Institute of Experimental Mineralogy Russian Academy of Sciences ------------------------------------------------- 142432, Chernogolovka, Moscow district A.V. Chichagov +7(496)52-22320 *** *** W W W - X R A Y P O L *** *********************** HOPEITE 3, syn, f-hopeite Zn(3)[PO(4)](2).4H(2)O Orthorhombic P nma Z = 4 Pnma 1 .2 .1908 Ref.Str.: Kawahara A., Takano Y., Takahashi M. (1973) * Mineral. J., 7, 289-297 Reserv: N.A.D. Initial data from BDM-file Lattice parameters (cub. angs.,degr.): a = 10.553 alpha = 90.0 b = 18.199 beta = 90.0 c = 5.031 gamma = 90.0 Unit cell volume (cub. angs.) = 966.22 Molar volume ( cub.cm/mol.) = 145.5 Co-ordinates, thermal parameters, occupation for atomic positions: NoP x/a y/b z/c B(j) atom / occupation 1 0.2638 0.25 0.4277 1.08 Zn = 1.00 2 0.1429 0.0007 0.2934 0.87 Zn = 1.00 3 0.397 0.0945 0.2751 0.87 P = 1.00 4 0.3028 0.0411 0.1318 1.02 O = 1.00 5 0.5252 0.0785 0.1334 1.43 O = 1.00 6 0.3611 0.1728 0.2133 1.63 O = 1.00 7 0.3994 0.0807 0.5691 2.01 O = 1.00 8 0.1633 0.169 0.6602 1.98 H(2)O = 1.00 9 0.3922 0.25 0.7409 1.87 H(2)O = 1.00 10 0.1136 0.25 0.1565 2.11 H(2)O = 1.00 Co-ordinates for all atomic positions : No NoP x/a y/b z/c 1 1 0.2638 0.25 0.4277 2 2 0.1429 0.0007 0.2934 3 3 0.397 0.0945 0.2751 4 4 0.3028 0.0411 0.1318 5 5 0.5252 0.0785 0.1334 6 6 0.3611 0.1728 0.2133 7 7 0.3994 0.0807 0.5691 8 8 0.1633 0.169 0.6602 9 9 0.3922 0.25 0.7409 10 10 0.1136 0.25 0.1565 11 1 0.2362 0.75 0.9277 12 2 0.3571 0.9993 0.7934 13 3 0.103 0.9055 0.7751 14 4 0.1972 0.9589 0.6318 15 5 0.9748 0.9215 0.6334 16 6 0.1389 0.8272 0.7133 17 7 0.1006 0.9193 0.0691 18 8 0.3367 0.831 0.1602 19 9 0.1078 0.75 0.2409 20 10 0.3864 0.75 0.6565 21 2 0.3571 0.5007 0.7934 22 3 0.103 0.5945 0.7751 23 4 0.1972 0.5411 0.6318 24 5 0.9748 0.5785 0.6334 25 6 0.1389 0.6728 0.7133 26 7 0.1006 0.5807 0.0691 27 8 0.3367 0.669 0.1602 28 2 0.1429 0.4993 0.2934 29 3 0.397 0.4055 0.2751 30 4 0.3028 0.4589 0.1318 31 5 0.5252 0.4215 0.1334 32 6 0.3611 0.3272 0.2133 33 7 0.3994 0.4193 0.5691 34 8 0.1633 0.331 0.6602 35 1 0.7638 0.25 0.0723 36 2 0.6429 0.0007 0.2066 37 3 0.8971 0.0945 0.2249 38 4 0.8028 0.0411 0.3682 39 5 0.0252 0.0785 0.3666 40 6 0.8611 0.1728 0.2867 41 7 0.8994 0.0807 0.9309 42 8 0.6633 0.169 0.8398 43 9 0.8922 0.25 0.7591 44 10 0.6136 0.25 0.3435 45 1 0.7362 0.75 0.5723 46 2 0.8571 0.9993 0.7066 47 3 0.6029 0.9055 0.7249 48 4 0.6972 0.9589 0.8682 49 5 0.4748 0.9215 0.8666 50 6 0.6389 0.8272 0.7867 51 7 0.6006 0.9193 0.4309 52 8 0.8367 0.831 0.3398 53 9 0.6078 0.75 0.2591 54 10 0.8864 0.75 0.8435 55 2 0.8571 0.5007 0.7066 56 3 0.6029 0.5945 0.7249 57 4 0.6972 0.5411 0.8682 58 5 0.4748 0.5785 0.8666 59 6 0.6389 0.6728 0.7867 60 7 0.6006 0.5807 0.4309 61 8 0.8367 0.669 0.3398 62 2 0.6429 0.4993 0.2066 63 3 0.8971 0.4055 0.2249 64 4 0.8028 0.4589 0.3682 65 5 0.0252 0.4215 0.3666 66 6 0.8611 0.3272 0.2867 67 7 0.8994 0.4193 0.9309 68 8 0.6633 0.331 0.8398 X-ray density (g/cm cub.) = 3.15 MU (1/cm) = 128.633 Mass attenuation coefficient (cm**2/g) = 40.857 Selected interatomic distances (cation-anion,anion-anion): NoP Atom Rad.sph. C.N. Distance NoP N. (angs.) (angs.) 1 Zn 2.796 6 2.0472 6 2.1603 8 2.0779 9 2.0917 10 2.0472 6 2.1603 8 2 Zn 2.796 4 2.0116 4 1.9508 4 1.9154 7 1.9192 5 3 P 2.4 4 1.5661 4 1.5562 5 1.5074 6 1.5004 7 4 O 3.432 9 2.4437 5 2.5083 6 2.5296 7 3.094 7 3.1317 4 3.1317 4 3.0929 7 3.2312 5 3.1325 5 5 O 3.432 10 2.4437 4 2.471 6 2.563 7 3.1343 7 3.2312 4 2.6492 8 3.4248 10 3.1325 4 3.2013 5 3.3567 7 6 O 3.432 9 2.5083 4 2.471 5 2.4854 7 3.0687 8 3.0211 9 2.7803 9 2.9795 10 2.8099 6 3.0827 10 7 O 3.432 9 3.094 4 2.5296 4 3.1343 5 2.563 5 2.4854 6 3.0001 8 3.2009 9 3.0929 4 3.3567 5 8 H(2)O 3.6 10 3.4792 6 3.0687 6 3.0001 7 2.8588 9 2.9466 10 2.9782 10 2.9482 8 2.6492 5 3.4918 7 3.2566 9 9 H(2)O 3.6 11 2.7803 6 3.0211 6 3.2009 7 2.8588 8 2.7803 6 3.0211 6 3.2009 7 2.8588 8 3.2566 8 3.0751 10 3.2566 8 10 H(2)O 3.6 11 2.9795 6 2.9782 8 2.9466 8 2.9795 6 2.9782 8 2.9466 8 3.4248 5 3.0827 6 3.0751 9 3.4248 5 3.0827 6 X-ray diffraction powder data (II), X-Ray W.L. = 1.54056(angs.): No H K L Theta 2*Theta S LPG MF F I int. ( degree ) *100 1 0 2 0 4.856 9.712 0.055 276.12 2 145.7 1256.1 2 2 0 0 8.394 16.788 0.095 90.91 2 120.8 284.4 3 2 1 0 8.743 17.485 0.099 83.63 4 107.3 412.4 4 0 1 1 9.14 18.28 0.103 76.33 4 126.6 523.9 5 2 2 0 9.715 19.43 0.11 67.31 4 74.5 160.2 6 0 4 0 9.747 19.494 0.11 66.86 2 226.3 733.6 7 1 0 1 9.765 19.531 0.11 66.6 4 33.0 31.1 8 1 1 1 10.068 20.136 0.113 62.53 8 109.5 642.3 9 1 2 1 10.927 21.855 0.123 52.76 8 46.5 97.8 10 2 3 0 11.156 22.312 0.126 50.53 4 127.9 354.4 11 0 3 1 11.473 22.946 0.129 47.66 4 100.2 205.2 12 2 0 1 12.213 24.426 0.137 41.82 4 51.9 48.3 13 1 3 1 12.232 24.465 0.138 41.68 8 60.0 128.7 14 2 1 1 12.459 24.918 0.14 40.1 8 14.0 6.7 15 2 4 0 12.918 25.835 0.145 37.16 4 181.1 522.1 16 2 2 1 13.171 26.342 0.148 35.67 8 153.9 724.3 17 1 4 1 13.866 27.732 0.156 31.99 8 21.5 12.7 18 2 3 1 14.284 28.568 0.16 30.03 8 74.8 143.9 19 0 6 0 14.712 29.423 0.165 28.19 2 35.2 7.5 20 2 5 0 14.898 29.795 0.167 27.45 4 70.8 59.0 21 0 5 1 15.142 30.283 0.17 26.51 4 98.6 110.4 22 3 0 1 15.497 30.994 0.173 25.22 4 30.6 10.1 23 3 1 1 15.695 31.391 0.176 24.54 8 54.4 62.2 24 2 4 1 15.721 31.442 0.176 24.45 8 274.3 1576.2 25 1 5 1 15.736 31.473 0.176 24.4 8 53.3 59.3 26 3 2 1 16.277 32.554 0.182 22.68 8 53.7 56.0 27 4 0 0 16.976 33.951 0.19 20.71 2 245.1 266.6 28 2 6 0 17.033 34.066 0.19 20.55 4 64.2 36.3 29 4 1 0 17.159 34.317 0.192 20.23 4 4.3 0.2 30 3 3 1 17.207 34.414 0.192 20.1 8 160.3 442.8 31 2 5 1 17.411 34.823 0.194 19.59 8 53.9 48.8 32 4 2 0 17.697 35.395 0.197 18.91 4 181.7 267.4 33 1 6 1 17.781 35.563 0.198 18.71 8 76.1 92.9 34 0 0 2 17.831 35.662 0.199 18.6 2 241.4 232.1 35 1 0 2 18.348 36.697 0.204 17.47 4 40.9 12.5 36 3 4 1 18.44 36.88 0.205 17.28 8 33.5 16.6 37 1 1 2 18.519 37.039 0.206 17.11 8 0.2 0.0 38 0 2 2 18.524 37.048 0.206 17.11 4 162.6 193.7 39 4 3 0 18.565 37.13 0.207 17.02 4 39.0 11.1 40 1 2 2 19.025 38.049 0.212 16.13 8 5.8 0.5 41 4 0 1 19.249 38.498 0.214 15.71 4 11.0 0.8 42 2 7 0 19.286 38.573 0.214 15.65 4 64.5 27.9 43 2 6 1 19.3 38.601 0.215 15.62 8 106.6 152.1 44 4 1 1 19.413 38.827 0.216 15.42 8 3.3 0.1 45 0 7 1 19.481 38.963 0.216 15.3 4 60.2 23.7 46 4 4 0 19.725 39.449 0.219 14.89 4 31.7 6.4 47 0 8 0 19.792 39.584 0.22 14.78 2 170.3 91.9 48 2 0 2 19.83 39.66 0.22 14.71 4 23.7 3.5 49 1 3 2 19.843 39.685 0.22 14.69 8 70.6 62.8 50 4 2 1 19.899 39.799 0.221 14.6 8 92.6 107.2 51 3 5 1 19.929 39.857 0.221 14.55 8 34.6 14.9 52 1 7 1 19.962 39.924 0.222 14.5 8 98.4 120.2 53 2 1 2 19.99 39.981 0.222 14.45 8 48.1 28.6 54 2 2 2 20.465 40.93 0.227 13.72 8 75.8 67.6 55 0 4 2 20.481 40.962 0.227 13.69 4 56.0 18.4 56 4 3 1 20.688 41.377 0.229 13.39 8 56.8 37.0 57 1 4 2 20.943 41.885 0.232 13.03 8 111.5 138.8 58 4 5 0 21.137 42.274 0.234 12.76 4 69.8 26.6 59 2 3 2 21.236 42.473 0.235 12.63 8 38.0 15.6 60 2 7 1 21.349 42.698 0.236 12.48 8 2.8 0.1 61 3 6 1 21.631 43.262 0.239 12.12 8 126.1 165.1 62 2 8 0 21.637 43.275 0.239 12.11 4 109.9 62.7 63 4 4 1 21.753 43.506 0.241 11.96 8 28.1 8.1 64 3 0 2 22.114 44.228 0.244 11.53 4 17.0 1.4 65 1 8 1 22.254 44.508 0.246 11.37 8 2.3 0.1 66 3 1 2 22.261 44.522 0.246 11.36 8 46.5 21.0 67 2 4 2 22.28 44.56 0.246 11.34 8 13.5 1.8 68 1 5 2 22.291 44.583 0.246 11.32 8 33.8 11.1 69 3 2 2 22.697 45.393 0.25 10.87 8 136.2 172.8 70 4 6 0 22.765 45.531 0.251 10.8 4 178.3 147.1 71 4 5 1 23.064 46.127 0.254 10.48 8 56.6 28.7 72 5 0 1 23.314 46.628 0.257 10.23 4 57.2 14.3 73 3 3 2 23.409 46.818 0.258 10.14 8 14.3 1.8 74 0 6 2 23.442 46.884 0.258 10.1 4 156.3 105.8 75 5 1 1 23.455 46.91 0.258 10.09 8 65.5 37.1 76 3 7 1 23.513 47.027 0.259 10.03 8 60.3 31.3 77 2 8 1 23.532 47.063 0.259 10.02 8 199.8 342.6 78 2 5 2 23.568 47.135 0.26 9.98 8 12.5 1.3 79 1 6 2 23.857 47.714 0.263 9.71 8 25.9 5.6 80 5 2 1 23.874 47.748 0.263 9.69 8 57.2 27.2 81 2 9 0 24.076 48.151 0.265 9.51 4 60.0 14.7 82 0 9 1 24.239 48.478 0.266 9.37 4 19.6 1.5 83 3 4 2 24.379 48.758 0.268 9.24 8 34.4 9.3 84 5 3 1 24.56 49.12 0.27 9.09 8 49.4 19.0 85 4 7 0 24.58 49.16 0.27 9.07 4 26.2 2.7 86 4 6 1 24.592 49.183 0.27 9.06 8 40.9 13.0 87 1 9 1 24.644 49.289 0.271 9.02 8 21.9 3.7 88 4 0 2 25.03 50.061 0.275 8.71 4 248.4 230.2 89 0 10 0 25.04 50.08 0.275 8.7 2 84.2 13.2 90 2 6 2 25.072 50.144 0.275 8.67 8 102.0 77.4 91 4 1 2 25.164 50.328 0.276 8.6 8 33.5 8.3 92 5 4 1 25.497 50.994 0.279 8.35 8 44.4 14.1 93 3 8 1 25.552 51.104 0.28 8.31 8 9.4 0.6 94 4 2 2 25.562 51.123 0.28 8.3 8 44.2 13.9 95 3 5 2 25.586 51.171 0.28 8.28 8 5.2 0.2 96 1 7 2 25.613 51.226 0.281 8.26 8 19.1 2.6 97 2 9 1 25.832 51.663 0.283 8.1 8 79.8 44.3 98 6 0 0 25.973 51.946 0.284 8.0 2 16.3 0.5 99 6 1 0 26.103 52.206 0.286 7.91 4 20.9 1.5 100 4 3 2 26.215 52.43 0.287 7.84 8 0.2 0.0 101 4 7 1 26.311 52.622 0.288 7.77 8 5.1 0.2 102 6 2 0 26.491 52.982 0.29 7.65 4 134.0 58.9 103 4 8 0 26.558 53.115 0.29 7.61 4 68.0 15.1 104 2 10 0 26.598 53.195 0.291 7.58 4 85.6 23.8 105 5 5 1 26.667 53.333 0.291 7.54 8 77.2 38.5 106 2 7 2 26.769 53.538 0.292 7.47 8 32.7 6.8 107 3 6 2 27.007 54.014 0.295 7.32 8 80.0 40.1 108 4 4 2 27.111 54.222 0.296 7.26 8 125.2 97.5 109 1 10 1 27.128 54.255 0.296 7.25 8 15.9 1.6 110 6 3 0 27.128 54.257 0.296 7.25 4 97.2 29.3 111 0 8 2 27.163 54.327 0.296 7.23 4 81.9 20.8 112 0 1 3 27.469 54.938 0.299 7.05 4 28.6 2.5 113 1 8 2 27.537 55.075 0.3 7.01 8 141.1 119.5 114 6 0 1 27.642 55.283 0.301 6.95 4 81.6 19.8 115 1 0 3 27.716 55.431 0.302 6.9 4 92.0 25.0 116 3 9 1 27.729 55.458 0.302 6.9 8 95.5 53.9 117 6 1 1 27.766 55.533 0.302 6.87 8 44.2 11.5 118 1 1 3 27.84 55.68 0.303 6.83 8 8.9 0.5 119 6 4 0 28.004 56.008 0.305 6.74 4 41.1 4.9 120 5 6 1 28.05 56.1 0.305 6.72 8 32.5 6.1 121 6 2 1 28.138 56.276 0.306 6.67 8 78.9 35.6 122 4 8 1 28.202 56.405 0.307 6.64 8 81.3 37.6 123 1 2 3 28.211 56.423 0.307 6.63 8 73.4 30.6 124 4 5 2 28.234 56.468 0.307 6.62 8 14.8 1.2 125 2 10 1 28.241 56.481 0.307 6.62 8 81.1 37.3 126 5 0 2 28.451 56.902 0.309 6.51 4 38.3 4.1 127 0 3 3 28.46 56.92 0.309 6.5 4 133.9 49.9 128 5 1 2 28.573 57.146 0.31 6.44 8 7.3 0.3 129 3 7 2 28.624 57.248 0.311 6.42 8 44.7 11.0 130 2 8 2 28.64 57.28 0.311 6.41 8 27.1 4.0 131 4 9 0 28.682 57.364 0.312 6.39 4 65.3 11.7 132 6 3 1 28.751 57.502 0.312 6.35 8 3.5 0.1 133 2 0 3 28.814 57.627 0.313 6.32 4 22.2 1.3 134 1 3 3 28.823 57.646 0.313 6.32 8 24.0 3.1 135 2 1 3 28.935 57.87 0.314 6.26 8 65.6 23.1 136 5 2 2 28.938 57.876 0.314 6.26 8 127.8 87.6 137 6 5 0 29.104 58.209 0.316 6.18 4 46.4 5.7 138 2 11 0 29.205 58.409 0.317 6.13 4 5.2 0.1 139 2 2 3 29.297 58.594 0.318 6.09 8 52.8 14.5 140 0 11 1 29.348 58.695 0.318 6.07 4 5.3 0.1 141 5 3 2 29.54 59.081 0.32 5.98 8 51.5 13.6 142 4 6 2 29.568 59.137 0.32 5.96 8 45.9 10.8 143 6 4 1 29.595 59.19 0.321 5.95 8 188.0 180.2 144 1 9 2 29.615 59.23 0.321 5.94 8 32.7 5.4 145 5 7 1 29.629 59.258 0.321 5.94 8 64.7 21.3 146 1 4 3 29.666 59.332 0.321 5.92 8 51.3 13.3 147 1 11 1 29.704 59.407 0.322 5.9 8 74.4 28.0 148 2 3 3 29.895 59.789 0.324 5.82 8 43.1 9.3 149 3 10 1 30.035 60.071 0.325 5.76 8 23.4 2.7 150 4 9 1 30.25 60.501 0.327 5.67 8 52.7 13.5 151 5 4 2 30.371 60.741 0.328 5.62 8 33.5 5.4 152 0 5 3 30.38 60.759 0.328 5.61 4 95.4 21.9 153 6 6 0 30.415 60.829 0.329 5.6 4 234.6 132.0 154 3 8 2 30.42 60.839 0.329 5.6 8 29.0 4.0 155 0 12 0 30.524 61.049 0.33 5.55 2 329.5 129.2 156 3 0 3 30.587 61.174 0.33 5.53 4 111.9 29.7 157 6 5 1 30.659 61.318 0.331 5.5 8 0.4 0.0 158 2 9 2 30.669 61.339 0.331 5.5 8 39.6 7.4 159 3 1 3 30.704 61.408 0.331 5.48 8 18.5 1.6 160 2 4 3 30.719 61.438 0.332 5.48 8 168.5 133.3 161 1 5 3 30.728 61.457 0.332 5.47 8 42.0 8.3 162 2 11 1 30.756 61.513 0.332 5.46 8 10.5 0.5 163 4 10 0 30.943 61.886 0.334 5.39 4 204.1 96.2 164 3 2 3 31.054 62.107 0.335 5.35 8 71.9 23.7 165 4 7 2 31.099 62.198 0.335 5.33 8 39.5 7.1 166 5 8 1 31.389 62.779 0.338 5.22 8 55.7 13.9 167 5 5 2 31.419 62.838 0.338 5.21 8 25.9 3.0 168 0 10 2 31.494 62.988 0.339 5.18 4 174.0 67.3 169 3 3 3 31.631 63.262 0.34 5.13 8 33.0 4.8 170 2 5 3 31.761 63.522 0.342 5.09 8 70.2 21.5 171 1 10 2 31.836 63.671 0.342 5.06 8 46.6 9.4 172 2 12 0 31.902 63.804 0.343 5.04 4 40.1 3.5 173 6 7 0 31.921 63.843 0.343 5.03 4 22.8 1.1 174 6 6 1 31.931 63.862 0.343 5.03 8 88.3 33.6 175 1 6 3 31.999 63.997 0.344 5.01 8 84.1 30.3 176 7 0 1 32.235 64.469 0.346 4.93 4 79.1 13.2 177 6 0 2 32.302 64.604 0.347 4.9 4 83.5 14.7 178 7 1 1 32.348 64.697 0.347 4.89 8 41.9 7.4 179 1 12 1 32.376 64.753 0.348 4.88 8 8.6 0.3 180 3 9 2 32.382 64.764 0.348 4.88 8 20.4 1.7 181 6 1 2 32.416 64.831 0.348 4.87 8 56.4 13.3 182 3 4 3 32.43 64.86 0.348 4.86 8 86.5 31.2 183 4 10 1 32.446 64.891 0.348 4.86 8 116.6 56.6 184 3 11 1 32.466 64.932 0.348 4.85 8 46.5 9.0 185 5 6 2 32.674 65.349 0.35 4.79 8 99.1 40.2 186 7 2 1 32.688 65.376 0.351 4.78 8 5.9 0.1 187 6 2 2 32.755 65.51 0.351 4.76 8 24.0 2.3 188 4 8 2 32.814 65.627 0.352 4.74 8 138.2 77.6 189 2 10 2 32.849 65.697 0.352 4.73 8 46.5 8.8 190 4 0 3 32.974 65.948 0.353 4.69 4 112.2 25.3 191 2 6 3 33.009 66.018 0.354 4.68 8 120.3 58.0 192 4 1 3 33.086 66.173 0.354 4.66 8 99.6 39.6 193 0 7 3 33.133 66.266 0.355 4.64 4 30.4 1.8 194 7 3 1 33.25 66.5 0.356 4.61 8 17.1 1.1 195 6 3 2 33.316 66.633 0.357 4.59 8 2.9 0.0 196 5 9 1 33.32 66.64 0.357 4.59 8 41.2 6.7 197 4 11 0 33.336 66.673 0.357 4.58 4 15.3 0.5 198 2 12 1 33.381 66.761 0.357 4.57 8 82.0 26.4 199 6 7 1 33.4 66.799 0.357 4.57 8 54.2 11.5 200 4 2 3 33.422 66.844 0.358 4.56 8 56.4 12.4 201 3 5 3 33.442 66.885 0.358 4.55 8 26.7 2.8 202 1 7 3 33.466 66.931 0.358 4.55 8 4.8 0.1 203 6 8 0 33.613 67.226 0.359 4.51 4 12.0 0.3 204 4 3 3 33.978 67.956 0.363 4.4 8 29.1 3.2 205 7 4 1 34.029 68.058 0.363 4.39 8 44.2 7.3 206 6 4 2 34.095 68.189 0.364 4.37 8 105.4 41.6 207 5 7 2 34.126 68.252 0.364 4.37 8 10.5 0.4 208 1 11 2 34.195 68.39 0.365 4.35 8 10.1 0.4 209 2 7 3 34.454 68.908 0.367 4.28 8 57.8 12.3 210 3 10 2 34.503 69.005 0.368 4.27 8 83.3 25.4 211 3 6 3 34.659 69.319 0.369 4.23 8 136.2 67.2 212 2 13 0 34.699 69.398 0.37 4.22 4 64.4 7.5 213 4 9 2 34.702 69.405 0.37 4.22 8 2.5 0.0 214 4 4 3 34.749 69.498 0.37 4.21 8 31.8 3.7 215 4 11 1 34.784 69.568 0.37 4.2 8 51.7 9.6 216 0 13 1 34.829 69.659 0.371 4.19 4 87.0 13.6 217 7 5 1 35.018 70.036 0.372 4.14 8 58.9 12.3 218 3 12 1 35.022 70.045 0.373 4.14 8 6.5 0.1 219 6 8 1 35.055 70.11 0.373 4.13 8 128.6 58.5 220 6 5 2 35.083 70.166 0.373 4.12 8 10.3 0.4 221 1 8 3 35.12 70.239 0.373 4.12 8 15.3 0.8 222 1 13 1 35.154 70.309 0.374 4.11 8 66.6 15.6 223 2 11 2 35.174 70.347 0.374 4.1 8 11.8 0.5 224 5 10 1 35.413 70.826 0.376 4.05 8 11.7 0.5 225 6 9 0 35.481 70.962 0.377 4.03 4 113.3 22.2 226 8 0 0 35.728 71.455 0.379 3.98 2 157.4 21.1 227 4 5 3 35.729 71.459 0.379 3.98 8 56.2 10.8 228 5 8 2 35.766 71.532 0.379 3.97 8 42.0 6.0 229 8 1 0 35.836 71.672 0.38 3.95 4 92.6 14.5 230 4 12 0 35.863 71.725 0.38 3.95 4 134.8 30.8 231 5 0 3 35.92 71.841 0.381 3.94 4 49.9 4.2 232 5 1 3 36.028 72.057 0.382 3.91 8 7.1 0.2 233 3 7 3 36.073 72.146 0.382 3.9 8 20.4 1.4 234 2 8 3 36.087 72.174 0.382 3.9 8 111.8 41.7 235 2 13 1 36.121 72.243 0.383 3.89 8 3.9 0.1 236 8 2 0 36.16 72.319 0.383 3.89 4 8.3 0.1 237 7 6 1 36.211 72.422 0.383 3.88 8 1.9 0.0 238 6 6 2 36.275 72.549 0.384 3.86 8 81.2 21.8 239 0 14 0 36.339 72.677 0.385 3.85 2 5.0 0.0 240 5 2 3 36.351 72.703 0.385 3.85 8 6.3 0.1 241 0 12 2 36.375 72.751 0.385 3.84 4 124.8 25.6 242 7 0 2 36.561 73.121 0.387 3.8 4 38.0 2.3 243 0 9 3 36.636 73.272 0.387 3.79 4 123.8 24.9 244 7 1 2 36.668 73.336 0.388 3.78 8 21.3 1.5 245 1 12 2 36.694 73.389 0.388 3.78 8 84.9 23.3 246 8 3 0 36.697 73.393 0.388 3.78 4 57.4 5.3 247 4 10 2 36.76 73.519 0.388 3.77 8 78.5 19.9 248 3 11 2 36.779 73.558 0.389 3.76 8 41.1 5.4 249 5 3 3 36.887 73.775 0.39 3.74 8 15.7 0.8 250 6 9 1 36.891 73.781 0.39 3.74 8 6.3 0.1 251 4 6 3 36.912 73.825 0.39 3.74 8 25.1 2.0 252 1 9 3 36.954 73.908 0.39 3.73 8 36.0 4.1 253 7 2 2 36.989 73.978 0.391 3.72 8 30.5 3.0 254 8 0 1 37.133 74.267 0.392 3.7 4 125.8 25.0 255 8 1 1 37.24 74.48 0.393 3.68 8 47.3 7.1 256 4 12 1 37.266 74.532 0.393 3.67 8 36.4 4.2 257 8 4 0 37.444 74.887 0.395 3.64 4 89.4 12.5 258 6 10 0 37.521 75.042 0.395 3.63 4 69.7 7.6 259 7 3 2 37.521 75.043 0.395 3.63 8 24.7 1.9 260 8 2 1 37.559 75.118 0.396 3.62 8 123.0 46.9 261 5 9 2 37.588 75.175 0.396 3.61 8 8.3 0.2 262 7 7 1 37.6 75.201 0.396 3.61 8 43.5 5.9 263 2 14 0 37.609 75.219 0.396 3.61 4 60.6 5.7 264 5 4 3 37.633 75.266 0.396 3.61 8 17.2 0.9 265 2 12 2 37.646 75.291 0.396 3.6 8 17.0 0.9 266 6 7 2 37.663 75.327 0.397 3.6 8 38.8 4.6 267 5 11 1 37.667 75.333 0.397 3.6 8 49.5 7.5 268 3 8 3 37.677 75.354 0.397 3.6 8 54.0 9.0 269 3 13 1 37.711 75.421 0.397 3.59 8 39.3 4.8 270 0 0 4 37.765 75.53 0.398 3.58 2 42.5 1.4 271 2 9 3 37.903 75.805 0.399 3.56 8 51.6 8.1 272 1 14 1 38.05 76.101 0.4 3.54 8 21.4 1.4 273 1 0 4 38.08 76.16 0.4 3.53 4 23.4 0.8 274 8 3 1 38.089 76.177 0.4 3.53 8 3.2 0.0 275 1 1 4 38.186 76.371 0.401 3.51 8 15.0 0.7 276 0 2 4 38.188 76.377 0.401 3.51 4 47.2 3.4 277 7 4 2 38.263 76.525 0.402 3.5 8 27.9 2.3 278 4 7 3 38.293 76.585 0.402 3.5 8 63.1 11.9 279 8 5 0 38.396 76.793 0.403 3.48 4 71.8 7.7 280 1 2 4 38.502 77.004 0.404 3.46 8 154.3 70.6 281 4 13 0 38.528 77.056 0.404 3.46 4 27.5 1.1 282 5 5 3 38.584 77.168 0.405 3.45 8 4.2 0.1 283 8 4 1 38.826 77.653 0.407 3.41 8 63.1 11.7 284 6 10 1 38.903 77.806 0.408 3.4 8 12.7 0.5 285 1 10 3 38.965 77.93 0.408 3.39 8 32.9 3.1 286 4 11 2 38.984 77.968 0.408 3.39 8 1.9 0.0 287 2 14 1 38.99 77.98 0.408 3.39 8 152.2 67.3 288 2 0 4 39.02 78.039 0.409 3.39 4 14.7 0.3 289 1 3 4 39.028 78.055 0.409 3.39 8 35.1 3.6 290 2 1 4 39.124 78.249 0.41 3.37 8 51.2 7.6 291 7 8 1 39.182 78.364 0.41 3.36 8 46.0 6.1 292 7 5 2 39.209 78.418 0.41 3.36 8 14.0 0.6 293 3 12 2 39.213 78.426 0.41 3.36 8 31.9 2.9 294 6 8 2 39.244 78.489 0.411 3.35 8 60.2 10.4 295 1 13 2 39.34 78.679 0.411 3.34 8 17.9 0.9 296 6 0 3 39.394 78.787 0.412 3.33 4 18.8 0.5 297 2 2 4 39.439 78.877 0.412 3.33 8 18.0 0.9 298 0 4 4 39.449 78.899 0.412 3.33 4 7.3 0.1 299 3 9 3 39.467 78.934 0.413 3.32 8 6.6 0.1 300 6 1 3 39.498 78.997 0.413 3.32 8 27.2 2.1 301 8 6 0 39.551 79.102 0.413 3.31 4 11.6 0.2 302 5 10 2 39.588 79.176 0.414 3.31 8 99.8 28.2 303 6 11 0 39.731 79.463 0.415 3.29 4 0.2 0.0 304 5 6 3 39.737 79.474 0.415 3.29 8 54.8 8.4 305 1 4 4 39.76 79.52 0.415 3.29 8 8.2 0.2 306 8 5 1 39.769 79.538 0.415 3.28 8 2.3 0.0 307 6 2 3 39.812 79.623 0.416 3.28 8 60.7 10.3 308 4 8 3 39.866 79.732 0.416 3.27 8 33.2 3.1 309 2 10 3 39.898 79.797 0.416 3.27 8 1.1 0.0 310 4 13 1 39.899 79.798 0.416 3.27 8 33.5 3.1 311 2 3 4 39.961 79.921 0.417 3.26 8 21.1 1.2 312 5 12 1 40.083 80.166 0.418 3.24 8 3.6 0.0 313 2 13 2 40.271 80.541 0.42 3.22 8 48.5 6.5 314 6 3 3 40.333 80.665 0.42 3.21 8 104.3 30.0 315 7 6 2 40.357 80.714 0.42 3.21 8 1.3 0.0 316 3 14 1 40.542 81.085 0.422 3.19 8 10.4 0.3 317 3 0 4 40.572 81.143 0.422 3.19 4 119.9 19.6 318 2 15 0 40.651 81.302 0.423 3.18 4 5.2 0.0 319 3 1 4 40.675 81.351 0.423 3.17 8 0.7 0.0 320 2 4 4 40.689 81.378 0.423 3.17 8 6.8 0.1 321 1 5 4 40.697 81.394 0.423 3.17 8 6.8 0.1 322 0 15 1 40.774 81.549 0.424 3.16 4 2.0 0.0 323 0 11 3 40.845 81.69 0.425 3.16 4 58.2 4.6 324 8 7 0 40.904 81.808 0.425 3.15 4 70.2 6.6 325 8 6 1 40.913 81.826 0.425 3.15 8 2.5 0.0 326 7 9 1 40.953 81.907 0.425 3.14 8 30.3 2.5 327 3 2 4 40.987 81.973 0.426 3.14 8 24.6 1.6 328 6 9 2 41.015 82.03 0.426 3.14 8 11.7 0.4 329 6 4 3 41.059 82.119 0.426 3.13 8 57.5 8.9 330 1 15 1 41.083 82.165 0.427 3.13 8 19.7 1.0 331 5 7 3 41.089 82.178 0.427 3.13 8 0.8 0.0 332 6 11 1 41.092 82.184 0.427 3.13 8 8.4 0.2 333 1 11 3 41.153 82.307 0.427 3.12 8 10.8 0.3 334 8 0 2 41.25 82.501 0.428 3.11 4 65.5 5.7 335 4 14 0 41.344 82.688 0.429 3.1 4 85.2 9.6 336 8 1 2 41.354 82.708 0.429 3.1 8 3.5 0.0 337 4 12 2 41.379 82.759 0.429 3.1 8 151.9 61.2 338 3 10 3 41.442 82.885 0.43 3.09 8 41.1 4.5 339 3 3 4 41.504 83.009 0.43 3.09 8 26.8 1.9 340 0 6 4 41.528 83.057 0.43 3.08 4 37.0 1.8 341 2 5 4 41.621 83.242 0.431 3.07 8 7.0 0.1 342 4 9 3 41.63 83.261 0.431 3.07 8 14.9 0.6 343 8 2 2 41.664 83.328 0.432 3.07 8 69.2 12.6 344 7 7 2 41.704 83.409 0.432 3.07 8 35.9 3.4 345 5 11 2 41.769 83.538 0.432 3.06 8 23.8 1.5 346 3 13 2 41.812 83.624 0.433 3.06 8 27.1 1.9 347 1 6 4 41.836 83.672 0.433 3.05 8 75.1 14.8 348 0 14 2 41.836 83.672 0.433 3.05 4 59.4 4.6 349 6 5 3 41.99 83.98 0.434 3.04 8 20.3 1.1 350 2 15 1 42.005 84.01 0.434 3.04 8 43.3 4.9 351 2 11 3 42.076 84.151 0.435 3.03 8 33.4 2.9 352 6 12 0 42.117 84.234 0.435 3.03 4 0.0 0.0 353 1 14 2 42.143 84.286 0.436 3.03 8 29.1 2.2 354 8 3 2 42.18 84.361 0.436 3.02 8 51.9 7.0 355 3 4 4 42.227 84.454 0.436 3.02 8 53.6 7.4 356 8 7 1 42.257 84.514 0.437 3.02 8 29.6 2.3 357 9 0 1 42.418 84.835 0.438 3.0 4 63.7 5.2 358 8 8 0 42.454 84.909 0.438 3.0 4 105.2 14.2 359 9 1 1 42.521 85.041 0.439 2.99 8 30.5 2.4 360 0 16 0 42.626 85.251 0.44 2.98 2 93.4 5.6 361 5 8 3 42.638 85.276 0.44 2.98 8 15.0 0.6 362 5 13 1 42.671 85.341 0.44 2.98 8 35.2 3.2 363 4 14 1 42.695 85.389 0.44 2.98 8 56.4 8.1 364 4 0 4 42.724 85.447 0.44 2.98 4 107.6 14.8 365 2 6 4 42.756 85.511 0.441 2.97 8 13.7 0.5 366 4 1 4 42.827 85.653 0.441 2.97 8 19.2 0.9 367 9 2 1 42.83 85.659 0.441 2.97 8 26.4 1.8 368 8 4 2 42.901 85.803 0.442 2.96 8 19.2 0.9 369 7 10 1 42.915 85.83 0.442 2.96 8 12.3 0.4 370 6 10 2 42.976 85.953 0.442 2.96 8 1.2 0.0 371 2 14 2 43.062 86.124 0.443 2.95 8 50.4 6.4 372 6 6 3 43.123 86.246 0.444 2.94 8 88.5 19.7 373 4 2 4 43.135 86.27 0.444 2.94 8 48.5 5.9 374 3 5 4 43.154 86.308 0.444 2.94 8 8.7 0.2 375 1 7 4 43.175 86.351 0.444 2.94 8 27.4 1.9 376 7 8 2 43.25 86.5 0.445 2.94 8 29.0 2.1 377 9 3 1 43.344 86.688 0.446 2.93 8 20.2 1.0 378 7 0 3 43.397 86.794 0.446 2.92 4 81.1 8.2 379 6 12 1 43.464 86.928 0.447 2.92 8 41.2 4.3 380 7 1 3 43.5 86.999 0.447 2.92 8 17.1 0.7 381 1 12 3 43.525 87.05 0.447 2.92 8 50.2 6.3 382 3 15 1 43.536 87.073 0.447 2.91 8 60.7 9.2 383 4 10 3 43.588 87.176 0.448 2.91 8 33.3 2.8 384 3 11 3 43.607 87.213 0.448 2.91 8 4.4 0.0 385 4 3 4 43.649 87.299 0.448 2.91 8 33.2 2.7 386 8 8 1 43.801 87.601 0.449 2.9 8 85.2 18.0 387 7 2 3 43.808 87.616 0.449 2.9 8 62.9 9.8 388 8 5 2 43.827 87.654 0.449 2.9 8 6.7 0.1 389 2 16 0 43.849 87.698 0.45 2.89 4 70.3 6.1 390 4 13 2 43.955 87.91 0.451 2.89 8 37.3 3.4 391 9 4 1 44.063 88.127 0.451 2.88 8 25.7 1.6 392 2 7 4 44.092 88.184 0.452 2.88 8 38.6 3.7 393 5 12 2 44.136 88.273 0.452 2.88 8 12.9 0.4 394 8 9 0 44.203 88.405 0.453 2.87 4 21.9 0.6 395 1 16 1 44.277 88.553 0.453 2.87 8 14.6 0.5 396 3 6 4 44.284 88.568 0.453 2.87 8 46.6 5.3 397 7 3 3 44.321 88.643 0.454 2.86 8 26.8 1.8 398 4 15 0 44.331 88.661 0.454 2.86 4 41.1 2.1 399 4 4 4 44.368 88.736 0.454 2.86 8 24.5 1.5 400 5 9 3 44.386 88.771 0.454 2.86 8 16.5 0.7 401 0 8 4 44.411 88.822 0.454 2.86 4 55.2 3.7 402 2 12 3 44.442 88.883 0.454 2.86 8 17.7 0.8 403 6 7 3 44.459 88.918 0.455 2.86 8 5.6 0.1 404 3 14 2 44.59 89.179 0.456 2.85 8 49.5 6.0 405 6 13 0 44.688 89.376 0.456 2.84 4 24.3 0.7 406 1 8 4 44.716 89.432 0.457 2.84 8 26.6 1.7 407 8 6 2 44.956 89.912 0.459 2.83 8 55.6 7.5 408 9 5 1 44.987 89.974 0.459 2.83 8 42.7 4.4 409 7 9 2 44.996 89.992 0.459 2.83 8 4.4 0.0 X-ray diffraction powder data (I)...X-Ray wave length = 1.54056 (angs.): No H K L Theta 2*Theta d I int I int.n. I p.h.n. H(Si) ( degree ) (angstrem) *100 *100 1 0 2 0 4.856 9.712 9.0995 1256.1 74.0 75.1 5.6 2 2 0 0 8.394 16.788 5.2765 284.4 16.7 16.9 5.6 3 2 1 0 8.743 17.485 5.06779 412.4 24.3 24.5 5.6 4 0 1 1 9.14 18.28 4.84912 523.9 30.9 31.2 5.6 5 2 2 0 9.715 19.43 4.5646 160.2 9.4 9.5 5.6 6 0 4 0 9.747 19.494 4.54975 764.7 45.0 45.5 5.6 7 1 1 1 10.068 20.136 4.40621 642.3 37.8 38.2 5.6 8 1 2 1 10.927 21.855 4.06339 97.8 5.8 5.8 5.6 9 2 3 0 11.156 22.312 3.98121 354.4 20.9 21.0 5.6 10 0 3 1 11.473 22.946 3.87253 205.2 12.1 12.2 5.6 11 1 3 1 12.232 24.465 3.63548 177.0 10.4 10.5 5.6 12 2 4 0 12.918 25.835 3.44569 522.1 30.8 30.9 5.6 13 2 2 1 13.171 26.342 3.38055 724.3 42.7 42.8 5.6 14 2 3 1 14.284 28.568 3.12195 143.9 8.5 8.5 5.6 15 2 5 0 14.898 29.795 2.99611 59.0 3.5 3.5 5.6 16 0 5 1 15.142 30.283 2.94896 110.4 6.5 6.5 5.6 17 2 4 1 15.721 31.442 2.84285 1697.8 100.0 100.0 5.6 18 3 2 1 16.277 32.554 2.74824 56.0 3.3 3.3 5.6 19 4 0 0 16.976 33.951 2.63825 266.6 15.7 15.7 5.7 20 2 6 0 17.033 34.066 2.62965 36.3 2.1 2.1 5.7 21 3 3 1 17.207 34.414 2.60381 442.8 26.1 26.0 5.7 22 2 5 1 17.411 34.823 2.57421 48.8 2.9 2.9 5.7 23 4 2 0 17.697 35.395 2.5339 267.4 15.7 15.7 5.7 24 1 6 1 17.781 35.563 2.52231 92.9 5.5 5.5 5.7 25 0 0 2 17.831 35.662 2.5155 232.1 13.7 13.6 5.7 26 0 2 2 18.524 37.048 2.42456 193.7 11.4 11.4 5.7 27 2 6 1 19.3 38.601 2.3305 179.9 10.6 10.5 5.7 28 0 7 1 19.481 38.963 2.30969 23.7 1.4 1.4 5.7 29 0 8 0 19.792 39.584 2.27487 91.9 5.4 5.4 5.7 30 1 3 2 19.843 39.685 2.26929 66.4 3.9 3.9 5.7 31 4 2 1 19.899 39.799 2.26307 107.2 6.3 6.3 5.7 32 1 7 1 19.962 39.924 2.25628 120.2 7.1 7.0 5.7 33 2 1 2 19.99 39.981 2.25319 28.6 1.7 1.7 5.7 34 2 2 2 20.465 40.93 2.20311 86.0 5.1 5.0 5.7 35 4 3 1 20.688 41.377 2.18035 37.0 2.2 2.2 5.7 36 1 4 2 20.943 41.885 2.15504 138.8 8.2 8.1 5.7 37 4 5 0 21.137 42.274 2.13612 26.6 1.6 1.6 5.7 38 3 6 1 21.631 43.262 2.08961 227.8 13.4 13.3 5.7 39 3 1 2 22.261 44.522 2.03334 22.8 1.3 1.3 5.7 40 3 2 2 22.697 45.393 1.99631 172.8 10.2 10.0 5.7 41 4 6 0 22.765 45.531 1.99061 147.1 8.7 8.5 5.7 42 4 5 1 23.064 46.127 1.96623 28.7 1.7 1.7 5.7 43 0 6 2 23.442 46.884 1.93627 143.0 8.4 8.3 5.7 44 2 8 1 23.532 47.063 1.92929 373.9 22.0 21.7 5.7 45 5 2 1 23.874 47.748 1.90322 32.7 1.9 1.9 5.7 46 5 3 1 24.56 49.12 1.85323 21.7 1.3 1.3 5.7 47 4 0 2 25.03 50.061 1.82058 243.4 14.3 14.1 5.7 48 2 6 2 25.072 50.144 1.81774 77.4 4.6 4.5 5.7 49 2 9 1 25.832 51.663 1.7678 44.3 2.6 2.6 5.8 50 6 2 0 26.491 52.982 1.72687 58.9 3.5 3.4 5.8 51 2 10 0 26.598 53.195 1.72044 23.8 1.4 1.4 5.8 52 5 5 1 26.667 53.333 1.71631 38.5 2.3 2.2 5.8 53 3 6 2 27.007 54.014 1.69627 40.1 2.4 2.3 5.8 54 4 4 2 27.111 54.222 1.69028 128.4 7.6 7.4 5.8 55 0 8 2 27.163 54.327 1.68725 20.8 1.2 1.2 5.8 56 1 8 2 27.537 55.075 1.66609 119.5 7.0 6.9 5.8 57 6 0 1 27.642 55.283 1.6603 19.8 1.2 1.1 5.8 58 3 9 1 27.729 55.458 1.65547 78.9 4.6 4.5 5.8 59 6 2 1 28.138 56.276 1.63333 35.6 2.1 2.0 5.8 60 4 8 1 28.202 56.405 1.62992 68.2 4.0 3.9 5.8 61 2 10 1 28.241 56.481 1.62789 38.5 2.3 2.2 5.8 62 0 3 3 28.46 56.92 1.61637 54.0 3.2 3.1 5.8 63 5 2 2 28.938 57.876 1.59193 110.7 6.5 6.3 5.8 64 5 3 2 29.54 59.081 1.56232 24.3 1.4 1.4 5.8 65 6 4 1 29.595 59.19 1.55969 185.7 10.9 10.6 5.8 66 5 7 1 29.629 59.258 1.55806 21.3 1.3 1.2 5.8 67 1 11 1 29.704 59.407 1.55451 28.0 1.6 1.6 5.8 68 0 5 3 30.38 60.759 1.52311 27.3 1.6 1.6 5.8 69 6 6 0 30.415 60.829 1.52153 136.0 8.0 7.7 5.8 70 0 12 0 30.524 61.049 1.51658 129.2 7.6 7.4 5.8 71 3 0 3 30.587 61.174 1.51378 29.7 1.7 1.7 5.8 72 1 5 3 30.728 61.457 1.50749 143.1 8.4 8.1 5.8 73 4 10 0 30.943 61.886 1.49805 96.2 5.7 5.5 5.8 74 3 2 3 31.054 62.107 1.49325 23.7 1.4 1.3 5.8 75 0 10 2 31.494 62.988 1.47448 67.3 4.0 3.8 5.9 76 2 5 3 31.761 63.522 1.46336 21.5 1.3 1.2 5.9 77 6 6 1 31.931 63.862 1.45639 38.2 2.3 2.2 5.9 78 1 6 3 31.999 63.997 1.45363 30.3 1.8 1.7 5.9 79 4 10 1 32.446 64.891 1.43576 110.0 6.5 6.2 5.9 80 5 6 2 32.674 65.349 1.4268 40.4 2.4 2.3 5.9 81 4 8 2 32.814 65.627 1.42142 77.6 4.6 4.4 5.9 82 4 0 3 32.974 65.948 1.41528 25.3 1.5 1.4 5.9 83 2 6 3 33.009 66.018 1.41395 58.0 3.4 3.3 5.9 84 4 1 3 33.086 66.173 1.41102 39.6 2.3 2.2 5.9 85 2 12 1 33.381 66.761 1.4 37.9 2.2 2.1 5.9 86 6 4 2 34.095 68.189 1.37412 41.6 2.5 2.3 5.9 87 3 10 2 34.503 69.005 1.35985 25.4 1.5 1.4 5.9 88 3 6 3 34.659 69.319 1.35446 67.2 4.0 3.8 5.9 89 6 8 1 35.055 70.11 1.3411 58.9 3.5 3.3 5.9 90 6 9 0 35.481 70.962 1.32707 22.2 1.3 1.2 5.9 91 8 0 0 35.728 71.455 1.31913 31.9 1.9 1.8 5.9 92 4 12 0 35.863 71.725 1.31482 45.3 2.7 2.5 5.9 93 2 8 3 36.087 72.174 1.30774 43.1 2.5 2.4 5.9 94 6 6 2 36.275 72.549 1.3019 21.8 1.3 1.2 6.0 95 0 12 2 36.375 72.751 1.2988 25.6 1.5 1.4 6.0 96 0 9 3 36.636 73.272 1.29084 24.9 1.5 1.4 6.0 97 8 3 0 36.697 73.393 1.289 30.1 1.8 1.7 6.0 98 4 10 2 36.76 73.519 1.2871 25.3 1.5 1.4 6.0 99 8 0 1 37.133 74.267 1.27599 25.0 1.5 1.4 6.0 100 8 2 1 37.559 75.118 1.26363 47.1 2.8 2.6 6.0 101 3 8 3 37.677 75.354 1.26026 21.2 1.2 1.2 6.0 102 1 2 4 38.502 77.004 1.23731 71.8 4.2 4.0 6.0 103 2 14 1 38.99 77.98 1.22425 70.4 4.1 3.9 6.0 104 5 10 2 39.588 79.176 1.20873 28.2 1.7 1.6 6.0 105 6 3 3 40.333 80.665 1.19013 30.0 1.8 1.6 6.1 106 3 0 4 40.572 81.143 1.18432 19.6 1.2 1.1 6.1 107 4 12 2 41.379 82.759 1.16525 61.2 3.6 3.3 6.1 108 0 14 2 41.836 83.672 1.15484 21.3 1.3 1.2 6.1 109 4 0 4 42.724 85.447 1.13533 26.0 1.5 1.4 6.1 110 6 6 3 43.123 86.246 1.12685 25.7 1.5 1.4 6.1 111 8 8 1 43.801 87.601 1.11288 28.0 1.6 1.5 6.2 Reference: Chichagov A.V. et al. Information-Calculating System on Crystal Structure Data of Minerals (MINCRYST) - Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian) |