Institute of Experimental Mineralogy Russian Academy of Sciences ------------------------------------------------- 142432, Chernogolovka, Moscow district A.V. Chichagov +7(496)52-22320 *** *** W W W - X R A Y P O L *** *********************** KARLITE 1, DN [Mg(6.05)Al(0.3)Fe(0.15)][BO(3)](3)(OH)(4)Cl(0.4) Orthorhombic P 2(1)2(1)2 Z = 4 R =0.042 NR =875 18 .10 .1997 Ref.Str.: Bonazzi P., Sabelli C. et al. (1986) * Neues Jb. Miner., Mh., H.6, 253-262 Reserv: N.A.D. Initial data from BDM-file Lattice parameters (cub. angs.,degr.): a = 17.637 alpha = 90.0 b = 17.967 beta = 90.0 c = 3.104 gamma = 90.0 Unit cell volume (cub. angs.) = 983.61 Molar volume ( cub.cm/mol.) = 148.12 Co-ordinates, thermal parameters, occupation for atomic positions: NoP x/a y/b z/c B(j) atom / occupation 1 0.1608 0.3954 0.467 0.79 O = 1.00 2 0.3045 0.1938 0.003 0.88 O = 1.00 3 0.1797 0.2472 0.954 0.3 O = 1.00 4 0.2915 0.3271 0.953 0.31 O = 1.00 5 0.0394 0.3228 0.991 0.62 O = 1.00 6 0.0643 0.1852 0.445 0.52 O = 1.00 7 0.4104 0.1291 0.504 0.75 O = 1.00 8 0.0816 0.0301 0.764 0.5 O = 1.00 9 0.3078 0.4569 0.464 0.57 O = 1.00 10 0.3143 0.0351 0.998 0.68 O = 1.00 11 0.187 0.0918 0.47 0.57 O = 1.00 12 0.4556 0.3914 0.772 0.68 O = 1.00 13 0.4335 0.2744 0.484 0.7 O = 1.00 14 0.0 0.5 0.943 10.16 Cl = 0.4 , Cl = 0.0 15 0.4259 0.1984 0.999 0.53 Mg = 1.00 16 0.2985 0.1089 0.498 0.29 Mg = 1.00 17 0.3596 0.3601 0.447 0.71 Mg = 1.00 18 0.1265 0.143 0.956 0.47 Mg = 1.00 19 0.2295 0.4303 0.96 0.48 Mg = 1.00 20 0.1108 0.2929 0.47 0.52 Mg = 1.00 21 0.0 0.0 0.23 0.89 Mg = 1.00 22 0.2582 0.2555 0.968 0.46 B = 1.00 23 0.1527 0.0245 0.585 0.46 B = 1.00 24 0.4869 0.3275 0.602 0.51 B = 1.00 25 0.114 0.426 0.46 2.0 H = 1.00 26 0.026 0.378 0.976 2.0 H = 1.00 27 0.058 0.583 0.513 2.0 H = 1.00 28 0.13 0.525 0.984 2.0 H = 1.00 Co-ordinates for all atomic positions : No NoP x/a y/b z/c 1 1 0.1608 0.3954 0.467 2 2 0.3045 0.1938 0.003 3 3 0.1797 0.2472 0.954 4 4 0.2915 0.3271 0.953 5 5 0.0394 0.3228 0.991 6 6 0.0643 0.1852 0.445 7 7 0.4104 0.1291 0.504 8 8 0.0816 0.0301 0.764 9 9 0.3078 0.4569 0.464 10 10 0.3143 0.0351 0.998 11 11 0.187 0.0918 0.47 12 12 0.4556 0.3914 0.772 13 13 0.4335 0.2744 0.484 14 14 0.0 0.5 0.943 15 15 0.4259 0.1984 0.999 16 16 0.2985 0.1089 0.498 17 17 0.3596 0.3601 0.447 18 18 0.1265 0.143 0.956 19 19 0.2295 0.4303 0.96 20 20 0.1108 0.2929 0.47 21 21 0.0 0.0 0.23 22 22 0.2582 0.2555 0.968 23 23 0.1527 0.0245 0.585 24 24 0.4869 0.3275 0.602 25 25 0.114 0.426 0.46 26 26 0.026 0.378 0.976 27 27 0.058 0.583 0.513 28 28 0.13 0.525 0.984 29 1 0.8392 0.6046 0.467 30 2 0.6955 0.8062 0.003 31 3 0.8203 0.7528 0.954 32 4 0.7085 0.6729 0.953 33 5 0.9606 0.6772 0.991 34 6 0.9357 0.8148 0.445 35 7 0.5896 0.8709 0.504 36 8 0.9184 0.9699 0.764 37 9 0.6922 0.5431 0.464 38 10 0.6857 0.9649 0.998 39 11 0.813 0.9082 0.47 40 12 0.5444 0.6086 0.772 41 13 0.5665 0.7256 0.484 42 15 0.5741 0.8016 0.999 43 16 0.7015 0.8911 0.498 44 17 0.6404 0.6399 0.447 45 18 0.8735 0.857 0.956 46 19 0.7705 0.5697 0.96 47 20 0.8892 0.7071 0.47 48 22 0.7418 0.7445 0.968 49 23 0.8473 0.9755 0.585 50 24 0.5131 0.6725 0.602 51 25 0.886 0.574 0.46 52 26 0.974 0.622 0.976 53 27 0.942 0.417 0.513 54 28 0.87 0.475 0.984 55 1 0.3392 0.8954 0.533 56 2 0.1955 0.6938 0.997 57 3 0.3203 0.7472 0.046 58 4 0.2085 0.8271 0.047 59 5 0.4606 0.8228 0.009 60 6 0.4357 0.6852 0.555 61 7 0.0896 0.6291 0.496 62 8 0.4184 0.5301 0.236 63 9 0.1922 0.9569 0.536 64 10 0.1857 0.5351 0.002 65 11 0.313 0.5918 0.53 66 12 0.0444 0.8914 0.228 67 13 0.0665 0.7744 0.516 68 14 0.5 0.0 0.057 69 15 0.0741 0.6984 0.001 70 16 0.2015 0.6089 0.502 71 17 0.1404 0.8601 0.553 72 18 0.3735 0.643 0.044 73 19 0.2705 0.9303 0.04 74 20 0.3892 0.7929 0.53 75 21 0.5 0.5 0.77 76 22 0.2418 0.7555 0.032 77 23 0.3473 0.5245 0.415 78 24 0.0131 0.8275 0.398 79 25 0.386 0.926 0.54 80 26 0.474 0.878 0.024 81 27 0.442 0.083 0.487 82 28 0.37 0.025 0.016 83 1 0.6608 0.1046 0.533 84 2 0.8045 0.3062 0.997 85 3 0.6797 0.2528 0.046 86 4 0.7915 0.1729 0.047 87 5 0.5394 0.1772 0.009 88 6 0.5643 0.3148 0.555 89 7 0.9104 0.3709 0.496 90 8 0.5816 0.4699 0.236 91 9 0.8078 0.0431 0.536 92 10 0.8143 0.4649 0.002 93 11 0.687 0.4082 0.53 94 12 0.9556 0.1086 0.228 95 13 0.9335 0.2256 0.516 96 15 0.9259 0.3016 0.001 97 16 0.7985 0.3911 0.502 98 17 0.8596 0.1399 0.553 99 18 0.6265 0.357 0.044 100 19 0.7295 0.0697 0.04 101 20 0.6108 0.2071 0.53 102 22 0.7582 0.2445 0.032 103 23 0.6527 0.4755 0.415 104 24 0.9869 0.1725 0.398 105 25 0.614 0.074 0.54 106 26 0.526 0.122 0.024 107 27 0.558 0.917 0.487 108 28 0.63 0.975 0.016 X-ray density (g/cm cub.) = 2.76 MU (1/cm) = 62.922 Mass attenuation coefficient (cm**2/g) = 22.76 Selected interatomic distances (cation-anion,anion-anion): NoP Atom Rad.sph. C.N. Distance NoP N. (angs.) (angs.) 1 O 3.804 13 3.104 1 3.104 1 3.08 3 3.1204 3 3.0158 4 3.0602 4 2.9885 5 2.9101 5 2.8183 9 3.7092 14 3.771 14 3.0415 10 2.9285 10 2 O 3.804 11 3.104 2 3.104 2 2.4059 3 2.411 4 2.6941 7 2.6905 7 2.8566 10 3.1232 11 3.2234 11 3.0826 13 3.1415 13 3 O 3.804 11 3.1204 1 3.08 1 2.4059 2 3.104 3 3.104 3 2.439 4 2.8251 5 2.776 6 2.8071 6 3.2214 11 3.1732 11 4 O 3.804 11 3.0602 1 3.0158 1 2.411 2 2.439 3 3.104 4 3.104 4 2.835 9 2.7974 9 3.1665 12 3.1441 13 3.0476 13 5 O 3.804 12 2.9101 1 2.9885 1 2.8251 3 3.104 5 3.104 5 2.8794 6 3.0294 6 3.2621 14 2.8949 7 2.8782 7 3.0322 13 2.9517 13 6 O 3.804 13 2.8071 3 2.776 3 3.0294 5 2.8794 5 3.104 6 3.104 6 2.9731 8 3.511 8 2.7396 11 3.3877 12 2.4542 12 2.4284 13 3.7635 13 7 O 3.804 11 2.6905 2 2.6941 2 3.104 7 3.104 7 2.8419 10 2.8622 10 2.6429 13 3.29 14 3.1309 14 2.8949 5 2.8782 5 8 O 3.804 13 3.511 6 2.9731 6 3.104 8 3.104 8 3.0801 11 2.3489 11 3.0749 8 3.3581 9 2.4567 9 2.9521 12 3.0674 12 3.0003 12 3.1138 12 9 O 3.804 13 2.8183 1 2.7974 4 2.835 4 3.104 9 3.104 9 3.0156 12 3.5768 12 3.3581 8 2.4567 8 3.066 10 2.9442 10 2.4341 11 3.7799 11 10 O 3.804 12 2.8566 2 2.8622 7 2.8419 7 3.104 10 3.104 10 2.868 11 2.9605 11 3.0415 1 2.9285 1 3.066 9 2.9442 9 3.3404 14 11 O 3.804 13 3.2234 2 3.1232 2 3.1732 3 3.2214 3 2.7396 6 2.3489 8 3.0801 8 2.9605 10 2.868 10 3.104 11 3.104 11 2.4341 9 3.7799 9 12 O 3.804 13 3.1665 4 3.5768 9 3.0156 9 3.104 12 3.104 12 3.0749 13 2.3173 13 2.9521 8 3.0674 8 3.3877 6 2.4542 6 3.0003 8 3.1138 8 13 O 3.804 13 3.1415 2 3.0826 2 3.0476 4 3.1441 4 2.6429 7 2.3173 12 3.0749 12 3.104 13 3.104 13 3.0322 5 2.9517 5 2.4284 6 3.7635 6 14 Cl ,Cl 4.344 14 3.771 1 3.7092 1 3.2621 5 3.104 14 3.104 14 3.771 1 3.7092 1 3.2621 5 3.29 7 3.1309 7 3.3404 10 3.29 7 3.1309 7 3.3404 10 15 Mg 3.06 6 2.1428 2 2.0204 7 1.9964 7 2.0369 13 2.1066 13 2.038 5 16 Mg 3.06 6 2.1898 2 2.1677 2 2.0068 7 2.0602 10 2.0602 10 1.9923 11 17 Mg 3.06 6 2.0642 4 2.036 4 1.9653 9 2.0496 12 2.7519 12 2.0206 13 18 Mg 3.06 6 2.0941 3 2.0205 6 2.0722 6 2.2577 8 2.1284 11 2.0641 11 19 Mg 3.06 6 2.0828 1 2.0501 1 2.1527 4 2.1408 9 2.1227 9 2.0394 10 20 Mg 3.06 6 2.0419 1 2.0995 3 2.1717 3 2.1189 5 2.0211 5 2.1031 6 21 Mg 3.06 6 2.2608 8 2.1109 8 2.2608 8 2.1109 8 2.1025 12 2.1025 12 22 B 2.412 3 1.3811 2 1.3932 3 1.4149 4 23 B 2.412 3 1.3753 8 1.3984 11 1.4084 9 24 B 2.412 3 1.3789 12 1.3897 13 1.3917 6 25 H 2.172 1 0.992 1 26 H 2.172 1 1.0206 5 27 H 2.172 1 0.9997 7 28 H 2.172 1 1.0006 10 X-ray diffraction powder data (II), X-Ray W.L. = 1.54056(angs.): No H K L Theta 2*Theta S LPG MF F I int. ( degree ) *100 1 1 1 0 3.509 7.017 0.04 530.99 4 49.9 546.5 2 0 2 0 4.919 9.838 0.056 269.05 2 57.4 183.3 3 2 0 0 5.011 10.022 0.057 259.15 2 45.7 111.8 4 1 2 0 5.522 11.044 0.062 213.02 4 9.9 8.6 5 2 1 0 5.584 11.168 0.063 208.27 4 7.0 4.2 6 2 2 0 7.031 14.061 0.079 130.54 4 51.9 145.6 7 1 3 0 7.807 15.613 0.088 105.46 4 31.7 43.9 8 3 1 0 7.924 15.848 0.089 102.29 4 18.1 13.8 9 2 3 0 8.944 17.888 0.101 79.81 4 15.7 8.1 10 3 2 0 9.009 18.017 0.102 78.64 4 29.0 27.4 11 0 4 0 9.874 19.749 0.111 65.09 2 48.9 32.2 12 4 0 0 10.061 20.122 0.113 62.62 2 42.4 23.3 13 1 4 0 10.193 20.386 0.115 60.95 4 0.7 0.0 14 4 1 0 10.363 20.726 0.117 58.9 4 2.6 0.2 15 3 3 0 10.58 21.159 0.119 56.43 4 19.1 8.5 16 2 4 0 11.096 22.192 0.125 51.1 4 31.7 21.2 17 4 2 0 11.222 22.443 0.126 49.92 4 51.9 55.6 18 3 4 0 12.463 24.926 0.14 40.07 4 24.0 9.6 19 4 3 0 12.529 25.058 0.141 39.63 4 14.4 3.4 20 1 5 0 12.636 25.273 0.142 38.93 4 14.2 3.2 21 5 1 0 12.858 25.716 0.144 37.52 4 29.5 13.5 22 2 5 0 13.384 26.768 0.15 34.48 4 40.1 22.9 23 5 2 0 13.568 27.136 0.152 33.49 4 15.3 3.2 24 4 4 0 14.17 28.34 0.159 30.54 4 49.3 30.7 25 0 0 1 14.368 28.737 0.161 29.65 2 16.1 1.6 26 3 5 0 14.55 29.101 0.163 28.87 4 4.1 0.2 27 0 1 1 14.586 29.172 0.163 28.71 4 6.9 0.6 28 1 0 1 14.594 29.188 0.164 28.68 4 16.3 3.2 29 5 3 0 14.681 29.361 0.165 28.32 4 19.0 4.2 30 1 1 1 14.809 29.617 0.166 27.8 8 33.4 25.6 31 0 6 0 14.906 29.812 0.167 27.41 2 37.7 8.1 32 1 6 0 15.124 30.248 0.169 26.57 4 22.9 5.8 33 6 0 0 15.191 30.383 0.17 26.32 2 6.8 0.2 34 0 2 1 15.222 30.443 0.17 26.21 4 32.5 11.4 35 2 0 1 15.253 30.506 0.171 26.09 4 33.6 12.1 36 6 1 0 15.398 30.797 0.172 25.57 4 90.3 86.2 37 1 2 1 15.436 30.872 0.173 25.43 8 10.7 2.4 38 2 1 1 15.459 30.918 0.173 25.35 8 26.1 14.2 39 2 6 0 15.763 31.526 0.176 24.31 4 118.2 140.4 40 6 2 0 16.005 32.009 0.179 23.53 4 82.5 66.2 41 4 5 0 16.053 32.106 0.179 23.37 4 38.4 14.2 42 2 2 1 16.063 32.127 0.18 23.34 8 65.9 83.7 43 5 4 0 16.12 32.241 0.18 23.16 4 41.6 16.6 44 0 3 1 16.231 32.462 0.181 22.82 4 13.2 1.6 45 3 0 1 16.297 32.595 0.182 22.62 4 57.7 31.1 46 1 3 1 16.433 32.867 0.184 22.22 8 18.2 6.1 47 3 1 1 16.492 32.984 0.184 22.05 8 15.8 4.6 48 3 6 0 16.779 33.558 0.187 21.24 4 40.2 14.2 49 6 3 0 16.972 33.944 0.189 20.71 4 3.4 0.1 50 2 3 1 17.028 34.056 0.19 20.57 8 51.4 45.0 51 3 2 1 17.063 34.127 0.19 20.47 8 85.5 123.9 52 0 4 1 17.556 35.113 0.196 19.24 4 89.0 63.1 53 1 7 0 17.654 35.308 0.197 19.01 4 80.9 51.5 54 4 0 1 17.667 35.334 0.197 18.98 4 106.5 89.0 55 1 4 1 17.746 35.491 0.198 18.79 8 69.8 75.7 56 5 5 0 17.818 35.637 0.199 18.63 4 57.3 25.3 57 4 1 1 17.848 35.696 0.199 18.56 8 69.8 74.8 58 3 3 1 17.98 35.961 0.2 18.26 8 111.5 187.9 59 7 1 0 17.982 35.963 0.2 18.26 4 63.5 30.5 60 4 6 0 18.116 36.232 0.202 17.96 4 32.2 7.7 61 2 7 0 18.213 36.427 0.203 17.75 4 1.3 0.0 62 6 4 0 18.25 36.501 0.203 17.67 4 21.0 3.2 63 2 4 1 18.303 36.605 0.204 17.56 8 60.0 52.3 64 4 2 1 18.383 36.765 0.205 17.4 8 26.7 10.2 65 7 2 0 18.513 37.025 0.206 17.13 4 13.5 1.3 66 3 7 0 19.115 38.229 0.213 15.96 4 69.8 32.2 67 0 5 1 19.143 38.285 0.213 15.91 4 10.0 0.7 68 3 4 1 19.2 38.401 0.213 15.8 8 25.0 8.2 69 4 3 1 19.245 38.49 0.214 15.72 8 14.5 2.7 70 5 0 1 19.303 38.605 0.215 15.62 4 37.2 9.0 71 1 5 1 19.318 38.637 0.215 15.59 8 95.4 117.4 72 7 3 0 19.37 38.741 0.215 15.5 4 59.9 23.0 73 5 1 1 19.471 38.941 0.216 15.32 8 70.9 63.7 74 5 6 0 19.72 39.44 0.219 14.9 4 7.9 0.4 75 6 5 0 19.789 39.577 0.22 14.78 4 3.3 0.1 76 2 5 1 19.838 39.675 0.22 14.7 8 53.6 34.9 77 5 2 1 19.968 39.936 0.222 14.49 8 123.7 183.3 78 0 8 0 20.058 40.117 0.223 14.34 2 0.1 0.0 79 1 8 0 20.227 40.455 0.224 14.08 4 9.9 0.6 80 4 7 0 20.319 40.638 0.225 13.94 4 153.2 135.2 81 4 4 1 20.401 40.801 0.226 13.81 8 37.6 16.2 82 8 0 0 20.45 40.9 0.227 13.74 2 101.0 28.9 83 7 4 0 20.52 41.04 0.228 13.63 4 17.7 1.8 84 8 1 0 20.611 41.221 0.228 13.5 4 46.7 12.2 85 3 5 1 20.679 41.357 0.229 13.4 8 10.6 1.3 86 2 8 0 20.727 41.455 0.23 13.33 4 10.1 0.6 87 5 3 1 20.775 41.55 0.23 13.26 8 45.2 22.4 88 0 6 1 20.942 41.884 0.232 13.03 4 54.8 16.2 89 8 2 0 21.085 42.171 0.234 12.83 4 24.8 3.3 90 1 6 1 21.105 42.21 0.234 12.8 8 56.1 33.3 91 6 0 1 21.156 42.311 0.234 12.73 4 27.7 4.0 92 6 1 1 21.312 42.623 0.236 12.53 8 22.8 5.4 93 3 8 0 21.54 43.08 0.238 12.23 4 86.9 38.2 94 6 6 0 21.543 43.086 0.238 12.23 4 11.6 0.7 95 2 6 1 21.589 43.177 0.239 12.17 8 13.7 1.9 96 6 2 1 21.774 43.548 0.241 11.94 8 47.8 22.5 97 5 7 0 21.786 43.572 0.241 11.92 4 30.7 4.6 98 4 5 1 21.811 43.623 0.241 11.89 8 26.4 6.9 99 8 3 0 21.858 43.717 0.242 11.83 4 22.0 2.4 100 5 4 1 21.863 43.726 0.242 11.83 8 1.9 0.0 101 7 5 0 21.924 43.849 0.242 11.75 4 27.9 3.8 102 3 6 1 22.376 44.752 0.247 11.23 8 30.6 8.7 103 6 3 1 22.528 45.056 0.249 11.06 8 30.3 8.4 104 4 8 0 22.638 45.276 0.25 10.93 4 49.4 11.1 105 1 9 0 22.849 45.699 0.252 10.71 4 13.3 0.8 106 8 4 0 22.905 45.811 0.253 10.65 4 23.9 2.5 107 0 7 1 22.918 45.836 0.253 10.63 4 7.1 0.2 108 1 7 1 23.07 46.14 0.254 10.48 8 37.6 12.3 109 7 0 1 23.189 46.377 0.256 10.36 4 8.5 0.3 110 5 5 1 23.202 46.404 0.256 10.34 8 17.2 2.5 111 9 1 0 23.291 46.582 0.257 10.25 4 23.3 2.3 112 2 9 0 23.304 46.608 0.257 10.24 4 20.3 1.7 113 7 1 1 23.334 46.667 0.257 10.21 8 22.7 4.3 114 4 6 1 23.443 46.885 0.258 10.1 8 15.0 1.9 115 6 7 0 23.479 46.957 0.259 10.07 4 10.1 0.4 116 2 7 1 23.521 47.043 0.259 10.03 8 81.3 54.8 117 7 6 0 23.549 47.099 0.259 10.0 4 71.5 21.2 118 6 4 1 23.551 47.103 0.259 10.0 8 55.0 25.0 119 9 2 0 23.723 47.445 0.261 9.84 4 133.7 72.7 120 7 2 1 23.765 47.53 0.262 9.8 8 48.0 18.7 121 5 8 0 23.991 47.982 0.264 9.59 4 1.6 0.0 122 3 9 0 24.047 48.094 0.265 9.54 4 81.1 26.0 123 8 5 0 24.199 48.398 0.266 9.4 4 38.6 5.8 124 3 7 1 24.259 48.519 0.267 9.35 8 10.2 0.8 125 9 3 0 24.43 48.859 0.268 9.2 4 0.5 0.0 126 7 3 1 24.471 48.942 0.269 9.17 8 16.7 2.1 127 5 6 1 24.762 49.524 0.272 8.92 8 54.3 21.8 128 6 5 1 24.82 49.639 0.272 8.88 8 99.7 72.9 129 0 8 1 25.045 50.091 0.275 8.69 4 74.2 19.8 130 4 9 0 25.059 50.118 0.275 8.68 4 24.8 2.2 131 1 8 1 25.188 50.375 0.276 8.58 8 42.3 12.7 132 4 7 1 25.265 50.53 0.277 8.52 8 31.0 6.8 133 7 7 0 25.366 50.732 0.278 8.45 4 49.8 8.7 134 8 0 1 25.376 50.751 0.278 8.44 4 15.7 0.9 135 0 10 0 25.386 50.773 0.278 8.43 2 50.9 4.5 136 9 4 0 25.394 50.789 0.278 8.42 4 8.5 0.2 137 7 4 1 25.435 50.869 0.279 8.39 8 79.9 44.4 138 8 1 1 25.511 51.023 0.28 8.34 8 48.4 16.2 139 1 10 0 25.527 51.054 0.28 8.33 4 49.1 8.3 140 6 8 0 25.571 51.141 0.28 8.29 4 77.5 20.6 141 2 8 1 25.611 51.221 0.281 8.26 8 39.6 10.7 142 8 6 0 25.713 51.427 0.282 8.19 4 48.3 7.9 143 10 0 0 25.896 51.792 0.283 8.06 2 56.0 5.2 144 8 2 1 25.916 51.831 0.284 8.04 8 66.0 28.9 145 2 10 0 25.946 51.892 0.284 8.02 4 59.0 11.5 146 10 1 0 26.03 52.06 0.285 7.96 4 44.0 6.4 147 3 8 1 26.305 52.61 0.288 7.77 8 73.2 34.5 148 6 6 1 26.308 52.615 0.288 7.77 8 37.2 8.9 149 5 9 0 26.318 52.636 0.288 7.77 4 10.3 0.3 150 10 2 0 26.428 52.857 0.289 7.69 4 24.5 1.9 151 5 7 1 26.517 53.034 0.29 7.63 8 23.4 3.4 152 8 3 1 26.579 53.159 0.29 7.59 8 112.1 78.8 153 9 5 0 26.597 53.195 0.291 7.58 4 21.2 1.4 154 3 10 0 26.634 53.269 0.291 7.56 4 42.7 5.7 155 7 5 1 26.636 53.273 0.291 7.56 8 61.3 23.4 156 10 3 0 27.083 54.167 0.296 7.28 4 3.4 0.0 157 4 8 1 27.256 54.512 0.297 7.17 8 22.8 3.1 158 0 9 1 27.307 54.614 0.298 7.14 4 13.2 0.5 159 7 8 0 27.352 54.703 0.298 7.11 4 69.1 14.0 160 8 7 0 27.425 54.85 0.299 7.07 4 14.3 0.6 161 1 9 1 27.441 54.882 0.299 7.06 8 44.3 11.4 162 8 4 1 27.49 54.98 0.3 7.03 8 55.8 18.1 163 4 10 0 27.577 55.155 0.301 6.98 4 30.1 2.6 164 9 0 1 27.7 55.401 0.302 6.91 4 3.3 0.0 165 6 9 0 27.802 55.604 0.303 6.85 4 1.2 0.0 166 9 1 1 27.828 55.656 0.303 6.84 8 32.8 6.1 167 2 9 1 27.84 55.68 0.303 6.83 8 140.0 110.7 168 10 4 0 27.983 55.965 0.305 6.76 4 32.1 2.9 169 6 7 1 27.994 55.987 0.305 6.75 8 38.4 8.2 170 9 6 0 28.018 56.037 0.305 6.74 4 7.9 0.2 171 7 6 1 28.056 56.112 0.305 6.71 8 24.9 3.4 172 9 2 1 28.209 56.418 0.307 6.63 8 58.2 18.6 173 1 11 0 28.269 56.538 0.307 6.6 4 35.2 3.4 174 5 8 1 28.447 56.893 0.309 6.51 8 47.0 11.9 175 3 9 1 28.496 56.993 0.31 6.48 8 48.0 12.3 176 8 5 1 28.631 57.263 0.311 6.41 8 51.0 13.8 177 2 11 0 28.66 57.32 0.311 6.4 4 30.1 2.4 178 5 10 0 28.759 57.518 0.312 6.35 4 22.9 1.4 179 9 3 1 28.837 57.673 0.313 6.31 8 82.0 35.1 180 11 1 0 28.837 57.675 0.313 6.31 4 6.6 0.1 181 10 5 0 29.112 58.223 0.316 6.18 4 9.6 0.2 182 11 2 0 29.21 58.419 0.317 6.13 4 11.7 0.3 183 3 11 0 29.305 58.609 0.318 6.09 4 55.4 7.7 184 8 8 0 29.314 58.628 0.318 6.08 4 50.9 6.5 185 4 9 1 29.4 58.799 0.319 6.04 8 19.5 1.9 186 7 9 0 29.491 58.981 0.32 6.0 4 9.3 0.2 187 9 7 0 29.639 59.278 0.321 5.93 4 82.1 16.5 188 7 7 1 29.675 59.351 0.321 5.92 8 99.7 48.7 189 0 10 1 29.694 59.387 0.322 5.91 4 60.9 9.1 190 9 4 1 29.701 59.402 0.322 5.9 8 39.2 7.5 191 0 0 2 29.756 59.513 0.322 5.88 2 275.7 92.4 192 1 10 1 29.82 59.641 0.323 5.85 8 87.4 37.0 193 11 3 0 29.824 59.647 0.323 5.85 4 94.1 21.4 194 6 8 1 29.86 59.719 0.323 5.83 8 26.6 3.4 195 0 1 2 29.879 59.757 0.323 5.83 4 32.9 2.6 196 1 0 2 29.883 59.766 0.323 5.82 4 21.5 1.1 197 8 6 1 29.988 59.977 0.324 5.78 8 58.2 16.2 198 1 1 2 30.005 60.01 0.325 5.77 8 78.0 29.1 199 10 0 1 30.154 60.307 0.326 5.71 4 20.7 1.0 200 6 10 0 30.163 60.326 0.326 5.7 4 15.6 0.6 201 4 11 0 30.193 60.385 0.326 5.69 4 29.0 2.0 202 2 10 1 30.199 60.398 0.327 5.69 8 62.2 18.2 203 0 2 2 30.243 60.486 0.327 5.67 4 88.9 18.5 204 2 0 2 30.261 60.522 0.327 5.66 4 92.2 19.9 205 10 1 1 30.275 60.549 0.327 5.66 8 49.1 11.3 206 1 2 2 30.368 60.737 0.328 5.62 8 24.3 2.7 207 2 1 2 30.382 60.764 0.328 5.61 8 19.6 1.8 208 10 6 0 30.455 60.91 0.329 5.58 4 13.7 0.4 209 5 9 1 30.536 61.072 0.33 5.55 8 39.3 7.1 210 10 2 1 30.636 61.272 0.331 5.51 8 9.3 0.4 211 11 4 0 30.671 61.342 0.331 5.5 4 64.2 9.4 212 2 2 2 30.743 61.486 0.332 5.47 8 79.0 28.2 213 9 5 1 30.79 61.58 0.332 5.45 8 77.8 27.3 214 3 10 1 30.824 61.647 0.333 5.44 8 11.4 0.6 215 0 3 2 30.844 61.689 0.333 5.43 4 8.1 0.1 216 3 0 2 30.885 61.77 0.333 5.41 4 0.3 0.0 217 0 12 0 30.962 61.923 0.334 5.38 2 45.8 2.3 218 1 3 2 30.968 61.937 0.334 5.38 8 19.2 1.6 219 3 1 2 31.004 62.009 0.334 5.37 8 25.9 3.0 220 1 12 0 31.085 62.171 0.335 5.33 4 76.8 13.0 221 10 3 1 31.233 62.467 0.337 5.28 8 74.3 24.1 222 5 11 0 31.312 62.624 0.337 5.25 4 30.2 2.0 223 2 3 2 31.339 62.677 0.338 5.24 8 16.9 1.2 224 3 2 2 31.361 62.722 0.338 5.23 8 23.1 2.3 225 8 9 0 31.368 62.736 0.338 5.23 4 3.6 0.0 226 9 8 0 31.444 62.888 0.339 5.2 4 40.5 3.5 227 2 12 0 31.455 62.91 0.339 5.2 4 14.5 0.5 228 7 8 1 31.479 62.958 0.339 5.19 8 23.5 2.4 229 8 7 1 31.546 63.092 0.34 5.16 8 65.0 18.1 230 12 0 0 31.607 63.214 0.34 5.14 2 26.0 0.7 231 0 4 2 31.675 63.351 0.341 5.12 4 53.1 6.0 232 4 10 1 31.686 63.372 0.341 5.12 8 24.6 2.6 233 12 1 0 31.725 63.45 0.341 5.1 4 32.8 2.3 234 11 5 0 31.74 63.48 0.341 5.1 4 6.5 0.1 235 4 0 2 31.747 63.493 0.342 5.09 4 51.8 5.6 236 7 10 0 31.773 63.546 0.342 5.08 4 11.1 0.3 237 1 4 2 31.798 63.595 0.342 5.08 8 10.2 0.4 238 4 1 2 31.864 63.728 0.343 5.05 8 10.6 0.5 239 6 9 1 31.892 63.785 0.343 5.04 8 44.7 8.3 240 3 3 2 31.95 63.901 0.344 5.02 8 11.9 0.6 241 10 7 0 31.999 63.999 0.344 5.01 4 46.8 4.5 242 10 4 1 32.059 64.117 0.345 4.99 8 32.6 4.4 243 3 12 0 32.065 64.131 0.345 4.98 4 21.7 1.0 244 12 2 0 32.077 64.154 0.345 4.98 4 26.3 1.4 245 9 6 1 32.092 64.183 0.345 4.98 8 147.6 89.6 246 2 4 2 32.162 64.325 0.346 4.95 8 19.7 1.6 247 0 11 1 32.201 64.403 0.346 4.94 4 58.8 7.1 248 4 2 2 32.215 64.431 0.346 4.93 8 26.0 2.8 249 1 11 1 32.323 64.645 0.347 4.9 8 31.4 4.0 250 6 11 0 32.65 65.3 0.35 4.79 4 92.9 17.1 251 12 3 0 32.659 65.318 0.35 4.79 4 81.2 13.1 252 2 11 1 32.684 65.369 0.351 4.78 8 84.7 28.3 253 0 5 2 32.726 65.453 0.351 4.77 4 0.9 0.0 254 11 0 1 32.733 65.466 0.351 4.77 4 8.2 0.1 255 3 4 2 32.766 65.531 0.351 4.76 8 3.2 0.0 256 5 10 1 32.776 65.552 0.351 4.75 8 13.2 0.7 257 4 3 2 32.796 65.593 0.352 4.75 8 26.7 2.8 258 5 0 2 32.836 65.671 0.352 4.73 4 9.4 0.2 259 1 5 2 32.846 65.693 0.352 4.73 8 32.6 4.2 260 11 1 1 32.848 65.697 0.352 4.73 8 12.8 0.6 261 4 12 0 32.91 65.819 0.353 4.71 4 97.6 18.6 262 5 1 2 32.951 65.902 0.353 4.7 8 28.9 3.3 263 11 6 0 33.021 66.042 0.354 4.68 4 105.8 21.7 264 10 5 1 33.103 66.206 0.355 4.65 8 48.7 9.1 265 11 2 1 33.194 66.388 0.355 4.63 8 22.2 1.9 266 2 5 2 33.205 66.41 0.355 4.62 8 6.4 0.2 267 3 11 1 33.283 66.565 0.356 4.6 8 42.3 6.8 268 8 8 1 33.291 66.583 0.356 4.6 8 48.7 9.0 269 5 2 2 33.296 66.592 0.356 4.6 8 12.2 0.6 270 9 9 0 33.422 66.844 0.358 4.56 4 31.7 1.9 271 7 9 1 33.456 66.912 0.358 4.55 8 16.5 1.0 272 12 4 0 33.465 66.931 0.358 4.55 4 89.9 15.2 273 8 10 0 33.577 67.154 0.359 4.52 4 60.0 6.7 274 9 7 1 33.594 67.188 0.359 4.51 8 11.3 0.5 275 4 4 2 33.601 67.202 0.359 4.51 8 23.7 2.1 276 10 8 0 33.732 67.465 0.36 4.47 4 11.7 0.3 277 11 3 1 33.766 67.533 0.361 4.46 8 16.4 1.0 278 3 5 2 33.799 67.598 0.361 4.45 8 29.4 3.2 279 5 3 2 33.868 67.735 0.362 4.43 8 8.7 0.3 280 5 12 0 33.979 67.958 0.363 4.4 4 33.5 2.0 281 0 6 2 33.988 67.975 0.363 4.4 4 8.9 0.1 282 1 13 0 33.99 67.979 0.363 4.4 4 60.0 6.5 283 6 10 1 34.084 68.167 0.364 4.38 8 15.6 0.9 284 1 6 2 34.105 68.211 0.364 4.37 8 39.6 5.7 285 4 11 1 34.111 68.223 0.364 4.37 8 9.7 0.3 286 6 0 2 34.142 68.284 0.364 4.36 4 9.2 0.2 287 7 11 0 34.195 68.391 0.365 4.35 4 16.7 0.5 288 6 1 2 34.255 68.51 0.365 4.33 8 42.1 6.3 289 2 13 0 34.342 68.685 0.366 4.31 4 29.6 1.6 290 10 6 1 34.357 68.715 0.366 4.3 8 46.9 7.8 291 2 6 2 34.458 68.915 0.367 4.28 8 53.9 10.3 292 12 5 0 34.488 68.976 0.368 4.27 4 18.2 0.6 293 11 7 0 34.503 69.005 0.368 4.27 4 59.4 6.2 294 11 4 1 34.56 69.119 0.368 4.25 8 9.2 0.3 295 6 2 2 34.594 69.188 0.369 4.24 8 48.4 8.2 296 4 5 2 34.621 69.243 0.369 4.24 8 43.5 6.6 297 5 4 2 34.66 69.319 0.369 4.23 8 28.5 2.8 298 13 1 0 34.707 69.414 0.37 4.22 4 1.7 0.0 299 0 12 1 34.833 69.666 0.371 4.19 4 65.8 7.5 300 3 13 0 34.927 69.854 0.372 4.16 4 48.2 4.0 301 1 12 1 34.949 69.899 0.372 4.16 8 33.5 3.9 X-ray diffraction powder data (I)...X-Ray wave length = 1.54056 (angs.): No H K L Theta 2*Theta d I int I int.n. I p.h.n. H(Si) ( degree ) (angstrem) *100 *100 1 1 1 0 3.509 7.017 12.58629 546.5 100.0 100.0 5.5 2 0 2 0 4.919 9.838 8.9835 183.3 33.5 33.5 5.6 3 2 0 0 5.011 10.022 8.8185 111.8 20.5 20.4 5.6 4 1 2 0 5.522 11.044 8.00491 8.6 1.6 1.6 5.6 5 2 2 0 7.031 14.061 6.29315 145.6 26.6 26.5 5.6 6 1 3 0 7.807 15.613 5.67096 43.9 8.0 8.0 5.6 7 3 1 0 7.924 15.848 5.58749 13.8 2.5 2.5 5.6 8 2 3 0 8.944 17.888 4.95444 8.1 1.5 1.5 5.6 9 3 2 0 9.009 18.017 4.91925 27.4 5.0 5.0 5.6 10 0 4 0 9.874 19.749 4.49175 32.2 5.9 5.8 5.6 11 4 0 0 10.061 20.122 4.40925 23.3 4.3 4.2 5.6 12 3 3 0 10.58 21.159 4.19543 8.5 1.5 1.5 5.6 13 2 4 0 11.096 22.192 4.00245 21.2 3.9 3.8 5.6 14 4 2 0 11.222 22.443 3.95819 55.6 10.2 10.1 5.6 15 3 4 0 12.463 24.926 3.56922 9.6 1.7 1.7 5.6 16 5 1 0 12.858 25.716 3.46132 13.5 2.5 2.4 5.6 17 2 5 0 13.384 26.768 3.32773 22.9 4.2 4.1 5.6 18 4 4 0 14.17 28.34 3.14657 30.7 5.6 5.5 5.6 19 1 1 1 14.809 29.617 3.01371 25.6 4.7 4.6 5.6 20 0 6 0 14.906 29.812 2.9945 8.1 1.5 1.5 5.6 21 1 6 0 15.124 30.248 2.95225 5.8 1.1 1.0 5.6 22 0 2 1 15.222 30.443 2.93381 11.4 2.1 2.1 5.6 23 2 0 1 15.253 30.506 2.92792 12.1 2.2 2.2 5.6 24 6 1 0 15.398 30.797 2.90093 86.2 15.8 15.5 5.6 25 2 1 1 15.459 30.918 2.8898 16.7 3.1 3.0 5.6 26 2 6 0 15.763 31.526 2.83548 140.4 25.7 25.3 5.6 27 6 2 0 16.005 32.009 2.79374 66.2 12.1 11.9 5.6 28 2 2 1 16.063 32.127 2.78379 97.9 17.9 17.6 5.6 29 5 4 0 16.12 32.241 2.77421 16.6 3.0 3.0 5.6 30 3 0 1 16.297 32.595 2.7449 31.1 5.7 5.6 5.6 31 1 3 1 16.433 32.867 2.72282 6.1 1.1 1.1 5.6 32 3 6 0 16.779 33.558 2.6683 14.2 2.6 2.5 5.7 33 2 3 1 17.028 34.056 2.6304 45.0 8.2 8.1 5.7 34 3 2 1 17.063 34.127 2.62509 123.9 22.7 22.2 5.7 35 0 4 1 17.556 35.113 2.55359 63.1 11.5 11.3 5.7 36 4 0 1 17.667 35.334 2.53815 140.5 25.7 25.2 5.7 37 1 4 1 17.746 35.491 2.52724 75.7 13.9 13.6 5.7 38 5 5 0 17.818 35.637 2.51726 25.3 4.6 4.5 5.7 39 4 1 1 17.848 35.696 2.51319 74.8 13.7 13.4 5.7 40 3 3 1 17.98 35.961 2.4953 218.3 40.0 39.1 5.7 41 4 6 0 18.116 36.232 2.47722 7.7 1.4 1.4 5.7 42 2 4 1 18.303 36.605 2.45283 52.3 9.6 9.4 5.7 43 4 2 1 18.383 36.765 2.44253 10.2 1.9 1.8 5.7 44 3 7 0 19.115 38.229 2.3523 32.8 6.0 5.9 5.7 45 3 4 1 19.2 38.401 2.34219 8.2 1.5 1.5 5.7 46 1 5 1 19.318 38.637 2.32842 126.3 23.1 22.6 5.7 47 7 3 0 19.37 38.741 2.32242 23.0 4.2 4.1 5.7 48 5 1 1 19.471 38.941 2.3109 63.7 11.7 11.4 5.7 49 2 5 1 19.838 39.675 2.26984 34.9 6.4 6.2 5.7 50 5 2 1 19.968 39.936 2.2556 183.3 33.5 32.7 5.7 51 4 7 0 20.319 40.638 2.21824 135.2 24.7 24.1 5.7 52 4 4 1 20.401 40.801 2.20976 16.2 3.0 2.9 5.7 53 8 0 0 20.45 40.9 2.20462 28.9 5.3 5.2 5.7 54 8 1 0 20.611 41.221 2.18821 12.2 2.2 2.2 5.7 55 5 3 1 20.775 41.55 2.17166 22.4 4.1 4.0 5.7 56 0 6 1 20.942 41.884 2.1551 16.2 3.0 2.9 5.7 57 1 6 1 21.105 42.21 2.13919 36.6 6.7 6.5 5.7 58 3 8 0 21.54 43.08 2.098 38.9 7.1 6.9 5.7 59 6 2 1 21.774 43.548 2.07653 27.2 5.0 4.8 5.7 60 4 5 1 21.811 43.623 2.07314 6.9 1.3 1.2 5.7 61 3 6 1 22.376 44.752 2.02343 8.7 1.6 1.5 5.7 62 6 3 1 22.528 45.056 2.01047 8.4 1.5 1.5 5.7 63 4 8 0 22.638 45.276 2.00123 11.1 2.0 2.0 5.7 64 1 7 1 23.07 46.14 1.96572 12.3 2.2 2.2 5.7 65 2 7 1 23.521 47.043 1.93008 75.9 13.9 13.5 5.7 66 6 4 1 23.551 47.103 1.92776 25.0 4.6 4.4 5.7 67 9 2 0 23.723 47.445 1.91464 72.7 13.3 12.9 5.7 68 7 2 1 23.765 47.53 1.91143 18.7 3.4 3.3 5.7 69 3 9 0 24.047 48.094 1.89032 26.0 4.7 4.6 5.7 70 8 5 0 24.199 48.398 1.87915 5.8 1.1 1.0 5.7 71 5 6 1 24.762 49.524 1.83903 21.8 4.0 3.8 5.7 72 6 5 1 24.82 49.639 1.83504 72.9 13.3 12.9 5.7 73 0 8 1 25.045 50.091 1.81954 22.0 4.0 3.9 5.7 74 1 8 1 25.188 50.375 1.80994 12.7 2.3 2.2 5.8 75 4 7 1 25.265 50.53 1.80476 6.8 1.2 1.2 5.8 76 7 7 0 25.366 50.732 1.79804 14.3 2.6 2.5 5.8 77 7 4 1 25.435 50.869 1.79351 44.4 8.1 7.8 5.8 78 8 1 1 25.511 51.023 1.78847 24.5 4.5 4.3 5.8 79 6 8 0 25.571 51.141 1.78461 20.6 3.8 3.6 5.8 80 2 8 1 25.611 51.221 1.78201 10.7 2.0 1.9 5.8 81 8 6 0 25.713 51.427 1.77537 7.9 1.4 1.4 5.8 82 8 2 1 25.916 51.831 1.76247 34.2 6.3 6.0 5.8 83 2 10 0 25.946 51.892 1.76053 11.5 2.1 2.0 5.8 84 10 1 0 26.03 52.06 1.75526 6.4 1.2 1.1 5.8 85 3 8 1 26.305 52.61 1.7382 43.7 8.0 7.7 5.8 86 8 3 1 26.579 53.159 1.72154 80.2 14.7 14.1 5.8 87 7 5 1 26.636 53.273 1.71813 29.2 5.3 5.1 5.8 88 7 8 0 27.352 54.703 1.67652 14.0 2.6 2.5 5.8 89 1 9 1 27.441 54.882 1.67149 11.4 2.1 2.0 5.8 90 8 4 1 27.49 54.98 1.66875 18.1 3.3 3.2 5.8 91 2 9 1 27.84 55.68 1.64942 116.8 21.4 20.5 5.8 92 6 7 1 27.994 55.987 1.64108 11.1 2.0 2.0 5.8 93 9 2 1 28.209 56.418 1.62957 18.6 3.4 3.3 5.8 94 5 8 1 28.447 56.893 1.61708 11.9 2.2 2.1 5.8 95 3 9 1 28.496 56.993 1.61449 12.3 2.3 2.2 5.8 96 8 5 1 28.631 57.263 1.60752 16.2 3.0 2.8 5.8 97 9 3 1 28.837 57.673 1.59706 35.2 6.4 6.2 5.8 98 3 11 0 29.305 58.609 1.57375 14.2 2.6 2.5 5.8 99 9 7 0 29.639 59.278 1.55759 16.5 3.0 2.9 5.8 100 7 7 1 29.675 59.351 1.55586 65.2 11.9 11.4 5.8 101 0 0 2 29.756 59.513 1.552 92.4 16.9 16.1 5.8 102 1 10 1 29.82 59.641 1.54898 58.4 10.7 10.2 5.8 103 6 8 1 29.86 59.719 1.54713 7.1 1.3 1.2 5.8 104 1 1 2 30.005 60.01 1.54033 45.3 8.3 7.9 5.8 105 2 10 1 30.199 60.398 1.53136 20.2 3.7 3.5 5.8 106 2 0 2 30.261 60.522 1.52851 49.7 9.1 8.7 5.8 107 5 9 1 30.536 61.072 1.51606 7.1 1.3 1.2 5.8 108 11 4 0 30.671 61.342 1.51004 9.4 1.7 1.6 5.8 109 2 2 2 30.743 61.486 1.50685 28.2 5.2 4.9 5.8 110 9 5 1 30.79 61.58 1.50477 27.3 5.0 4.7 5.8 111 1 12 0 31.085 62.171 1.49188 13.0 2.4 2.3 5.8 112 10 3 1 31.233 62.467 1.48553 24.1 4.4 4.2 5.8 113 8 7 1 31.546 63.092 1.4723 18.1 3.3 3.1 5.9 114 0 4 2 31.675 63.351 1.4669 8.5 1.6 1.5 5.9 115 4 0 2 31.747 63.493 1.46396 8.0 1.5 1.4 5.9 116 6 9 1 31.892 63.785 1.45797 8.3 1.5 1.4 5.9 117 10 4 1 32.059 64.117 1.45121 6.8 1.2 1.2 5.9 118 9 6 1 32.092 64.183 1.44987 89.6 16.4 15.5 5.9 119 0 11 1 32.201 64.403 1.44545 9.8 1.8 1.7 5.9 120 6 11 0 32.65 65.3 1.42775 30.2 5.5 5.2 5.9 121 2 11 1 32.684 65.369 1.42642 28.3 5.2 4.9 5.9 122 4 12 0 32.91 65.819 1.41774 18.6 3.4 3.2 5.9 123 11 6 0 33.021 66.042 1.4135 21.7 4.0 3.7 5.9 124 10 5 1 33.103 66.206 1.41039 9.1 1.7 1.6 5.9 125 8 8 1 33.291 66.583 1.40332 16.4 3.0 2.8 5.9 126 12 4 0 33.465 66.931 1.39687 16.2 3.0 2.8 5.9 127 8 10 0 33.577 67.154 1.39276 9.3 1.7 1.6 5.9 128 1 13 0 33.99 67.979 1.37785 8.7 1.6 1.5 5.9 129 1 6 2 34.105 68.211 1.37374 6.0 1.1 1.0 5.9 130 6 1 2 34.255 68.51 1.36846 6.3 1.2 1.1 5.9 131 10 6 1 34.357 68.715 1.36489 9.4 1.7 1.6 5.9 132 2 6 2 34.458 68.915 1.36141 10.3 1.9 1.8 5.9 133 11 7 0 34.503 69.005 1.35985 6.2 1.1 1.1 5.9 134 6 2 2 34.594 69.188 1.35671 14.8 2.7 2.5 5.9 135 0 12 1 34.833 69.666 1.34856 7.5 1.4 1.3 5.9 136 3 13 0 34.927 69.854 1.3454 7.8 1.4 1.3 5.9 Reference: Chichagov A.V. et al. Information-Calculating System on Crystal Structure Data of Minerals (MINCRYST) - Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian) |