Institute of Experimental Mineralogy Russian Academy of Sciences ------------------------------------------------- 142432, Chernogolovka, Moscow district A.V. Chichagov +7(496)52-22320 *** *** W W W - X R A Y P O L *** *********************** LARDERELLITE 1 NH(4)B(5)O(7)(OH)(2).H(2)O Monoclinic P 2(1)/c Z = 4 R =0.119 NR =600 11 .6 .1990 Ref.Str.: S. Merlino, F. Sartori (1969) * Acta Cryst., B 25, 2264-2270 Initial data from BDM-file Lattice parameters (cub. angs.,degr.): a = 9.47 alpha = 90.0 b = 7.63 beta = 97.08 c = 11.65 gamma = 90.0 Unit cell volume (cub. angs.) = 835.36 Molar volume ( cub.cm/mol.) = 125.79 Co-ordinates, thermal parameters, occupation for atomic positions: NoP x/a y/b z/c B(j) atom / occupation 1 0.4562 0.2012 0.0219 0.0 O = 1.00 2 0.6369 0.4037 0.9964 0.0 O = 1.00 3 0.8215 0.5942 0.9643 0.0 O = 1.00 4 0.5997 0.3232 0.1879 0.0 O = 1.00 5 0.7736 0.5426 0.1583 0.0 O = 1.00 6 0.6205 0.5779 0.3047 0.0 O = 1.00 7 0.8069 0.3614 0.3275 0.0 O = 1.00 8 0.735 0.5005 0.4926 0.0 O = 1.00 9 0.9322 0.3067 0.5088 0.0 O = 1.00 10 0.9552 0.1128 0.2295 0.0 O = 1.00 11 0.5656 0.3091 0.071 0.0 B = 1.00 12 0.7487 0.5111 0.0448 0.0 B = 1.00 13 0.7 0.4533 0.2431 0.0 B = 1.00 14 0.6314 0.5935 0.4192 0.0 B = 1.00 15 0.8246 0.3909 0.4418 0.0 B = 1.00 16 0.3219 0.4393 0.2658 0.0 N = 1.00 17 0.056 0.089 0.26 0.0 H = 1.00 18 0.899 0.208 0.267 0.0 H = 1.00 19 0.941 0.338 0.597 0.0 H = 1.00 20 0.911 0.671 0.974 0.0 H = 1.00 Co-ordinates for all atomic positions : No NoP x/a y/b z/c 1 1 0.4562 0.2012 0.0219 2 2 0.6369 0.4037 0.9964 3 3 0.8215 0.5942 0.9643 4 4 0.5997 0.3232 0.1879 5 5 0.7736 0.5426 0.1583 6 6 0.6205 0.5779 0.3047 7 7 0.8069 0.3614 0.3275 8 8 0.735 0.5005 0.4926 9 9 0.9322 0.3067 0.5088 10 10 0.9552 0.1128 0.2295 11 11 0.5656 0.3091 0.071 12 12 0.7487 0.5111 0.0448 13 13 0.7 0.4533 0.2431 14 14 0.6314 0.5935 0.4192 15 15 0.8246 0.3909 0.4418 16 16 0.3219 0.4393 0.2658 17 17 0.056 0.089 0.26 18 18 0.899 0.208 0.267 19 19 0.941 0.338 0.597 20 20 0.911 0.671 0.974 21 1 0.5438 0.7012 0.4781 22 2 0.3631 0.9037 0.5036 23 3 0.1785 0.0942 0.5357 24 4 0.4003 0.8232 0.3121 25 5 0.2264 0.0426 0.3417 26 6 0.3795 0.0779 0.1953 27 7 0.1931 0.8614 0.1725 28 8 0.265 0.0005 0.0074 29 9 0.0678 0.8067 0.9912 30 10 0.0448 0.6128 0.2705 31 11 0.4344 0.8091 0.429 32 12 0.2513 0.0111 0.4552 33 13 0.3 0.9533 0.2569 34 14 0.3686 0.0935 0.0808 35 15 0.1754 0.8909 0.0582 36 16 0.6781 0.9393 0.2342 37 17 0.944 0.589 0.24 38 18 0.101 0.708 0.233 39 19 0.059 0.838 0.903 40 20 0.089 0.171 0.526 41 1 0.4562 0.2988 0.5219 42 2 0.6369 0.0963 0.4964 43 3 0.8215 0.9058 0.4643 44 4 0.5997 0.1768 0.6879 45 5 0.7736 0.9574 0.6583 46 6 0.6205 0.9221 0.8047 47 7 0.8069 0.1386 0.8275 48 8 0.735 0.9995 0.9926 49 9 0.9322 0.1933 0.0088 50 10 0.9552 0.3872 0.7295 51 11 0.5656 0.1909 0.571 52 12 0.7487 0.9889 0.5448 53 13 0.7 0.0467 0.7431 54 14 0.6314 0.9065 0.9192 55 15 0.8246 0.1091 0.9418 56 16 0.3219 0.0607 0.7658 57 17 0.056 0.411 0.76 58 18 0.899 0.292 0.767 59 19 0.941 0.162 0.097 60 20 0.911 0.829 0.474 61 1 0.5438 0.7988 0.9781 62 2 0.3631 0.5963 0.0036 63 3 0.1785 0.4058 0.0357 64 4 0.4003 0.6768 0.8121 65 5 0.2264 0.4574 0.8417 66 6 0.3795 0.4221 0.6953 67 7 0.1931 0.6386 0.6725 68 8 0.265 0.4995 0.5074 69 9 0.0678 0.6933 0.4912 70 10 0.0448 0.8872 0.7705 71 11 0.4344 0.6909 0.929 72 12 0.2513 0.4889 0.9552 73 13 0.3 0.5467 0.7569 74 14 0.3686 0.4065 0.5808 75 15 0.1754 0.6091 0.5582 76 16 0.6781 0.5607 0.7342 77 17 0.944 0.911 0.74 78 18 0.101 0.792 0.733 79 19 0.059 0.662 0.403 80 20 0.089 0.329 0.026 X-ray density (g/cm cub.) = 1.84 MU (1/cm) = 16.502 Mass attenuation coefficient (cm**2/g) = 8.946 Selected interatomic distances (cation-anion,anion-anion): NoP Atom Rad.sph. C.N. Distance NoP N. (angs.) (angs.) 1 O 3.408 9 2.3514 2 2.4094 4 2.4198 6 2.3615 8 3.1109 8 3.2761 16 3.2372 1 3.1408 2 3.0795 3 2 O 3.408 10 2.3514 1 2.3388 3 2.3817 4 2.3989 5 3.3669 7 3.2228 8 3.2123 9 3.1408 1 2.9905 2 3.3484 16 3 O 3.408 7 2.3388 2 2.392 5 2.8262 9 3.2264 8 3.2543 9 3.0795 1 2.8632 16 4 O 3.408 8 2.4094 1 2.3817 2 2.4028 5 2.3666 6 2.407 7 3.0196 16 2.8113 6 3.0534 16 5 O 3.408 7 2.3989 2 2.392 3 2.4028 4 2.386 6 2.3965 7 2.7864 10 3.3104 16 6 O 3.408 8 2.3666 4 2.386 5 2.4083 7 2.394 8 3.0007 16 2.4198 1 2.8113 4 2.9472 16 7 O 3.408 8 2.407 4 2.3965 5 2.4083 6 2.3691 8 2.3293 9 2.6961 10 3.0927 10 3.3669 2 8 O 3.408 9 2.394 6 2.3691 7 2.3712 9 2.3615 1 3.1109 1 3.2228 2 3.2264 3 3.3607 10 2.966 16 9 O 3.408 7 2.3293 7 2.3712 8 2.8262 3 3.2123 2 3.2543 3 2.6263 10 3.2337 9 10 O 3.408 6 2.6961 7 2.7864 5 3.0927 7 2.9457 16 3.3607 8 2.6263 9 11 B 2.016 3 1.39 1 1.37 2 1.3646 4 12 B 2.016 3 1.4012 2 1.3843 3 1.336 5 13 B 2.016 4 1.4665 4 1.4477 5 1.4556 6 1.496 7 14 B 2.016 3 1.3305 6 1.4108 8 1.4052 1 15 B 2.016 3 1.3405 7 1.376 8 1.3654 9 16 N 3.552 10 3.0196 4 3.0007 6 3.0534 4 3.3104 5 2.9472 6 2.9457 10 3.2761 1 3.3484 2 2.8632 3 2.966 8 17 H 1.776 1 0.9934 10 18 H 1.776 2 1.667 7 1.0291 10 19 H 1.776 2 1.0482 9 1.5782 10 20 H 1.776 1 1.0251 3 X-ray diffraction powder data (II), X-Ray W.L. = 1.54056(angs.): No H K L Theta 2*Theta S LPG MF F I int. ( degree ) *100 1 1 0 0 4.701 9.403 0.053 294.72 2 39.7 132.8 2 0 1 1 6.947 13.895 0.079 133.74 4 4.6 1.6 3 1 1 0 7.472 14.944 0.084 115.32 4 31.6 66.1 4 0 0 2 7.658 15.315 0.086 109.68 2 45.2 64.2 5 1 1 -1 8.131 16.261 0.092 97.04 4 68.6 261.5 6 1 0 -2 8.487 16.974 0.096 88.88 2 2.3 0.1 7 1 1 1 8.665 17.329 0.098 85.19 4 55.5 150.2 8 2 0 0 9.435 18.87 0.106 71.5 2 57.6 68.0 9 1 0 2 9.487 18.974 0.107 70.69 2 19.0 7.3 10 0 1 2 9.624 19.247 0.109 68.64 4 35.8 50.6 11 1 1 -2 10.301 20.601 0.116 59.64 4 45.7 71.3 12 2 1 0 11.1 22.2 0.125 51.06 4 27.6 22.2 13 1 1 2 11.144 22.289 0.125 50.64 4 31.6 29.0 14 2 1 -1 11.362 22.724 0.128 48.64 4 12.8 4.6 15 2 0 -2 11.426 22.852 0.129 48.07 2 11.9 2.0 16 0 2 0 11.649 23.297 0.131 46.17 2 62.2 51.2 17 2 1 1 12.136 24.271 0.136 42.38 4 42.6 44.1 18 0 2 1 12.276 24.552 0.138 41.37 4 6.3 0.9 19 1 2 0 12.586 25.173 0.141 39.25 4 0.9 0.0 20 2 1 -2 12.847 25.693 0.144 37.6 4 37.4 30.1 21 2 0 2 12.923 25.845 0.145 37.13 2 14.9 2.4 22 0 1 3 12.94 25.88 0.145 37.03 4 14.8 4.6 23 1 2 -1 12.997 25.993 0.146 36.69 4 43.6 39.9 24 1 1 -3 13.287 26.574 0.149 35.01 4 25.2 12.8 25 1 2 1 13.344 26.689 0.15 34.69 4 8.8 1.6 26 0 2 2 14.0 27.999 0.157 31.34 4 23.6 10.0 27 2 1 2 14.204 28.407 0.159 30.39 4 49.3 42.4 28 3 0 0 14.235 28.469 0.16 30.25 2 27.5 6.5 29 1 1 3 14.287 28.574 0.16 30.01 4 12.6 2.7 30 1 2 -2 14.483 28.967 0.162 29.15 4 2.4 0.1 31 2 2 0 15.075 30.149 0.169 26.76 4 117.9 213.4 32 1 2 2 15.108 30.216 0.169 26.63 4 13.3 2.7 33 2 1 -3 15.222 30.444 0.17 26.21 4 11.1 1.8 34 2 2 -1 15.273 30.545 0.171 26.02 4 157.1 368.0 35 3 0 -2 15.358 30.715 0.172 25.71 2 52.8 20.6 36 3 1 0 15.415 30.83 0.173 25.51 4 42.9 26.9 37 0 0 4 15.456 30.913 0.173 25.36 2 143.6 149.8 38 3 1 -1 15.46 30.92 0.173 25.35 4 2.8 0.1 39 1 0 -4 15.605 31.209 0.175 24.85 2 34.5 8.5 40 2 2 1 15.869 31.738 0.177 23.96 4 68.5 64.4 41 3 1 1 16.338 32.676 0.183 22.5 4 26.0 8.7 42 2 2 -2 16.431 32.862 0.184 22.22 4 75.2 72.1 43 3 1 -2 16.465 32.93 0.184 22.12 4 24.6 7.7 44 0 2 3 16.506 33.011 0.184 22.01 4 13.0 2.1 45 0 1 4 16.558 33.116 0.185 21.86 4 21.9 6.0 46 1 1 -4 16.697 33.395 0.187 21.46 4 13.1 2.1 47 1 0 4 16.757 33.515 0.187 21.3 2 32.8 6.6 48 1 2 -3 16.785 33.571 0.187 21.22 4 45.0 24.6 49 2 1 3 16.96 33.92 0.189 20.75 4 3.9 0.2 50 3 0 2 17.083 34.167 0.191 20.42 2 54.4 17.4 51 2 0 -4 17.168 34.336 0.192 20.2 2 9.9 0.6 52 2 2 2 17.536 35.071 0.196 19.29 4 25.3 7.1 53 1 2 3 17.605 35.21 0.196 19.13 4 37.7 15.6 54 1 1 4 17.787 35.574 0.198 18.7 4 3.8 0.2 55 0 3 1 18.066 36.131 0.201 18.07 4 21.9 5.0 56 3 1 2 18.097 36.194 0.202 18.0 4 21.9 4.9 57 2 1 -4 18.177 36.355 0.202 17.83 4 2.3 0.1 58 1 3 0 18.286 36.572 0.204 17.6 4 34.1 11.7 59 3 1 -3 18.29 36.581 0.204 17.59 4 15.7 2.5 60 2 2 -3 18.388 36.777 0.205 17.38 4 19.3 3.7 61 3 2 0 18.552 37.104 0.207 17.05 4 37.9 14.1 62 1 3 -1 18.581 37.162 0.207 16.99 4 34.5 11.6 63 3 2 -1 18.59 37.18 0.207 16.97 4 10.7 1.1 64 1 3 1 18.835 37.67 0.21 16.49 4 17.8 3.0 65 4 0 0 19.139 38.277 0.213 15.92 2 14.4 0.9 66 2 0 4 19.247 38.495 0.214 15.72 2 11.9 0.6 67 0 3 2 19.322 38.644 0.215 15.58 4 8.7 0.7 68 3 2 1 19.343 38.686 0.215 15.55 4 69.5 43.0 69 3 2 -2 19.453 38.906 0.216 15.35 4 30.4 8.1 70 0 2 4 19.533 39.066 0.217 15.21 4 20.2 3.6 71 1 2 -4 19.654 39.308 0.218 15.01 4 1.6 0.0 72 1 3 -2 19.689 39.377 0.219 14.95 4 8.3 0.6 73 4 0 -2 19.776 39.552 0.22 14.8 2 8.6 0.3 74 3 0 -4 19.853 39.706 0.22 14.67 2 57.4 13.8 75 2 2 3 19.883 39.766 0.221 14.63 4 18.5 2.9 76 4 1 -1 19.978 39.957 0.222 14.47 4 36.4 11.0 77 4 1 0 20.063 40.125 0.223 14.34 4 22.9 4.3 78 2 3 0 20.144 40.288 0.224 14.21 4 11.4 1.1 79 2 1 4 20.167 40.334 0.224 14.17 4 23.1 4.3 80 1 3 2 20.17 40.34 0.224 14.17 4 18.6 2.8 81 2 3 -1 20.298 40.597 0.225 13.97 4 5.8 0.3 82 1 1 -5 20.37 40.739 0.226 13.86 4 20.0 3.2 83 0 1 5 20.371 40.741 0.226 13.86 4 25.2 5.1 84 3 1 3 20.507 41.013 0.227 13.65 4 9.8 0.8 85 1 2 4 20.609 41.218 0.228 13.5 4 27.3 5.8 86 4 1 -2 20.676 41.352 0.229 13.4 4 21.1 3.4 87 3 1 -4 20.75 41.501 0.23 13.3 4 19.0 2.7 88 2 3 1 20.768 41.536 0.23 13.27 4 41.2 12.9 89 3 2 2 20.883 41.766 0.231 13.11 4 47.3 16.8 90 4 1 1 20.921 41.842 0.232 13.06 4 60.3 27.2 91 2 2 -4 20.954 41.909 0.232 13.01 4 19.5 2.8 92 3 2 -3 21.055 42.109 0.233 12.87 4 50.3 18.7 93 2 3 -2 21.217 42.434 0.235 12.65 4 52.0 19.6 94 0 3 3 21.277 42.554 0.236 12.57 4 5.3 0.2 95 1 3 -3 21.503 43.006 0.238 12.28 4 31.2 6.9 96 2 1 -5 21.522 43.043 0.238 12.25 4 21.8 3.3 97 1 1 5 21.525 43.05 0.238 12.25 4 38.1 10.2 98 4 0 2 21.642 43.284 0.239 12.1 2 34.3 4.1 99 4 1 -3 22.095 44.189 0.244 11.55 4 69.9 32.3 100 2 3 2 22.116 44.232 0.244 11.53 4 83.2 45.7 101 1 3 3 22.173 44.346 0.245 11.46 4 12.7 1.1 102 4 1 2 22.481 44.961 0.248 11.11 4 64.0 26.0 103 4 2 -1 22.57 45.14 0.249 11.01 4 0.5 0.0 104 3 0 4 22.597 45.193 0.249 10.98 2 42.0 5.5 105 4 2 0 22.646 45.293 0.25 10.93 4 25.2 4.0 106 2 2 4 22.741 45.482 0.251 10.82 4 74.6 34.5 107 2 3 -3 22.824 45.649 0.252 10.73 4 61.2 23.0 108 1 2 -5 22.925 45.85 0.253 10.63 4 0.6 0.0 109 0 2 5 22.926 45.852 0.253 10.63 4 0.3 0.0 110 3 3 0 22.962 45.923 0.253 10.59 4 3.8 0.1 111 3 3 -1 22.993 45.987 0.254 10.56 4 4.0 0.1 112 3 2 3 23.05 46.1 0.254 10.5 4 2.9 0.1 113 4 2 -2 23.204 46.408 0.256 10.34 4 4.4 0.1 114 3 2 -4 23.272 46.544 0.256 10.27 4 10.2 0.6 115 4 0 -4 23.341 46.682 0.257 10.2 2 10.3 0.3 116 3 1 4 23.408 46.817 0.258 10.14 4 51.0 15.1 117 4 2 1 23.428 46.856 0.258 10.12 4 16.0 1.5 118 1 0 -6 23.457 46.913 0.258 10.09 2 9.5 0.3 119 0 0 6 23.563 47.126 0.259 9.99 2 69.3 13.7 120 3 3 1 23.63 47.26 0.26 9.92 4 39.9 9.0 121 3 1 -5 23.69 47.381 0.261 9.87 4 6.3 0.2 122 2 1 5 23.695 47.391 0.261 9.86 4 22.5 2.9 123 3 3 -2 23.724 47.448 0.261 9.83 4 36.5 7.5 124 0 3 4 23.792 47.585 0.262 9.77 4 0.4 0.0 125 0 4 0 23.817 47.634 0.262 9.75 2 41.0 4.7 126 1 3 -4 23.896 47.791 0.263 9.67 4 17.8 1.8 127 2 2 -5 23.978 47.957 0.264 9.6 4 111.9 69.0 128 1 2 5 23.981 47.963 0.264 9.6 4 13.9 1.1 129 2 3 3 24.092 48.184 0.265 9.5 4 60.7 20.0 130 4 1 -4 24.133 48.267 0.265 9.46 4 71.0 27.3 131 0 4 1 24.159 48.319 0.266 9.44 4 34.3 6.4 132 5 0 0 24.194 48.387 0.266 9.41 2 57.7 9.0 133 1 1 -6 24.246 48.492 0.267 9.36 4 2.2 0.0 134 1 4 0 24.334 48.667 0.267 9.28 4 17.8 1.7 135 0 1 6 24.35 48.7 0.268 9.27 4 49.2 12.9 136 2 0 -6 24.39 48.78 0.268 9.23 2 15.3 0.6 137 4 2 -3 24.506 49.013 0.269 9.14 4 7.4 0.3 138 5 0 -2 24.521 49.042 0.269 9.12 2 62.8 10.3 139 1 4 -1 24.569 49.138 0.27 9.08 4 6.6 0.2 140 4 1 3 24.638 49.275 0.271 9.03 4 31.9 5.3 141 1 0 6 24.699 49.398 0.271 8.97 2 34.5 3.1 142 1 3 4 24.718 49.436 0.271 8.96 4 4.9 0.1 143 1 4 1 24.772 49.544 0.272 8.91 4 20.0 2.0 144 5 1 -1 24.793 49.587 0.272 8.9 4 24.8 3.1 145 4 2 2 24.863 49.727 0.273 8.84 4 5.4 0.1 146 3 3 2 24.956 49.913 0.274 8.77 4 12.6 0.8 147 5 1 0 24.965 49.931 0.274 8.76 4 14.5 1.1 148 2 3 -4 25.019 50.037 0.275 8.72 4 61.3 18.7 149 3 3 -3 25.106 50.212 0.275 8.65 4 30.3 4.6 150 2 1 -6 25.158 50.315 0.276 8.61 4 23.0 2.6 151 0 4 2 25.165 50.331 0.276 8.6 4 26.2 3.4 152 5 1 -2 25.285 50.571 0.277 8.51 4 10.9 0.6 153 1 1 6 25.46 50.919 0.279 8.38 4 31.3 4.7 154 1 4 -2 25.464 50.928 0.279 8.37 4 26.0 3.2 155 3 2 4 25.726 51.451 0.282 8.18 4 51.6 12.5 156 5 1 1 25.792 51.584 0.282 8.13 4 20.0 1.9 157 2 4 0 25.838 51.675 0.283 8.1 4 19.1 1.7 158 1 4 2 25.859 51.718 0.283 8.08 4 46.7 10.1 159 2 4 -1 25.965 51.93 0.284 8.01 4 11.3 0.6 160 3 2 -5 25.989 51.977 0.284 7.99 4 4.4 0.1 161 2 2 5 25.993 51.987 0.284 7.99 4 29.8 4.1 162 3 0 -6 26.28 52.561 0.287 7.79 2 36.4 3.0 163 2 4 1 26.355 52.709 0.288 7.74 4 8.6 0.3 164 4 2 -4 26.403 52.806 0.289 7.71 4 6.0 0.2 165 5 1 -3 26.415 52.829 0.289 7.7 4 7.6 0.3 166 4 3 -1 26.441 52.882 0.289 7.68 4 19.4 1.7 167 5 0 2 26.506 53.011 0.29 7.64 2 32.4 2.3 168 4 3 0 26.509 53.018 0.29 7.64 4 6.8 0.2 169 1 2 -6 26.509 53.018 0.29 7.64 4 8.2 0.3 170 4 0 4 26.569 53.138 0.29 7.6 2 6.6 0.1 171 2 3 4 26.593 53.186 0.291 7.58 4 8.9 0.3 172 0 2 6 26.606 53.212 0.291 7.58 4 5.0 0.1 173 4 1 -5 26.689 53.378 0.292 7.52 4 34.1 5.0 174 3 1 5 26.695 53.391 0.292 7.52 4 7.7 0.3 175 2 4 -2 26.73 53.461 0.292 7.5 4 0.9 0.0 176 1 3 -5 26.757 53.514 0.292 7.48 4 9.8 0.4 177 0 3 5 26.758 53.516 0.292 7.48 4 2.5 0.0 178 2 0 6 26.767 53.535 0.292 7.47 2 33.6 2.4 179 0 4 3 26.781 53.561 0.292 7.46 4 1.1 0.0 180 3 3 3 26.869 53.737 0.293 7.41 4 5.9 0.1 181 4 2 3 26.876 53.752 0.293 7.4 4 13.7 0.8 182 1 4 -3 26.971 53.942 0.294 7.34 4 19.7 1.6 183 4 3 -2 27.007 54.013 0.295 7.32 4 31.5 4.2 184 3 1 -6 27.009 54.017 0.295 7.32 4 5.3 0.1 185 5 2 -1 27.023 54.045 0.295 7.31 4 8.0 0.3 186 3 3 -4 27.067 54.135 0.295 7.29 4 7.0 0.2 187 5 2 0 27.185 54.369 0.297 7.21 4 1.4 0.0 188 4 3 1 27.207 54.414 0.297 7.2 4 43.4 7.8 189 5 1 2 27.23 54.46 0.297 7.19 4 21.7 1.9 190 4 1 4 27.292 54.584 0.298 7.15 4 25.4 2.6 191 2 2 -6 27.366 54.731 0.298 7.11 4 33.3 4.5 192 5 0 -4 27.419 54.838 0.299 7.07 2 33.9 2.3 193 5 2 -2 27.486 54.972 0.3 7.04 4 2.5 0.0 194 2 1 6 27.487 54.974 0.3 7.03 4 27.8 3.1 195 2 4 2 27.491 54.982 0.3 7.03 4 19.4 1.5 196 1 4 3 27.539 55.079 0.3 7.0 4 8.6 0.3 197 1 2 6 27.651 55.301 0.301 6.94 4 12.2 0.6 198 2 3 -5 27.702 55.405 0.302 6.91 4 11.3 0.5 199 1 3 5 27.705 55.41 0.302 6.91 4 36.9 5.4 200 5 2 1 27.964 55.929 0.304 6.76 4 12.3 0.6 201 2 4 -3 28.097 56.195 0.306 6.69 4 27.2 2.8 202 5 1 -4 28.127 56.254 0.306 6.68 4 1.3 0.0 203 4 3 -3 28.18 56.36 0.307 6.65 4 32.4 4.0 204 3 4 0 28.216 56.431 0.307 6.63 4 1.9 0.0 205 3 4 -1 28.243 56.486 0.307 6.61 4 20.1 1.5 206 1 1 -7 28.317 56.633 0.308 6.58 4 38.9 5.7 207 0 1 7 28.502 57.004 0.31 6.48 4 25.7 2.4 208 4 3 2 28.504 57.008 0.31 6.48 4 16.9 1.1 209 5 2 -3 28.554 57.109 0.31 6.45 4 34.5 4.4 210 3 4 1 28.795 57.589 0.313 6.33 4 11.3 0.5 211 4 2 -5 28.815 57.63 0.313 6.32 4 8.3 0.3 212 3 2 5 28.821 57.642 0.313 6.32 4 31.9 3.7 213 3 4 -2 28.876 57.752 0.313 6.29 4 27.0 2.6 214 0 4 4 28.936 57.872 0.314 6.26 4 2.4 0.0 215 4 0 -6 28.996 57.993 0.315 6.23 2 45.7 3.7 216 1 4 -4 29.026 58.052 0.315 6.22 4 16.4 1.0 217 2 1 -7 29.047 58.094 0.315 6.21 4 14.4 0.7 218 3 2 -6 29.119 58.238 0.316 6.17 4 0.7 0.0 219 2 4 3 29.197 58.395 0.317 6.14 4 12.6 0.6 220 5 1 3 29.219 58.438 0.317 6.13 4 39.9 5.6 221 3 3 4 29.291 58.583 0.318 6.09 4 27.1 2.6 222 5 2 2 29.33 58.659 0.318 6.07 4 36.0 4.5 223 4 2 4 29.389 58.778 0.319 6.05 4 0.5 0.0 224 6 0 0 29.458 58.916 0.319 6.01 2 19.6 0.7 225 3 3 -5 29.533 59.066 0.32 5.98 4 18.7 1.2 226 2 3 5 29.537 59.074 0.32 5.98 4 39.1 5.2 227 6 0 -2 29.565 59.13 0.32 5.97 2 3.6 0.0 228 2 2 6 29.575 59.15 0.32 5.96 4 28.9 2.8 229 1 1 7 29.591 59.183 0.321 5.95 4 26.7 2.4 230 3 0 6 29.635 59.27 0.321 5.93 2 15.2 0.4 231 4 1 -6 29.68 59.36 0.321 5.91 4 9.4 0.3 232 1 4 4 29.748 59.495 0.322 5.88 4 8.8 0.3 233 6 1 -1 29.894 59.789 0.324 5.82 4 11.6 0.4 234 4 3 -4 29.914 59.828 0.324 5.81 4 9.3 0.3 235 3 4 2 29.958 59.916 0.324 5.79 4 7.6 0.2 236 1 3 -6 30.011 60.023 0.325 5.77 4 14.9 0.7 237 2 4 -4 30.013 60.026 0.325 5.77 4 23.8 1.9 238 3 4 -3 30.09 60.181 0.325 5.73 4 11.0 0.4 239 0 3 6 30.101 60.203 0.326 5.73 4 13.1 0.6 240 6 1 0 30.135 60.27 0.326 5.72 4 36.7 4.4 241 5 2 -4 30.186 60.373 0.326 5.69 4 7.9 0.2 242 6 1 -2 30.241 60.481 0.327 5.67 4 7.3 0.2 243 3 1 6 30.31 60.619 0.328 5.64 4 6.4 0.1 244 4 3 3 30.351 60.702 0.328 5.63 4 22.7 1.7 245 5 1 -5 30.36 60.721 0.328 5.62 4 9.4 0.3 246 1 2 -7 30.368 60.735 0.328 5.62 4 15.1 0.7 247 4 1 5 30.368 60.736 0.328 5.62 4 15.6 0.8 248 5 3 -1 30.486 60.973 0.329 5.57 4 20.8 1.4 249 0 2 7 30.545 61.09 0.33 5.55 4 20.1 1.3 250 0 5 1 30.607 61.214 0.33 5.52 4 32.6 3.4 251 5 3 0 30.636 61.272 0.331 5.51 4 13.4 0.6 252 3 1 -7 30.651 61.302 0.331 5.5 4 23.9 1.8 253 1 5 0 30.756 61.512 0.332 5.46 4 53.6 9.0 254 2 3 -6 30.804 61.608 0.332 5.44 4 38.4 4.6 255 5 3 -2 30.916 61.832 0.334 5.4 4 27.3 2.3 256 6 1 1 30.954 61.908 0.334 5.38 4 28.1 2.4 257 1 5 -1 30.957 61.914 0.334 5.38 4 11.1 0.4 258 5 0 4 31.041 62.083 0.335 5.35 2 29.8 1.4 259 2 2 -7 31.068 62.135 0.335 5.34 4 6.2 0.1 260 1 3 6 31.069 62.138 0.335 5.34 4 11.1 0.4 261 1 5 1 31.132 62.263 0.336 5.32 4 1.6 0.0 262 6 1 -3 31.162 62.324 0.336 5.31 4 39.2 4.7 263 5 2 3 31.233 62.466 0.337 5.28 4 8.7 0.2 264 4 4 -1 31.281 62.563 0.337 5.26 4 68.7 14.2 265 4 4 0 31.342 62.685 0.338 5.24 4 49.7 7.4 266 5 3 1 31.361 62.722 0.338 5.23 4 17.5 0.9 267 2 4 4 31.418 62.837 0.338 5.21 4 14.7 0.6 268 0 5 2 31.471 62.941 0.339 5.19 4 6.3 0.1 269 2 1 7 31.527 63.054 0.339 5.17 4 12.7 0.5 270 1 4 -5 31.566 63.132 0.34 5.16 4 7.2 0.2 271 0 4 5 31.567 63.134 0.34 5.16 4 48.6 7.0 272 1 2 7 31.591 63.182 0.34 5.15 4 40.7 4.9 273 3 4 3 31.667 63.333 0.341 5.12 4 29.0 2.5 274 4 2 -6 31.677 63.353 0.341 5.12 4 6.1 0.1 275 6 0 2 31.677 63.354 0.341 5.12 2 20.9 0.6 276 5 1 4 31.698 63.396 0.341 5.11 4 10.3 0.3 277 1 5 -2 31.729 63.458 0.341 5.1 4 22.0 1.4 278 4 4 -2 31.791 63.582 0.342 5.08 4 60.2 10.6 279 3 4 -4 31.846 63.692 0.342 5.06 4 18.9 1.0 280 6 2 -1 31.883 63.766 0.343 5.05 4 7.3 0.2 281 5 3 -3 31.912 63.824 0.343 5.04 4 3.5 0.0 282 1 0 -8 31.951 63.903 0.344 5.02 2 39.0 2.2 283 4 4 1 31.972 63.945 0.344 5.02 4 42.1 5.1 284 6 0 -4 31.984 63.969 0.344 5.01 2 3.1 0.0 285 2 5 0 32.054 64.108 0.344 4.99 4 2.3 0.0 286 1 5 2 32.073 64.146 0.345 4.98 4 16.1 0.7 287 6 2 0 32.115 64.23 0.345 4.97 4 11.0 0.3 288 4 3 -5 32.156 64.312 0.345 4.95 4 2.8 0.0 289 3 3 5 32.162 64.324 0.346 4.95 4 25.5 1.8 290 2 5 -1 32.165 64.331 0.346 4.95 4 4.3 0.1 291 0 0 8 32.209 64.418 0.346 4.94 2 5.6 0.0 292 6 2 -2 32.217 64.433 0.346 4.93 4 2.7 0.0 293 3 2 6 32.283 64.566 0.347 4.91 4 18.0 0.9 294 6 1 2 32.327 64.653 0.347 4.9 4 26.7 2.0 295 5 2 -5 32.332 64.665 0.347 4.9 4 29.8 2.5 296 4 2 5 32.34 64.679 0.347 4.89 4 2.8 0.0 297 5 0 -6 32.417 64.833 0.348 4.87 2 8.2 0.1 298 2 4 -5 32.422 64.844 0.348 4.87 4 28.6 2.3 299 1 4 5 32.424 64.849 0.348 4.87 4 15.8 0.7 300 3 3 -6 32.441 64.883 0.348 4.86 4 11.7 0.4 301 2 5 1 32.507 65.013 0.349 4.84 4 3.7 0.0 302 2 0 -8 32.547 65.094 0.349 4.83 2 14.7 0.3 303 1 1 -8 32.598 65.196 0.35 4.81 4 9.9 0.3 304 3 2 -7 32.613 65.225 0.35 4.8 4 28.9 2.3 305 6 1 -4 32.631 65.261 0.35 4.8 4 40.1 4.4 306 5 3 2 32.639 65.278 0.35 4.8 4 24.2 1.6 307 4 3 4 32.695 65.39 0.351 4.78 4 4.9 0.1 308 2 5 -2 32.837 65.674 0.352 4.73 4 12.8 0.4 309 0 1 8 32.853 65.706 0.352 4.73 4 2.0 0.0 310 4 4 -3 32.857 65.714 0.352 4.73 4 22.9 1.4 311 2 3 6 32.87 65.74 0.352 4.72 4 28.5 2.2 312 0 5 3 32.882 65.763 0.352 4.72 4 88.1 21.0 313 6 2 1 32.906 65.812 0.353 4.71 4 28.6 2.2 314 1 5 -3 33.05 66.099 0.354 4.67 4 10.1 0.3 315 4 1 -7 33.055 66.109 0.354 4.67 4 23.0 1.4 316 5 1 -6 33.059 66.117 0.354 4.67 4 8.3 0.2 317 6 2 -3 33.107 66.214 0.355 4.65 4 4.2 0.0 318 4 4 2 33.154 66.307 0.355 4.64 4 11.3 0.3 319 4 0 6 33.186 66.372 0.355 4.63 2 47.1 2.9 320 2 1 -8 33.188 66.375 0.355 4.63 4 18.5 0.9 321 1 0 8 33.31 66.62 0.356 4.59 2 1.8 0.0 322 5 3 -4 33.447 66.894 0.358 4.55 4 20.8 1.1 323 2 2 7 33.461 66.921 0.358 4.55 4 15.5 0.6 324 2 5 2 33.511 67.021 0.358 4.53 4 11.3 0.3 325 1 5 3 33.554 67.108 0.359 4.52 4 17.6 0.8 326 1 3 -7 33.618 67.236 0.359 4.5 4 6.3 0.1 327 5 2 4 33.626 67.253 0.359 4.5 4 8.6 0.2 328 0 3 7 33.786 67.572 0.361 4.46 4 13.1 0.4 329 4 1 6 33.821 67.641 0.361 4.45 4 20.2 1.0 330 3 4 4 33.877 67.754 0.362 4.43 4 4.5 0.1 331 1 1 8 33.943 67.887 0.362 4.41 4 3.6 0.0 332 3 0 -8 33.973 67.946 0.363 4.41 2 50.1 3.2 333 2 5 -3 34.052 68.104 0.363 4.38 4 2.9 0.0 334 3 4 -5 34.1 68.2 0.364 4.37 4 3.2 0.0 335 2 4 5 34.104 68.208 0.364 4.37 4 23.2 1.3 336 3 5 0 34.158 68.316 0.364 4.36 4 4.8 0.1 337 3 5 -1 34.183 68.365 0.365 4.35 4 4.7 0.1 338 6 1 3 34.218 68.436 0.365 4.34 4 40.7 4.1 339 3 1 7 34.231 68.462 0.365 4.34 4 15.4 0.6 340 6 2 2 34.236 68.473 0.365 4.34 4 9.7 0.2 341 2 3 -7 34.282 68.564 0.366 4.32 4 12.0 0.4 342 5 3 3 34.439 68.878 0.367 4.28 4 15.5 0.6 343 4 4 -4 34.453 68.905 0.367 4.28 4 12.8 0.4 344 1 2 -8 34.5 69.0 0.368 4.27 4 22.6 1.2 345 6 2 -4 34.532 69.064 0.368 4.26 4 15.6 0.6 346 1 4 -6 34.543 69.086 0.368 4.26 4 5.1 0.1 347 3 1 -8 34.6 69.2 0.369 4.24 4 6.6 0.1 348 6 1 -5 34.612 69.223 0.369 4.24 4 50.3 6.1 349 5 1 5 34.62 69.24 0.369 4.24 4 18.5 0.8 350 0 4 6 34.626 69.253 0.369 4.24 4 8.5 0.2 351 3 5 1 34.679 69.358 0.369 4.22 4 7.4 0.1 352 0 2 8 34.748 69.497 0.37 4.21 4 12.4 0.4 353 3 5 -2 34.752 69.505 0.37 4.2 4 2.2 0.0 354 1 3 7 34.78 69.559 0.37 4.2 4 9.8 0.2 355 0 5 4 34.806 69.613 0.371 4.19 4 3.5 0.0 356 4 4 3 34.858 69.716 0.371 4.18 4 30.2 2.2 357 4 3 -6 34.861 69.722 0.371 4.18 4 12.9 0.4 358 1 5 -4 34.888 69.776 0.371 4.17 4 5.7 0.1 359 4 2 -7 34.944 69.889 0.372 4.16 4 2.4 0.0 360 7 0 -2 34.945 69.891 0.372 4.16 2 22.5 0.6 361 5 2 -6 34.948 69.896 0.372 4.16 4 4.2 0.0 362 5 4 -1 34.984 69.968 0.372 4.15 4 69.0 11.3 363 7 0 0 35.012 70.024 0.372 4.14 2 35.5 1.5 364 2 5 3 35.043 70.086 0.373 4.13 4 8.0 0.1 365 6 3 -1 35.058 70.116 0.373 4.13 4 3.3 0.0 366 2 2 -8 35.074 70.148 0.373 4.13 4 10.0 0.2 367 5 4 0 35.124 70.247 0.373 4.12 4 46.8 5.2 368 2 0 8 35.215 70.429 0.374 4.09 2 1.9 0.0 369 6 3 0 35.279 70.558 0.375 4.08 4 14.6 0.5 370 2 4 -6 35.28 70.56 0.375 4.08 4 1.2 0.0 371 7 1 -1 35.329 70.658 0.375 4.07 4 22.3 1.2 372 6 3 -2 35.376 70.753 0.376 4.06 4 2.6 0.0 373 5 4 -2 35.385 70.769 0.376 4.05 4 4.2 0.0 374 3 3 6 35.44 70.88 0.376 4.04 4 4.8 0.1 375 5 3 -5 35.487 70.974 0.377 4.03 4 7.1 0.1 376 4 3 5 35.494 70.988 0.377 4.03 4 28.4 1.9 377 1 4 6 35.528 71.055 0.377 4.02 4 29.5 2.0 378 1 5 4 35.543 71.086 0.377 4.02 4 8.3 0.2 379 7 1 -2 35.565 71.13 0.378 4.01 4 8.1 0.2 380 7 1 0 35.631 71.262 0.378 4.0 4 1.7 0.0 381 4 2 6 35.691 71.382 0.379 3.99 4 24.7 1.4 382 3 5 2 35.734 71.469 0.379 3.98 4 14.1 0.5 383 3 3 -7 35.755 71.51 0.379 3.97 4 11.0 0.3 384 2 5 -4 35.785 71.569 0.38 3.97 4 3.5 0.0 385 5 4 1 35.801 71.602 0.38 3.96 4 27.3 1.7 386 1 2 8 35.811 71.622 0.38 3.96 4 10.1 0.2 387 2 1 8 35.832 71.664 0.38 3.96 4 1.0 0.0 388 3 5 -3 35.855 71.711 0.38 3.95 4 0.5 0.0 389 6 0 4 35.982 71.963 0.381 3.92 2 5.0 0.0 390 6 3 1 36.036 72.072 0.382 3.91 4 0.3 0.0 391 6 2 3 36.079 72.158 0.382 3.9 4 0.3 0.0 392 3 2 7 36.092 72.183 0.382 3.9 4 24.0 1.3 393 4 0 -8 36.182 72.364 0.383 3.88 2 14.2 0.2 394 5 1 -7 36.184 72.367 0.383 3.88 4 4.3 0.0 395 6 3 -3 36.229 72.458 0.384 3.87 4 20.4 0.9 396 5 4 -3 36.318 72.636 0.384 3.85 4 35.3 2.8 397 7 1 -3 36.335 72.67 0.385 3.85 4 26.7 1.6 398 3 2 -8 36.453 72.905 0.386 3.83 4 16.0 0.6 399 6 0 -6 36.463 72.926 0.386 3.82 2 25.5 0.7 400 6 2 -5 36.464 72.928 0.386 3.82 4 10.3 0.2 401 7 1 1 36.466 72.931 0.386 3.82 4 38.9 3.3 402 5 2 5 36.472 72.944 0.386 3.82 4 19.9 0.9 403 4 4 -5 36.548 73.095 0.387 3.81 4 33.4 2.4 404 3 4 5 36.553 73.106 0.387 3.81 4 16.4 0.6 405 2 3 7 36.569 73.137 0.387 3.8 4 28.5 1.8 406 6 1 4 36.594 73.187 0.387 3.8 4 18.7 0.8 407 5 3 4 36.728 73.456 0.388 3.77 4 5.5 0.1 408 4 1 -8 36.793 73.585 0.389 3.76 4 43.0 4.0 409 3 4 -6 36.817 73.633 0.389 3.75 4 17.4 0.6 410 4 5 -1 36.95 73.899 0.39 3.73 4 12.8 0.4 411 5 4 2 37.003 74.007 0.391 3.72 4 17.3 0.6 412 4 5 0 37.006 74.012 0.391 3.72 4 20.7 0.9 413 7 0 -4 37.02 74.04 0.391 3.72 2 13.6 0.2 414 4 4 4 37.056 74.112 0.391 3.71 4 24.3 1.3 415 6 1 -6 37.072 74.144 0.391 3.71 4 13.8 0.4 416 2 5 4 37.076 74.152 0.391 3.71 4 2.6 0.0 417 1 1 -9 37.13 74.26 0.392 3.7 4 5.5 0.1 418 7 2 -1 37.166 74.332 0.392 3.69 4 5.5 0.1 419 1 5 -5 37.213 74.426 0.393 3.68 4 13.1 0.4 420 0 5 5 37.214 74.427 0.393 3.68 4 30.2 1.9 421 7 0 2 37.215 74.43 0.393 3.68 2 21.1 0.5 422 2 4 6 37.221 74.443 0.393 3.68 4 10.5 0.2 423 0 6 0 37.281 74.562 0.393 3.67 2 7.3 0.1 424 3 5 3 37.306 74.612 0.393 3.66 4 19.4 0.8 425 6 3 2 37.316 74.632 0.393 3.66 4 9.2 0.2 426 5 0 6 37.355 74.71 0.394 3.65 2 53.1 3.0 427 7 2 -2 37.397 74.795 0.394 3.65 4 6.0 0.1 428 4 5 -2 37.422 74.843 0.394 3.64 4 14.5 0.4 429 0 1 9 37.451 74.901 0.395 3.64 4 30.6 2.0 430 7 2 0 37.462 74.924 0.395 3.64 4 7.4 0.1 431 3 5 -4 37.473 74.945 0.395 3.63 4 10.0 0.2 432 0 6 1 37.545 75.089 0.396 3.62 4 4.1 0.0 433 1 3 -8 37.57 75.141 0.396 3.62 4 17.8 0.7 434 4 5 1 37.59 75.18 0.396 3.61 4 1.7 0.0 435 6 3 -4 37.601 75.202 0.396 3.61 4 19.8 0.8 436 2 1 -9 37.607 75.214 0.396 3.61 4 2.2 0.0 437 7 1 -4 37.626 75.251 0.396 3.61 4 18.4 0.7 438 4 1 7 37.636 75.273 0.396 3.61 4 32.9 2.2 439 2 2 8 37.659 75.319 0.397 3.6 4 25.3 1.3 440 1 6 0 37.68 75.359 0.397 3.6 4 2.7 0.0 441 5 4 -4 37.768 75.537 0.398 3.58 4 15.7 0.5 442 0 3 8 37.81 75.62 0.398 3.58 4 28.2 1.6 443 7 1 2 37.819 75.639 0.398 3.57 4 23.8 1.2 444 1 6 -1 37.863 75.725 0.398 3.57 4 2.6 0.0 445 3 0 8 37.872 75.744 0.398 3.57 2 22.9 0.5 446 1 4 -7 37.931 75.863 0.399 3.56 4 13.3 0.4 447 5 1 6 37.959 75.917 0.399 3.55 4 33.5 2.3 448 4 3 -7 38.0 76.0 0.4 3.54 4 31.1 2.0 449 5 3 -6 38.004 76.007 0.4 3.54 4 7.2 0.1 450 5 2 -7 38.005 76.009 0.4 3.54 4 32.6 2.2 451 2 5 -5 38.008 76.017 0.4 3.54 4 5.2 0.1 452 1 5 5 38.011 76.021 0.4 3.54 4 24.3 1.2 453 1 6 1 38.022 76.043 0.4 3.54 4 7.4 0.1 454 0 4 7 38.091 76.182 0.4 3.53 4 19.3 0.8 455 2 3 -8 38.125 76.25 0.401 3.52 4 47.6 4.6 456 7 2 -3 38.153 76.306 0.401 3.52 4 17.1 0.6 457 7 2 1 38.282 76.563 0.402 3.5 4 45.1 4.1 458 0 6 2 38.331 76.663 0.403 3.49 4 14.9 0.4 459 6 2 4 38.407 76.815 0.403 3.48 4 8.4 0.1 460 4 5 -3 38.415 76.83 0.403 3.48 4 37.7 2.8 461 3 1 8 38.473 76.946 0.404 3.47 4 15.9 0.5 462 1 1 9 38.563 77.125 0.405 3.45 4 22.8 1.0 463 2 4 -7 38.564 77.127 0.405 3.45 4 37.5 2.8 464 1 6 -2 38.568 77.136 0.405 3.45 4 12.7 0.3 465 4 2 -8 38.603 77.206 0.405 3.45 4 30.0 1.8 466 4 5 2 38.693 77.386 0.406 3.43 4 6.7 0.1 467 5 4 3 38.714 77.428 0.406 3.43 4 8.3 0.1 468 4 3 6 38.724 77.447 0.406 3.43 4 1.1 0.0 469 1 3 8 38.84 77.68 0.407 3.41 4 13.1 0.3 470 2 6 0 38.867 77.734 0.407 3.41 4 2.5 0.0 471 3 1 -9 38.873 77.746 0.407 3.41 4 24.9 1.2 472 6 2 -6 38.878 77.756 0.407 3.41 4 7.8 0.1 473 1 6 2 38.884 77.769 0.407 3.41 4 22.4 1.0 474 1 2 -9 38.935 77.87 0.408 3.4 4 30.5 1.8 475 2 6 -1 38.969 77.939 0.408 3.39 4 16.6 0.5 476 1 4 7 39.04 78.08 0.409 3.38 4 22.2 1.0 477 6 3 3 39.1 78.201 0.409 3.38 4 4.4 0.0 478 3 3 7 39.113 78.226 0.409 3.37 4 34.4 2.3 479 4 4 -6 39.118 78.236 0.41 3.37 4 41.4 3.3 480 5 0 -8 39.127 78.253 0.41 3.37 2 59.3 3.4 481 0 2 9 39.251 78.502 0.411 3.35 4 3.8 0.0 482 2 6 1 39.285 78.569 0.411 3.35 4 21.7 0.9 483 6 4 -1 39.306 78.613 0.411 3.35 4 54.0 5.6 484 3 5 4 39.374 78.748 0.412 3.34 4 18.4 0.7 485 2 2 -9 39.405 78.811 0.412 3.33 4 25.6 1.3 486 7 1 -5 39.421 78.842 0.412 3.33 4 9.1 0.2 487 7 2 -4 39.424 78.847 0.412 3.33 4 37.9 2.7 488 6 1 5 39.431 78.861 0.412 3.33 4 17.7 0.6 489 4 2 7 39.434 78.868 0.412 3.33 4 8.9 0.2 490 3 3 -8 39.464 78.928 0.413 3.32 4 12.3 0.3 491 6 3 -5 39.475 78.95 0.413 3.32 4 8.8 0.1 492 5 3 5 39.483 78.967 0.413 3.32 4 2.6 0.0 493 6 4 0 39.519 79.038 0.413 3.32 4 40.2 3.1 494 3 5 -5 39.584 79.169 0.414 3.31 4 6.4 0.1 495 2 5 5 39.588 79.176 0.414 3.31 4 2.8 0.0 496 2 6 -2 39.59 79.181 0.414 3.31 4 20.7 0.8 497 6 4 -2 39.612 79.225 0.414 3.3 4 50.8 4.9 498 7 2 2 39.614 79.229 0.414 3.3 4 12.6 0.3 499 0 6 3 39.632 79.264 0.414 3.3 4 31.6 1.9 500 3 4 6 39.673 79.347 0.414 3.3 4 6.1 0.1 501 7 1 3 39.675 79.35 0.414 3.3 4 8.4 0.1 502 5 4 -5 39.719 79.437 0.415 3.29 4 9.4 0.2 503 5 1 -8 39.722 79.444 0.415 3.29 4 20.2 0.8 504 4 4 5 39.725 79.451 0.415 3.29 4 21.7 0.9 505 5 2 6 39.752 79.503 0.415 3.29 4 24.9 1.2 506 1 6 -3 39.788 79.576 0.415 3.28 4 17.3 0.6 507 4 5 -4 39.918 79.836 0.417 3.27 4 10.4 0.2 508 3 4 -7 39.977 79.953 0.417 3.26 4 3.5 0.0 509 6 1 -7 39.991 79.982 0.417 3.26 4 6.8 0.1 510 1 5 -6 40.004 80.008 0.417 3.25 4 21.5 0.9 511 0 5 6 40.083 80.166 0.418 3.24 4 0.2 0.0 512 7 3 -1 40.16 80.32 0.419 3.23 4 22.7 1.0 513 2 6 2 40.217 80.435 0.419 3.23 4 16.3 0.5 514 6 4 1 40.248 80.495 0.419 3.22 4 3.0 0.0 515 1 6 3 40.258 80.516 0.419 3.22 4 3.6 0.0 516 3 2 8 40.26 80.519 0.419 3.22 4 12.4 0.3 517 4 5 3 40.303 80.606 0.42 3.22 4 13.3 0.3 518 1 2 9 40.348 80.696 0.42 3.21 4 32.9 2.0 519 7 3 -2 40.386 80.772 0.421 3.21 4 20.5 0.8 520 5 5 -1 40.423 80.846 0.421 3.2 4 5.2 0.0 521 6 4 -3 40.434 80.867 0.421 3.2 4 21.9 0.9 522 2 1 9 40.447 80.893 0.421 3.2 4 19.4 0.7 523 7 3 0 40.449 80.899 0.421 3.2 4 25.3 1.2 524 5 5 0 40.556 81.112 0.422 3.19 4 5.2 0.0 525 2 3 8 40.642 81.285 0.423 3.18 4 27.0 1.3 526 3 2 -9 40.655 81.309 0.423 3.18 4 17.7 0.6 527 2 5 -6 40.705 81.41 0.423 3.17 4 14.2 0.4 528 2 6 -3 40.724 81.448 0.423 3.17 4 6.0 0.1 529 8 0 -2 40.755 81.509 0.424 3.17 2 4.4 0.0 530 2 4 7 40.762 81.524 0.424 3.16 4 8.1 0.1 531 5 5 -2 40.805 81.609 0.424 3.16 4 3.5 0.0 532 3 6 0 40.824 81.647 0.424 3.16 4 16.9 0.5 533 3 6 -1 40.847 81.694 0.425 3.15 4 40.6 3.0 534 4 1 -9 40.906 81.811 0.425 3.15 4 39.2 2.8 535 5 4 4 40.916 81.833 0.425 3.15 4 20.0 0.7 536 1 5 6 40.941 81.882 0.425 3.14 4 22.6 0.9 537 8 0 0 40.974 81.947 0.426 3.14 2 23.3 0.5 538 5 3 -7 40.981 81.961 0.426 3.14 4 5.6 0.1 539 7 0 -6 41.118 82.236 0.427 3.13 2 18.4 0.3 540 7 3 -3 41.126 82.252 0.427 3.12 4 22.3 0.9 541 7 2 -5 41.197 82.393 0.428 3.12 4 9.7 0.2 542 8 1 -1 41.197 82.394 0.428 3.12 4 7.5 0.1 543 5 5 1 41.203 82.405 0.428 3.12 4 40.9 3.0 544 6 2 5 41.206 82.413 0.428 3.12 4 20.7 0.8 545 4 0 8 41.246 82.492 0.428 3.11 2 33.1 1.0 546 7 3 1 41.252 82.504 0.428 3.11 4 25.9 1.2 547 3 6 1 41.314 82.628 0.429 3.11 4 28.6 1.5 548 8 1 -2 41.344 82.688 0.429 3.1 4 5.6 0.1 549 6 3 4 41.376 82.751 0.429 3.1 4 2.9 0.0 550 3 6 -2 41.383 82.767 0.429 3.1 4 1.9 0.0 551 1 0 -10 41.39 82.781 0.429 3.1 2 28.8 0.7 552 7 0 4 41.433 82.866 0.43 3.09 2 16.6 0.2 553 0 6 4 41.434 82.869 0.43 3.09 4 8.3 0.1 554 7 2 3 41.449 82.897 0.43 3.09 4 12.2 0.3 555 6 4 2 41.486 82.973 0.43 3.09 4 13.8 0.3 556 5 2 -8 41.495 82.989 0.43 3.09 4 20.8 0.8 557 1 6 -4 41.511 83.023 0.43 3.09 4 11.6 0.2 558 8 1 0 41.563 83.125 0.431 3.08 4 21.1 0.8 559 4 3 -8 41.568 83.135 0.431 3.08 4 6.3 0.1 560 2 6 3 41.658 83.316 0.431 3.07 4 7.8 0.1 561 5 5 -3 41.698 83.397 0.432 3.07 4 23.5 1.0 562 7 1 -6 41.707 83.413 0.432 3.07 4 12.0 0.3 563 5 1 7 41.714 83.428 0.432 3.07 4 39.3 2.7 564 1 4 -8 41.734 83.468 0.432 3.06 4 22.6 0.9 565 6 2 -7 41.761 83.523 0.432 3.06 4 9.9 0.2 566 6 4 -4 41.764 83.527 0.432 3.06 4 18.8 0.6 567 2 0 -10 41.776 83.553 0.432 3.06 2 13.3 0.2 568 0 0 10 41.779 83.559 0.432 3.06 2 7.7 0.1 569 4 1 8 41.834 83.669 0.433 3.05 4 36.9 2.4 570 6 3 -6 41.838 83.676 0.433 3.05 4 5.6 0.1 571 1 3 -9 41.894 83.788 0.433 3.05 4 25.2 1.1 572 4 5 -5 41.919 83.839 0.434 3.05 4 1.6 0.0 573 3 5 5 41.925 83.849 0.434 3.05 4 3.2 0.0 574 0 4 8 41.967 83.935 0.434 3.04 4 22.2 0.9 575 1 1 -10 41.978 83.956 0.434 3.04 4 32.5 1.8 576 8 1 -3 42.003 84.007 0.434 3.04 4 2.6 0.0 577 7 1 4 42.021 84.042 0.435 3.04 4 8.4 0.1 578 1 6 4 42.132 84.264 0.435 3.03 4 17.7 0.5 579 6 0 6 42.137 84.275 0.435 3.03 2 30.4 0.8 580 4 4 -7 42.152 84.305 0.436 3.02 4 15.5 0.4 581 5 4 -6 42.156 84.312 0.436 3.02 4 7.4 0.1 582 3 5 -6 42.178 84.357 0.436 3.02 4 2.7 0.0 583 0 3 9 42.205 84.41 0.436 3.02 4 13.0 0.3 584 2 2 9 42.213 84.426 0.436 3.02 4 16.3 0.5 585 2 4 -8 42.275 84.549 0.437 3.01 4 45.2 3.5 586 3 6 2 42.315 84.629 0.437 3.01 4 35.9 2.2 587 2 3 -9 42.357 84.714 0.437 3.01 4 47.4 3.9 588 5 5 2 42.359 84.717 0.437 3.01 4 8.7 0.1 589 2 6 -4 42.362 84.725 0.437 3.01 4 26.4 1.2 590 2 1 -10 42.363 84.727 0.437 3.01 4 2.6 0.0 591 0 1 10 42.366 84.733 0.437 3.01 4 18.0 0.6 592 7 3 -4 42.375 84.749 0.437 3.0 4 12.8 0.3 593 4 3 7 42.385 84.77 0.438 3.0 4 9.9 0.2 594 4 5 4 42.409 84.819 0.438 3.0 4 15.0 0.4 595 3 6 -3 42.43 84.86 0.438 3.0 4 22.7 0.9 596 8 1 1 42.439 84.878 0.438 3.0 4 2.0 0.0 597 7 3 2 42.563 85.126 0.439 2.99 4 13.8 0.3 598 2 5 6 42.569 85.139 0.439 2.99 4 2.2 0.0 599 8 0 -4 42.585 85.171 0.439 2.99 2 11.9 0.1 600 4 2 -9 42.669 85.338 0.44 2.98 4 42.6 3.1 601 5 3 6 42.698 85.397 0.44 2.98 4 38.3 2.5 602 6 1 6 42.724 85.447 0.44 2.98 4 38.8 2.6 603 6 0 -8 42.782 85.565 0.441 2.97 2 14.7 0.2 604 4 4 6 42.859 85.719 0.442 2.96 4 5.9 0.1 605 3 0 -10 42.935 85.87 0.442 2.96 2 33.8 1.0 606 1 0 10 42.941 85.881 0.442 2.96 2 16.2 0.2 607 8 2 -1 42.958 85.916 0.442 2.96 4 36.3 2.2 608 1 4 8 42.973 85.947 0.442 2.96 4 16.4 0.5 609 3 1 9 43.083 86.166 0.443 2.95 4 38.5 2.5 610 5 5 -4 43.099 86.198 0.444 2.95 4 2.7 0.0 611 8 2 -2 43.105 86.209 0.444 2.95 4 52.5 4.7 612 8 1 -4 43.171 86.342 0.444 2.94 4 18.5 0.6 613 3 3 8 43.2 86.399 0.444 2.94 4 28.2 1.3 614 6 4 3 43.229 86.457 0.445 2.94 4 27.2 1.2 615 8 0 2 43.237 86.474 0.445 2.94 2 6.5 0.0 616 3 4 7 43.241 86.482 0.445 2.94 4 45.6 3.5 617 1 5 -7 43.257 86.515 0.445 2.93 4 0.8 0.0 618 1 3 9 43.287 86.575 0.445 2.93 4 28.7 1.4 619 8 2 0 43.322 86.643 0.445 2.93 4 31.0 1.6 620 6 1 -8 43.368 86.736 0.446 2.93 4 19.2 0.6 621 0 5 7 43.413 86.825 0.446 2.92 4 72.0 8.7 622 7 2 -6 43.465 86.93 0.447 2.92 4 11.0 0.2 623 5 2 7 43.472 86.945 0.447 2.92 4 32.7 1.8 624 4 6 -1 43.478 86.956 0.447 2.92 4 40.1 2.7 625 3 1 -10 43.52 87.04 0.447 2.92 4 14.1 0.3 626 1 1 10 43.526 87.051 0.447 2.92 4 15.1 0.4 627 4 6 0 43.532 87.064 0.447 2.92 4 35.9 2.1 628 3 4 -8 43.586 87.171 0.448 2.91 4 7.0 0.1 629 3 3 -9 43.59 87.181 0.448 2.91 4 10.5 0.2 630 4 2 8 43.592 87.184 0.448 2.91 4 19.9 0.7 631 6 4 -5 43.596 87.193 0.448 2.91 4 23.3 0.9 632 2 6 4 43.6 87.199 0.448 2.91 4 23.5 0.9 633 5 4 5 43.604 87.209 0.448 2.91 4 12.7 0.3 634 5 1 -9 43.689 87.379 0.448 2.9 4 19.6 0.6 635 1 6 -5 43.731 87.463 0.449 2.9 4 10.6 0.2 636 0 6 5 43.732 87.464 0.449 2.9 4 21.0 0.7 637 1 2 -10 43.735 87.47 0.449 2.9 4 14.1 0.3 638 8 2 -3 43.76 87.52 0.449 2.9 4 38.9 2.5 639 7 2 4 43.778 87.555 0.449 2.9 4 0.7 0.0 640 3 6 3 43.821 87.642 0.449 2.9 4 7.9 0.1 641 8 1 2 43.822 87.644 0.449 2.9 4 14.3 0.3 642 2 5 -7 43.873 87.746 0.45 2.89 4 3.1 0.0 643 4 6 -2 43.933 87.866 0.45 2.89 4 38.2 2.4 644 3 6 -4 43.982 87.964 0.451 2.89 4 11.5 0.2 645 5 5 3 44.019 88.039 0.451 2.88 4 5.3 0.0 646 4 6 1 44.095 88.191 0.452 2.88 4 26.7 1.2 647 2 2 -10 44.119 88.238 0.452 2.88 4 30.6 1.5 648 0 2 10 44.122 88.244 0.452 2.88 4 18.5 0.6 649 7 3 -5 44.127 88.255 0.452 2.88 4 7.7 0.1 650 6 3 5 44.137 88.274 0.452 2.88 4 15.0 0.4 651 8 2 1 44.194 88.388 0.452 2.87 4 15.0 0.4 652 7 4 -1 44.271 88.541 0.453 2.87 4 0.6 0.0 653 1 5 7 44.338 88.676 0.454 2.86 4 26.3 1.1 654 7 3 3 44.377 88.755 0.454 2.86 4 13.5 0.3 655 4 5 -6 44.414 88.829 0.454 2.86 4 18.0 0.5 656 5 3 -8 44.423 88.846 0.454 2.86 4 14.0 0.3 657 6 2 6 44.478 88.956 0.455 2.86 4 32.0 1.7 658 7 1 -7 44.48 88.961 0.455 2.86 4 20.1 0.7 659 7 4 -2 44.494 88.987 0.455 2.86 4 3.9 0.0 660 2 6 -5 44.501 89.002 0.455 2.85 4 21.8 0.8 661 1 6 5 44.503 89.006 0.455 2.85 4 4.8 0.0 662 7 4 0 44.556 89.112 0.455 2.85 4 27.3 1.2 663 6 5 -1 44.599 89.199 0.456 2.85 4 1.4 0.0 664 6 3 -7 44.688 89.376 0.456 2.84 4 6.7 0.1 665 2 4 8 44.747 89.494 0.457 2.84 4 7.4 0.1 666 6 5 0 44.808 89.615 0.457 2.84 4 35.5 2.0 667 3 2 9 44.836 89.673 0.458 2.84 4 35.8 2.1 668 8 1 -5 44.844 89.688 0.458 2.84 4 1.5 0.0 669 7 1 5 44.855 89.71 0.458 2.84 4 23.1 0.9 670 4 0 -10 44.86 89.719 0.458 2.84 2 71.2 4.1 671 2 0 10 44.868 89.737 0.458 2.84 2 40.9 1.4 672 4 6 -3 44.896 89.793 0.458 2.83 4 35.9 2.1 673 6 5 -2 44.9 89.799 0.458 2.83 4 39.3 2.5 674 8 2 -4 44.924 89.848 0.458 2.83 4 0.4 0.0 675 3 5 6 44.96 89.919 0.459 2.83 4 21.2 0.7 X-ray diffraction powder data (I)...X-Ray wave length = 1.54056 (angs.): No H K L Theta 2*Theta d I int I int.n. I p.h.n. H(Si) ( degree ) (angstrem) *100 *100 1 1 0 0 4.701 9.403 9.39779 132.8 36.1 36.6 5.6 2 1 1 0 7.472 14.944 5.92351 66.1 18.0 18.2 5.6 3 0 0 2 7.658 15.315 5.78058 64.2 17.4 17.6 5.6 4 1 1 -1 8.131 16.261 5.44633 261.5 71.1 71.8 5.6 5 1 1 1 8.665 17.329 5.11308 150.2 40.8 41.2 5.6 6 2 0 0 9.435 18.87 4.6989 68.0 18.5 18.7 5.6 7 1 0 2 9.487 18.974 4.67336 7.3 2.0 2.0 5.6 8 0 1 2 9.624 19.247 4.60758 50.6 13.7 13.9 5.6 9 1 1 -2 10.301 20.601 4.30776 71.3 19.4 19.5 5.6 10 2 1 0 11.1 22.2 4.00103 22.2 6.0 6.1 5.6 11 1 1 2 11.144 22.289 3.98523 29.0 7.9 7.9 5.6 12 2 1 -1 11.362 22.724 3.90996 4.6 1.2 1.3 5.6 13 0 2 0 11.649 23.297 3.815 51.2 13.9 14.0 5.6 14 2 1 1 12.136 24.271 3.66403 44.1 12.0 12.0 5.6 15 2 1 -2 12.847 25.693 3.4644 30.1 8.2 8.2 5.6 16 0 1 3 12.94 25.88 3.43986 7.0 1.9 1.9 5.6 17 1 2 -1 12.997 25.993 3.42506 39.9 10.8 10.9 5.6 18 1 1 -3 13.287 26.574 3.35148 12.8 3.5 3.5 5.6 19 0 2 2 14.0 27.999 3.18408 10.0 2.7 2.7 5.6 20 2 1 2 14.204 28.407 3.13929 42.4 11.5 11.5 5.6 21 3 0 0 14.235 28.469 3.1326 6.5 1.8 1.8 5.6 22 2 2 0 15.075 30.149 2.96176 213.4 58.0 58.0 5.6 23 2 2 -1 15.273 30.545 2.92424 368.0 100.0 100.0 5.6 24 3 0 -2 15.358 30.715 2.90844 20.6 5.6 5.6 5.6 25 3 1 0 15.415 30.83 2.89787 26.9 7.3 7.3 5.6 26 0 0 4 15.456 30.913 2.89029 149.9 40.7 40.7 5.6 27 1 0 -4 15.605 31.209 2.86354 8.5 2.3 2.3 5.6 28 2 2 1 15.869 31.738 2.81697 64.4 17.5 17.5 5.6 29 3 1 1 16.338 32.676 2.73824 8.7 2.4 2.4 5.6 30 2 2 -2 16.431 32.862 2.72317 72.1 19.6 19.6 5.6 31 3 1 -2 16.465 32.93 2.71769 7.7 2.1 2.1 5.6 32 0 1 4 16.558 33.116 2.70287 6.0 1.6 1.6 5.6 33 1 2 -3 16.785 33.571 2.66729 31.2 8.5 8.5 5.7 34 3 0 2 17.083 34.167 2.62212 17.4 4.7 4.7 5.7 35 2 2 2 17.536 35.071 2.55654 7.1 1.9 1.9 5.7 36 1 2 3 17.605 35.21 2.54681 15.6 4.2 4.2 5.7 37 0 3 1 18.066 36.131 2.48394 5.0 1.4 1.3 5.7 38 3 1 2 18.097 36.194 2.47977 4.9 1.3 1.3 5.7 39 1 3 0 18.286 36.572 2.45502 14.2 3.9 3.8 5.7 40 2 2 -3 18.388 36.777 2.44178 3.7 1.0 1.0 5.7 41 3 2 0 18.552 37.104 2.421 14.1 3.8 3.8 5.7 42 1 3 -1 18.581 37.162 2.41734 12.7 3.4 3.4 5.7 43 3 2 1 19.343 38.686 2.32558 43.0 11.7 11.6 5.7 44 3 2 -2 19.453 38.906 2.31295 8.1 2.2 2.2 5.7 45 3 0 -4 19.853 39.706 2.26814 13.8 3.8 3.7 5.7 46 4 1 -1 19.978 39.957 2.25448 11.0 3.0 3.0 5.7 47 4 1 0 20.063 40.125 2.24541 4.3 1.2 1.2 5.7 48 1 3 2 20.17 40.34 2.23394 8.2 2.2 2.2 5.7 49 0 1 5 20.371 40.741 2.21286 8.2 2.2 2.2 5.7 50 1 2 4 20.609 41.218 2.18837 5.8 1.6 1.6 5.7 51 2 3 1 20.768 41.536 2.17235 15.6 4.2 4.2 5.7 52 3 2 2 20.883 41.766 2.16092 16.8 4.6 4.5 5.7 53 4 1 1 20.921 41.842 2.15717 27.2 7.4 7.3 5.7 54 3 2 -3 21.055 42.109 2.14409 18.7 5.1 5.0 5.7 55 2 3 -2 21.217 42.434 2.12845 19.6 5.3 5.3 5.7 56 1 1 5 21.525 43.05 2.09941 20.4 5.5 5.5 5.7 57 4 0 2 21.642 43.284 2.0886 4.1 1.1 1.1 5.7 58 2 3 2 22.116 44.232 2.04599 78.1 21.2 20.9 5.7 59 4 1 2 22.481 44.961 2.01449 26.0 7.1 7.0 5.7 60 3 0 4 22.597 45.193 2.00467 5.5 1.5 1.5 5.7 61 4 2 0 22.646 45.293 2.00052 4.0 1.1 1.1 5.7 62 2 2 4 22.741 45.482 1.99262 34.5 9.4 9.2 5.7 63 2 3 -3 22.824 45.649 1.98573 23.0 6.3 6.2 5.7 64 3 1 4 23.408 46.817 1.93887 16.6 4.5 4.4 5.7 65 0 0 6 23.563 47.126 1.92686 13.7 3.7 3.7 5.7 66 3 3 1 23.63 47.26 1.9217 9.0 2.5 2.4 5.7 67 3 3 -2 23.724 47.448 1.91456 10.3 2.8 2.8 5.7 68 0 4 0 23.817 47.634 1.9075 4.7 1.3 1.3 5.7 69 2 2 -5 23.978 47.957 1.89541 70.0 19.0 18.7 5.7 70 2 3 3 24.092 48.184 1.88702 20.0 5.4 5.4 5.7 71 4 1 -4 24.133 48.267 1.88396 33.7 9.1 9.0 5.7 72 5 0 0 24.194 48.387 1.87956 9.0 2.4 2.4 5.7 73 0 1 6 24.35 48.7 1.86821 14.6 4.0 3.9 5.7 74 5 0 -2 24.521 49.042 1.85598 10.3 2.8 2.7 5.7 75 4 1 3 24.638 49.275 1.84774 5.3 1.4 1.4 5.7 76 5 1 -1 24.793 49.587 1.83686 5.2 1.4 1.4 5.7 77 2 3 -4 25.019 50.037 1.82138 18.7 5.1 5.0 5.7 78 3 3 -3 25.106 50.212 1.81544 4.6 1.2 1.2 5.8 79 0 4 2 25.165 50.331 1.81143 6.0 1.6 1.6 5.8 80 1 1 6 25.46 50.919 1.79186 7.9 2.2 2.1 5.8 81 3 2 4 25.726 51.451 1.77459 12.5 3.4 3.3 5.8 82 1 4 2 25.859 51.718 1.76605 11.8 3.2 3.1 5.8 83 2 2 5 25.993 51.987 1.75756 4.1 1.1 1.1 5.8 84 4 1 -5 26.689 53.378 1.71498 5.3 1.4 1.4 5.8 85 4 3 -2 27.007 54.013 1.6963 4.5 1.2 1.2 5.8 86 4 3 1 27.207 54.414 1.68475 9.7 2.6 2.6 5.8 87 2 2 -6 27.366 54.731 1.67574 4.5 1.2 1.2 5.8 88 2 1 6 27.487 54.974 1.66891 4.6 1.3 1.2 5.8 89 1 3 5 27.705 55.41 1.6568 5.4 1.5 1.4 5.8 90 4 3 -3 28.18 56.36 1.63111 4.0 1.1 1.1 5.8 91 1 1 -7 28.317 56.633 1.62389 5.7 1.6 1.5 5.8 92 5 2 -3 28.554 57.109 1.61149 4.4 1.2 1.2 5.8 93 3 2 5 28.821 57.642 1.59783 3.7 1.0 1.0 5.8 94 4 0 -6 28.996 57.993 1.58901 3.7 1.0 1.0 5.8 95 5 1 3 29.219 58.438 1.57796 5.6 1.5 1.5 5.8 96 5 2 2 29.33 58.659 1.57253 4.5 1.2 1.2 5.8 97 2 3 5 29.537 59.074 1.56247 6.4 1.7 1.7 5.8 98 2 2 6 29.575 59.15 1.56066 5.3 1.4 1.4 5.8 99 6 1 0 30.135 60.27 1.5343 4.4 1.2 1.2 5.8 100 0 5 1 30.607 61.214 1.51288 3.9 1.1 1.0 5.8 101 1 5 0 30.756 61.512 1.50627 9.0 2.4 2.4 5.8 102 2 3 -6 30.804 61.608 1.50415 4.6 1.3 1.2 5.8 103 6 1 -3 31.162 62.324 1.48858 4.7 1.3 1.2 5.8 104 4 4 -1 31.281 62.563 1.48347 14.2 3.9 3.7 5.8 105 4 4 0 31.342 62.685 1.48088 8.3 2.3 2.2 5.8 106 0 4 5 31.567 63.134 1.47142 11.9 3.2 3.1 5.9 107 4 4 -2 31.791 63.582 1.46212 10.6 2.9 2.8 5.9 108 4 4 1 31.972 63.945 1.4547 7.3 2.0 1.9 5.9 109 5 2 -5 32.332 64.665 1.44024 4.5 1.2 1.2 5.9 110 6 1 -4 32.631 65.261 1.4285 8.3 2.3 2.2 5.9 111 0 5 3 32.882 65.763 1.41881 26.8 7.3 7.0 5.9 112 4 0 6 33.186 66.372 1.40726 3.8 1.0 1.0 5.9 113 6 1 3 34.218 68.436 1.36978 4.9 1.3 1.3 5.9 114 6 1 -5 34.612 69.223 1.3561 7.2 1.9 1.9 5.9 115 5 4 -1 34.984 69.968 1.34348 12.8 3.5 3.3 5.9 116 5 4 0 35.124 70.247 1.33882 5.2 1.4 1.3 5.9 117 5 4 -3 36.318 72.636 1.30056 4.3 1.2 1.1 6.0 118 7 1 1 36.466 72.931 1.29603 4.2 1.1 1.1 6.0 119 4 4 -5 36.548 73.095 1.29352 4.8 1.3 1.2 6.0 120 4 1 -8 36.793 73.585 1.28612 4.6 1.3 1.2 6.0 121 5 2 -7 38.005 76.009 1.25101 5.6 1.5 1.4 6.0 122 2 3 -8 38.125 76.25 1.24766 5.2 1.4 1.3 6.0 123 7 2 1 38.282 76.563 1.24333 4.1 1.1 1.0 6.0 124 2 4 -7 38.564 77.127 1.23564 4.1 1.1 1.1 6.0 125 5 0 -8 39.127 78.253 1.22066 9.0 2.4 2.3 6.0 126 6 4 -1 39.306 78.613 1.21597 5.6 1.5 1.4 6.0 127 7 2 -4 39.424 78.847 1.21295 4.9 1.3 1.2 6.0 128 6 4 -2 39.612 79.225 1.20811 7.1 1.9 1.8 6.0 129 5 5 1 41.203 82.405 1.16935 3.7 1.0 0.9 6.1 130 2 3 -9 42.357 84.714 1.14328 6.2 1.7 1.6 6.1 131 4 2 -9 42.669 85.338 1.13651 5.6 1.5 1.4 6.1 132 8 2 -2 43.105 86.209 1.12724 7.2 1.9 1.8 6.1 133 0 5 7 43.413 86.825 1.12082 8.7 2.4 2.2 6.1 134 4 6 -1 43.478 86.956 1.11947 4.5 1.2 1.1 6.1 135 4 0 -10 44.86 89.719 1.09202 9.6 2.6 2.4 6.2 136 6 5 -2 44.9 89.799 1.09126 4.6 1.3 1.1 6.2 Reference: Chichagov A.V. et al. Information-Calculating System on Crystal Structure Data of Minerals (MINCRYST) - Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian) |