Institute of Experimental Mineralogy Russian Academy of Sciences ------------------------------------------------- 142432, Chernogolovka, Moscow district A.V. Chichagov +7(496)52-22320 *** *** W W W - X R A Y P O L *** *********************** LOMONOSOVITE 3, beta, td-lomonosovite, f-murmanite-lomonosovite, DF (Ti,Fe)(2)NaO(4)(Ti,Nb,Mn)(2)(Na,Ca,K)(2)[Si(2)O(7)](2)Na(3)[H(2)PO(4)](2) Triclinic P 1(-) Z = 2 R =0.087 NR =1640 13 .3 .1992 Ref.Str.: Rastsvetaeva R.K. (1986) * Kristallogr., (SSSR), 31, 1070-176 Initial data from BDM-file Lattice parameters (cub. angs.,degr.): a = 5.326 alpha = 102.2 b = 14.184 beta = 95.5 c = 14.47 gamma = 90.17 Unit cell volume (cub. angs.) = 1063.21 Molar volume ( cub.cm/mol.) = 320.21 Co-ordinates, thermal parameters, occupation for atomic positions: NoP x/a y/b z/c B(j) atom / occupation 1 0.2311 0.3089 0.0065 1.42 Ti = 1.00 2 0.751 0.1859 0.9922 1.55 Ti = 1.00 3 0.1526 0.4726 0.2203 0.8 Ti = 1.00 4 0.8496 0.029 0.7789 1.13 Ti = 1.00 5 0.6333 0.3269 0.198 1.28 Si = 1.00 6 0.3534 0.174 0.7975 1.99 Si = 1.00 7 0.6502 0.109 0.1813 1.33 Si = 1.00 8 0.3455 0.3899 0.8168 2.59 Si = 1.00 9 0.269 0.1239 0.4448 2.35 P = 0.6 , P = 0.0 10 0.8408 0.3812 0.558 2.63 P = 1.00 11 0.138 0.122 0.435 3.0 P = 0.2 , P = 0.0 12 0.225 0.057 0.01 2.17 Na = 0.6 , Na = 0.0 13 0.782 0.45 0.986 3.21 Na = 0.5 , Na = 0.0 14 0.159 0.234 0.258 2.45 Na = 0.6 , Na = 0.0 15 0.847 0.273 0.745 2.6 Na = 0.6 , Na = 0.0 16 0.79 0.145 0.608 1.79 Na = 0.3 , Na = 0.0 17 0.356 0.51 0.624 2.85 Na = 0.8 , Na = 0.0 18 0.271 0.009 0.628 3.77 Na = 0.7 , Na = 0.0 19 0.236 0.36 0.396 2.91 Na = 0.4 , Na = 0.0 20 0.588 0.242 0.397 4.0 Na = 0.2 , Na = 0.0 21 0.337 0.27 0.602 4.94 Na = 0.2 , Na = 0.0 22 0.901 0.279 0.929 2.3 O = 1.00 23 0.613 0.099 0.071 2.69 O = 1.00 24 0.369 0.397 0.936 3.97 O = 1.00 25 0.136 0.422 0.092 2.64 O = 1.00 26 0.866 0.085 0.909 2.36 O = 1.00 27 0.365 0.077 0.212 3.45 O = 1.00 28 0.554 0.449 0.782 3.8 O = 1.00 29 0.679 0.223 0.229 3.32 O = 1.00 30 0.361 0.276 0.765 2.37 O = 1.00 31 0.392 0.376 0.249 2.94 O = 1.00 32 0.566 0.112 0.749 2.57 O = 1.00 33 0.868 0.053 0.217 2.52 O = 1.00 34 0.058 0.421 0.787 3.15 O = 1.00 35 0.879 0.395 0.246 3.02 O = 1.00 36 0.08 0.125 0.759 2.53 O = 1.00 37 0.186 0.027 0.372 2.68 O = 1.00 38 0.794 0.468 0.626 4.95 O = 1.00 39 0.577 0.3 0.082 2.36 O = 1.00 40 0.801 0.296 0.6 6.71 O = 0.95, O = 0.0 41 0.566 0.118 0.461 2.45 O = 0.4 , O = 0.0 42 0.119 0.375 0.54 7.69 O = 1.00 43 0.665 0.384 0.466 4.98 O = 0.8 , O = 0.0 44 0.166 0.126 0.537 4.93 O = 0.85, O = 0.0 45 0.244 0.22 0.415 4.13 O = 0.9 , O = 0.0 46 0.41 0.193 0.916 2.57 O = 1.00 47 0.073 0.211 0.071 1.87 O = 1.00 48 0.892 0.121 0.471 3.04 O = 0.2 , O = 0.0 49 0.343 0.098 0.531 5.0 O = 0.2 , O = 0.0 Co-ordinates for all atomic positions : No NoP x/a y/b z/c 1 1 0.2311 0.3089 0.0065 2 2 0.751 0.1859 0.9922 3 3 0.1526 0.4726 0.2203 4 4 0.8496 0.029 0.7789 5 5 0.6333 0.3269 0.198 6 6 0.3534 0.174 0.7975 7 7 0.6502 0.109 0.1813 8 8 0.3455 0.3899 0.8168 9 9 0.269 0.1239 0.4448 10 10 0.8408 0.3812 0.558 11 11 0.138 0.122 0.435 12 12 0.225 0.057 0.01 13 13 0.782 0.45 0.986 14 14 0.159 0.234 0.258 15 15 0.847 0.273 0.745 16 16 0.79 0.145 0.608 17 17 0.356 0.51 0.624 18 18 0.271 0.009 0.628 19 19 0.236 0.36 0.396 20 20 0.588 0.242 0.397 21 21 0.337 0.27 0.602 22 22 0.901 0.279 0.929 23 23 0.613 0.099 0.071 24 24 0.369 0.397 0.936 25 25 0.136 0.422 0.092 26 26 0.866 0.085 0.909 27 27 0.365 0.077 0.212 28 28 0.554 0.449 0.782 29 29 0.679 0.223 0.229 30 30 0.361 0.276 0.765 31 31 0.392 0.376 0.249 32 32 0.566 0.112 0.749 33 33 0.868 0.053 0.217 34 34 0.058 0.421 0.787 35 35 0.879 0.395 0.246 36 36 0.08 0.125 0.759 37 37 0.186 0.027 0.372 38 38 0.794 0.468 0.626 39 39 0.577 0.3 0.082 40 40 0.801 0.296 0.6 41 41 0.566 0.118 0.461 42 42 0.119 0.375 0.54 43 43 0.665 0.384 0.466 44 44 0.166 0.126 0.537 45 45 0.244 0.22 0.415 46 46 0.41 0.193 0.916 47 47 0.073 0.211 0.071 48 48 0.892 0.121 0.471 49 49 0.343 0.098 0.531 50 1 0.7689 0.6911 0.9935 51 2 0.249 0.8141 0.0078 52 3 0.8474 0.5274 0.7797 53 4 0.1504 0.971 0.2211 54 5 0.3667 0.6731 0.802 55 6 0.6466 0.826 0.2025 56 7 0.3498 0.891 0.8187 57 8 0.6545 0.6101 0.1832 58 9 0.731 0.8761 0.5552 59 10 0.1592 0.6188 0.442 60 11 0.862 0.878 0.565 61 12 0.775 0.943 0.99 62 13 0.218 0.55 0.014 63 14 0.841 0.766 0.742 64 15 0.153 0.727 0.255 65 16 0.21 0.855 0.392 66 17 0.644 0.49 0.376 67 18 0.729 0.991 0.372 68 19 0.764 0.64 0.604 69 20 0.412 0.758 0.603 70 21 0.663 0.73 0.398 71 22 0.099 0.721 0.071 72 23 0.387 0.901 0.929 73 24 0.631 0.603 0.064 74 25 0.864 0.578 0.908 75 26 0.134 0.915 0.091 76 27 0.635 0.923 0.788 77 28 0.446 0.551 0.218 78 29 0.321 0.777 0.771 79 30 0.639 0.724 0.235 80 31 0.608 0.624 0.751 81 32 0.434 0.888 0.251 82 33 0.132 0.947 0.783 83 34 0.942 0.579 0.213 84 35 0.121 0.605 0.754 85 36 0.92 0.875 0.241 86 37 0.814 0.973 0.628 87 38 0.206 0.532 0.374 88 39 0.423 0.7 0.918 89 40 0.199 0.704 0.4 90 41 0.434 0.882 0.539 91 42 0.881 0.625 0.46 92 43 0.335 0.616 0.534 93 44 0.834 0.874 0.463 94 45 0.756 0.78 0.585 95 46 0.59 0.807 0.084 96 47 0.927 0.789 0.929 97 48 0.108 0.879 0.529 98 49 0.657 0.902 0.469 X-ray density (g/cm cub.) = 2.74 MU (1/cm) = 275.707 Mass attenuation coefficient (cm**2/g) = 100.663 Selected interatomic distances (cation-anion,anion-anion): NoP Atom Rad.sph. C.N. Distance NoP N. (angs.) (angs.) 1 Ti 2.568 6 1.9862 22 1.9541 24 1.9097 25 2.0682 39 2.1596 46 2.0493 47 2 Ti 2.568 6 1.9653 22 2.027 23 1.8141 26 2.1254 39 2.0466 46 1.954 47 3 Ti 2.568 6 1.837 25 1.9557 31 1.9341 35 1.9222 28 1.8978 34 2.196 38 4 Ti 2.568 6 1.8758 26 1.9888 32 1.9148 36 1.92 27 1.9081 33 2.1497 37 5 Si 2.1 4 1.641 29 1.6282 31 1.6317 35 1.6386 39 6 Si 2.1 4 1.6146 30 1.5638 32 1.6089 36 1.6759 46 7 Si 2.1 4 1.5653 23 1.7091 27 1.619 29 1.519 33 8 Si 2.1 4 1.6988 24 1.5715 28 1.6369 30 1.638 34 9 P ,P 2.232 6 1.5778 37 1.5818 41 1.485 44 1.5166 45 2.0807 48 1.3951 49 10 P 2.232 4 1.4432 38 1.486 40 1.5284 42 1.5602 43 11 P ,P 2.232 5 1.4965 37 1.4582 44 1.591 45 1.4567 48 1.7745 49 12 Na ,Na 2.808 5 2.1966 23 2.3798 26 2.3534 47 2.4745 23 2.6012 26 13 Na ,Na 2.808 5 2.4957 22 2.32 24 2.4026 25 2.404 24 2.391 25 14 Na ,Na 2.808 6 2.4767 27 2.5496 29 2.396 31 2.7581 35 2.3237 45 2.6508 47 15 Na ,Na 2.808 7 2.6336 22 2.7243 30 2.6315 30 2.7405 32 2.3141 34 2.4769 36 2.1817 40 16 Na ,Na 2.808 8 2.583 32 2.6187 36 2.1701 40 2.2937 41 2.3279 44 2.0648 48 2.5538 49 2.519 37 17 Na ,Na 2.808 6 2.7326 28 2.4084 38 2.3335 42 2.46 31 2.5121 35 2.184 43 18 Na ,Na 2.808 8 2.459 32 2.5291 36 2.364 44 2.1354 49 2.7386 33 2.4855 37 2.2136 41 2.2003 48 19 Na ,Na 2.808 5 2.41 31 2.1995 42 2.4018 43 2.0615 45 2.5297 38 20 Na ,Na 2.808 5 2.4833 29 2.1617 41 2.0709 43 1.909 45 2.6785 48 21 Na ,Na 2.808 6 2.3332 30 2.5014 40 2.1786 42 2.2133 44 2.6458 45 2.4405 49 22 O 3.264 8 2.9799 24 2.9395 25 2.7093 26 3.15 36 2.9025 39 2.9821 46 2.8551 46 2.5443 47 23 O 3.264 8 2.7858 26 2.6054 27 2.5665 29 2.6022 33 2.8298 39 2.9639 46 2.916 47 3.2596 23 24 O 3.264 7 2.9799 22 2.6387 25 2.7553 28 2.6934 30 2.6715 34 2.8935 39 2.8576 46 25 O 3.264 8 2.9395 22 2.6387 24 2.7356 31 2.8157 35 2.9181 39 2.9584 47 2.719 28 2.7937 34 26 O 3.264 9 2.7093 22 2.7858 23 2.7801 32 2.7061 36 3.2563 46 2.8738 46 2.7617 47 2.7801 27 2.8576 33 27 O 3.264 7 2.6054 23 2.6136 29 2.6975 33 2.6776 33 2.808 37 2.7801 26 2.8715 32 28 O 3.264 8 2.7553 24 2.6115 30 2.711 34 2.6803 34 2.7587 38 2.719 25 2.6337 31 3.2571 35 29 O 3.264 7 2.5665 23 2.6136 27 2.6399 31 2.594 33 2.613 35 2.6031 39 3.2275 47 30 O 3.264 6 2.6934 24 2.6115 28 2.5481 32 2.6033 34 2.5908 36 2.6847 46 31 O 3.264 7 2.7356 25 2.6399 29 2.6124 35 2.7434 35 2.7081 39 2.6337 28 2.7953 38 32 O 3.264 8 2.7801 26 2.5481 30 2.7311 36 2.6112 36 2.6584 46 3.2274 49 2.8715 27 2.7744 37 33 O 3.264 7 2.6022 23 2.6776 27 2.6975 27 2.594 29 2.7677 37 2.8576 26 2.6321 36 34 O 3.264 8 2.6715 24 2.6803 28 2.711 28 2.6033 30 2.8076 38 3.0963 40 2.7937 25 2.7756 35 35 O 3.264 8 2.8157 25 2.613 29 2.7434 31 2.6124 31 2.8175 39 3.2571 28 2.7756 34 2.8426 38 36 O 3.264 8 3.15 22 2.7061 26 2.5908 30 2.6112 32 2.7311 32 2.7347 46 2.6321 33 2.8264 37 37 O 3.264 9 2.808 27 2.7677 33 2.4906 41 2.5132 44 2.686 45 2.4324 48 2.3777 49 2.7744 32 2.8264 36 38 O 3.264 7 2.7587 28 2.8076 34 2.3896 40 2.4531 42 2.4034 43 2.7953 31 2.8426 35 39 O 3.264 10 2.9025 22 2.8298 23 2.8935 24 2.9181 25 2.6031 29 2.7081 31 2.8175 35 2.6279 46 2.9348 47 2.939 47 40 O ,O 3.264 7 3.0963 34 2.3896 38 3.0559 41 2.3579 42 2.5693 43 3.1405 44 2.8465 48 41 O ,O 3.264 7 2.4906 37 3.0559 40 2.4817 44 2.3833 45 1.7281 48 1.6933 49 3.1277 49 42 O 3.264 5 2.4531 38 2.3579 40 3.205 43 2.5638 43 2.6659 45 43 O ,O 3.264 5 2.4034 38 2.5693 40 2.5638 42 3.205 42 3.148 45 44 O ,O 3.264 6 2.5132 37 3.1405 40 2.4817 41 2.4897 45 1.6584 48 1.0282 49 45 O ,O 3.264 7 2.686 37 2.3833 41 2.6659 42 3.148 43 2.4897 44 2.6267 48 2.6746 49 46 O 3.264 11 2.8551 22 2.9821 22 2.9639 23 2.8576 24 2.8738 26 3.2563 26 2.6847 30 2.6584 32 2.7347 36 2.6279 39 2.9748 47 47 O 3.264 8 2.5443 22 2.916 23 2.9584 25 2.7617 26 3.2275 29 2.939 39 2.9348 39 2.9748 46 48 O ,O 3.264 7 2.4324 37 2.8465 40 1.7281 41 1.6584 44 2.6267 45 2.5208 49 3.1639 49 49 O ,O 3.264 9 3.2274 32 2.3777 37 1.6933 41 1.0282 44 2.6746 45 3.1639 48 2.5208 48 3.1277 41 3.2545 49 X-ray diffraction powder data (II), X-Ray W.L. = 1.78892(angs.): No H K L Theta 2*Theta S LPG MF F I int. ( degree ) *100 1 0 0 1 3.644 7.288 0.036 492.18 2 103.5 933.3 2 0 1 0 3.7 7.4 0.036 477.21 2 8.1 5.5 3 0 -1 1 4.61 9.22 0.045 306.61 2 8.9 4.3 4 0 1 1 5.724 11.448 0.056 198.08 2 20.2 14.2 5 0 0 2 7.302 14.605 0.071 120.84 2 51.7 57.1 6 0 2 0 7.416 14.832 0.072 117.09 2 12.8 3.4 7 0 -1 2 7.455 14.91 0.073 115.86 2 4.8 0.5 8 0 -2 1 7.538 15.077 0.073 113.25 2 75.3 113.6 9 0 1 2 8.876 17.753 0.086 81.07 2 8.0 0.9 10 0 2 1 8.947 17.894 0.087 79.76 2 54.2 41.5 11 0 -2 2 9.25 18.501 0.09 74.47 2 136.8 246.6 12 1 0 0 9.716 19.432 0.094 67.3 2 10.7 1.4 13 -1 0 1 10.042 20.084 0.097 62.87 2 8.5 0.8 14 -1 1 0 10.326 20.651 0.1 59.34 2 8.0 0.7 15 1 1 0 10.493 20.986 0.102 57.39 2 14.7 2.2 16 -1 -1 1 10.522 21.043 0.102 57.07 2 9.8 1.0 17 1 0 1 10.726 21.452 0.104 54.84 2 44.4 19.2 18 0 -1 3 10.827 21.654 0.105 53.78 2 0.9 0.0 19 -1 1 1 10.906 21.811 0.106 52.98 2 5.5 0.3 20 0 -3 1 10.982 21.965 0.106 52.21 2 12.4 1.4 21 0 0 3 10.991 21.983 0.107 52.12 2 65.0 38.9 22 1 -1 1 11.02 22.04 0.107 51.84 2 14.0 1.8 23 0 3 0 11.164 22.327 0.108 50.46 2 1.1 0.0 24 0 2 2 11.506 23.013 0.112 47.37 2 76.9 49.5 25 -1 0 2 11.596 23.192 0.112 46.61 2 37.8 11.8 26 1 1 1 11.692 23.384 0.113 45.82 2 27.5 6.1 27 -1 -1 2 11.769 23.538 0.114 45.19 2 0.5 0.0 28 0 -2 3 11.904 23.808 0.115 44.12 2 19.0 2.8 29 0 -3 2 11.993 23.986 0.116 43.44 2 7.9 0.5 30 -1 2 0 12.123 24.245 0.117 42.47 2 18.5 2.6 31 -1 -2 1 12.194 24.388 0.118 41.95 2 182.4 246.9 32 0 1 3 12.35 24.701 0.12 40.85 2 5.0 0.2 33 1 2 0 12.41 24.819 0.12 40.44 2 83.3 49.7 34 0 3 1 12.488 24.975 0.121 39.91 2 8.5 0.5 35 1 -2 1 12.49 24.98 0.121 39.89 2 173.7 212.9 36 -1 1 2 12.593 25.187 0.122 39.21 2 15.6 1.7 37 1 0 2 12.772 25.544 0.124 38.06 2 84.2 47.7 38 1 -1 2 12.793 25.586 0.124 37.93 2 3.5 0.1 39 -1 2 1 12.857 25.713 0.124 37.53 2 34.2 7.8 40 -1 -2 2 13.068 26.137 0.126 36.26 2 46.4 13.8 41 1 2 1 13.667 27.334 0.132 32.98 2 75.3 33.1 42 1 1 2 13.818 27.636 0.134 32.22 2 28.6 4.7 43 1 -2 2 13.876 27.753 0.134 31.93 2 129.3 94.4 44 -1 -1 3 13.928 27.855 0.135 31.68 2 8.3 0.4 45 0 -3 3 13.953 27.906 0.135 31.56 2 6.2 0.2 46 -1 0 3 13.995 27.989 0.135 31.36 2 64.1 22.8 47 0 -1 4 14.396 28.792 0.139 29.53 2 5.0 0.1 48 -1 2 2 14.537 29.073 0.14 28.92 2 39.9 8.2 49 0 2 3 14.592 29.185 0.141 28.69 2 121.3 74.7 50 0 -4 1 14.619 29.239 0.141 28.58 2 46.7 11.0 51 0 3 2 14.666 29.332 0.142 28.38 2 7.4 0.3 52 -1 -3 1 14.679 29.359 0.142 28.33 2 27.4 3.8 53 -1 3 0 14.702 29.403 0.142 28.23 2 20.2 2.0 54 0 0 4 14.727 29.454 0.142 28.13 2 181.1 163.2 55 1 -3 1 14.809 29.618 0.143 27.8 2 18.2 1.6 56 -1 -2 3 14.854 29.708 0.143 27.62 2 63.5 19.7 57 0 4 0 14.96 29.92 0.144 27.2 2 46.2 10.3 58 0 -2 4 15.04 30.079 0.145 26.89 2 88.4 37.2 59 -1 1 3 15.042 30.085 0.145 26.88 2 23.6 2.7 60 1 3 0 15.062 30.123 0.145 26.81 2 20.0 1.9 61 0 -4 2 15.212 30.423 0.147 26.25 2 18.5 1.6 62 -1 -3 2 15.227 30.455 0.147 26.19 2 4.2 0.1 63 1 -1 3 15.297 30.593 0.147 25.93 2 11.7 0.6 64 1 0 3 15.474 30.949 0.149 25.3 2 18.9 1.6 65 -1 3 1 15.516 31.032 0.15 25.15 2 0.0 0.0 66 1 2 2 15.736 31.471 0.152 24.4 2 70.2 21.3 67 1 -3 2 15.822 31.643 0.152 24.12 2 17.9 1.4 68 0 1 4 15.977 31.954 0.154 23.61 2 2.3 0.0 69 1 -2 3 16.04 32.079 0.154 23.41 2 10.6 0.5 70 0 4 1 16.181 32.361 0.156 22.98 2 5.5 0.1 71 1 3 1 16.315 32.63 0.157 22.57 2 9.8 0.4 72 1 1 3 16.546 33.092 0.159 21.89 2 32.3 4.0 73 0 -3 4 16.554 33.109 0.159 21.87 2 6.2 0.2 74 -1 -3 3 16.622 33.245 0.16 21.67 2 9.0 0.3 75 0 -4 3 16.647 33.293 0.16 21.6 2 115.1 50.7 76 -1 -1 4 16.676 33.352 0.16 21.52 2 12.8 0.6 77 -1 2 3 16.906 33.812 0.163 20.89 2 153.7 87.4 78 -1 0 4 16.913 33.827 0.163 20.87 2 57.0 12.0 79 -1 3 2 17.134 34.268 0.165 20.29 2 4.6 0.1 80 -1 -2 4 17.295 34.591 0.166 19.88 2 5.5 0.1 81 0 3 3 17.411 34.821 0.167 19.59 2 9.9 0.3 82 1 -3 3 17.599 35.198 0.169 19.14 2 11.6 0.5 83 -1 -4 1 17.671 35.343 0.17 18.97 2 28.5 2.7 84 1 -4 1 17.679 35.358 0.17 18.95 2 75.6 19.2 85 -1 4 0 17.76 35.52 0.171 18.76 2 32.3 3.5 86 -1 -4 2 17.969 35.938 0.172 18.29 2 180.5 105.5 87 0 2 4 17.975 35.95 0.173 18.27 2 25.3 2.1 88 -1 1 4 17.977 35.954 0.173 18.27 2 21.0 1.4 89 0 -1 5 18.09 36.181 0.174 18.02 2 14.7 0.7 90 0 4 2 18.122 36.244 0.174 17.95 2 93.4 27.7 91 1 4 0 18.166 36.332 0.174 17.85 2 64.2 13.0 92 1 -1 4 18.267 36.534 0.175 17.64 2 22.9 1.6 93 1 3 2 18.28 36.56 0.175 17.61 2 3.6 0.0 94 1 2 3 18.373 36.745 0.176 17.42 2 44.5 6.1 95 0 -5 1 18.382 36.764 0.176 17.4 2 0.3 0.0 96 1 -4 2 18.385 36.771 0.176 17.39 2 75.9 17.7 97 0 -2 5 18.454 36.908 0.177 17.25 2 24.5 1.8 98 0 0 5 18.528 37.056 0.178 17.1 2 245.3 182.1 99 1 0 4 18.585 37.17 0.178 16.98 2 5.7 0.1 100 -1 4 1 18.619 37.239 0.178 16.91 2 199.7 119.3 101 -1 -3 4 18.697 37.393 0.179 16.76 2 19.5 1.1 102 0 -5 2 18.705 37.409 0.179 16.74 2 0.8 0.0 103 1 -2 4 18.743 37.485 0.18 16.67 2 37.9 4.2 104 0 -4 4 18.754 37.507 0.18 16.65 2 53.0 8.3 105 0 5 0 18.825 37.651 0.18 16.51 2 4.2 0.1 106 -1 -4 3 19.026 38.052 0.182 16.13 2 219.9 138.0 107 -1 3 3 19.379 38.758 0.185 15.48 2 12.0 0.4 108 1 4 1 19.4 38.8 0.186 15.45 2 39.4 4.2 109 0 -3 5 19.58 39.159 0.187 15.13 2 7.2 0.1 110 1 1 4 19.664 39.328 0.188 14.99 2 40.8 4.4 111 -2 0 1 19.709 39.418 0.189 14.91 2 157.2 65.2 112 0 1 5 19.72 39.441 0.189 14.89 2 3.3 0.0 113 2 0 0 19.727 39.453 0.189 14.88 2 164.3 71.1 114 -1 2 4 19.752 39.504 0.189 14.84 2 42.6 4.8 115 0 -5 3 19.762 39.523 0.189 14.83 2 3.7 0.0 116 1 -4 3 19.807 39.614 0.189 14.75 2 154.2 62.1 117 -1 -1 5 19.808 39.617 0.189 14.75 2 10.5 0.3 118 1 -3 4 19.964 39.928 0.191 14.49 2 17.1 0.7 119 0 5 1 19.992 39.983 0.191 14.45 2 17.6 0.8 120 -2 1 0 20.007 40.014 0.191 14.42 2 17.8 0.8 121 -2 -1 1 20.019 40.039 0.191 14.4 2 28.5 2.1 122 -2 1 1 20.144 40.289 0.193 14.21 2 3.7 0.0 123 -1 0 5 20.168 40.336 0.193 14.17 2 61.4 9.4 124 -1 4 2 20.172 40.344 0.193 14.16 2 202.9 103.2 125 -1 -2 5 20.191 40.383 0.193 14.13 2 99.5 24.7 126 2 1 0 20.191 40.383 0.193 14.13 2 12.7 0.4 127 -2 0 2 20.41 40.82 0.195 13.8 2 1.0 0.0 128 2 0 1 20.461 40.923 0.195 13.72 2 163.7 65.0 129 0 3 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36.14 72.28 0.33 3.89 2 6.0 0.0 646 -1 -8 6 36.163 72.326 0.33 3.89 2 82.7 4.7 647 -3 3 4 36.229 72.457 0.33 3.87 2 11.9 0.1 648 1 2 8 36.242 72.485 0.33 3.87 2 97.7 6.5 649 1 -9 2 36.281 72.562 0.331 3.86 2 14.3 0.1 650 2 6 3 36.304 72.609 0.331 3.86 2 17.3 0.2 651 -1 -9 2 36.335 72.669 0.331 3.85 2 16.6 0.2 652 3 -4 3 36.345 72.689 0.331 3.85 2 38.7 1.0 653 1 -9 1 36.369 72.738 0.331 3.84 2 10.4 0.1 654 -3 5 0 36.431 72.862 0.332 3.83 2 7.1 0.0 655 0 -5 9 36.44 72.88 0.332 3.83 2 6.2 0.0 656 -2 3 7 36.462 72.925 0.332 3.82 2 8.0 0.0 657 -1 -9 3 36.478 72.955 0.332 3.82 2 3.9 0.0 658 -2 -4 8 36.484 72.968 0.332 3.82 2 93.7 5.9 659 -3 -5 2 36.528 73.056 0.333 3.81 2 8.2 0.0 660 3 -5 1 36.531 73.063 0.333 3.81 2 2.4 0.0 661 -3 4 3 36.569 73.138 0.333 3.8 2 35.1 0.8 662 2 -4 7 36.579 73.158 0.333 3.8 2 99.5 6.7 663 -2 1 8 36.609 73.217 0.333 3.8 2 4.3 0.0 664 -1 1 9 36.627 73.253 0.333 3.79 2 1.3 0.0 665 1 -7 7 36.643 73.287 0.334 3.79 2 1.2 0.0 666 -3 2 5 36.663 73.326 0.334 3.78 2 1.0 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76.126 0.345 3.53 2 4.0 0.0 732 -1 7 5 38.077 76.155 0.345 3.53 2 19.9 0.2 733 -2 -8 4 38.097 76.195 0.345 3.53 2 47.3 1.4 734 0 4 8 38.112 76.225 0.345 3.53 2 50.9 1.6 735 -2 2 8 38.118 76.235 0.345 3.52 2 2.3 0.0 736 3 -5 3 38.17 76.339 0.345 3.52 2 22.4 0.3 737 -1 -9 5 38.201 76.401 0.346 3.51 2 9.1 0.1 738 0 -6 9 38.23 76.459 0.346 3.51 2 81.2 4.1 739 3 -1 5 38.231 76.463 0.346 3.51 2 21.3 0.3 740 -1 2 9 38.269 76.538 0.346 3.5 2 24.5 0.4 741 1 8 3 38.278 76.556 0.346 3.5 2 17.3 0.2 742 -3 4 4 38.284 76.569 0.346 3.5 2 57.9 2.1 743 -3 3 5 38.323 76.646 0.347 3.49 2 22.3 0.3 744 -1 -8 7 38.33 76.66 0.347 3.49 2 12.1 0.1 745 2 2 7 38.33 76.66 0.347 3.49 2 5.0 0.0 746 1 3 8 38.341 76.681 0.347 3.49 2 4.1 0.0 747 0 9 2 38.346 76.692 0.347 3.49 2 2.9 0.0 748 -2 5 6 38.361 76.723 0.347 3.49 2 6.1 0.0 749 3 -2 5 38.362 76.724 0.347 3.49 2 28.0 0.5 750 0 -2 10 38.392 76.784 0.347 3.48 2 37.0 0.8 751 -2 8 1 38.406 76.812 0.347 3.48 2 20.5 0.3 752 0 8 4 38.468 76.937 0.348 3.47 2 103.6 6.6 753 3 5 1 38.491 76.982 0.348 3.47 2 27.3 0.5 754 0 -9 6 38.563 77.126 0.348 3.45 2 3.5 0.0 755 2 8 0 38.575 77.151 0.349 3.45 2 117.0 8.4 756 2 5 5 38.587 77.173 0.349 3.45 2 2.6 0.0 757 0 -3 10 38.591 77.182 0.349 3.45 2 8.6 0.0 758 3 0 5 38.591 77.182 0.349 3.45 2 12.7 0.1 759 -2 6 5 38.631 77.261 0.349 3.44 2 118.9 8.6 760 -2 -2 9 38.665 77.33 0.349 3.44 2 85.2 4.4 761 -1 4 8 38.669 77.339 0.349 3.44 2 5.4 0.0 762 0 -1 10 38.682 77.365 0.349 3.44 2 5.5 0.0 763 1 9 1 38.785 77.57 0.35 3.42 2 10.8 0.1 764 -2 -1 9 38.792 77.583 0.35 3.42 2 9.6 0.1 765 2 -2 8 38.821 77.641 0.35 3.42 2 26.8 0.4 766 -2 4 7 38.851 77.703 0.351 3.41 2 2.8 0.0 767 2 6 4 38.852 77.705 0.351 3.41 2 75.6 3.4 768 -3 -5 5 38.873 77.747 0.351 3.41 2 8.7 0.0 769 -1 -2 10 38.882 77.765 0.351 3.41 2 106.9 6.9 770 1 -9 5 38.895 77.79 0.351 3.4 2 24.8 0.4 771 -3 -4 6 38.919 77.838 0.351 3.4 2 61.4 2.3 772 1 1 9 38.943 77.887 0.351 3.4 2 18.4 0.2 773 -1 -6 9 38.967 77.934 0.352 3.39 2 101.0 6.1 774 2 -1 8 38.967 77.934 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54.6 1.8 796 -2 0 9 39.406 78.811 0.355 3.33 2 112.2 7.4 797 0 -10 1 39.413 78.825 0.355 3.33 2 49.4 1.4 798 -3 -1 7 39.425 78.85 0.355 3.33 2 18.2 0.2 799 3 1 5 39.437 78.874 0.355 3.33 2 10.2 0.1 800 0 0 10 39.46 78.919 0.355 3.33 2 59.8 2.1 801 -1 9 2 39.493 78.986 0.356 3.32 2 7.1 0.0 802 3 -6 2 39.515 79.03 0.356 3.32 2 51.9 1.6 803 -3 6 1 39.528 79.056 0.356 3.32 2 32.0 0.6 804 -3 -2 7 39.533 79.065 0.356 3.32 2 34.2 0.7 805 3 4 3 39.556 79.112 0.356 3.31 2 104.5 6.4 806 1 -8 7 39.58 79.159 0.356 3.31 2 31.2 0.6 807 2 0 8 39.6 79.199 0.356 3.31 2 3.9 0.0 808 1 -7 8 39.623 79.246 0.356 3.3 2 10.2 0.1 809 -2 7 4 39.655 79.31 0.357 3.3 2 15.0 0.1 810 -2 8 2 39.684 79.369 0.357 3.3 2 91.2 4.9 811 3 -5 4 39.688 79.376 0.357 3.29 2 24.4 0.3 812 -2 -7 7 39.705 79.41 0.357 3.29 2 20.2 0.2 813 2 -7 6 39.716 79.433 0.357 3.29 2 9.5 0.1 814 1 7 5 39.745 79.491 0.357 3.29 2 9.5 0.1 815 1 5 7 39.755 79.511 0.357 3.29 2 22.3 0.3 816 -1 -9 6 39.76 79.52 0.358 3.29 2 21.9 0.3 817 3 3 4 39.784 79.568 0.358 3.28 2 21.1 0.3 818 -3 0 7 39.803 79.606 0.358 3.28 2 43.3 1.1 819 -1 -4 10 39.825 79.651 0.358 3.28 2 4.7 0.0 820 2 7 3 39.872 79.743 0.358 3.27 2 8.8 0.0 821 -2 -4 9 39.873 79.747 0.358 3.27 2 65.5 2.5 822 -2 -6 8 39.875 79.749 0.358 3.27 2 110.8 7.1 823 2 8 1 39.875 79.75 0.358 3.27 2 33.5 0.6 824 -1 0 10 39.886 79.771 0.358 3.27 2 61.5 2.2 825 0 -10 4 39.895 79.79 0.359 3.27 2 4.0 0.0 826 0 3 9 39.916 79.832 0.359 3.27 2 5.0 0.0 827 2 -6 7 39.928 79.856 0.359 3.26 2 64.9 2.4 828 2 -4 8 39.989 79.977 0.359 3.26 2 71.0 2.9 829 -3 -6 4 39.99 79.98 0.359 3.26 2 56.2 1.8 830 0 -8 8 40.016 80.032 0.359 3.25 2 13.3 0.1 831 3 5 2 40.081 80.161 0.36 3.24 2 2.4 0.0 832 3 -4 5 40.083 80.166 0.36 3.24 2 85.9 4.2 833 -2 3 8 40.093 80.185 0.36 3.24 2 9.9 0.1 834 -3 -3 7 40.125 80.251 0.36 3.24 2 1.2 0.0 835 3 6 0 40.143 80.286 0.36 3.24 2 40.6 0.9 836 0 10 0 40.193 80.386 0.361 3.23 2 66.8 2.6 837 2 3 7 40.322 80.643 0.362 3.22 2 1.2 0.0 838 -1 3 9 40.373 80.746 0.362 3.21 2 8.8 0.0 839 0 9 3 40.443 80.886 0.363 3.2 2 9.9 0.1 840 0 -5 10 40.445 80.89 0.363 3.2 2 3.4 0.0 841 -3 4 5 40.445 80.89 0.363 3.2 2 85.0 4.1 842 3 -6 3 40.451 80.902 0.363 3.2 2 9.5 0.1 843 0 6 7 40.46 80.92 0.363 3.2 2 61.0 2.1 844 -3 6 2 40.472 80.944 0.363 3.2 2 36.8 0.8 845 0 -7 9 40.477 80.953 0.363 3.2 2 1.6 0.0 846 -2 1 9 40.501 81.002 0.363 3.19 2 11.7 0.1 847 1 9 2 40.53 81.061 0.363 3.19 2 4.2 0.0 848 0 7 6 40.555 81.11 0.363 3.19 2 0.4 0.0 849 -3 -5 6 40.585 81.169 0.364 3.18 2 15.4 0.1 850 1 2 9 40.616 81.233 0.364 3.18 2 56.9 1.8 851 2 -8 5 40.661 81.322 0.364 3.18 2 9.0 0.0 852 -3 1 7 40.663 81.327 0.364 3.18 2 15.1 0.1 853 -2 -8 6 40.692 81.384 0.364 3.17 2 42.6 1.0 854 1 -9 6 40.693 81.385 0.364 3.17 2 2.9 0.0 855 1 -10 2 40.704 81.407 0.365 3.17 2 85.0 4.1 856 0 -9 7 40.71 81.421 0.365 3.17 2 10.1 0.1 857 2 1 8 40.713 81.426 0.365 3.17 2 9.1 0.0 858 0 1 10 40.716 81.432 0.365 3.17 2 6.6 0.0 859 3 2 5 40.762 81.523 0.365 3.16 2 65.6 2.4 860 -3 5 4 40.789 81.577 0.365 3.16 2 6.0 0.0 861 -1 -10 2 40.815 81.631 0.365 3.16 2 117.7 7.7 862 1 -6 9 40.823 81.645 0.365 3.16 2 143.9 11.6 863 -3 3 6 40.85 81.701 0.366 3.15 2 16.1 0.1 864 -1 -10 3 40.852 81.705 0.366 3.15 2 6.3 0.0 865 1 8 4 40.866 81.732 0.366 3.15 2 66.5 2.5 866 1 4 8 40.886 81.772 0.366 3.15 2 109.6 6.7 867 1 -10 1 40.889 81.778 0.366 3.15 2 25.8 0.4 868 -1 -8 8 40.927 81.854 0.366 3.15 2 13.0 0.1 869 1 -10 3 40.986 81.972 0.367 3.14 2 119.0 7.9 870 0 -10 5 40.992 81.985 0.367 3.14 2 7.9 0.0 871 -1 -5 10 41.019 82.038 0.367 3.14 2 16.0 0.1 872 -1 6 7 41.071 82.141 0.367 3.13 2 14.2 0.1 873 3 -1 6 41.092 82.183 0.367 3.13 2 25.2 0.4 874 -1 1 10 41.109 82.218 0.368 3.13 2 3.2 0.0 875 0 5 8 41.114 82.227 0.368 3.13 2 3.3 0.0 876 3 -2 6 41.119 82.238 0.368 3.13 2 43.6 1.1 877 -3 -6 5 41.123 82.246 0.368 3.12 2 30.1 0.5 878 -2 -5 9 41.198 82.395 0.368 3.12 2 8.7 0.0 879 -3 -4 7 41.198 82.396 0.368 3.12 2 61.5 2.1 880 1 -2 10 41.225 82.45 0.368 3.11 2 49.8 1.4 881 -1 -7 9 41.233 82.467 0.368 3.11 2 9.3 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0.4 925 -1 8 5 42.189 84.379 0.375 3.02 2 45.6 1.1 926 -4 0 1 42.204 84.409 0.376 3.02 2 82.7 3.7 927 -2 7 5 42.221 84.442 0.376 3.02 2 5.5 0.0 928 -3 -7 3 42.247 84.493 0.376 3.02 2 9.9 0.1 929 -2 -7 8 42.26 84.521 0.376 3.01 2 5.6 0.0 930 2 -7 7 42.294 84.588 0.376 3.01 2 2.7 0.0 931 2 2 8 42.3 84.6 0.376 3.01 2 39.3 0.8 932 -1 -10 5 42.325 84.649 0.376 3.01 2 37.8 0.8 933 1 0 10 42.335 84.671 0.376 3.01 2 90.7 4.4 934 3 -7 2 42.358 84.716 0.377 3.01 2 26.5 0.4 935 1 -8 8 42.402 84.803 0.377 3.0 2 19.4 0.2 936 -4 0 2 42.414 84.829 0.377 3.0 2 111.2 6.6 937 -4 1 1 42.425 84.85 0.377 3.0 2 16.7 0.1 938 0 2 10 42.444 84.887 0.377 3.0 2 11.4 0.1 939 2 7 4 42.458 84.915 0.377 3.0 2 3.4 0.0 940 4 0 0 42.459 84.919 0.377 3.0 2 86.7 4.0 941 -4 -1 1 42.463 84.927 0.377 3.0 2 4.3 0.0 942 -3 -1 8 42.464 84.928 0.377 3.0 2 26.0 0.4 943 -3 -2 8 42.47 84.94 0.377 3.0 2 26.3 0.4 944 3 1 6 42.478 84.957 0.377 3.0 2 7.3 0.0 945 0 4 9 42.509 85.018 0.378 2.99 2 25.6 0.3 946 -3 -7 1 42.523 85.046 0.378 2.99 2 12.4 0.1 947 -2 4 8 42.524 85.047 0.378 2.99 2 64.6 2.2 948 0 -10 6 42.549 85.098 0.378 2.99 2 8.5 0.0 949 3 3 5 42.556 85.112 0.378 2.99 2 23.7 0.3 950 -2 9 1 42.558 85.116 0.378 2.99 2 0.0 0.0 951 -4 -1 2 42.573 85.146 0.378 2.99 2 9.1 0.0 952 -4 1 0 42.579 85.159 0.378 2.99 2 27.3 0.4 953 3 -4 6 42.614 85.228 0.378 2.98 2 17.1 0.2 954 -1 10 1 42.656 85.313 0.379 2.98 2 17.2 0.2 955 2 -8 6 42.664 85.328 0.379 2.98 2 82.6 3.6 956 -2 -2 10 42.668 85.337 0.379 2.98 2 104.8 5.8 957 -3 7 1 42.671 85.343 0.379 2.98 2 4.4 0.0 958 -2 -8 7 42.672 85.345 0.379 2.98 2 14.8 0.1 959 -1 -6 10 42.685 85.37 0.379 2.98 2 45.0 1.1 960 -3 -6 6 42.715 85.429 0.379 2.98 2 33.9 0.6 961 1 9 3 42.724 85.447 0.379 2.98 2 20.1 0.2 962 -4 1 2 42.735 85.47 0.379 2.97 2 12.4 0.1 963 2 9 0 42.743 85.486 0.379 2.97 2 9.0 0.0 964 -3 -5 7 42.745 85.489 0.379 2.97 2 6.7 0.0 965 2 -9 4 42.747 85.494 0.379 2.97 2 8.7 0.0 966 1 3 9 42.753 85.507 0.379 2.97 2 2.9 0.0 967 2 4 7 42.77 85.539 0.38 2.97 2 85.7 3.9 968 -1 2 10 42.804 85.608 0.38 2.97 2 20.7 0.2 969 -3 -7 4 42.805 85.61 0.38 2.97 2 23.5 0.3 970 4 1 0 42.818 85.637 0.38 2.97 2 0.0 0.0 971 -2 -9 5 42.819 85.639 0.38 2.97 2 9.9 0.1 972 2 -2 9 42.843 85.686 0.38 2.97 2 29.4 0.5 973 -2 -1 10 42.893 85.785 0.38 2.96 2 27.1 0.4 974 -2 -3 10 42.923 85.845 0.381 2.96 2 1.2 0.0 975 -1 4 9 42.931 85.863 0.381 2.96 2 37.3 0.7 976 -3 0 8 42.937 85.874 0.381 2.96 2 71.8 2.7 977 1 -9 7 42.938 85.875 0.381 2.96 2 11.0 0.1 978 1 -10 5 42.944 85.888 0.381 2.96 2 48.1 1.2 979 -3 -3 8 42.955 85.91 0.381 2.96 2 2.8 0.0 980 0 9 4 42.98 85.959 0.381 2.96 2 7.3 0.0 981 -2 -6 9 42.992 85.985 0.381 2.95 2 19.0 0.2 982 1 -7 9 43.009 86.018 0.381 2.95 2 9.3 0.0 983 3 6 2 43.017 86.035 0.381 2.95 2 20.3 0.2 984 -3 5 5 43.021 86.041 0.381 2.95 2 1.2 0.0 985 -3 4 6 43.044 86.088 0.382 2.95 2 53.3 1.5 986 2 -6 8 43.068 86.135 0.382 2.95 2 18.3 0.2 987 2 -3 9 43.078 86.156 0.382 2.95 2 6.1 0.0 988 2 -1 9 43.087 86.174 0.382 2.95 2 12.2 0.1 989 -4 0 3 43.088 86.177 0.382 2.95 2 150.1 11.8 990 0 -2 11 43.109 86.218 0.382 2.95 2 74.6 2.9 991 -4 2 1 43.124 86.247 0.382 2.94 2 52.2 1.4 992 1 6 7 43.138 86.275 0.382 2.94 2 3.5 0.0 993 0 10 2 43.138 86.277 0.382 2.94 2 28.7 0.4 994 1 7 6 43.14 86.28 0.382 2.94 2 2.3 0.0 995 -4 -1 3 43.147 86.293 0.382 2.94 2 45.5 1.1 996 1 -5 10 43.159 86.318 0.382 2.94 2 9.7 0.0 997 0 -8 9 43.175 86.349 0.382 2.94 2 9.6 0.0 998 -4 2 0 43.178 86.355 0.383 2.94 2 33.1 0.6 999 4 0 1 43.178 86.356 0.383 2.94 2 81.2 3.4 1000 3 -7 3 43.182 86.364 0.383 2.94 2 23.4 0.3 1001 4 -1 1 43.198 86.396 0.383 2.94 2 32.6 0.6 1002 -4 -2 1 43.201 86.402 0.383 2.94 2 37.5 0.7 1003 0 -3 11 43.203 86.406 0.383 2.94 2 6.5 0.0 1004 -4 -2 2 43.21 86.42 0.383 2.94 2 6.1 0.0 1005 0 -9 8 43.297 86.595 0.383 2.93 2 5.6 0.0 1006 3 7 0 43.357 86.714 0.384 2.93 2 16.4 0.1 1007 -1 -2 11 43.467 86.933 0.385 2.92 2 9.1 0.0 1008 0 -1 11 43.493 86.985 0.385 2.92 2 3.6 0.0 1009 1 10 1 43.497 86.993 0.385 2.92 2 65.3 2.2 1010 -4 1 3 43.508 87.017 0.385 2.92 2 8.7 0.0 1011 -4 2 2 43.533 87.066 0.385 2.92 2 28.2 0.4 1012 -1 -3 11 43.591 87.181 0.385 2.91 2 4.3 0.0 1013 -2 0 10 43.595 87.19 0.385 2.91 2 65.1 2.2 1014 -2 8 4 43.605 87.21 0.386 2.91 2 2.8 0.0 1015 1 1 10 43.606 87.212 0.386 2.91 2 0.3 0.0 1016 4 1 1 43.637 87.273 0.386 2.91 2 6.9 0.0 1017 -2 -4 10 43.655 87.31 0.386 2.91 2 20.8 0.2 1018 4 2 0 43.655 87.31 0.386 2.91 2 39.4 0.8 1019 -4 -2 3 43.683 87.365 0.386 2.9 2 48.7 1.2 1020 4 -2 1 43.695 87.391 0.386 2.9 2 24.2 0.3 1021 3 -6 5 43.701 87.403 0.386 2.9 2 16.3 0.1 1022 -3 7 2 43.703 87.406 0.386 2.9 2 6.0 0.0 1023 -3 6 4 43.739 87.477 0.386 2.9 2 16.0 0.1 1024 -1 -10 6 43.753 87.507 0.387 2.9 2 69.4 2.5 1025 0 -4 11 43.775 87.551 0.387 2.9 2 6.7 0.0 1026 2 -4 9 43.791 87.582 0.387 2.9 2 110.0 6.2 1027 2 0 9 43.808 87.616 0.387 2.9 2 11.7 0.1 1028 -3 3 7 43.809 87.618 0.387 2.9 2 16.4 0.1 1029 -1 -1 11 43.82 87.641 0.387 2.9 2 1.7 0.0 1030 -3 -7 5 43.826 87.653 0.387 2.9 2 20.0 0.2 1031 2 8 3 43.837 87.675 0.387 2.89 2 21.6 0.2 1032 -1 9 4 43.86 87.719 0.387 2.89 2 6.3 0.0 1033 1 5 8 43.877 87.753 0.387 2.89 2 10.2 0.1 1034 1 8 5 43.883 87.767 0.387 2.89 2 7.8 0.0 1035 3 2 6 43.886 87.772 0.388 2.89 2 36.1 0.7 1036 -3 1 8 43.887 87.774 0.388 2.89 2 5.5 0.0 1037 -2 9 2 43.912 87.823 0.388 2.89 2 4.0 0.0 1038 -3 -4 8 43.917 87.834 0.388 2.89 2 20.7 0.2 1039 -1 -8 9 43.954 87.908 0.388 2.89 2 9.5 0.0 1040 0 -11 2 43.954 87.909 0.388 2.89 2 7.8 0.0 1041 0 -11 3 44.012 88.025 0.388 2.88 2 9.2 0.0 1042 3 -5 6 44.075 88.151 0.389 2.88 2 14.1 0.1 1043 -2 3 9 44.108 88.215 0.389 2.88 2 3.6 0.0 1044 2 9 1 44.119 88.237 0.389 2.88 2 26.7 0.4 1045 2 -9 5 44.175 88.351 0.39 2.87 2 13.7 0.1 1046 -4 -1 4 44.182 88.365 0.39 2.87 2 12.7 0.1 1047 -1 -4 11 44.192 88.384 0.39 2.87 2 23.8 0.3 1048 0 -7 10 44.193 88.386 0.39 2.87 2 6.6 0.0 1049 -4 0 4 44.224 88.449 0.39 2.87 2 49.8 1.3 1050 -2 -9 6 44.225 88.45 0.39 2.87 2 13.6 0.1 1051 -1 -9 8 44.228 88.456 0.39 2.87 2 1.6 0.0 1052 -1 10 2 44.231 88.462 0.39 2.87 2 115.3 6.8 1053 -4 3 0 44.253 88.506 0.39 2.87 2 10.1 0.1 1054 4 -1 2 44.279 88.557 0.39 2.87 2 3.6 0.0 1055 0 7 7 44.281 88.561 0.39 2.87 2 0.8 0.0 1056 -4 3 1 44.299 88.598 0.39 2.87 2 23.7 0.3 1057 3 -2 7 44.303 88.607 0.39 2.87 2 64.4 2.1 1058 -4 -3 2 44.324 88.647 0.391 2.86 2 6.9 0.0 1059 0 0 11 44.354 88.708 0.391 2.86 2 55.3 1.5 1060 2 3 8 44.356 88.712 0.391 2.86 2 18.2 0.2 1061 4 0 2 44.359 88.718 0.391 2.86 2 101.7 5.2 1062 0 -11 1 44.359 88.719 0.391 2.86 2 10.4 0.1 1063 3 -1 7 44.376 88.753 0.391 2.86 2 18.9 0.2 1064 -4 2 3 44.405 88.811 0.391 2.86 2 16.4 0.1 1065 -4 -3 1 44.414 88.829 0.391 2.86 2 12.5 0.1 1066 3 -7 4 44.468 88.935 0.392 2.86 2 8.3 0.0 1067 0 -11 4 44.533 89.067 0.392 2.85 2 1.0 0.0 1068 0 6 8 44.55 89.1 0.392 2.85 2 1.3 0.0 1069 0 -10 7 44.561 89.122 0.392 2.85 2 48.4 1.2 1070 4 2 1 44.572 89.144 0.392 2.85 2 7.8 0.0 1071 3 5 4 44.609 89.218 0.393 2.85 2 8.3 0.0 1072 1 -10 6 44.614 89.227 0.393 2.85 2 18.0 0.2 1073 -4 -2 4 44.618 89.236 0.393 2.85 2 47.0 1.1 1074 0 3 10 44.639 89.279 0.393 2.85 2 4.7 0.0 1075 -1 0 11 44.651 89.303 0.393 2.85 2 24.7 0.3 1076 3 7 1 44.653 89.306 0.393 2.85 2 8.2 0.0 1077 4 -3 1 44.67 89.34 0.393 2.85 2 23.7 0.3 1078 4 -2 2 44.675 89.351 0.393 2.85 2 1.1 0.0 1079 -4 -3 3 44.696 89.391 0.393 2.84 2 11.4 0.1 1080 3 -3 7 44.708 89.416 0.393 2.84 2 5.8 0.0 1081 -4 1 4 44.744 89.487 0.393 2.84 2 18.7 0.2 1082 0 8 6 44.752 89.504 0.394 2.84 2 16.8 0.1 1083 1 -6 10 44.756 89.513 0.394 2.84 2 82.9 3.5 1084 -3 -6 7 44.762 89.524 0.394 2.84 2 19.6 0.2 1085 -2 1 10 44.774 89.547 0.394 2.84 2 7.6 0.0 1086 -4 3 2 44.808 89.615 0.394 2.84 2 13.8 0.1 1087 3 4 5 44.819 89.637 0.394 2.84 2 26.2 0.3 1088 -1 -7 10 44.82 89.641 0.394 2.84 2 5.7 0.0 1089 0 -5 11 44.824 89.649 0.394 2.84 2 2.9 0.0 1090 -1 7 7 44.855 89.71 0.394 2.84 2 10.3 0.1 1091 -2 -5 10 44.863 89.727 0.394 2.84 2 9.0 0.0 1092 4 1 2 44.917 89.833 0.395 2.83 2 27.2 0.4 1093 3 0 7 44.926 89.853 0.395 2.83 2 16.8 0.1 1094 -2 6 7 44.951 89.902 0.395 2.83 2 12.8 0.1 1095 4 3 0 44.968 89.936 0.395 2.83 2 29.3 0.4 1096 -1 3 10 44.969 89.937 0.395 2.83 2 2.7 0.0 1097 2 -5 9 44.98 89.96 0.395 2.83 2 5.3 0.0 X-ray diffraction powder data (I)...X-Ray wave length = 1.78892 (angs.): No H K L Theta 2*Theta d I int I int.n. I p.h.n. H(Si) ( degree ) (angstrem) *100 *100 1 0 0 1 3.644 7.288 14.07415 933.3 100.0 100.0 5.5 2 0 1 1 5.724 11.448 8.968 14.2 1.5 1.5 5.6 3 0 0 2 7.302 14.605 7.03707 57.1 6.1 6.1 5.6 4 0 -2 1 7.538 15.077 6.81797 113.6 12.2 12.1 5.6 5 0 2 1 8.947 17.894 5.75139 41.5 4.4 4.4 5.6 6 0 -2 2 9.25 18.501 5.56429 246.6 26.4 26.2 5.6 7 1 0 1 10.726 21.452 4.80596 19.2 2.1 2.0 5.6 8 0 0 3 10.991 21.983 4.69138 40.4 4.3 4.3 5.6 9 0 2 2 11.506 23.013 4.484 49.5 5.3 5.3 5.6 10 -1 0 2 11.596 23.192 4.44989 11.8 1.3 1.3 5.6 11 -1 -2 1 12.194 24.388 4.23463 246.9 26.5 26.2 5.6 12 1 2 0 12.41 24.819 4.16221 49.7 5.3 5.3 5.6 13 1 -2 1 12.49 24.98 4.13593 212.9 22.8 22.6 5.6 14 1 0 2 12.772 25.544 4.046 47.8 5.1 5.1 5.6 15 -1 -2 2 13.068 26.137 3.95577 13.8 1.5 1.5 5.6 16 1 2 1 13.667 27.334 3.78566 33.1 3.5 3.5 5.6 17 1 -2 2 13.876 27.753 3.72958 94.4 10.1 10.0 5.6 18 -1 0 3 13.995 27.989 3.69872 22.8 2.4 2.4 5.6 19 0 2 3 14.592 29.185 3.55027 85.7 9.2 9.1 5.6 20 0 0 4 14.727 29.454 3.51854 163.2 17.5 17.2 5.6 21 -1 -2 3 14.854 29.708 3.48914 19.7 2.1 2.1 5.6 22 0 4 0 14.96 29.92 3.46493 10.3 1.1 1.1 5.6 23 0 -2 4 15.04 30.079 3.44703 41.7 4.5 4.4 5.6 24 1 2 2 15.736 31.471 3.29818 21.3 2.3 2.2 5.6 25 0 -4 3 16.647 33.293 3.12236 50.7 5.4 5.3 5.6 26 -1 2 3 16.906 33.812 3.07585 99.3 10.6 10.4 5.7 27 1 -4 1 17.679 35.358 2.94538 21.9 2.3 2.3 5.7 28 -1 -4 2 17.969 35.938 2.89938 109.0 11.7 11.4 5.7 29 0 4 2 18.122 36.244 2.87569 27.7 3.0 2.9 5.7 30 1 4 0 18.166 36.332 2.86896 13.0 1.4 1.4 5.7 31 1 -4 2 18.385 36.771 2.83589 23.8 2.6 2.5 5.7 32 0 0 5 18.528 37.056 2.81483 182.1 19.5 19.1 5.7 33 -1 4 1 18.619 37.239 2.80149 119.3 12.8 12.5 5.7 34 0 -4 4 18.754 37.507 2.78215 12.5 1.3 1.3 5.7 35 -1 -4 3 19.026 38.052 2.74376 138.0 14.8 14.5 5.7 36 2 0 0 19.727 39.453 2.64999 141.1 15.1 14.8 5.7 37 1 -4 3 19.807 39.614 2.6397 62.3 6.7 6.5 5.7 38 -1 -2 5 20.191 40.383 2.59147 137.8 14.8 14.4 5.7 39 2 0 1 20.461 40.923 2.55871 65.0 7.0 6.8 5.7 40 0 4 3 20.611 41.222 2.54094 12.7 1.4 1.3 5.7 41 1 4 2 21.265 42.531 2.46619 45.3 4.9 4.7 5.7 42 1 2 4 21.408 42.815 2.45056 19.9 2.1 2.1 5.7 43 2 0 2 21.853 43.706 2.40298 62.0 6.6 6.5 5.7 44 1 0 5 21.976 43.953 2.39016 12.5 1.3 1.3 5.7 45 0 0 6 22.415 44.831 2.34569 22.8 2.4 2.4 5.7 46 1 4 3 23.643 47.286 2.23036 14.3 1.5 1.5 5.7 47 -2 0 4 23.704 47.408 2.22495 10.6 1.1 1.1 5.7 48 2 0 3 23.811 47.621 2.21558 26.7 2.9 2.8 5.7 49 -2 -4 1 24.921 49.843 2.12272 10.3 1.1 1.1 5.7 50 1 -2 6 25.2 50.4 2.10078 18.6 2.0 1.9 5.8 51 1 -6 3 25.594 51.188 2.07056 12.1 1.3 1.2 5.8 52 -2 -4 3 25.655 51.31 2.06595 55.9 6.0 5.8 5.8 53 -1 -4 6 25.699 51.399 2.06264 10.4 1.1 1.1 5.8 54 -2 0 5 26.113 52.227 2.03217 13.1 1.4 1.3 5.8 55 -1 -6 4 26.266 52.532 2.02119 38.6 4.1 4.0 5.8 56 0 0 7 26.415 52.831 2.01059 23.3 2.5 2.4 5.8 57 0 -6 5 26.465 52.929 2.00712 10.3 1.1 1.1 5.8 58 2 4 1 26.563 53.127 2.00019 11.2 1.2 1.2 5.8 59 -1 4 5 27.855 55.71 1.91437 15.4 1.6 1.6 5.8 60 -1 -4 7 28.758 57.516 1.85917 19.6 2.1 2.0 5.8 61 2 0 5 29.07 58.14 1.84091 27.1 2.9 2.8 5.8 62 0 2 7 29.266 58.532 1.82967 24.2 2.6 2.5 5.8 63 0 -8 2 30.317 60.635 1.77194 9.5 1.0 1.0 5.8 64 0 -8 1 30.438 60.876 1.7656 68.5 7.3 7.0 5.8 65 -2 6 0 30.502 61.004 1.76223 20.2 2.2 2.1 5.8 66 -2 -6 3 30.812 61.623 1.74626 30.2 3.2 3.1 5.8 67 -1 4 6 31.151 62.302 1.7291 25.1 2.7 2.6 5.8 68 0 -4 8 31.263 62.527 1.72352 10.4 1.1 1.1 5.8 69 -3 -2 2 31.474 62.948 1.71317 10.7 1.2 1.1 5.9 70 -1 6 4 31.52 63.039 1.71093 18.2 1.9 1.8 5.9 71 -1 -4 8 32.136 64.273 1.68151 10.9 1.2 1.1 5.9 72 2 0 6 32.25 64.5 1.67624 18.3 2.0 1.9 5.9 73 3 -2 2 32.694 65.388 1.65594 15.9 1.7 1.6 5.9 74 0 -8 5 33.072 66.144 1.63913 11.6 1.2 1.2 5.9 75 -2 -4 7 33.471 66.942 1.62182 14.1 1.5 1.4 5.9 76 1 -4 8 33.999 67.997 1.59961 16.0 1.7 1.6 5.9 77 0 4 7 34.042 68.085 1.59781 20.0 2.1 2.0 5.9 78 -3 4 0 34.25 68.499 1.58931 21.4 2.3 2.2 5.9 79 -3 -4 2 34.371 68.743 1.58437 23.4 2.5 2.4 5.9 80 -3 -4 1 34.446 68.891 1.58137 19.6 2.1 2.0 5.9 81 -3 4 1 34.536 69.072 1.57774 25.3 2.7 2.5 5.9 82 -1 4 7 34.754 69.508 1.56908 10.2 1.1 1.0 5.9 83 0 0 9 34.888 69.777 1.56379 13.0 1.4 1.3 5.9 84 0 -8 6 34.955 69.911 1.56118 20.2 2.2 2.0 5.9 85 -2 4 6 35.563 71.126 1.53793 15.6 1.7 1.6 5.9 86 1 4 7 36.796 73.592 1.49333 18.5 2.0 1.8 6.0 87 2 -8 2 37.399 74.798 1.47269 14.4 1.5 1.4 6.0 88 -2 -8 1 37.741 75.482 1.46131 9.8 1.0 1.0 6.0 89 3 -4 4 37.99 75.98 1.45317 9.5 1.0 0.9 6.0 90 -1 -2 10 38.882 77.765 1.42493 10.4 1.1 1.0 6.0 91 -2 0 9 39.406 78.811 1.40903 10.8 1.2 1.1 6.0 92 -2 -6 8 39.875 79.749 1.39517 12.4 1.3 1.2 6.0 93 1 -6 9 40.823 81.645 1.36826 19.3 2.1 1.9 6.1 94 1 4 8 40.886 81.772 1.36652 9.5 1.0 0.9 6.1 95 -2 -2 10 42.668 85.337 1.31974 10.6 1.1 1.0 6.1 96 -4 0 3 43.088 86.177 1.30936 14.7 1.6 1.4 6.1 Reference: Chichagov A.V. et al. Information-Calculating System on Crystal Structure Data of Minerals (MINCRYST) - Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian) |