89.245 0.456 2.85 8 6.4 0.1 396 1 11 1 44.629 89.257 0.456 2.85 8 27.1 1.7 397 4 7 5 44.715 89.43 0.457 2.84 8 41.4 4.0 398 8 3 0 44.73 89.46 0.457 2.84 4 6.6 0.0 399 4 2 7 44.751 89.502 0.457 2.84 8 37.1 3.2 400 1 2 8 44.978 89.957 0.459 2.83 8 2.9 0.0 401 5 8 3 44.993 89.986 0.459 2.83 8 3.9 0.0 X-ray diffraction powder data (I)...X-Ray wave length = 1.54056 (angs.): No H K L Theta 2*Theta d I int I int.n. I p.h.n. H(Si) ( degree ) (angstrem) *100 *100 1 0 2 0 7.228 14.456 6.122 2191.6 100.0 100.0 5.6 2 1 1 1 7.836 15.672 5.64992 114.1 5.2 5.2 5.6 3 2 0 0 9.759 19.517 4.5445 1177.7 53.7 53.6 5.6 4 0 0 2 9.939 19.877 4.463 1031.2 47.1 46.9 5.6 5 1 2 1 10.051 20.103 4.41347 30.4 1.4 1.4 5.6 6 2 1 1 11.557 23.113 3.84496 72.4 3.3 3.3 5.6 7 2 2 0 12.186 24.373 3.649 170.0 7.8 7.7 5.6 8 0 2 2 12.333 24.665 3.60641 162.8 7.4 7.4 5.6 9 1 3 1 12.954 25.907 3.43624 40.6 1.9 1.8 5.6 10 2 0 2 13.999 27.998 3.18424 1230.4 56.1 55.6 5.6 11 0 4 0 14.575 29.15 3.061 542.7 24.8 24.5 5.6 12 2 3 1 15.542 31.084 2.87473 32.6 1.5 1.5 5.6 13 2 2 2 15.823 31.646 2.82496 782.8 35.7 35.3 5.6 14 3 1 1 16.008 32.015 2.79326 47.8 2.2 2.2 5.6 15 1 4 1 16.213 32.425 2.75886 581.8 26.5 26.2 5.6 16 3 2 1 17.248 34.496 2.59781 74.3 3.4 3.3 5.7 17 1 2 3 17.461 34.923 2.56708 156.9 7.2 7.1 5.7 18 2 4 0 17.662 35.324 2.5388 299.3 13.7 13.4 5.7 19 0 4 2 17.767 35.534 2.52432 355.9 16.2 16.0 5.7 20 3 0 2 17.896 35.792 2.50666 25.6 1.2 1.1 5.7 21 2 4 1 18.387 36.774 2.44194 26.1 1.2 1.2 5.7 22 3 3 1 19.159 38.318 2.34706 27.5 1.3 1.2 5.7 23 1 3 3 19.354 38.707 2.32432 90.7 4.1 4.1 5.7 24 1 5 1 19.695 39.389 2.28565 32.2 1.5 1.4 5.7 25 4 0 0 19.816 39.631 2.27225 28.6 1.3 1.3 5.7 26 0 0 4 20.193 40.386 2.2315 61.6 2.8 2.8 5.7 27 2 4 2 20.43 40.859 2.20674 580.0 26.5 25.9 5.7 28 4 1 1 20.819 41.638 2.16725 153.8 7.0 6.9 5.7 29 4 2 0 21.198 42.396 2.13025 310.5 14.2 13.8 5.7 30 0 2 4 21.555 43.111 2.09656 370.3 16.9 16.5 5.7 31 3 1 3 21.609 43.218 2.09162 232.5 10.6 10.4 5.7 32 1 4 3 21.768 43.536 2.07706 27.3 1.2 1.2 5.7 33 0 6 0 22.177 44.353 2.04067 293.8 13.4 13.1 5.7 34 4 0 2 22.359 44.717 2.02491 259.1 11.8 11.5 5.7 35 3 2 3 22.585 45.17 2.00567 173.0 7.9 7.7 5.7 36 2 0 4 22.616 45.232 2.00305 112.6 5.1 5.0 5.7 37 1 6 1 23.351 46.703 1.94334 47.2 2.2 2.1 5.7 38 4 3 1 23.42 46.84 1.93795 84.4 3.8 3.7 5.7 39 4 2 2 23.62 47.24 1.92248 515.8 23.5 22.9 5.7 40 2 2 4 23.867 47.734 1.90374 279.3 12.7 12.4 5.7 41 3 3 3 24.142 48.285 1.88331 108.9 5.0 4.8 5.7 42 2 6 0 24.442 48.884 1.8616 225.1 10.3 10.0 5.7 43 0 6 2 24.523 49.045 1.85587 279.2 12.7 12.4 5.7 44 1 5 3 24.589 49.179 1.85113 60.2 2.7 2.7 5.7 45 4 4 0 24.973 49.945 1.8245 223.3 10.2 9.9 5.7 46 0 4 4 25.288 50.577 1.8032 185.7 8.5 8.2 5.8 47 4 1 3 25.541 51.082 1.78653 34.8 1.6 1.5 5.8 48 3 4 3 26.204 52.409 1.74439 61.9 2.8 2.7 5.8 49 1 1 5 26.372 52.745 1.73407 146.4 6.7 6.5 5.8 50 2 6 2 26.636 53.273 1.71812 228.5 10.4 10.1 5.8 51 4 4 2 27.136 54.272 1.68883 318.6 14.5 14.0 5.8 52 2 4 4 27.359 54.719 1.67608 234.1 10.7 10.3 5.8 53 4 3 3 27.803 55.606 1.65142 31.4 1.4 1.4 5.8 54 4 5 1 28.062 56.125 1.63738 34.8 1.6 1.5 5.8 55 5 2 2 28.329 56.657 1.62325 36.2 1.7 1.6 5.8 56 1 3 5 28.589 57.177 1.60972 145.8 6.7 6.4 5.8 57 3 5 3 28.7 57.399 1.60402 42.5 1.9 1.9 5.8 58 4 0 4 28.934 57.869 1.59212 107.1 4.9 4.7 5.8 59 4 2 4 29.993 59.987 1.54087 41.7 1.9 1.8 5.8 60 5 1 3 30.036 60.071 1.5389 34.1 1.6 1.5 5.8 61 3 1 5 30.315 60.63 1.52606 58.8 2.7 2.6 5.8 62 4 6 0 30.487 60.974 1.51826 35.1 1.6 1.5 5.8 63 6 2 0 31.589 63.179 1.47049 105.4 4.8 4.6 5.9 64 2 8 0 32.077 64.154 1.45045 85.8 3.9 3.7 5.9 65 0 8 2 32.145 64.289 1.44774 92.6 4.2 4.0 5.9 66 0 2 6 32.198 64.396 1.4456 36.8 1.7 1.6 5.9 67 3 3 5 32.357 64.715 1.43924 50.8 2.3 2.2 5.9 68 4 6 2 32.405 64.809 1.43737 61.4 2.8 2.7 5.9 69 6 0 2 32.479 64.957 1.43446 35.4 1.6 1.5 5.9 70 2 6 4 32.606 65.211 1.42948 61.1 2.8 2.6 5.9 71 1 5 5 32.728 65.456 1.42473 51.4 2.3 2.2 5.9 72 2 0 6 33.012 66.024 1.41384 33.3 1.5 1.4 5.9 73 4 4 4 33.048 66.096 1.41248 76.3 3.5 3.3 5.9 74 6 3 1 33.313 66.626 1.40253 23.4 1.1 1.0 5.9 75 6 2 2 33.472 66.944 1.39663 103.8 4.7 4.5 5.9 76 2 8 2 33.945 67.891 1.37943 101.1 4.6 4.4 5.9 77 2 2 6 33.997 67.995 1.37758 93.6 4.3 4.0 5.9 78 6 4 0 34.566 69.132 1.35768 61.9 2.8 2.7 5.9 79 3 7 3 34.793 69.585 1.34993 26.8 1.2 1.2 5.9 80 6 1 3 35.034 70.068 1.34181 40.4 1.8 1.7 5.9 81 0 4 6 35.148 70.296 1.33801 29.2 1.3 1.3 5.9 82 3 5 5 36.257 72.514 1.30246 47.0 2.1 2.0 5.9 83 6 4 2 36.372 72.744 1.2989 96.1 4.4 4.1 6.0 84 2 4 6 36.879 73.757 1.28354 79.0 3.6 3.4 6.0 85 6 3 3 36.942 73.884 1.28165 24.8 1.1 1.1 6.0 86 4 8 0 37.359 74.718 1.2694 108.1 4.9 4.6 6.0 87 0 8 4 37.61 75.22 1.26216 57.7 2.6 2.5 6.0 88 4 6 4 37.853 75.706 1.25527 133.2 6.1 5.7 6.0 89 6 0 4 37.922 75.844 1.25333 57.4 2.6 2.4 6.0 90 4 0 6 38.234 76.469 1.24464 35.6 1.6 1.5 6.0 91 1 7 5 38.486 76.972 1.23774 30.3 1.4 1.3 6.0 92 1 9 3 38.926 77.852 1.22594 26.9 1.2 1.1 6.0 93 4 8 2 39.115 78.229 1.22097 89.9 4.1 3.8 6.0 94 5 3 5 39.311 78.621 1.21586 113.6 5.2 4.8 6.0 95 1 3 7 39.682 79.363 1.20635 59.6 2.7 2.5 6.0 96 7 4 1 40.554 81.107 1.18476 27.2 1.2 1.1 6.1 97 2 10 0 40.658 81.316 1.18224 62.2 2.8 2.6 6.1 98 0 10 2 40.719 81.439 1.18077 53.4 2.4 2.2 6.1 99 6 6 2 41.024 82.048 1.17353 24.7 1.1 1.0 6.1 100 3 1 7 41.179 82.357 1.16991 70.3 3.2 2.9 6.1 101 6 4 4 41.614 83.228 1.15987 43.7 2.0 1.8 6.1 102 3 7 5 41.828 83.656 1.15503 38.5 1.8 1.6 6.1 103 4 4 6 41.919 83.839 1.15297 23.7 1.1 1.0 6.1 104 2 10 2 42.378 84.755 1.14283 54.9 2.5 2.3 6.1 105 8 0 0 42.687 85.373 1.13612 43.8 2.0 1.8 6.1 106 3 3 7 43.003 86.005 1.12939 75.3 3.4 3.1 6.1 107 8 1 1 43.342 86.683 1.12229 86.1 3.9 3.6 6.1 108 8 2 0 43.596 87.191 1.11705 40.2 1.8 1.7 6.2 109 4 8 4 44.276 88.552 1.10337 39.9 1.8 1.6 6.2 Reference: Chichagov A.V. et al. Information-Calculating System on Crystal Structure Data of Minerals (MINCRYST) - Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian) |