Institute of Experimental Mineralogy Russian Academy of Sciences ------------------------------------------------- 142432, Chernogolovka, Moscow district A.V. Chichagov +7(496)52-22320 *** *** W W W - X R A Y P O L *** *********************** JERRYGIBBSITE 1 [Mn(7.86)Zn(0.59)Mg(0.24)Ca(0.16)Fe(0.14)][SiO(4)](4)(OH)(2) Orthorhombic P bn2(1) Z = 4 R =0.088 19 .4 .1995 Ref.Str.: Toshio Kato et al. (1989) * Neues Jb. Miner., Mh., H.9, 410-430 Reserv: Pos. Mn(1-9) = Mn+Zn+Mg+Ca+Fe. N.A.D. Initial data from BDM-file Lattice parameters (cub. angs.,degr.): a = 4.875 alpha = 90.0 b = 10.709 beta = 90.0 c = 28.18 gamma = 90.0 Unit cell volume (cub. angs.) = 1471.18 Molar volume ( cub.cm/mol.) = 221.54 Co-ordinates, thermal parameters, occupation for atomic positions: NoP x/a y/b z/c B(j) atom / occupation 1 0.998 0.3804 0.25 0.63 Mn = 1.00 2 0.997 0.3725 0.137 0.69 Mn = 1.00 3 0.9961 0.3658 0.3619 0.62 Mn = 1.00 4 0.0157 0.0976 0.0817 0.86 Mn = 1.00 5 0.0013 0.6494 0.4087 0.84 Mn = 1.00 6 0.9987 0.6567 0.1927 0.64 Mn = 1.00 7 0.0091 0.091 0.301 0.81 Mn = 1.00 8 0.9813 0.3722 0.0202 0.92 Mn = 1.00 9 0.9937 0.3578 0.4782 0.76 Mn = 1.00 10 0.0748 0.9681 0.1942 0.66 Si = 1.00 11 0.9353 0.7812 0.3016 0.73 Si = 1.00 12 0.0847 0.9618 0.4171 0.94 Si = 1.00 13 0.9205 0.7773 0.0806 0.84 Si = 1.00 14 0.7435 0.9673 0.1949 1.14 O = 1.00 15 0.263 0.7724 0.3026 1.45 O = 1.00 16 0.2082 0.8216 0.1974 0.29 O = 1.00 17 0.7951 0.9177 0.303 0.95 O = 1.00 18 0.228 0.0414 0.1434 2.13 O = 1.00 19 0.786 0.7031 0.3494 0.95 O = 1.00 20 0.2202 0.0371 0.2338 0.63 O = 1.00 21 0.7816 0.7189 0.2529 1.75 O = 1.00 22 0.2656 0.8039 0.0814 2.28 O = 1.00 23 0.7685 0.9718 0.4207 0.89 O = 1.00 24 0.7728 0.9228 0.0788 0.83 O = 1.00 25 0.2412 0.8098 0.4199 1.55 O = 1.00 26 0.7835 0.7097 0.1274 1.29 O = 1.00 27 0.2256 0.0367 0.3682 2.26 O = 1.00 28 0.7949 0.7225 0.0379 0.84 O = 1.00 29 0.2288 0.0308 0.4674 1.03 O = 1.00 30 0.7705 0.973 0.5189 2.03 OH = 1.00 31 0.7615 0.2255 0.4704 2.77 OH = 1.00 Co-ordinates for all atomic positions : No NoP x/a y/b z/c 1 1 0.998 0.3804 0.25 2 2 0.997 0.3725 0.137 3 3 0.9961 0.3658 0.3619 4 4 0.0157 0.0976 0.0817 5 5 0.0013 0.6494 0.4087 6 6 0.9987 0.6567 0.1927 7 7 0.0091 0.091 0.301 8 8 0.9813 0.3722 0.0202 9 9 0.9937 0.3578 0.4782 10 10 0.0748 0.9681 0.1942 11 11 0.9353 0.7812 0.3016 12 12 0.0847 0.9618 0.4171 13 13 0.9205 0.7773 0.0806 14 14 0.7435 0.9673 0.1949 15 15 0.263 0.7724 0.3026 16 16 0.2082 0.8216 0.1974 17 17 0.7951 0.9177 0.303 18 18 0.228 0.0414 0.1434 19 19 0.786 0.7031 0.3494 20 20 0.2202 0.0371 0.2338 21 21 0.7816 0.7189 0.2529 22 22 0.2656 0.8039 0.0814 23 23 0.7685 0.9718 0.4207 24 24 0.7728 0.9228 0.0788 25 25 0.2412 0.8098 0.4199 26 26 0.7835 0.7097 0.1274 27 27 0.2256 0.0367 0.3682 28 28 0.7949 0.7225 0.0379 29 29 0.2288 0.0308 0.4674 30 30 0.7705 0.973 0.5189 31 31 0.7615 0.2255 0.4704 32 1 0.002 0.6196 0.75 33 2 0.003 0.6275 0.637 34 3 0.0039 0.6342 0.8619 35 4 0.9843 0.9024 0.5817 36 5 0.9987 0.3506 0.9087 37 6 0.0013 0.3433 0.6927 38 7 0.9909 0.909 0.801 39 8 0.0187 0.6278 0.5202 40 9 0.0063 0.6422 0.9782 41 10 0.9252 0.0319 0.6942 42 11 0.0647 0.2188 0.8016 43 12 0.9153 0.0382 0.9171 44 13 0.0795 0.2227 0.5806 45 14 0.2565 0.0327 0.6949 46 15 0.737 0.2276 0.8026 47 16 0.7918 0.1784 0.6974 48 17 0.2049 0.0823 0.803 49 18 0.772 0.9586 0.6434 50 19 0.214 0.2969 0.8494 51 20 0.7798 0.9629 0.7338 52 21 0.2184 0.2811 0.7529 53 22 0.7344 0.1961 0.5814 54 23 0.2315 0.0282 0.9207 55 24 0.2272 0.0772 0.5788 56 25 0.7588 0.1902 0.9199 57 26 0.2165 0.2903 0.6274 58 27 0.7744 0.9633 0.8682 59 28 0.2051 0.2775 0.5379 60 29 0.7712 0.9692 0.9674 61 30 0.2295 0.027 0.0189 62 31 0.2385 0.7745 0.9704 63 1 0.502 0.8804 0.25 64 2 0.503 0.8725 0.137 65 3 0.5039 0.8658 0.3619 66 4 0.4843 0.5976 0.0817 67 5 0.4987 0.1494 0.4087 68 6 0.5013 0.1567 0.1927 69 7 0.4909 0.591 0.301 70 8 0.5187 0.8722 0.0202 71 9 0.5063 0.8578 0.4782 72 10 0.4252 0.4681 0.1942 73 11 0.5647 0.2812 0.3016 74 12 0.4153 0.4618 0.4171 75 13 0.5795 0.2773 0.0806 76 14 0.7565 0.4673 0.1949 77 15 0.237 0.2724 0.3026 78 16 0.2918 0.3216 0.1974 79 17 0.7049 0.4177 0.303 80 18 0.272 0.5414 0.1434 81 19 0.714 0.2031 0.3494 82 20 0.2798 0.5371 0.2338 83 21 0.7184 0.2189 0.2529 84 22 0.2344 0.3039 0.0814 85 23 0.7315 0.4718 0.4207 86 24 0.7272 0.4228 0.0788 87 25 0.2588 0.3098 0.4199 88 26 0.7165 0.2097 0.1274 89 27 0.2744 0.5367 0.3682 90 28 0.7051 0.2225 0.0379 91 29 0.2712 0.5308 0.4674 92 30 0.7295 0.473 0.5189 93 31 0.7385 0.7255 0.4704 94 1 0.498 0.1196 0.75 95 2 0.497 0.1275 0.637 96 3 0.4961 0.1342 0.8619 97 4 0.5157 0.4024 0.5817 98 5 0.5013 0.8506 0.9087 99 6 0.4987 0.8433 0.6927 100 7 0.5091 0.409 0.801 101 8 0.4813 0.1278 0.5202 102 9 0.4937 0.1422 0.9782 103 10 0.5748 0.5319 0.6942 104 11 0.4353 0.7188 0.8016 105 12 0.5847 0.5382 0.9171 106 13 0.4205 0.7227 0.5806 107 14 0.2435 0.5327 0.6949 108 15 0.763 0.7276 0.8026 109 16 0.7082 0.6784 0.6974 110 17 0.2951 0.5823 0.803 111 18 0.728 0.4586 0.6434 112 19 0.286 0.7969 0.8494 113 20 0.7202 0.4629 0.7338 114 21 0.2816 0.7811 0.7529 115 22 0.7656 0.6961 0.5814 116 23 0.2685 0.5282 0.9207 117 24 0.2728 0.5772 0.5788 118 25 0.7412 0.6902 0.9199 119 26 0.2835 0.7903 0.6274 120 27 0.7256 0.4633 0.8682 121 28 0.2949 0.7775 0.5379 122 29 0.7288 0.4692 0.9674 123 30 0.2705 0.527 0.0189 124 31 0.2615 0.2745 0.9704 X-ray density (g/cm cub.) = 4.05 MU (1/cm) = 681.789 Mass attenuation coefficient (cm**2/g) = 168.445 Selected interatomic distances (cation-anion,anion-anion): NoP Atom Rad.sph. C.N. Distance NoP N. (angs.) (angs.) 1 Mn 2.772 6 2.1594 14 2.2119 15 2.1552 16 2.1052 17 2.2162 20 2.2036 21 2 Mn 2.772 6 2.2511 14 2.2934 16 2.2586 18 2.0818 22 2.1702 24 2.2322 26 3 Mn 2.772 6 2.2742 15 2.2537 17 2.2475 19 2.3871 23 2.1613 25 2.2851 27 4 Mn 2.772 6 2.111 18 2.2165 24 2.1886 30 2.4531 22 2.2863 26 2.3675 28 5 Mn 2.772 6 2.0554 19 2.1019 25 2.337 23 2.1288 27 2.4659 29 2.3084 31 6 Mn 2.772 6 2.0443 16 2.1075 21 2.1929 26 2.3477 14 2.2869 18 2.2045 20 7 Mn 2.772 6 2.1297 17 2.2312 20 2.2446 27 2.2383 15 2.3175 19 2.392 21 8 Mn 2.772 6 2.2431 22 2.1343 24 2.1522 28 2.1927 29 2.1765 30 2.2204 31 9 Mn 2.772 6 1.8267 31 2.1522 28 2.3979 23 2.1526 25 2.3141 29 2.1204 30 10 Si 2.148 4 1.6152 14 1.7007 16 1.7953 18 1.5145 20 11 Si 2.148 4 1.6006 15 1.6142 17 1.7446 19 1.7 21 12 Si 2.148 4 1.5485 23 1.7994 25 1.7361 27 1.746 29 13 Si 2.148 4 1.7065 22 1.7172 24 1.646 26 1.4721 28 14 O 3.312 11 2.7517 16 3.0413 16 3.1024 17 2.8835 18 3.0085 18 2.676 20 2.8755 20 3.1276 21 3.3093 24 3.1537 21 3.2209 26 15 O 3.312 9 3.0228 16 3.0249 17 2.7612 17 2.9649 19 2.7744 19 2.9464 21 2.7924 21 3.1804 20 3.1291 27 16 O 3.312 9 3.0413 14 2.7517 14 3.0228 15 2.8046 18 2.5262 20 2.825 21 3.2863 22 3.1006 26 3.2336 20 17 O 3.312 7 3.1024 14 2.7612 15 3.0249 15 2.6445 19 3.1197 20 2.5554 21 3.0666 27 18 O 3.312 9 3.0085 14 2.8835 14 2.8046 16 2.5482 20 3.0911 22 3.1387 24 3.31 22 3.0204 26 3.1096 26 19 O 3.312 8 2.7744 15 2.9649 15 2.6445 17 2.7247 21 3.1901 25 3.2005 23 3.0208 27 3.1107 27 20 O 3.312 9 2.8755 14 2.676 14 2.5262 16 3.1197 17 2.5482 18 3.1804 15 3.2336 16 3.1589 21 3.1724 21 21 O 3.312 9 3.1276 14 2.7924 15 2.9464 15 2.825 16 2.5554 17 2.7247 19 3.1537 14 3.1589 20 3.1724 20 22 O 3.312 11 3.2863 16 3.0911 18 2.7822 24 2.72 24 3.012 26 2.8673 26 2.9868 28 2.7437 28 2.9734 30 3.1466 31 3.31 18 23 O 3.312 10 2.8845 25 3.1013 25 2.7636 27 3.1107 27 2.677 29 3.0089 29 2.7673 30 3.0568 31 3.2005 19 2.99 31 24 O 3.312 8 3.3093 14 3.1387 18 2.72 22 2.7822 22 2.662 26 2.4374 28 3.1783 29 3.0086 30 25 O 3.312 9 3.1901 19 3.1013 23 2.8845 23 2.8342 27 2.7197 29 3.2714 27 3.2772 29 2.9526 31 2.9742 31 26 O 3.312 8 3.1006 16 2.8673 22 3.012 22 2.662 24 2.5264 28 3.2209 14 3.0204 18 3.1096 18 27 O 3.312 9 3.0666 17 3.1107 23 2.7636 23 2.8342 25 2.7962 29 3.1292 15 3.0208 19 3.1107 19 3.2714 25 28 O 3.312 7 2.7437 22 2.9868 22 2.4374 24 2.5264 26 3.3076 29 2.9334 31 3.1695 30 29 O 3.312 10 3.0089 23 2.677 23 2.7197 25 2.7962 27 3.0762 30 2.7351 30 3.0894 31 3.1783 24 3.3076 28 3.2772 25 30 OH 3.36 10 2.7673 23 2.7351 29 3.0762 29 3.0301 31 2.9734 22 3.0086 24 3.3331 24 2.9862 31 3.3474 28 3.1695 28 31 OH 3.36 11 3.0568 23 3.0894 29 3.3314 29 3.0301 30 3.1466 22 2.9334 28 3.3594 28 2.99 23 2.9526 25 2.9742 25 2.9862 30 X-ray diffraction powder data (II), X-Ray W.L. = 1.54056(angs.): No H K L Theta 2*Theta S LPG MF F I int. ( degree ) *100 1 0 0 2 3.134 6.268 0.035 666.21 2 28.2 49.0 2 0 0 4 6.277 12.554 0.071 164.33 2 5.1 0.4 3 0 2 0 8.271 16.542 0.093 93.7 2 31.0 8.3 4 0 2 1 8.42 16.84 0.095 90.33 4 85.4 121.7 5 0 2 2 8.853 17.705 0.1 81.51 4 17.6 4.7 6 1 0 1 9.227 18.455 0.104 74.85 4 31.3 13.6 7 0 0 6 9.439 18.879 0.106 71.43 2 51.4 17.4 8 0 2 3 9.531 19.063 0.107 70.02 4 18.7 4.5 9 1 1 0 9.998 19.995 0.113 63.44 4 121.8 174.0 10 1 1 1 10.122 20.244 0.114 61.84 8 49.1 55.0 11 1 0 3 10.254 20.509 0.116 60.2 4 49.5 27.2 12 0 2 4 10.41 20.82 0.117 58.35 4 115.7 144.4 13 1 1 2 10.487 20.974 0.118 57.46 8 53.4 60.7 14 1 1 3 11.07 22.139 0.125 51.36 8 57.4 62.6 15 0 2 5 11.445 22.89 0.129 47.91 4 35.0 10.9 16 1 1 4 11.839 23.679 0.133 44.63 8 150.6 374.0 17 1 0 5 12.059 24.117 0.136 42.95 4 112.4 100.3 18 1 2 0 12.338 24.677 0.139 40.93 4 27.7 5.8 19 1 2 1 12.44 24.881 0.14 40.23 8 77.8 90.0 20 0 2 6 12.601 25.202 0.142 39.16 4 48.5 17.0 21 0 0 8 12.631 25.262 0.142 38.96 2 78.2 22.0 22 1 2 2 12.742 25.485 0.143 38.25 8 12.0 2.0 23 1 1 5 12.765 25.53 0.143 38.1 8 164.6 381.7 24 1 2 3 13.231 26.462 0.149 35.33 8 35.9 16.9 25 1 1 6 13.817 27.634 0.155 32.23 8 134.4 215.2 26 0 2 7 13.85 27.701 0.155 32.06 4 19.4 2.2 27 1 2 4 13.888 27.777 0.156 31.88 8 58.6 40.5 28 1 0 7 14.368 28.736 0.161 29.65 4 22.0 2.7 29 1 2 5 14.694 29.388 0.165 28.27 8 21.4 4.8 30 1 1 7 14.973 29.946 0.168 27.15 8 9.1 0.8 31 0 2 8 15.174 30.348 0.17 26.39 4 32.3 5.1 32 1 3 0 15.513 31.025 0.174 25.16 4 448.0 933.3 33 1 3 1 15.595 31.191 0.175 24.88 8 269.5 668.0 34 1 2 6 15.627 31.253 0.175 24.77 8 24.3 5.4 35 1 3 2 15.842 31.683 0.177 24.05 8 52.8 24.8 36 0 0 10 15.863 31.727 0.177 23.98 2 211.4 99.0 37 1 1 8 16.213 32.426 0.181 22.88 8 292.4 722.8 38 1 3 3 16.245 32.489 0.182 22.78 8 127.7 137.3 39 0 2 9 16.558 33.116 0.185 21.86 4 376.0 571.0 40 1 2 7 16.668 33.337 0.186 21.54 8 20.5 3.3 41 0 4 0 16.721 33.442 0.187 21.4 2 292.0 168.6 42 1 3 4 16.794 33.588 0.188 21.19 8 231.3 419.1 43 0 4 1 16.799 33.597 0.188 21.18 4 34.6 4.7 44 1 0 9 17.001 34.001 0.19 20.64 4 33.0 4.1 45 0 4 2 17.029 34.059 0.19 20.56 4 12.6 0.6 46 0 4 3 17.408 34.816 0.194 19.6 4 97.4 34.3 47 1 3 5 17.478 34.957 0.195 19.43 8 241.5 418.8 48 1 1 9 17.524 35.047 0.195 19.32 8 369.4 974.5 49 1 2 8 17.803 35.606 0.198 18.66 8 6.0 0.3 50 0 4 4 17.926 35.852 0.2 18.38 4 22.7 1.8 51 0 2 10 17.992 35.984 0.201 18.24 4 45.9 7.1 52 1 3 6 18.284 36.568 0.204 17.6 8 139.5 126.6 53 2 0 0 18.422 36.844 0.205 17.31 2 366.7 215.1 54 0 4 5 18.574 37.147 0.207 17.0 4 245.4 189.2 55 2 0 2 18.706 37.411 0.208 16.74 4 25.6 2.0 56 1 1 10 18.894 37.788 0.21 16.38 8 173.8 182.8 57 2 1 0 18.911 37.821 0.21 16.34 4 78.3 18.5 58 2 1 1 18.98 37.961 0.211 16.21 8 69.2 28.7 59 1 2 9 19.017 38.035 0.212 16.14 8 216.3 279.1 60 0 0 12 19.148 38.296 0.213 15.9 2 47.5 3.3 61 1 4 0 19.162 38.325 0.213 15.87 4 241.7 171.4 62 2 1 2 19.188 38.377 0.213 15.83 8 25.6 3.8 63 1 3 7 19.199 38.398 0.213 15.81 8 12.4 0.9 64 1 4 1 19.231 38.462 0.214 15.75 8 7.8 0.4 65 0 4 6 19.34 38.68 0.215 15.55 4 40.5 4.7 66 1 4 2 19.437 38.874 0.216 15.38 8 16.4 1.5 67 0 2 11 19.47 38.941 0.216 15.32 4 9.3 0.2 68 2 1 3 19.53 39.061 0.217 15.22 8 39.1 8.6 69 2 0 4 19.536 39.071 0.217 15.21 4 18.6 1.0 70 1 4 3 19.775 39.551 0.22 14.8 8 25.2 3.5 71 1 0 11 19.856 39.713 0.22 14.67 4 18.0 0.9 72 2 1 4 20.001 40.003 0.222 14.43 8 112.6 67.6 73 1 3 8 20.21 40.421 0.224 14.1 8 141.4 104.2 74 0 4 7 20.214 40.428 0.224 14.1 4 40.2 4.2 75 1 4 4 20.241 40.483 0.225 14.06 8 9.6 0.5 76 1 2 10 20.301 40.602 0.225 13.96 8 26.2 3.6 77 1 1 11 20.316 40.632 0.225 13.94 8 34.5 6.1 78 2 2 0 20.317 40.634 0.225 13.94 4 26.6 1.8 79 2 2 1 20.383 40.765 0.226 13.84 8 19.2 1.9 80 2 2 2 20.579 41.157 0.228 13.55 8 25.0 3.1 81 2 1 5 20.593 41.187 0.228 13.53 8 80.1 32.1 82 1 4 5 20.828 41.656 0.231 13.19 8 22.1 2.4 83 2 0 6 20.857 41.714 0.231 13.15 4 17.9 0.8 84 2 2 3 20.902 41.804 0.232 13.08 8 12.5 0.8 85 0 2 12 20.988 41.976 0.232 12.96 4 26.2 1.6 86 0 4 8 21.185 42.37 0.235 12.69 4 161.6 61.3 87 2 1 6 21.299 42.597 0.236 12.54 8 53.1 13.1 88 1 3 9 21.308 42.617 0.236 12.53 8 119.3 66.0 89 2 2 4 21.347 42.695 0.236 12.48 8 68.0 21.3 90 1 4 6 21.527 43.054 0.238 12.25 8 6.8 0.2 91 1 2 11 21.646 43.292 0.239 12.1 8 19.4 1.7 92 1 1 12 21.785 43.57 0.241 11.92 8 44.6 8.8 93 2 2 5 21.91 43.819 0.242 11.77 8 27.4 3.3 94 2 1 7 22.109 44.217 0.244 11.53 8 16.5 1.2 95 0 4 9 22.244 44.488 0.246 11.38 4 36.9 2.9 96 1 4 7 22.33 44.66 0.247 11.28 8 24.4 2.5 97 1 3 10 22.484 44.967 0.248 11.1 8 34.5 4.9 98 2 3 0 22.498 44.997 0.248 11.09 4 72.1 10.7 99 0 0 14 22.5 45.0 0.248 11.09 2 109.1 12.2 100 0 2 13 22.542 45.084 0.249 11.04 4 28.3 1.6 101 2 3 1 22.559 45.118 0.249 11.02 8 37.6 5.8 102 2 2 6 22.582 45.163 0.249 11.0 8 51.1 10.6 103 2 0 8 22.6 45.2 0.249 10.98 4 61.7 7.7 104 2 3 2 22.74 45.479 0.251 10.82 8 8.3 0.3 105 1 0 13 22.886 45.771 0.252 10.67 4 35.6 2.5 106 2 1 8 23.015 46.029 0.254 10.53 8 39.3 6.0 107 2 3 3 23.038 46.077 0.254 10.51 8 16.7 1.1 108 1 2 12 23.046 46.093 0.254 10.5 8 43.2 7.2 109 1 5 0 23.13 46.26 0.255 10.42 4 110.1 23.3 110 1 5 1 23.189 46.379 0.256 10.36 8 80.9 25.1 111 1 4 8 23.229 46.459 0.256 10.31 8 29.8 3.4 112 1 1 13 23.296 46.593 0.257 10.25 8 112.6 48.0 113 2 2 7 23.356 46.712 0.257 10.19 8 14.7 0.8 114 1 5 2 23.366 46.732 0.257 10.18 8 8.0 0.2 115 0 4 10 23.382 46.764 0.258 10.16 4 37.9 2.7 116 2 3 4 23.451 46.903 0.258 10.1 8 5.1 0.1 117 1 5 3 23.659 47.317 0.26 9.9 8 65.9 15.9 118 1 3 11 23.729 47.458 0.261 9.83 8 53.6 10.4 119 2 3 5 23.975 47.949 0.264 9.6 8 12.9 0.6 120 2 1 9 24.009 48.019 0.264 9.57 8 14.4 0.7 121 1 5 4 24.064 48.128 0.265 9.52 8 98.8 34.3 122 0 2 14 24.131 48.262 0.265 9.46 4 54.9 5.3 123 1 4 9 24.217 48.435 0.266 9.39 8 17.3 1.0 124 2 2 8 24.226 48.452 0.266 9.38 8 23.6 1.9 125 1 2 13 24.497 48.994 0.269 9.14 8 29.6 3.0 126 1 5 5 24.577 49.154 0.27 9.08 8 100.1 33.6 127 0 4 11 24.592 49.184 0.27 9.06 4 60.4 6.1 128 2 3 6 24.603 49.205 0.27 9.05 8 19.8 1.3 129 2 0 10 24.698 49.395 0.271 8.98 4 142.1 33.5 130 1 1 14 24.848 49.697 0.273 8.85 8 141.4 65.4 131 1 3 12 25.038 50.077 0.275 8.7 8 61.5 12.2 132 2 1 10 25.086 50.171 0.275 8.66 8 30.0 2.9 133 2 2 9 25.184 50.369 0.276 8.59 8 607.2 1169.9 134 1 5 6 25.194 50.388 0.276 8.58 8 56.2 10.0 135 1 4 10 25.287 50.574 0.277 8.51 8 22.4 1.6 136 2 4 0 25.301 50.601 0.277 8.5 4 536.3 451.5 137 2 3 7 25.33 50.66 0.278 8.47 8 3.1 0.0 138 2 4 1 25.356 50.712 0.278 8.45 8 22.5 1.6 139 2 4 2 25.521 51.043 0.28 8.33 8 36.4 4.1 140 0 6 0 25.567 51.134 0.28 8.3 2 40.6 1.3 141 0 6 1 25.622 51.244 0.281 8.25 4 44.7 3.0 142 0 2 15 25.755 51.509 0.282 8.16 4 75.7 8.6 143 0 6 2 25.786 51.573 0.282 8.14 4 63.8 6.1 144 2 4 3 25.796 51.591 0.282 8.13 8 105.2 33.3 145 0 4 12 25.869 51.738 0.283 8.08 4 40.2 2.4 146 1 5 7 25.909 51.818 0.284 8.05 8 28.6 2.4 147 0 0 16 25.935 51.87 0.284 8.03 2 54.8 2.2 148 1 2 14 25.995 51.991 0.285 7.99 8 87.5 22.6 149 0 6 3 26.059 52.117 0.285 7.94 4 31.2 1.4 150 1 0 15 26.066 52.132 0.285 7.94 4 29.4 1.3 151 2 3 8 26.151 52.301 0.286 7.88 8 30.4 2.7 152 2 4 4 26.176 52.352 0.286 7.86 8 41.2 4.9 153 2 2 10 26.225 52.45 0.287 7.83 8 25.4 1.9 154 2 1 11 26.237 52.475 0.287 7.82 8 20.7 1.2 155 1 3 13 26.407 52.814 0.289 7.71 8 184.5 96.9 156 1 4 11 26.432 52.865 0.289 7.69 8 28.2 2.3 157 0 6 4 26.436 52.873 0.289 7.69 4 312.3 138.5 158 1 1 15 26.44 52.879 0.289 7.69 8 107.4 32.8 159 2 4 5 26.66 53.319 0.291 7.54 8 240.5 161.2 160 1 5 8 26.717 53.434 0.292 7.5 8 169.6 79.8 161 0 6 5 26.917 53.833 0.294 7.38 4 42.5 2.5 162 2 3 9 27.059 54.119 0.295 7.29 8 72.2 14.0 163 2 0 12 27.095 54.191 0.296 7.27 4 50.3 3.4 164 0 4 13 27.208 54.416 0.297 7.2 4 260.8 90.5 165 2 4 6 27.242 54.485 0.297 7.18 8 37.7 3.8 166 2 2 11 27.343 54.685 0.298 7.12 8 13.3 0.5 167 1 6 0 27.36 54.721 0.298 7.11 4 27.0 1.0 168 1 6 1 27.413 54.825 0.299 7.08 8 51.1 6.8 169 0 2 16 27.413 54.826 0.299 7.08 4 17.6 0.4 170 2 1 12 27.459 54.918 0.299 7.05 8 38.0 3.8 171 0 6 6 27.496 54.991 0.3 7.03 4 178.2 41.3 172 1 2 15 27.539 55.078 0.3 7.0 8 12.2 0.4 173 1 6 2 27.57 55.139 0.3 6.99 8 9.5 0.2 174 1 5 9 27.613 55.226 0.301 6.96 8 259.9 173.8 175 1 4 12 27.648 55.297 0.301 6.94 8 15.1 0.6 176 1 6 3 27.83 55.659 0.303 6.84 8 23.9 1.4 177 1 3 14 27.832 55.663 0.303 6.84 8 196.2 97.3 178 2 4 7 27.92 55.841 0.304 6.79 8 40.4 4.1 179 2 3 10 28.051 56.102 0.305 6.72 8 26.4 1.7 180 1 1 16 28.07 56.139 0.305 6.71 8 23.7 1.4 181 0 6 7 28.17 56.339 0.306 6.65 4 4.1 0.0 182 1 6 4 28.191 56.382 0.307 6.64 8 11.2 0.3 183 3 0 1 28.347 56.693 0.308 6.56 4 34.0 1.4 184 2 2 12 28.532 57.064 0.31 6.46 8 19.0 0.9 185 1 5 10 28.592 57.183 0.311 6.43 8 126.9 38.3 186 2 5 0 28.604 57.208 0.311 6.43 4 46.9 2.6 187 0 4 14 28.605 57.21 0.311 6.43 4 22.8 0.6 188 3 1 0 28.649 57.298 0.311 6.4 4 199.3 47.0 189 1 6 5 28.651 57.302 0.311 6.4 8 42.2 4.2 190 2 5 1 28.655 57.31 0.311 6.4 8 21.6 1.1 191 2 4 8 28.69 57.379 0.312 6.38 8 156.4 57.7 192 3 1 1 28.7 57.4 0.312 6.38 8 113.9 30.6 193 2 1 13 28.747 57.494 0.312 6.35 8 51.7 6.3 194 3 0 3 28.755 57.509 0.312 6.35 4 56.3 3.7 195 2 5 2 28.807 57.615 0.313 6.32 8 18.1 0.8 196 3 1 2 28.852 57.704 0.313 6.3 8 34.2 2.7 197 1 4 13 28.931 57.861 0.314 6.26 8 43.1 4.3 198 0 6 8 28.934 57.869 0.314 6.26 4 54.0 3.4 199 2 5 3 29.06 58.12 0.315 6.2 8 37.9 3.3 200 3 1 3 29.105 58.209 0.316 6.18 8 64.8 9.6 201 0 2 17 29.107 58.214 0.316 6.18 4 212.7 51.7 202 2 3 11 29.121 58.242 0.316 6.17 8 0.2 0.0 203 1 2 16 29.128 58.256 0.316 6.17 8 10.5 0.2 204 1 6 6 29.207 58.415 0.317 6.13 8 8.3 0.2 205 1 3 15 29.31 58.62 0.318 6.08 8 122.5 33.7 206 1 0 17 29.394 58.788 0.319 6.04 4 5.6 0.0 207 2 5 4 29.412 58.823 0.319 6.04 8 79.4 14.1 208 3 1 4 29.456 58.912 0.319 6.02 8 140.1 43.7 209 0 0 18 29.473 58.946 0.319 6.01 2 740.0 304.0 210 2 4 9 29.546 59.091 0.32 5.97 8 31.0 2.1 211 3 0 5 29.56 59.119 0.32 5.97 4 59.0 3.8 212 1 5 11 29.649 59.298 0.321 5.93 8 25.7 1.4 213 3 2 0 29.694 59.388 0.322 5.91 4 49.2 2.6 214 1 1 17 29.739 59.479 0.322 5.89 8 127.5 35.4 215 3 2 1 29.744 59.487 0.322 5.89 8 80.5 14.1 216 2 0 14 29.755 59.51 0.322 5.88 4 31.6 1.1 217 0 6 9 29.786 59.572 0.322 5.87 4 626.0 424.9 218 2 2 13 29.79 59.58 0.322 5.87 8 21.1 1.0 219 1 6 7 29.856 59.712 0.323 5.84 8 26.5 1.5 220 2 5 5 29.86 59.72 0.323 5.83 8 68.7 10.2 221 3 2 2 29.892 59.785 0.324 5.82 8 24.3 1.3 222 3 1 5 29.904 59.807 0.324 5.82 8 126.5 34.4 223 0 4 15 30.059 60.118 0.325 5.75 4 162.2 28.0 224 2 1 14 30.098 60.196 0.326 5.73 8 63.1 8.4 225 3 2 3 30.14 60.279 0.326 5.71 8 27.5 1.6 226 2 3 12 30.265 60.53 0.327 5.66 8 24.6 1.3 227 1 4 14 30.276 60.553 0.327 5.66 8 19.6 0.8 228 2 5 6 30.402 60.804 0.328 5.6 8 22.1 1.0 229 3 1 6 30.446 60.891 0.329 5.59 8 81.0 13.6 230 3 2 4 30.483 60.967 0.329 5.57 8 66.2 9.0 231 2 4 10 30.485 60.969 0.329 5.57 8 39.1 3.1 232 1 6 8 30.594 61.189 0.33 5.53 8 17.2 0.6 233 0 6 10 30.721 61.441 0.332 5.48 4 36.1 1.3 234 3 0 7 30.742 61.485 0.332 5.47 4 17.2 0.3 235 1 2 17 30.761 61.522 0.332 5.46 8 25.6 1.3 236 1 5 12 30.781 61.562 0.332 5.45 8 37.7 2.9 237 0 2 18 30.838 61.677 0.333 5.43 4 14.2 0.2 238 1 3 16 30.84 61.68 0.333 5.43 8 17.1 0.6 239 3 2 5 30.922 61.845 0.334 5.4 8 26.4 1.4 240 2 5 7 31.036 62.072 0.335 5.35 8 5.7 0.1 241 3 1 7 31.079 62.157 0.335 5.34 8 18.0 0.6 242 2 2 14 31.113 62.225 0.335 5.32 8 22.9 1.0 243 3 3 0 31.387 62.775 0.338 5.22 4 238.7 55.0 244 1 6 9 31.419 62.837 0.338 5.21 8 16.1 0.5 245 3 3 1 31.436 62.871 0.339 5.2 8 149.2 42.8 246 1 1 18 31.45 62.899 0.339 5.2 8 57.5 6.4 247 3 2 6 31.454 62.908 0.339 5.2 8 16.3 0.5 248 2 3 13 31.48 62.96 0.339 5.19 8 13.7 0.4 249 2 4 11 31.503 63.006 0.339 5.18 8 27.5 1.5 250 2 1 15 31.509 63.019 0.339 5.18 8 33.9 2.2 251 0 4 16 31.567 63.135 0.34 5.16 4 42.3 1.7 252 3 3 2 31.58 63.159 0.34 5.15 8 14.8 0.4 253 1 4 15 31.683 63.366 0.341 5.12 8 25.1 1.2 254 0 6 11 31.735 63.469 0.341 5.1 4 15.6 0.2 255 2 5 8 31.758 63.516 0.342 5.09 8 23.9 1.1 256 3 1 8 31.8 63.6 0.342 5.07 8 158.6 47.2 257 3 3 3 31.819 63.638 0.342 5.07 8 71.2 9.5 258 1 7 0 31.851 63.702 0.343 5.06 4 395.0 145.8 259 1 7 1 31.898 63.797 0.343 5.04 8 212.6 84.2 260 1 5 13 31.985 63.97 0.344 5.01 8 39.2 2.8 261 1 7 2 32.041 64.083 0.344 4.99 8 35.7 2.3 262 3 2 7 32.075 64.151 0.345 4.98 8 15.7 0.5 263 3 3 4 32.153 64.305 0.345 4.95 8 136.1 33.9 264 1 7 3 32.279 64.558 0.347 4.91 8 24.3 1.1 265 3 0 9 32.28 64.56 0.347 4.91 4 60.0 3.3 266 1 6 10 32.326 64.651 0.347 4.9 8 21.8 0.9 267 2 6 0 32.337 64.674 0.347 4.89 4 34.6 1.1 268 2 6 1 32.384 64.769 0.348 4.88 8 11.7 0.2 269 1 3 17 32.422 64.844 0.348 4.87 8 206.4 76.6 270 1 2 18 32.44 64.88 0.348 4.86 8 20.8 0.8 271 2 2 15 32.499 64.997 0.349 4.84 8 33.9 2.1 272 2 6 2 32.526 65.052 0.349 4.83 8 42.1 3.2 273 2 5 9 32.565 65.131 0.349 4.82 8 30.5 1.7 274 3 3 5 32.579 65.157 0.35 4.82 8 147.5 38.7 275 2 4 12 32.597 65.195 0.35 4.81 8 10.6 0.2 276 3 1 9 32.607 65.214 0.35 4.81 8 222.9 88.3 277 0 2 19 32.609 65.218 0.35 4.81 4 84.0 6.3 278 1 7 4 32.61 65.22 0.35 4.81 8 18.3 0.6 279 2 0 16 32.654 65.309 0.35 4.79 4 44.4 1.7 280 2 6 3 32.762 65.524 0.351 4.76 8 13.0 0.3 281 2 3 14 32.764 65.527 0.351 4.76 8 19.5 0.7 282 3 2 8 32.785 65.57 0.351 4.75 8 10.1 0.2 283 0 6 12 32.825 65.65 0.352 4.74 4 104.5 9.6 284 1 0 19 32.878 65.756 0.352 4.72 4 31.7 0.9 285 2 1 16 32.98 65.96 0.353 4.69 8 7.3 0.1 286 1 7 5 33.033 66.066 0.354 4.67 8 57.7 5.8 287 2 6 4 33.09 66.18 0.354 4.66 8 138.7 33.1 288 3 3 6 33.095 66.191 0.354 4.66 8 89.2 13.7 289 0 4 17 33.13 66.26 0.355 4.65 4 49.1 2.1 290 0 0 20 33.14 66.28 0.355 4.64 2 49.7 1.1 291 1 4 16 33.15 66.299 0.355 4.64 8 3.9 0.0 292 1 1 19 33.202 66.405 0.355 4.62 8 51.5 4.5 293 1 5 14 33.258 66.516 0.356 4.61 8 53.9 5.0 294 1 6 11 33.312 66.625 0.356 4.59 8 19.3 0.6 295 2 5 10 33.456 66.911 0.358 4.55 8 19.9 0.7 296 3 1 10 33.497 66.994 0.358 4.54 8 86.0 12.4 297 2 6 5 33.51 67.02 0.358 4.53 8 12.6 0.3 298 1 7 6 33.546 67.092 0.359 4.52 8 28.4 1.3 299 3 2 9 33.579 67.159 0.359 4.51 8 248.4 103.0 300 3 4 0 33.676 67.353 0.36 4.49 4 209.9 36.6 301 3 3 7 33.701 67.402 0.36 4.48 8 19.5 0.6 302 3 4 1 33.723 67.446 0.36 4.47 8 21.3 0.8 303 2 4 13 33.766 67.532 0.361 4.46 8 122.5 24.8 304 3 4 2 33.862 67.723 0.362 4.44 8 7.0 0.1 305 2 2 16 33.947 67.893 0.362 4.41 8 13.9 0.3 306 0 6 13 33.989 67.979 0.363 4.4 4 24.4 0.5 307 2 6 6 34.02 68.039 0.363 4.39 8 91.3 13.5 308 1 3 18 34.056 68.113 0.364 4.38 8 243.8 96.3 309 3 4 3 34.093 68.185 0.364 4.37 8 49.2 3.9 310 2 3 15 34.114 68.227 0.364 4.37 8 9.1 0.1 311 1 7 7 34.148 68.295 0.364 4.36 8 20.4 0.7 312 3 0 11 34.148 68.297 0.364 4.36 4 37.5 1.1 313 1 2 19 34.166 68.332 0.365 4.35 8 29.0 1.4 314 1 6 12 34.377 68.754 0.367 4.3 8 34.4 1.9 315 3 3 8 34.393 68.786 0.367 4.3 8 72.2 8.3 316 3 4 4 34.415 68.829 0.367 4.29 8 29.1 1.3 317 0 2 20 34.423 68.846 0.367 4.29 4 28.8 0.7 318 2 5 11 34.426 68.852 0.367 4.29 8 15.5 0.4 319 3 2 10 34.456 68.913 0.367 4.28 8 10.7 0.2 320 3 1 11 34.467 68.933 0.367 4.28 8 19.0 0.6 321 2 1 17 34.509 69.019 0.368 4.27 8 47.1 3.5 322 1 5 15 34.598 69.197 0.369 4.24 8 105.0 17.3 323 2 6 7 34.617 69.234 0.369 4.24 8 17.1 0.5 324 1 4 17 34.675 69.35 0.369 4.22 8 16.1 0.4 325 0 4 18 34.748 69.496 0.37 4.21 4 207.5 33.5 326 3 4 5 34.827 69.653 0.371 4.19 8 112.3 19.5 327 1 7 8 34.835 69.671 0.371 4.18 8 20.6 0.7 X-ray diffraction powder data (I)...X-Ray wave length = 1.54056 (angs.): No H K L Theta 2*Theta d I int I int.n. I p.h.n. H(Si) ( degree ) (angstrem) *100 *100 1 0 0 2 3.134 6.268 14.09 49.0 4.2 4.3 5.5 2 0 2 1 8.42 16.84 5.26038 121.7 10.3 10.6 5.6 3 1 0 1 9.227 18.455 4.80365 13.6 1.1 1.2 5.6 4 0 0 6 9.439 18.879 4.69667 17.4 1.5 1.5 5.6 5 1 1 0 9.998 19.995 4.4369 174.0 14.7 15.2 5.6 6 1 1 1 10.122 20.244 4.38291 55.0 4.7 4.8 5.6 7 1 0 3 10.254 20.509 4.32698 27.2 2.3 2.4 5.6 8 0 2 4 10.41 20.82 4.26296 144.4 12.2 12.6 5.6 9 1 1 2 10.487 20.974 4.23203 60.7 5.1 5.3 5.6 10 1 1 3 11.07 22.139 4.01187 62.6 5.3 5.4 5.6 11 1 1 4 11.839 23.679 3.75437 374.0 31.7 32.5 5.6 12 1 0 5 12.059 24.117 3.68707 100.3 8.5 8.7 5.6 13 1 2 1 12.44 24.881 3.57563 90.0 7.6 7.8 5.6 14 0 2 6 12.601 25.202 3.53085 17.0 1.4 1.5 5.6 15 0 0 8 12.631 25.262 3.5225 22.0 1.9 1.9 5.6 16 1 1 5 12.765 25.53 3.48623 383.8 32.5 33.3 5.6 17 1 2 3 13.231 26.462 3.36546 16.9 1.4 1.5 5.6 18 1 1 6 13.817 27.634 3.22529 215.2 18.2 18.7 5.6 19 1 2 4 13.888 27.777 3.20907 40.5 3.4 3.5 5.6 20 1 3 0 15.513 31.025 2.8801 933.3 79.1 80.7 5.6 21 1 3 1 15.595 31.191 2.86517 668.0 56.6 57.7 5.6 22 0 0 10 15.863 31.727 2.818 123.8 10.5 10.7 5.6 23 1 1 8 16.213 32.426 2.75879 722.8 61.3 62.4 5.6 24 1 3 3 16.245 32.489 2.75357 137.3 11.6 11.9 5.6 25 0 2 9 16.558 33.116 2.70291 571.0 48.4 49.3 5.6 26 0 4 0 16.721 33.442 2.67725 168.6 14.3 14.5 5.7 27 1 3 4 16.794 33.588 2.66592 423.7 35.9 36.5 5.7 28 0 4 3 17.408 34.816 2.57471 34.3 2.9 3.0 5.7 29 1 3 5 17.478 34.957 2.56464 418.8 35.5 36.1 5.7 30 1 1 9 17.524 35.047 2.55824 974.5 82.6 83.9 5.7 31 1 3 6 18.284 36.568 2.45523 126.6 10.7 10.9 5.7 32 2 0 0 18.422 36.844 2.4375 215.1 18.2 18.5 5.7 33 0 4 5 18.574 37.147 2.41827 189.2 16.0 16.3 5.7 34 1 1 10 18.894 37.788 2.37877 201.3 17.1 17.3 5.7 35 2 1 1 18.98 37.961 2.3683 28.7 2.4 2.5 5.7 36 1 2 9 19.017 38.035 2.36388 279.1 23.7 24.0 5.7 37 1 4 0 19.162 38.325 2.34666 179.4 15.2 15.4 5.7 38 2 1 4 20.001 40.003 2.25201 67.6 5.7 5.8 5.7 39 1 3 8 20.21 40.421 2.22968 108.4 9.2 9.3 5.7 40 2 1 5 20.593 41.187 2.18995 35.2 3.0 3.0 5.7 41 0 4 8 21.185 42.37 2.13148 61.3 5.2 5.2 5.7 42 1 3 9 21.308 42.617 2.11973 79.0 6.7 6.8 5.7 43 2 2 4 21.347 42.695 2.11602 21.3 1.8 1.8 5.7 44 0 0 14 22.5 45.0 2.01286 27.7 2.3 2.4 5.7 45 2 2 6 22.582 45.163 2.00594 25.8 2.2 2.2 5.7 46 1 5 0 23.13 46.26 1.9609 23.3 2.0 2.0 5.7 47 1 5 1 23.189 46.379 1.95617 25.1 2.1 2.1 5.7 48 1 1 13 23.296 46.593 1.94767 48.0 4.1 4.1 5.7 49 1 5 3 23.659 47.317 1.91952 15.9 1.3 1.3 5.7 50 1 5 4 24.064 48.128 1.88908 34.3 2.9 2.9 5.7 51 1 5 5 24.577 49.154 1.852 41.0 3.5 3.5 5.7 52 2 0 10 24.698 49.395 1.84353 33.5 2.8 2.8 5.7 53 1 1 14 24.848 49.697 1.83305 65.4 5.5 5.5 5.7 54 1 3 12 25.038 50.077 1.82002 12.2 1.0 1.0 5.7 55 2 2 9 25.184 50.369 1.81015 1179.9 100.0 100.0 5.8 56 2 4 0 25.301 50.601 1.80238 453.1 38.4 38.4 5.8 57 2 4 3 25.796 51.591 1.77009 39.4 3.3 3.3 5.8 58 1 2 14 25.995 51.991 1.75744 22.6 1.9 1.9 5.8 59 1 3 13 26.407 52.814 1.73195 99.2 8.4 8.4 5.8 60 0 6 4 26.436 52.873 1.73017 171.3 14.5 14.5 5.8 61 2 4 5 26.66 53.319 1.71674 161.2 13.7 13.6 5.8 62 1 5 8 26.717 53.434 1.71331 79.8 6.8 6.7 5.8 63 2 3 9 27.059 54.119 1.69324 14.0 1.2 1.2 5.8 64 0 4 13 27.208 54.416 1.68471 90.5 7.7 7.6 5.8 65 0 6 6 27.496 54.991 1.66842 41.3 3.5 3.5 5.8 66 1 5 9 27.613 55.226 1.66189 173.8 14.7 14.6 5.8 67 1 3 14 27.832 55.663 1.64986 98.7 8.4 8.3 5.8 68 1 5 10 28.592 57.183 1.60956 41.6 3.5 3.5 5.8 69 3 1 0 28.649 57.298 1.60661 52.3 4.4 4.4 5.8 70 2 4 8 28.69 57.379 1.60454 88.3 7.5 7.4 5.8 71 0 2 17 29.107 58.214 1.5835 61.5 5.2 5.2 5.8 72 1 3 15 29.31 58.62 1.57351 33.7 2.9 2.8 5.8 73 2 5 4 29.412 58.823 1.56854 14.1 1.2 1.2 5.8 74 0 0 18 29.473 58.946 1.56556 347.6 29.5 29.1 5.8 75 1 1 17 29.739 59.479 1.55281 50.6 4.3 4.2 5.8 76 0 6 9 29.786 59.572 1.5506 425.9 36.1 35.7 5.8 77 3 1 5 29.904 59.807 1.54506 35.7 3.0 3.0 5.8 78 0 4 15 30.059 60.118 1.53782 28.0 2.4 2.3 5.8 79 3 1 6 30.446 60.891 1.52013 13.6 1.1 1.1 5.8 80 3 2 4 30.483 60.967 1.51842 12.2 1.0 1.0 5.8 81 3 3 0 31.387 62.775 1.47897 55.0 4.7 4.6 5.9 82 3 3 1 31.436 62.871 1.47693 49.7 4.2 4.1 5.9 83 3 1 8 31.8 63.6 1.46175 56.7 4.8 4.7 5.9 84 1 7 0 31.851 63.702 1.45967 145.8 12.4 12.1 5.9 85 1 7 1 31.898 63.797 1.45772 84.2 7.1 7.0 5.9 86 3 3 4 32.153 64.305 1.44742 33.9 2.9 2.8 5.9 87 1 3 17 32.422 64.844 1.43668 77.4 6.6 6.4 5.9 88 3 1 9 32.607 65.214 1.42942 135.5 11.5 11.2 5.9 89 2 6 4 33.09 66.18 1.41088 46.8 4.0 3.9 5.9 90 3 1 10 33.497 66.994 1.39571 12.7 1.1 1.0 5.9 91 3 2 9 33.579 67.159 1.39269 103.0 8.7 8.5 5.9 92 3 4 0 33.676 67.353 1.38914 37.2 3.2 3.1 5.9 93 2 4 13 33.766 67.532 1.3859 24.8 2.1 2.0 5.9 94 2 6 6 34.02 68.039 1.37679 13.5 1.1 1.1 5.9 95 1 3 18 34.056 68.113 1.37548 96.3 8.2 8.0 5.9 96 3 3 8 34.393 68.786 1.36365 12.5 1.1 1.0 5.9 97 1 5 15 34.598 69.197 1.35656 17.7 1.5 1.5 5.9 98 0 4 18 34.748 69.496 1.35145 33.5 2.8 2.8 5.9 99 3 4 5 34.827 69.653 1.34877 20.2 1.7 1.7 5.9 Reference: Chichagov A.V. et al. Information-Calculating System on Crystal Structure Data of Minerals (MINCRYST) - Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian) |