Institute of Experimental Mineralogy Russian Academy of Sciences ------------------------------------------------- 142432, Chernogolovka, Moscow district A.V. Chichagov +7(496)52-22320 *** *** W W W - X R A Y P O L *** *********************** MAKATITE 1 Na(2)Si(4)O(8)(OH)(2).4H(2)O Monoclinic P 2(1)/c Z = 4 R =0.051 NR =834 9 .12 .1991 Ref.Str.: Annehed H., Falth L., Lincoln (1982) * Z. Kristallogr., 159, 203-210 Initial data from BDM-file Lattice parameters (cub. angs.,degr.): a = 7.3881 alpha = 90.0 b = 18.094 beta = 90.64 c = 9.5234 gamma = 90.0 Unit cell volume (cub. angs.) = 1273.01 Molar volume ( cub.cm/mol.) = 191.7 Co-ordinates, thermal parameters, occupation for atomic positions: NoP x/a y/b z/c B(j) atom / occupation 1 0.2822 0.2143 0.1876 0.96 Si = 1.00 2 0.6997 0.2182 0.1748 1.08 Si = 1.00 3 0.7776 0.3388 0.3891 0.83 Si = 1.00 4 0.2001 0.3349 0.399 1.01 Si = 1.00 5 0.2421 0.2241 0.0224 1.74 O = 1.00 6 0.2476 0.2971 0.2507 1.41 O = 1.00 7 0.4931 0.1951 0.205 1.49 O = 1.00 8 0.7307 0.2232 0.0064 1.58 O = 1.00 9 0.7429 0.3001 0.2358 1.11 O = 1.00 10 0.9902 0.3597 0.3992 1.43 O = 1.00 11 0.1619 0.1517 0.2585 1.78 O = 1.00 12 0.824 0.1546 0.2444 1.58 O = 1.00 13 0.6662 0.4126 0.4075 1.3 O = 1.00 14 0.3175 0.4083 0.4202 1.4 O = 1.00 15 0.7506 0.4108 0.0029 1.93 H(2)O = 1.00 16 0.245 0.408 0.0187 2.03 H(2)O = 1.00 17 0.0296 0.0123 0.2336 2.46 H(2)O = 1.00 18 0.4714 0.024 0.2529 2.18 H(2)O = 1.00 19 0.5 0.5 0.0 2.73 Na = 1.00 20 0.0 0.5 0.0 2.71 Na = 1.00 21 0.7478 0.0324 0.1285 2.72 Na = 1.00 Co-ordinates for all atomic positions : No NoP x/a y/b z/c 1 1 0.2822 0.2143 0.1876 2 2 0.6997 0.2182 0.1748 3 3 0.7776 0.3388 0.3891 4 4 0.2001 0.3349 0.399 5 5 0.2421 0.2241 0.0224 6 6 0.2476 0.2971 0.2507 7 7 0.4931 0.1951 0.205 8 8 0.7307 0.2232 0.0064 9 9 0.7429 0.3001 0.2358 10 10 0.9902 0.3597 0.3992 11 11 0.1619 0.1517 0.2585 12 12 0.824 0.1546 0.2444 13 13 0.6662 0.4126 0.4075 14 14 0.3175 0.4083 0.4202 15 15 0.7506 0.4108 0.0029 16 16 0.245 0.408 0.0187 17 17 0.0296 0.0123 0.2336 18 18 0.4714 0.024 0.2529 19 19 0.5 0.5 0.0 20 20 0.0 0.5 0.0 21 21 0.7478 0.0324 0.1285 22 1 0.7178 0.7143 0.3124 23 2 0.3003 0.7182 0.3252 24 3 0.2224 0.8388 0.1109 25 4 0.7999 0.8349 0.101 26 5 0.7579 0.7241 0.4776 27 6 0.7524 0.7971 0.2493 28 7 0.5069 0.6951 0.295 29 8 0.2693 0.7232 0.4936 30 9 0.2571 0.8001 0.2642 31 10 0.0098 0.8597 0.1008 32 11 0.8381 0.6517 0.2415 33 12 0.176 0.6546 0.2556 34 13 0.3338 0.9126 0.0925 35 14 0.6825 0.9083 0.0798 36 15 0.2494 0.9108 0.4971 37 16 0.755 0.908 0.4813 38 17 0.9704 0.5123 0.2664 39 18 0.5286 0.524 0.2471 40 19 0.5 0.0 0.5 41 20 0.0 0.0 0.5 42 21 0.2522 0.5324 0.3715 43 1 0.2822 0.2857 0.6876 44 2 0.6997 0.2818 0.6748 45 3 0.7776 0.1612 0.8891 46 4 0.2001 0.1651 0.899 47 5 0.2421 0.2759 0.5224 48 6 0.2476 0.2029 0.7507 49 7 0.4931 0.3049 0.705 50 8 0.7307 0.2768 0.5064 51 9 0.7429 0.1999 0.7358 52 10 0.9902 0.1403 0.8992 53 11 0.1619 0.3483 0.7585 54 12 0.824 0.3454 0.7444 55 13 0.6662 0.0874 0.9075 56 14 0.3175 0.0917 0.9202 57 15 0.7506 0.0892 0.5029 58 16 0.245 0.092 0.5187 59 17 0.0296 0.4877 0.7336 60 18 0.4714 0.476 0.7529 61 21 0.7478 0.4676 0.6285 62 1 0.7178 0.7857 0.8124 63 2 0.3003 0.7818 0.8252 64 3 0.2224 0.6612 0.6109 65 4 0.7999 0.6651 0.601 66 5 0.7579 0.7759 0.9776 67 6 0.7524 0.7029 0.7493 68 7 0.5069 0.8049 0.795 69 8 0.2693 0.7768 0.9936 70 9 0.2571 0.6999 0.7642 71 10 0.0098 0.6403 0.6008 72 11 0.8381 0.8483 0.7415 73 12 0.176 0.8454 0.7556 74 13 0.3338 0.5874 0.5925 75 14 0.6825 0.5917 0.5798 76 15 0.2494 0.5892 0.9971 77 16 0.755 0.592 0.9813 78 17 0.9704 0.9877 0.7664 79 18 0.5286 0.976 0.7471 80 21 0.2522 0.9676 0.8715 X-ray density (g/cm cub.) = 2.04 MU (1/cm) = 56.649 Mass attenuation coefficient (cm**2/g) = 27.821 Selected interatomic distances (cation-anion,anion-anion): NoP Atom Rad.sph. C.N. Distance NoP N. (angs.) (angs.) 1 Si 2.268 4 1.6075 5 1.6354 6 1.6032 7 1.5944 11 2 Si 2.268 4 1.6115 7 1.6251 8 1.6221 9 1.6104 12 3 Si 2.268 4 1.6368 9 1.6174 10 1.5794 13 1.6233 8 4 Si 2.268 4 1.6114 6 1.6144 10 1.5978 14 1.6152 5 5 O 3.432 8 2.5439 6 2.5819 7 2.6744 11 3.3277 16 2.6166 6 2.6628 10 3.4182 11 2.6474 14 6 O 3.432 7 2.5439 5 2.6274 7 2.6381 10 2.7072 11 2.6272 14 2.9845 16 2.6166 5 7 O 3.432 7 2.5819 5 2.6274 6 2.6441 8 2.6626 9 2.6252 11 2.5756 12 3.1337 18 8 O 3.432 8 2.6441 7 2.5909 9 2.668 12 3.3978 15 2.6138 9 2.648 10 3.41 12 2.6724 13 9 O 3.432 7 2.6626 7 2.5909 8 2.619 10 2.701 12 2.6757 13 2.9896 15 2.6138 8 10 O 3.432 7 2.6381 6 2.619 9 2.5801 13 2.5787 14 3.0398 17 2.6628 5 2.648 8 11 O 3.432 8 2.6744 5 2.7072 6 2.6252 7 2.4991 12 2.7145 17 3.2516 18 3.4182 5 2.7659 16 12 O 3.432 7 2.5756 7 2.668 8 2.701 9 2.4991 11 2.9918 17 3.41 8 2.7901 15 13 O 3.432 6 2.6757 9 2.5801 10 2.5816 14 3.1904 17 2.7194 18 2.6724 8 14 O 3.432 5 2.6272 6 2.5787 10 2.5816 13 3.0968 18 2.6474 5 15 H(2)O 3.6 8 3.3978 8 2.9896 9 3.4952 17 3.5184 18 2.7901 12 3.5889 17 3.3475 18 3.2853 16 16 H(2)O 3.6 6 3.3277 5 2.9845 6 2.7659 11 3.4478 17 3.2884 18 3.2853 15 17 H(2)O 3.6 9 2.7145 11 2.9918 12 3.274 18 3.0398 10 3.1904 13 3.4898 14 3.4952 15 3.5889 15 3.4478 16 18 H(2)O 3.6 10 3.1337 7 3.2516 11 3.5188 12 3.274 17 2.7194 13 3.0968 14 3.5184 15 3.571 14 3.3475 15 3.2884 16 19 Na 2.976 6 2.4561 15 2.5218 16 2.4 18 2.4 18 2.4561 15 2.5218 16 20 Na 2.976 6 2.4499 15 2.4641 16 2.5586 17 2.5586 17 2.4499 15 2.4641 16 21 Na 2.976 5 2.5318 12 2.3285 17 2.3771 18 2.342 14 2.399 13 X-ray diffraction powder data (II), X-Ray W.L. = 1.54056(angs.): No H K L Theta 2*Theta S LPG MF F I int. ( degree ) *100 1 0 2 0 4.884 9.768 0.055 272.91 2 115.8 451.7 2 0 1 1 5.245 10.489 0.059 236.4 4 63.1 232.2 3 1 0 0 5.985 11.97 0.068 181.0 2 2.5 0.1 4 1 1 0 6.466 12.933 0.073 154.72 4 6.1 1.4 5 0 2 1 6.744 13.489 0.076 142.05 4 0.2 0.0 6 1 2 0 7.736 15.472 0.087 107.42 4 11.2 3.4 7 1 1 -1 7.931 15.862 0.09 102.1 4 10.7 2.9 8 1 1 1 8.01 16.019 0.09 100.07 4 15.0 5.5 9 0 3 1 8.695 17.39 0.098 84.58 4 166.4 577.8 10 1 2 -1 9.001 18.001 0.102 78.78 4 10.5 2.2 11 1 2 1 9.07 18.14 0.102 77.55 4 32.3 20.0 12 0 0 2 9.31 18.62 0.105 73.49 2 49.7 22.4 13 1 3 0 9.49 18.979 0.107 70.65 4 22.3 8.7 14 0 1 2 9.63 19.26 0.109 68.55 4 15.8 4.2 15 0 4 0 9.804 19.609 0.111 66.05 2 49.7 20.1 16 0 2 2 10.534 21.067 0.119 56.94 4 90.9 116.1 17 1 3 -1 10.552 21.104 0.119 56.73 4 39.1 21.4 18 1 3 1 10.612 21.224 0.12 56.07 4 2.9 0.1 19 0 4 1 10.866 21.733 0.122 53.37 4 4.8 0.3 20 1 0 -2 11.039 22.079 0.124 51.65 2 17.6 2.0 21 1 0 2 11.154 22.307 0.126 50.55 2 46.1 13.3 22 1 1 -2 11.312 22.625 0.127 49.08 4 56.3 38.3 23 1 1 2 11.424 22.848 0.129 48.09 4 58.8 41.0 24 1 4 0 11.518 23.035 0.13 47.28 4 61.6 44.3 25 0 3 2 11.895 23.789 0.134 44.2 4 109.4 130.5 26 2 0 0 12.036 24.073 0.135 43.11 2 269.4 386.0 27 1 2 -2 12.097 24.193 0.136 42.67 4 53.5 30.1 28 1 2 2 12.201 24.403 0.137 41.9 4 4.5 0.2 29 2 1 0 12.288 24.577 0.138 41.28 4 28.5 8.3 30 1 4 -1 12.415 24.83 0.14 40.4 4 59.6 35.4 31 1 4 1 12.467 24.933 0.14 40.05 4 23.8 5.6 32 2 2 0 13.017 26.034 0.146 36.56 4 192.0 332.8 33 2 1 -1 13.112 26.224 0.147 36.01 4 67.4 40.3 34 0 5 1 13.162 26.324 0.148 35.72 4 81.4 58.4 35 2 1 1 13.209 26.419 0.148 35.45 4 62.6 34.3 36 1 3 -2 13.307 26.614 0.149 34.9 4 24.6 5.2 37 1 3 2 13.403 26.806 0.15 34.37 4 34.6 10.1 38 0 4 2 13.584 27.169 0.152 33.41 4 56.1 26.0 39 1 5 0 13.711 27.422 0.154 32.76 4 24.0 4.6 40 2 2 -1 13.8 27.601 0.155 32.31 4 26.3 5.5 41 2 2 1 13.893 27.786 0.156 31.85 4 41.6 13.6 42 2 3 0 14.154 28.308 0.159 30.62 4 12.8 1.2 43 0 1 3 14.263 28.526 0.16 30.12 4 141.9 149.7 44 1 5 -1 14.481 28.963 0.162 29.16 4 5.9 0.3 45 1 5 1 14.526 29.052 0.163 28.97 4 6.3 0.3 46 0 6 0 14.799 29.598 0.166 27.84 2 98.2 33.1 47 1 4 -2 14.848 29.695 0.166 27.64 4 5.8 0.2 48 2 3 -1 14.882 29.764 0.167 27.51 4 22.6 3.5 49 0 2 3 14.902 29.804 0.167 27.43 4 174.6 206.4 50 1 4 2 14.934 29.869 0.167 27.3 4 52.2 18.4 51 2 3 1 14.969 29.938 0.168 27.17 4 14.9 1.5 52 2 0 -2 15.218 30.436 0.17 26.22 2 26.8 2.3 53 2 0 2 15.388 30.776 0.172 25.6 2 22.2 1.6 54 2 1 -2 15.422 30.844 0.173 25.48 4 13.1 1.1 55 1 1 -3 15.454 30.908 0.173 25.37 4 41.6 10.8 56 0 5 2 15.507 31.014 0.174 25.18 4 145.5 131.6 57 0 6 1 15.541 31.082 0.174 25.06 4 100.5 62.5 58 1 1 3 15.58 31.159 0.174 24.93 4 30.1 5.6 59 2 1 2 15.59 31.179 0.174 24.9 4 0.6 0.0 60 2 4 0 15.618 31.236 0.175 24.8 4 39.1 9.4 61 0 3 3 15.916 31.831 0.178 23.81 4 21.8 2.8 62 1 6 0 16.015 32.03 0.179 23.49 4 72.5 30.5 63 2 2 -2 16.019 32.038 0.179 23.48 4 57.0 18.8 64 1 2 -3 16.05 32.1 0.179 23.38 4 45.1 11.8 65 1 2 3 16.172 32.343 0.181 23.0 4 3.7 0.1 66 2 2 2 16.181 32.362 0.181 22.97 4 52.4 15.6 67 2 4 -1 16.287 32.573 0.182 22.65 4 5.2 0.2 68 2 4 1 16.367 32.733 0.183 22.41 4 26.1 3.8 69 1 5 -2 16.637 33.274 0.186 21.63 4 51.0 13.9 70 1 6 -1 16.689 33.378 0.186 21.49 4 28.9 4.4 71 1 5 2 16.716 33.431 0.187 21.41 4 28.3 4.2 72 1 6 1 16.728 33.456 0.187 21.38 4 58.6 18.1 73 2 3 -2 16.973 33.945 0.189 20.71 4 41.5 8.8 74 1 3 -3 17.002 34.004 0.19 20.64 4 36.8 6.9 75 1 3 3 17.118 34.235 0.191 20.33 4 0.4 0.0 76 2 3 2 17.127 34.253 0.191 20.31 4 34.4 5.9 77 0 4 3 17.244 34.489 0.192 20.01 4 32.3 5.1 78 2 5 0 17.336 34.673 0.193 19.78 4 5.7 0.2 79 0 6 2 17.599 35.197 0.196 19.14 4 105.4 52.5 80 2 5 -1 17.948 35.896 0.2 18.33 4 133.0 80.1 81 0 7 1 17.986 35.971 0.2 18.25 4 42.0 8.0 82 2 5 1 18.022 36.043 0.201 18.17 4 131.3 77.3 83 3 0 0 18.228 36.456 0.203 17.72 2 7.7 0.1 84 2 4 -2 18.233 36.467 0.203 17.71 4 38.4 6.4 85 1 4 -3 18.261 36.523 0.203 17.65 4 15.2 1.0 86 1 4 3 18.37 36.74 0.205 17.42 4 60.5 15.8 87 2 4 2 18.378 36.757 0.205 17.4 4 11.8 0.6 88 3 1 0 18.402 36.804 0.205 17.36 4 7.9 0.3 89 1 7 0 18.404 36.808 0.205 17.35 4 25.4 2.8 90 1 6 -2 18.616 37.233 0.207 16.92 4 14.1 0.8 91 1 6 2 18.688 37.375 0.208 16.78 4 12.6 0.7 92 2 1 -3 18.725 37.449 0.208 16.7 4 27.0 3.0 93 0 5 3 18.832 37.663 0.21 16.49 4 60.2 14.8 94 0 0 4 18.878 37.756 0.21 16.41 2 85.6 14.8 95 3 2 0 18.916 37.832 0.21 16.33 4 14.0 0.8 96 2 1 3 18.937 37.873 0.211 16.29 4 35.2 5.0 97 3 1 -1 18.966 37.933 0.211 16.24 4 71.0 20.2 98 1 7 -1 19.003 38.006 0.211 16.17 4 54.2 11.7 99 1 7 1 19.038 38.076 0.212 16.1 4 48.8 9.4 100 0 1 4 19.047 38.094 0.212 16.09 4 131.2 68.4 101 3 1 1 19.071 38.143 0.212 16.04 4 15.3 0.9 102 2 2 -3 19.231 38.462 0.214 15.75 4 38.1 5.6 103 2 6 0 19.253 38.506 0.214 15.71 4 75.3 22.0 104 2 2 3 19.438 38.877 0.216 15.38 4 38.0 5.5 105 3 2 -1 19.467 38.935 0.216 15.33 4 42.7 6.9 106 0 2 4 19.546 39.092 0.217 15.19 4 0.8 0.0 107 3 2 1 19.57 39.141 0.217 15.15 4 32.0 3.8 108 3 3 0 19.747 39.494 0.219 14.85 4 26.1 2.5 109 2 5 -2 19.752 39.504 0.219 14.84 4 90.9 30.3 110 1 5 -3 19.778 39.556 0.22 14.8 4 6.4 0.2 111 1 0 -4 19.805 39.611 0.22 14.75 2 5.3 0.1 112 2 6 -1 19.814 39.627 0.22 14.74 4 4.6 0.1 113 0 7 2 19.821 39.641 0.22 14.73 4 0.3 0.0 114 1 5 3 19.88 39.759 0.221 14.63 4 36.8 4.9 115 2 6 1 19.881 39.762 0.221 14.63 4 25.8 2.4 116 2 5 2 19.887 39.775 0.221 14.62 4 83.6 25.2 117 0 8 0 19.911 39.823 0.221 14.58 2 18.1 0.6 118 1 0 4 19.94 39.881 0.221 14.53 2 25.4 1.2 119 1 1 -4 19.968 39.935 0.222 14.49 4 6.0 0.1 120 2 3 -3 20.051 40.102 0.223 14.35 4 39.9 5.6 121 1 1 4 20.102 40.204 0.223 14.27 4 47.4 7.9 122 2 3 3 20.251 40.503 0.225 14.04 4 45.2 7.1 123 3 3 -1 20.279 40.559 0.225 14.0 4 53.1 9.8 124 0 3 4 20.356 40.711 0.226 13.88 4 26.3 2.4 125 3 3 1 20.379 40.758 0.226 13.84 4 28.8 2.8 126 1 2 -4 20.448 40.896 0.227 13.74 4 7.5 0.2 127 0 8 1 20.49 40.98 0.227 13.68 4 8.7 0.3 128 3 0 -2 20.521 41.042 0.228 13.63 2 56.0 5.3 129 1 2 4 20.58 41.16 0.228 13.55 4 17.7 1.0 130 0 6 3 20.629 41.258 0.229 13.47 4 63.8 13.5 131 3 1 -2 20.678 41.357 0.229 13.4 4 38.9 5.0 132 3 0 2 20.717 41.435 0.23 13.35 2 13.9 0.3 133 1 7 -2 20.745 41.491 0.23 13.3 4 23.1 1.7 134 1 7 2 20.81 41.621 0.231 13.21 4 29.7 2.9 135 3 4 0 20.864 41.727 0.231 13.14 4 50.3 8.2 136 1 8 0 20.865 41.731 0.231 13.13 4 42.0 5.7 137 3 1 2 20.874 41.748 0.231 13.12 4 32.5 3.4 138 3 2 -2 21.146 42.291 0.234 12.75 4 45.6 6.5 139 2 4 -3 21.155 42.309 0.234 12.74 4 9.4 0.3 140 1 3 -4 21.229 42.458 0.235 12.64 4 31.5 3.1 141 2 7 0 21.328 42.657 0.236 12.5 4 0.3 0.0 142 3 2 2 21.337 42.675 0.236 12.49 4 20.9 1.3 143 2 4 3 21.346 42.693 0.236 12.48 4 24.7 1.9 144 1 3 4 21.357 42.713 0.236 12.47 4 1.2 0.0 145 3 4 -1 21.373 42.746 0.237 12.45 4 36.0 4.0 146 1 8 -1 21.407 42.813 0.237 12.4 4 30.1 2.8 147 1 8 1 21.438 42.877 0.237 12.36 4 15.2 0.7 148 0 4 4 21.446 42.892 0.237 12.35 4 85.0 22.0 149 3 4 1 21.468 42.937 0.238 12.32 4 18.6 1.0 150 2 6 -2 21.485 42.97 0.238 12.3 4 54.0 8.9 151 1 6 -3 21.509 43.019 0.238 12.27 4 35.4 3.8 152 1 6 3 21.604 43.208 0.239 12.15 4 48.7 7.1 153 2 6 2 21.612 43.223 0.239 12.14 4 71.7 15.4 154 2 7 -1 21.845 43.69 0.242 11.85 4 2.0 0.0 155 3 3 -2 21.906 43.812 0.242 11.78 4 44.9 5.9 156 2 7 1 21.907 43.815 0.242 11.77 4 6.5 0.1 157 3 3 2 22.093 44.185 0.244 11.55 4 76.0 16.5 158 0 8 2 22.15 44.301 0.245 11.49 4 47.1 6.3 159 3 5 0 22.232 44.463 0.246 11.39 4 15.8 0.7 160 1 4 -4 22.285 44.569 0.246 11.33 4 8.3 0.2 161 1 4 4 22.408 44.815 0.247 11.19 4 1.6 0.0 162 2 5 -3 22.508 45.016 0.248 11.08 4 31.1 2.6 163 2 0 -4 22.518 45.035 0.249 11.07 2 26.0 0.9 164 0 7 3 22.6 45.201 0.249 10.98 4 7.4 0.1 165 2 1 -4 22.664 45.328 0.25 10.91 4 59.6 9.6 166 2 5 3 22.691 45.382 0.25 10.88 4 35.4 3.4 167 3 5 -1 22.716 45.433 0.251 10.85 4 20.8 1.2 168 2 0 4 22.761 45.521 0.251 10.8 2 37.4 1.9 169 0 5 4 22.786 45.572 0.251 10.77 4 4.8 0.1 170 3 5 1 22.807 45.614 0.252 10.75 4 42.8 4.9 171 2 1 4 22.906 45.812 0.253 10.65 4 50.1 6.6 172 3 4 -2 22.937 45.874 0.253 10.62 4 28.6 2.1 173 1 8 -2 22.999 45.997 0.254 10.55 4 18.8 0.9 174 0 9 1 23.053 46.106 0.254 10.49 4 25.0 1.6 175 1 8 2 23.059 46.117 0.254 10.49 4 24.5 1.5 176 2 2 -4 23.099 46.198 0.255 10.45 4 99.8 25.7 177 3 4 2 23.117 46.234 0.255 10.43 4 69.6 12.5 178 3 1 -3 23.331 46.661 0.257 10.21 4 0.7 0.0 179 2 2 4 23.337 46.674 0.257 10.21 4 94.5 22.5 180 1 9 0 23.395 46.791 0.258 10.15 4 31.1 2.4 181 2 7 -2 23.398 46.797 0.258 10.15 4 17.3 0.8 182 1 7 -3 23.421 46.842 0.258 10.12 4 35.6 3.2 183 1 7 3 23.51 47.019 0.259 10.04 4 39.3 3.8 184 2 7 2 23.517 47.033 0.259 10.03 4 31.2 2.4 185 2 8 0 23.537 47.074 0.259 10.01 4 93.0 21.4 186 1 5 -4 23.587 47.174 0.26 9.96 4 2.0 0.0 187 3 1 3 23.597 47.193 0.26 9.95 4 9.5 0.2 188 1 5 4 23.704 47.409 0.261 9.85 4 47.1 5.4 189 3 2 -3 23.756 47.512 0.261 9.8 4 36.5 3.2 190 2 3 -4 23.81 47.62 0.262 9.75 4 21.9 1.2 191 3 6 0 23.818 47.637 0.262 9.75 4 113.3 30.9 192 1 9 -1 23.891 47.782 0.263 9.68 4 20.2 1.0 193 1 9 1 23.92 47.84 0.263 9.65 4 30.0 2.1 194 0 1 5 23.996 47.992 0.264 9.58 4 110.1 28.7 195 2 8 -1 24.016 48.031 0.264 9.57 4 34.1 2.8 196 3 2 3 24.018 48.037 0.264 9.56 4 17.1 0.7 197 2 3 4 24.043 48.085 0.264 9.54 4 29.2 2.0 198 2 8 1 24.074 48.147 0.265 9.51 4 24.6 1.4 199 2 6 -3 24.081 48.162 0.265 9.51 4 71.7 12.1 200 3 5 -2 24.212 48.424 0.266 9.39 4 12.9 0.4 201 2 6 3 24.254 48.508 0.267 9.35 4 79.2 14.5 202 3 6 -1 24.279 48.557 0.267 9.33 4 32.9 2.5 203 0 6 4 24.345 48.689 0.268 9.27 4 10.7 0.3 204 3 6 1 24.365 48.73 0.268 9.26 4 55.5 7.0 205 3 5 2 24.385 48.769 0.268 9.24 4 11.8 0.3 206 0 2 5 24.413 48.825 0.268 9.22 4 8.3 0.2 207 3 3 -3 24.452 48.905 0.269 9.18 4 0.4 0.0 208 0 9 2 24.576 49.151 0.27 9.08 4 7.5 0.1 209 4 0 0 24.649 49.299 0.271 9.02 2 241.6 65.0 210 3 3 3 24.709 49.418 0.271 8.97 4 7.3 0.1 211 0 8 3 24.72 49.439 0.271 8.96 4 74.6 12.3 212 1 1 -5 24.753 49.506 0.272 8.93 4 2.7 0.0 213 2 4 -4 24.779 49.558 0.272 8.91 4 37.5 3.1 214 4 1 0 24.786 49.572 0.272 8.9 4 34.1 2.6 215 1 1 5 24.894 49.789 0.273 8.81 4 17.4 0.7 216 2 4 4 25.005 50.01 0.274 8.73 4 54.6 6.4 217 0 3 5 25.095 50.191 0.275 8.65 4 2.5 0.0 218 1 6 -4 25.108 50.215 0.275 8.65 4 27.6 1.6 219 1 2 -5 25.16 50.32 0.276 8.6 4 8.3 0.1 220 4 2 0 25.193 50.386 0.276 8.58 4 33.9 2.4 221 0 10 0 25.196 50.391 0.276 8.58 2 71.3 5.4 222 4 1 -1 25.219 50.438 0.277 8.56 4 4.6 0.0 223 1 6 4 25.22 50.439 0.277 8.56 4 6.8 0.1 224 1 2 5 25.3 50.6 0.277 8.5 4 34.8 2.5 225 4 1 1 25.331 50.662 0.278 8.47 4 12.5 0.3 226 1 9 -2 25.361 50.723 0.278 8.45 4 15.9 0.5 227 3 4 -3 25.403 50.807 0.278 8.42 4 50.0 5.2 228 1 9 2 25.417 50.834 0.279 8.41 4 15.4 0.5 229 2 8 -2 25.467 50.934 0.279 8.37 4 12.3 0.3 230 1 8 -3 25.488 50.976 0.279 8.35 4 80.8 13.5 231 1 8 3 25.571 51.143 0.28 8.29 4 27.8 1.6 232 2 8 2 25.578 51.156 0.28 8.29 4 11.9 0.3 233 3 7 0 25.596 51.192 0.28 8.27 4 46.7 4.5 234 4 2 -1 25.621 51.242 0.281 8.26 4 11.6 0.3 235 3 4 3 25.653 51.306 0.281 8.23 4 87.0 15.4 236 0 10 1 25.679 51.358 0.281 8.21 4 113.5 26.1 237 3 6 -2 25.705 51.41 0.282 8.19 4 18.0 0.7 238 4 2 1 25.731 51.463 0.282 8.18 4 32.7 2.2 239 1 3 -5 25.828 51.656 0.283 8.11 4 83.0 13.8 240 2 7 -3 25.845 51.69 0.283 8.09 4 55.7 6.2 241 4 3 0 25.86 51.721 0.283 8.08 4 16.3 0.5 242 2 9 0 25.862 51.725 0.283 8.08 4 4.8 0.0 243 3 6 2 25.87 51.74 0.283 8.08 4 13.2 0.3 244 1 3 5 25.966 51.931 0.284 8.01 4 32.1 2.0 245 2 5 -4 25.986 51.971 0.284 7.99 4 12.3 0.3 246 1 10 0 25.995 51.99 0.285 7.99 4 61.9 7.6 247 2 7 3 26.01 52.02 0.285 7.98 4 41.8 3.4 248 0 4 5 26.029 52.058 0.285 7.96 4 3.3 0.0 249 3 7 -1 26.033 52.066 0.285 7.96 4 27.7 1.5 250 0 7 4 26.096 52.192 0.286 7.92 4 26.4 1.4 251 3 7 1 26.115 52.23 0.286 7.9 4 60.5 7.1 252 2 5 4 26.204 52.408 0.287 7.84 4 6.7 0.1 253 4 3 -1 26.281 52.561 0.287 7.79 4 73.2 10.3 254 2 9 -1 26.31 52.619 0.288 7.77 4 6.4 0.1 255 2 9 1 26.364 52.728 0.288 7.74 4 33.7 2.2 256 4 3 1 26.389 52.778 0.289 7.72 4 58.0 6.4 257 1 10 -1 26.454 52.908 0.289 7.68 4 3.7 0.0 258 4 0 -2 26.465 52.93 0.289 7.67 2 16.4 0.3 259 1 10 1 26.481 52.963 0.289 7.66 4 40.2 3.0 260 3 0 -4 26.584 53.168 0.29 7.59 2 42.6 1.7 261 3 5 -3 26.589 53.179 0.291 7.59 4 30.0 1.7 262 4 1 -2 26.595 53.19 0.291 7.58 4 18.9 0.7 263 4 0 2 26.681 53.362 0.291 7.53 2 10.3 0.1 264 3 1 -4 26.714 53.427 0.292 7.51 4 24.2 1.1 265 1 4 -5 26.744 53.487 0.292 7.49 4 23.9 1.1 266 4 4 0 26.775 53.55 0.292 7.47 4 74.9 10.3 267 4 1 2 26.81 53.62 0.293 7.45 4 1.0 0.0 268 1 7 -4 26.822 53.645 0.293 7.44 4 29.0 1.5 269 3 5 3 26.831 53.663 0.293 7.43 4 6.5 0.1 270 1 4 5 26.878 53.755 0.293 7.4 4 8.1 0.1 271 3 0 4 26.907 53.813 0.294 7.38 2 26.9 0.7 272 1 7 4 26.93 53.859 0.294 7.37 4 12.9 0.3 273 0 9 3 26.97 53.94 0.294 7.35 4 34.6 2.2 274 4 2 -2 26.982 53.964 0.295 7.34 4 36.1 2.4 275 3 1 4 27.035 54.07 0.295 7.31 4 42.8 3.3 276 2 1 -5 27.062 54.124 0.295 7.29 4 41.5 3.1 277 0 10 2 27.091 54.183 0.296 7.27 4 1.0 0.0 278 3 2 -4 27.1 54.199 0.296 7.27 4 8.1 0.1 279 4 4 -1 27.185 54.37 0.297 7.21 4 23.5 1.0 280 4 2 2 27.195 54.39 0.297 7.21 4 25.5 1.2 281 0 5 5 27.196 54.392 0.297 7.21 4 76.3 10.4 282 4 4 1 27.291 54.583 0.298 7.15 4 61.9 6.8 283 2 1 5 27.328 54.655 0.298 7.13 4 43.7 3.4 284 3 7 -2 27.393 54.786 0.299 7.09 4 55.7 5.4 285 2 6 -4 27.409 54.817 0.299 7.08 4 97.8 16.7 286 3 2 4 27.418 54.836 0.299 7.08 4 3.8 0.0 287 2 2 -5 27.445 54.889 0.299 7.06 4 42.6 3.2 288 3 8 0 27.543 55.086 0.3 7.0 4 27.7 1.3 289 3 7 2 27.551 55.103 0.3 7.0 4 33.0 1.9 290 4 3 -2 27.619 55.238 0.301 6.96 4 17.9 0.5 291 2 6 4 27.619 55.239 0.301 6.96 4 100.6 17.4 292 2 9 -2 27.674 55.347 0.301 6.93 4 23.4 0.9 293 1 9 -3 27.694 55.387 0.302 6.92 4 12.5 0.3 294 2 2 5 27.708 55.416 0.302 6.91 4 16.3 0.5 295 3 3 -4 27.735 55.47 0.302 6.89 4 0.3 0.0 296 1 9 3 27.772 55.545 0.302 6.87 4 19.7 0.7 297 2 9 2 27.778 55.557 0.303 6.87 4 27.2 1.3 298 2 8 -3 27.78 55.56 0.303 6.87 4 4.2 0.0 299 1 10 -2 27.826 55.653 0.303 6.84 4 18.5 0.6 300 4 3 2 27.829 55.658 0.303 6.84 4 5.8 0.1 301 1 10 2 27.879 55.757 0.304 6.81 4 4.9 0.0 302 1 5 -5 27.89 55.779 0.304 6.81 4 1.2 0.0 303 4 5 0 27.92 55.84 0.304 6.79 4 9.0 0.1 304 2 8 3 27.937 55.873 0.304 6.78 4 18.4 0.6 305 3 8 -1 27.959 55.918 0.304 6.77 4 58.7 5.8 306 3 6 -3 27.991 55.982 0.305 6.75 4 9.2 0.1 307 0 8 4 28.019 56.037 0.305 6.74 4 30.2 1.5 308 1 5 5 28.02 56.04 0.305 6.73 4 60.5 6.1 309 3 8 1 28.037 56.074 0.305 6.73 4 5.2 0.0 310 3 3 4 28.048 56.096 0.305 6.72 4 1.1 0.0 311 2 3 -5 28.075 56.149 0.305 6.7 4 24.0 1.0 312 3 6 3 28.225 56.45 0.307 6.62 4 1.6 0.0 313 2 10 0 28.297 56.594 0.308 6.59 4 0.8 0.0 314 4 5 -1 28.319 56.638 0.308 6.57 4 61.4 6.1 315 2 3 5 28.334 56.668 0.308 6.57 4 36.2 2.1 316 0 11 1 28.373 56.747 0.308 6.55 4 72.5 8.5 317 4 5 1 28.422 56.845 0.309 6.52 4 55.2 4.9 318 4 4 -2 28.495 56.989 0.31 6.48 4 45.6 3.3 319 0 6 5 28.577 57.155 0.311 6.44 4 56.0 5.0 320 3 4 -4 28.608 57.216 0.311 6.43 4 11.5 0.2 321 1 11 0 28.669 57.338 0.311 6.39 4 5.7 0.1 322 4 4 2 28.7 57.4 0.312 6.38 4 20.2 0.6 323 1 8 -4 28.712 57.424 0.312 6.37 4 13.2 0.3 324 2 10 -1 28.718 57.436 0.312 6.37 4 68.5 7.4 325 2 10 1 28.769 57.539 0.312 6.34 4 68.8 7.4 326 1 8 4 28.814 57.629 0.313 6.32 4 0.5 0.0 327 4 1 -3 28.82 57.64 0.313 6.32 4 72.0 8.1 328 3 4 4 28.915 57.83 0.314 6.27 4 22.2 0.8 329 2 4 -5 28.941 57.882 0.314 6.26 4 4.1 0.0 330 2 7 -4 29.029 58.058 0.315 6.22 4 16.0 0.4 331 0 0 6 29.034 58.068 0.315 6.21 2 31.3 0.8 332 1 11 -1 29.099 58.199 0.316 6.18 4 4.8 0.0 333 1 11 1 29.125 58.25 0.316 6.17 4 22.1 0.7 334 4 1 3 29.126 58.251 0.316 6.17 4 76.1 8.8 335 0 1 6 29.156 58.312 0.316 6.16 4 108.5 17.9 336 4 2 -3 29.187 58.374 0.317 6.14 4 16.6 0.4 337 2 4 5 29.195 58.391 0.317 6.14 4 14.8 0.3 338 2 7 4 29.232 58.464 0.317 6.12 4 1.8 0.0 339 1 6 -5 29.25 58.499 0.317 6.11 4 29.9 1.3 340 3 8 -2 29.258 58.516 0.317 6.11 4 1.6 0.0 341 4 6 0 29.279 58.558 0.317 6.1 4 46.9 3.3 342 0 10 3 29.342 58.683 0.318 6.07 4 47.2 3.3 343 1 6 5 29.376 58.752 0.318 6.05 4 18.0 0.5 344 3 8 2 29.41 58.819 0.319 6.04 4 2.0 0.0 345 4 2 3 29.49 58.981 0.32 6.0 4 13.7 0.3 346 0 2 6 29.521 59.042 0.32 5.99 4 17.5 0.5 347 3 7 -3 29.59 59.181 0.321 5.95 4 11.5 0.2 348 4 5 -2 29.596 59.191 0.321 5.95 4 68.3 6.8 349 3 9 0 29.644 59.288 0.321 5.93 4 42.0 2.6 350 4 6 -1 29.666 59.333 0.321 5.92 4 67.5 6.7 351 1 0 -6 29.687 59.374 0.321 5.91 2 13.7 0.1 352 0 11 2 29.699 59.397 0.322 5.91 4 118.5 20.5 353 3 5 -4 29.706 59.413 0.322 5.9 4 32.4 1.5 354 4 6 1 29.767 59.533 0.322 5.88 4 38.8 2.2 355 4 3 -3 29.793 59.586 0.323 5.86 4 6.2 0.1 356 4 5 2 29.796 59.593 0.323 5.86 4 79.9 9.2 357 1 1 -6 29.808 59.615 0.323 5.86 4 14.6 0.3 358 3 7 3 29.816 59.632 0.323 5.85 4 51.4 3.8 359 1 0 6 29.837 59.675 0.323 5.84 2 52.8 2.0 360 2 9 -3 29.87 59.74 0.323 5.83 4 8.1 0.1 361 1 1 6 29.957 59.915 0.324 5.79 4 24.6 0.9 X-ray diffraction powder data (I)...X-Ray wave length = 1.54056 (angs.): No H K L Theta 2*Theta d I int I int.n. I p.h.n. H(Si) ( degree ) (angstrem) *100 *100 1 0 2 0 4.884 9.768 9.047 451.7 78.2 78.5 5.6 2 0 1 1 5.245 10.489 8.42697 232.2 40.2 40.3 5.6 3 0 3 1 8.695 17.39 5.09533 577.8 100.0 100.0 5.6 4 1 2 1 9.07 18.14 4.88618 20.0 3.5 3.5 5.6 5 0 0 2 9.31 18.62 4.7614 22.4 3.9 3.9 5.6 6 1 3 0 9.49 18.979 4.67205 8.7 1.5 1.5 5.6 7 0 4 0 9.804 19.609 4.5235 20.1 3.5 3.5 5.6 8 0 2 2 10.534 21.067 4.21349 137.4 23.8 23.7 5.6 9 1 0 2 11.154 22.307 3.98198 13.3 2.3 2.3 5.6 10 1 1 -2 11.312 22.625 3.92682 38.3 6.6 6.6 5.6 11 1 1 2 11.424 22.848 3.88892 41.0 7.1 7.1 5.6 12 1 4 0 11.518 23.035 3.85777 44.3 7.7 7.6 5.6 13 0 3 2 11.895 23.789 3.7372 130.5 22.6 22.5 5.6 14 2 0 0 12.036 24.073 3.69382 386.0 66.8 66.5 5.6 15 1 2 -2 12.097 24.193 3.67571 30.1 5.2 5.2 5.6 16 2 1 0 12.288 24.577 3.61917 8.3 1.4 1.4 5.6 17 1 4 -1 12.415 24.83 3.58279 35.4 6.1 6.1 5.6 18 2 2 0 13.017 26.034 3.41976 332.8 57.6 57.2 5.6 19 2 1 -1 13.112 26.224 3.39545 40.3 7.0 6.9 5.6 20 0 5 1 13.162 26.324 3.38278 58.4 10.1 10.0 5.6 21 2 1 1 13.209 26.419 3.37086 34.3 5.9 5.9 5.6 22 1 3 2 13.403 26.806 3.32307 10.1 1.8 1.7 5.6 23 0 4 2 13.584 27.169 3.27948 26.0 4.5 4.5 5.6 24 2 2 1 13.893 27.786 3.20798 13.6 2.4 2.3 5.6 25 0 1 3 14.263 28.526 3.12652 149.7 25.9 25.7 5.6 26 0 6 0 14.799 29.598 3.01567 33.1 5.7 5.7 5.6 27 0 2 3 14.902 29.804 2.99525 209.9 36.3 36.0 5.6 28 1 4 2 14.934 29.869 2.9889 18.4 3.2 3.1 5.6 29 1 1 -3 15.454 30.908 2.89072 10.8 1.9 1.9 5.6 30 0 5 2 15.507 31.014 2.88111 131.6 22.8 22.5 5.6 31 0 6 1 15.541 31.082 2.87495 62.5 10.8 10.7 5.6 32 2 4 0 15.618 31.236 2.8611 9.4 1.6 1.6 5.6 33 1 6 0 16.015 32.03 2.79201 49.3 8.5 8.4 5.6 34 1 2 -3 16.05 32.1 2.78603 11.8 2.0 2.0 5.6 35 2 2 2 16.181 32.362 2.76408 15.6 2.7 2.7 5.6 36 1 5 -2 16.637 33.274 2.69037 13.9 2.4 2.4 5.6 37 1 6 -1 16.689 33.378 2.68229 8.6 1.5 1.5 5.7 38 1 6 1 16.728 33.456 2.67618 18.1 3.1 3.1 5.7 39 2 3 -2 16.973 33.945 2.63872 8.8 1.5 1.5 5.7 40 1 3 -3 17.002 34.004 2.63426 6.9 1.2 1.2 5.7 41 2 3 2 17.127 34.253 2.61569 5.9 1.0 1.0 5.7 42 0 6 2 17.599 35.197 2.54767 52.5 9.1 9.0 5.7 43 2 5 -1 17.948 35.896 2.49966 80.1 13.9 13.7 5.7 44 0 7 1 17.986 35.971 2.49459 8.0 1.4 1.4 5.7 45 2 5 1 18.022 36.043 2.4898 77.3 13.4 13.2 5.7 46 2 4 -2 18.233 36.467 2.46182 7.4 1.3 1.3 5.7 47 1 4 3 18.37 36.74 2.44418 16.3 2.8 2.8 5.7 48 0 5 3 18.832 37.663 2.38632 14.8 2.6 2.5 5.7 49 0 0 4 18.878 37.756 2.3807 14.8 2.6 2.5 5.7 50 3 1 -1 18.966 37.933 2.37001 20.2 3.5 3.4 5.7 51 1 7 -1 19.003 38.006 2.36558 11.7 2.0 2.0 5.7 52 0 1 4 19.047 38.094 2.36036 77.8 13.5 13.2 5.7 53 2 6 0 19.253 38.506 2.33603 27.6 4.8 4.7 5.7 54 3 2 -1 19.467 38.935 2.31127 6.9 1.2 1.2 5.7 55 2 5 -2 19.752 39.504 2.27927 32.8 5.7 5.6 5.7 56 2 5 2 19.887 39.775 2.26437 32.5 5.6 5.5 5.7 57 1 1 4 20.102 40.204 2.2412 7.9 1.4 1.3 5.7 58 3 3 -1 20.279 40.559 2.22239 16.8 2.9 2.9 5.7 59 0 6 3 20.629 41.258 2.18632 13.5 2.3 2.3 5.7 60 3 4 0 20.864 41.727 2.16283 17.4 3.0 2.9 5.7 61 3 2 -2 21.146 42.291 2.13528 6.8 1.2 1.2 5.7 62 3 4 -1 21.373 42.746 2.11359 7.2 1.2 1.2 5.7 63 0 4 4 21.446 42.892 2.10674 23.1 4.0 3.9 5.7 64 2 6 -2 21.485 42.97 2.1031 12.6 2.2 2.1 5.7 65 2 6 2 21.612 43.223 2.09138 22.5 3.9 3.8 5.7 66 3 3 -2 21.906 43.812 2.06461 6.0 1.0 1.0 5.7 67 3 3 2 22.093 44.185 2.04804 16.5 2.8 2.8 5.7 68 0 8 2 22.15 44.301 2.04297 6.3 1.1 1.1 5.7 69 2 1 -4 22.664 45.328 1.99903 12.9 2.2 2.2 5.7 70 2 1 4 22.906 45.812 1.97904 6.6 1.1 1.1 5.7 71 2 2 -4 23.099 46.198 1.96341 38.1 6.6 6.4 5.7 72 2 2 4 23.337 46.674 1.94446 22.5 3.9 3.8 5.7 73 1 7 -3 23.421 46.842 1.93789 6.3 1.1 1.1 5.7 74 2 8 0 23.537 47.074 1.92888 27.6 4.8 4.7 5.7 75 3 6 0 23.818 47.637 1.9074 32.0 5.5 5.4 5.7 76 0 1 5 23.996 47.992 1.8941 32.1 5.6 5.4 5.7 77 2 6 -3 24.081 48.162 1.88783 13.5 2.3 2.3 5.7 78 2 6 3 24.254 48.508 1.87514 17.0 2.9 2.9 5.7 79 3 6 1 24.365 48.73 1.86714 7.4 1.3 1.2 5.7 80 4 0 0 24.649 49.299 1.84691 65.0 11.2 10.9 5.7 81 0 8 3 24.72 49.439 1.84199 12.3 2.1 2.1 5.7 82 2 4 4 25.005 50.01 1.82229 6.4 1.1 1.1 5.7 83 0 10 0 25.196 50.391 1.8094 8.0 1.4 1.3 5.8 84 1 8 -3 25.488 50.976 1.79 13.5 2.3 2.3 5.8 85 3 7 0 25.596 51.192 1.78296 6.3 1.1 1.1 5.8 86 0 10 1 25.679 51.358 1.7776 41.5 7.2 7.0 5.8 87 1 3 -5 25.828 51.656 1.76802 20.0 3.5 3.4 5.8 88 1 10 0 25.995 51.99 1.75746 11.0 1.9 1.8 5.8 89 3 7 1 26.115 52.23 1.74994 8.5 1.5 1.4 5.8 90 4 3 -1 26.281 52.561 1.7397 10.3 1.8 1.7 5.8 91 4 3 1 26.389 52.778 1.73305 8.6 1.5 1.4 5.8 92 4 4 0 26.775 53.55 1.70988 10.3 1.8 1.7 5.8 93 3 1 4 27.035 54.07 1.69466 6.4 1.1 1.1 5.8 94 0 5 5 27.196 54.392 1.68539 11.5 2.0 1.9 5.8 95 4 4 1 27.291 54.583 1.67995 6.8 1.2 1.1 5.8 96 2 6 -4 27.409 54.817 1.67331 22.2 3.8 3.7 5.8 97 2 6 4 27.619 55.239 1.66153 17.4 3.0 2.9 5.8 98 1 5 5 28.02 56.04 1.63967 7.6 1.3 1.3 5.8 99 4 5 -1 28.319 56.638 1.62375 8.2 1.4 1.4 5.8 100 0 11 1 28.373 56.747 1.62091 8.5 1.5 1.4 5.8 101 2 10 -1 28.718 57.436 1.60308 7.4 1.3 1.2 5.8 102 2 10 1 28.769 57.539 1.60047 7.4 1.3 1.2 5.8 103 4 1 -3 28.82 57.64 1.5979 8.1 1.4 1.3 5.8 104 4 1 3 29.126 58.251 1.58258 8.8 1.5 1.5 5.8 105 0 1 6 29.156 58.312 1.58106 17.9 3.1 3.0 5.8 106 4 5 -2 29.596 59.191 1.55966 6.8 1.2 1.1 5.8 107 4 6 -1 29.666 59.333 1.55628 9.3 1.6 1.5 5.8 108 0 11 2 29.699 59.397 1.55475 22.0 3.8 3.7 5.8 109 4 5 2 29.796 59.593 1.55011 13.4 2.3 2.2 5.8 Reference: Chichagov A.V. et al. Information-Calculating System on Crystal Structure Data of Minerals (MINCRYST) - Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian) |