Institute of Experimental Mineralogy Russian Academy of Sciences ------------------------------------------------- 142432, Chernogolovka, Moscow district A.V. Chichagov +7(496)52-22320 *** *** W W W - X R A Y P O L *** *********************** HOPEITE 1, f-hopeite Zn(3)[PO(4)](2).4H(2)O Orthorhombic P nma Z = 4 R =0.068 NR =1471 14 .10 .1993 Ref.Str.: Whitaker A.(1975) * Acta Cryst., B 31, 2026-2035 Reserv: T.V.Ush. Initial data from BDM-file Lattice parameters (cub. angs.,degr.): a = 10.629 alpha = 90.0 b = 18.339 beta = 90.0 c = 5.04 gamma = 90.0 Unit cell volume (cub. angs.) = 982.42 Molar volume ( cub.cm/mol.) = 147.94 Co-ordinates, thermal parameters, occupation for atomic positions: NoP x/a y/b z/c B(j) atom / occupation 1 0.2362 0.25 0.5728 0.0 Zn = 1.00 2 0.1427 0.9991 0.2077 0.0 Zn = 1.00 3 0.1028 0.0942 0.7259 0.0 P = 1.00 4 0.1074 0.25 0.2573 0.0 O = 1.00 5 0.3861 0.25 0.849 0.0 O = 1.00 6 0.3352 0.1698 0.3392 0.0 O = 1.00 7 0.1401 0.1726 0.7847 0.0 O = 1.00 8 0.1 0.0799 0.4298 0.0 O = 1.00 9 0.4755 0.0787 0.6414 0.0 O = 1.00 10 0.198 0.0407 0.8607 0.0 O = 1.00 11 0.122 0.188 0.121 0.0 H = 1.00 12 0.456 0.198 0.792 0.0 H = 1.00 13 0.233 0.134 0.248 0.0 H = 1.00 14 0.396 0.136 0.493 0.0 H = 1.00 Co-ordinates for all atomic positions : No NoP x/a y/b z/c 1 1 0.2362 0.25 0.5728 2 2 0.1427 0.9991 0.2077 3 3 0.1028 0.0942 0.7259 4 4 0.1074 0.25 0.2573 5 5 0.3861 0.25 0.849 6 6 0.3352 0.1698 0.3392 7 7 0.1401 0.1726 0.7847 8 8 0.1 0.0799 0.4298 9 9 0.4755 0.0787 0.6414 10 10 0.198 0.0407 0.8607 11 11 0.122 0.188 0.121 12 12 0.456 0.198 0.792 13 13 0.233 0.134 0.248 14 14 0.396 0.136 0.493 15 1 0.2638 0.75 0.0728 16 2 0.3573 0.0009 0.7077 17 3 0.3972 0.9058 0.2259 18 4 0.3926 0.75 0.7573 19 5 0.1139 0.75 0.349 20 6 0.1648 0.8302 0.8392 21 7 0.3599 0.8274 0.2847 22 8 0.4 0.9201 0.9298 23 9 0.0245 0.9213 0.1414 24 10 0.302 0.9593 0.3607 25 11 0.378 0.812 0.621 26 12 0.044 0.802 0.292 27 13 0.267 0.866 0.748 28 14 0.104 0.864 0.993 29 2 0.3573 0.4991 0.7077 30 3 0.3972 0.5942 0.2259 31 6 0.1648 0.6698 0.8392 32 7 0.3599 0.6726 0.2847 33 8 0.4 0.5799 0.9298 34 9 0.0245 0.5787 0.1414 35 10 0.302 0.5407 0.3607 36 11 0.378 0.688 0.621 37 12 0.044 0.698 0.292 38 13 0.267 0.634 0.748 39 14 0.104 0.636 0.993 40 2 0.1427 0.5009 0.2077 41 3 0.1028 0.4058 0.7259 42 6 0.3352 0.3302 0.3392 43 7 0.1401 0.3274 0.7847 44 8 0.1 0.4201 0.4298 45 9 0.4755 0.4213 0.6414 46 10 0.198 0.4593 0.8607 47 11 0.122 0.312 0.121 48 12 0.456 0.302 0.792 49 13 0.233 0.366 0.248 50 14 0.396 0.364 0.493 51 1 0.7362 0.25 0.9272 52 2 0.6427 0.9991 0.2923 53 3 0.6029 0.0942 0.7741 54 4 0.6074 0.25 0.2427 55 5 0.8861 0.25 0.651 56 6 0.8352 0.1698 0.1608 57 7 0.6401 0.1726 0.7153 58 8 0.6 0.0799 0.0702 59 9 0.9755 0.0787 0.8586 60 10 0.698 0.0407 0.6393 61 11 0.622 0.188 0.379 62 12 0.956 0.198 0.708 63 13 0.733 0.134 0.252 64 14 0.896 0.136 0.007 65 1 0.7638 0.75 0.4272 66 2 0.8573 0.0009 0.7923 67 3 0.8972 0.9058 0.2741 68 4 0.8926 0.75 0.7427 69 5 0.6139 0.75 0.151 70 6 0.6648 0.8302 0.6608 71 7 0.8599 0.8274 0.2153 72 8 0.9 0.9201 0.5702 73 9 0.5245 0.9213 0.3586 74 10 0.802 0.9593 0.1393 75 11 0.878 0.812 0.879 76 12 0.544 0.802 0.208 77 13 0.767 0.866 0.752 78 14 0.604 0.864 0.507 79 2 0.8573 0.4991 0.7923 80 3 0.8972 0.5942 0.2741 81 6 0.6648 0.6698 0.6608 82 7 0.8599 0.6726 0.2153 83 8 0.9 0.5799 0.5702 84 9 0.5245 0.5787 0.3586 85 10 0.802 0.5407 0.1393 86 11 0.878 0.688 0.879 87 12 0.544 0.698 0.208 88 13 0.767 0.634 0.752 89 14 0.604 0.636 0.507 90 2 0.6427 0.5009 0.2923 91 3 0.6028 0.4058 0.7741 92 6 0.8352 0.3302 0.1608 93 7 0.6401 0.3274 0.7153 94 8 0.6 0.4201 0.0702 95 9 0.9755 0.4213 0.8586 96 10 0.698 0.4593 0.6393 97 11 0.622 0.312 0.379 98 12 0.956 0.302 0.708 99 13 0.733 0.366 0.252 100 14 0.896 0.364 0.007 X-ray density (g/cm cub.) = 3.1 MU (1/cm) = 125.909 Mass attenuation coefficient (cm**2/g) = 40.662 Selected interatomic distances (cation-anion,anion-anion): NoP Atom Rad.sph. C.N. Distance NoP N. (angs.) (angs.) 1 Zn 2.628 6 2.0985 4 2.1161 5 2.1586 6 2.0481 7 2.1586 6 2.0481 7 2 Zn 2.628 4 1.9118 8 1.9961 10 1.9301 9 1.9992 10 3 P 2.232 4 1.5211 7 1.5152 8 1.5644 10 1.5363 9 4 O 3.264 9 2.8635 6 3.0327 7 2.7943 7 3.2386 8 2.8635 6 3.0327 7 2.7943 7 3.2386 8 3.0767 5 5 O 3.264 9 2.9259 6 3.0101 6 2.9927 7 2.9259 6 3.0101 6 2.9927 7 3.0767 4 3.1229 7 3.1229 7 6 O 3.264 7 2.8635 4 3.0101 5 2.9259 5 3.0569 7 3.0283 8 2.7084 9 2.9427 6 7 O 3.264 9 2.7943 4 3.0327 4 2.9927 5 3.0569 6 2.504 8 2.5265 10 2.837 7 3.1229 5 2.4838 9 8 O 3.264 8 3.2386 4 3.0283 6 2.504 7 2.5134 10 3.1354 10 3.1022 10 2.5342 9 3.1687 9 9 O 3.264 8 2.7084 6 3.2265 10 3.1925 10 2.4838 7 2.5342 8 3.1687 8 2.4649 10 3.2601 9 10 O 3.264 9 2.5265 7 3.1354 8 2.5134 8 3.2265 9 3.1022 8 3.1925 9 3.1304 10 3.1304 10 2.4649 9 11 H 1.632 1 1.3375 4 12 H 1.632 1 1.2423 5 13 H 1.632 1 1.3497 6 14 H 1.632 2 1.1841 6 1.5425 9 X-ray diffraction powder data (II), X-Ray W.L. = 1.54056(angs.): No H K L Theta 2*Theta S LPG MF F I int. ( degree ) *100 1 0 2 0 4.819 9.638 0.055 280.44 2 133.0 1028.1 2 2 0 0 8.334 16.668 0.094 92.26 2 121.4 281.9 3 2 1 0 8.679 17.358 0.098 84.89 4 106.9 402.2 4 0 1 1 9.12 18.24 0.103 76.68 4 125.4 499.4 5 2 2 0 9.644 19.288 0.109 68.34 4 73.8 154.1 6 0 4 0 9.672 19.344 0.109 67.93 2 220.5 684.4 7 1 0 1 9.738 19.476 0.11 66.99 4 35.8 35.6 8 1 1 1 10.037 20.074 0.113 62.93 8 110.3 634.1 9 1 2 1 10.886 21.772 0.123 53.17 8 43.1 82.0 10 2 3 0 11.073 22.145 0.125 51.33 4 127.9 348.2 11 0 3 1 11.425 22.849 0.129 48.08 4 100.5 201.3 12 2 0 1 12.159 24.319 0.137 42.2 4 60.8 64.6 13 1 3 1 12.176 24.353 0.137 42.08 8 56.4 110.8 14 2 1 1 12.403 24.805 0.139 40.49 8 5.3 1.0 15 2 4 0 12.82 25.64 0.144 37.76 4 179.4 503.6 16 2 2 1 13.107 26.213 0.147 36.04 8 152.5 694.6 17 1 4 1 13.792 27.585 0.155 32.35 8 15.9 6.7 18 2 3 1 14.208 28.416 0.159 30.37 8 78.7 155.8 19 0 6 0 14.597 29.193 0.164 28.67 2 27.9 4.6 20 2 5 0 14.784 29.567 0.166 27.9 4 75.2 65.5 21 0 5 1 15.054 30.109 0.169 26.84 4 110.1 134.9 22 3 0 1 15.412 30.823 0.173 25.52 4 35.1 13.1 23 3 1 1 15.608 31.216 0.175 24.83 8 58.0 69.3 24 2 4 1 15.63 31.261 0.175 24.76 8 282.7 1640.0 25 1 5 1 15.644 31.288 0.175 24.71 8 54.3 60.5 26 3 2 1 16.183 32.367 0.181 22.97 8 50.8 49.2 27 4 0 0 16.851 33.701 0.188 21.04 2 256.8 287.6 28 2 6 0 16.901 33.802 0.189 20.9 4 70.2 42.7 29 4 1 0 17.032 34.064 0.19 20.56 4 0.6 0.0 30 3 3 1 17.104 34.209 0.191 20.37 8 171.5 496.6 31 2 5 1 17.304 34.608 0.193 19.86 8 61.5 62.3 32 4 2 0 17.566 35.132 0.196 19.22 4 185.3 273.4 33 1 6 1 17.669 35.338 0.197 18.97 8 84.0 110.9 34 0 0 2 17.798 35.597 0.198 18.67 2 266.2 274.2 35 1 0 2 18.309 36.618 0.204 17.55 4 40.1 11.7 36 3 4 1 18.325 36.65 0.204 17.52 8 30.5 13.5 37 4 3 0 18.426 36.852 0.205 17.31 4 42.0 12.7 38 1 1 2 18.478 36.955 0.206 17.2 8 6.5 0.6 39 0 2 2 18.482 36.963 0.206 17.19 4 171.4 209.4 40 1 2 2 18.976 37.953 0.211 16.22 8 2.5 0.1 41 4 0 1 19.129 38.259 0.213 15.93 4 22.5 3.4 42 2 7 0 19.135 38.271 0.213 15.92 4 64.6 27.5 43 2 6 1 19.174 38.349 0.213 15.85 8 108.9 155.7 44 4 1 1 19.292 38.584 0.214 15.64 8 6.7 0.6 45 0 7 1 19.352 38.703 0.215 15.53 4 59.9 23.1 46 4 4 0 19.575 39.151 0.217 15.14 4 35.1 7.7 47 0 8 0 19.634 39.269 0.218 15.04 2 173.3 93.6 48 2 0 2 19.773 39.545 0.22 14.81 4 22.0 3.0 49 4 2 1 19.773 39.546 0.22 14.81 8 99.9 122.6 50 1 3 2 19.784 39.567 0.22 14.79 8 80.8 80.0 51 3 5 1 19.799 39.598 0.22 14.76 8 39.3 18.9 52 1 7 1 19.828 39.656 0.22 14.72 8 102.3 127.5 53 2 1 2 19.931 39.862 0.221 14.55 8 54.0 35.2 54 2 2 2 20.399 40.799 0.226 13.81 8 80.9 74.9 55 0 4 2 20.414 40.827 0.226 13.79 4 60.3 20.8 56 4 3 1 20.554 41.108 0.228 13.58 8 61.5 42.5 57 1 4 2 20.87 41.74 0.231 13.13 8 116.2 147.0 58 4 5 0 20.975 41.95 0.232 12.98 4 68.4 25.1 59 2 3 2 21.161 42.323 0.234 12.73 8 40.9 17.6 60 2 7 1 21.203 42.407 0.235 12.67 8 3.2 0.1 61 2 8 0 21.466 42.931 0.238 12.33 4 121.2 75.1 62 3 6 1 21.484 42.968 0.238 12.3 8 136.1 188.8 63 4 4 1 21.608 43.217 0.239 12.14 8 26.3 7.0 64 3 0 2 22.03 44.061 0.243 11.63 4 21.4 2.2 65 1 8 1 22.098 44.196 0.244 11.55 8 0.1 0.0 66 3 1 2 22.175 44.351 0.245 11.46 8 53.9 27.6 67 2 4 2 22.192 44.384 0.245 11.44 8 17.5 2.9 68 1 5 2 22.202 44.404 0.245 11.42 8 37.8 13.5 69 4 6 0 22.589 45.177 0.249 10.99 4 191.0 166.1 70 3 2 2 22.606 45.212 0.25 10.97 8 143.2 186.4 71 4 5 1 22.906 45.812 0.253 10.65 8 65.5 37.8 72 5 0 1 23.158 46.315 0.255 10.39 4 58.7 14.8 73 5 1 1 23.297 46.594 0.257 10.25 8 70.6 42.3 74 3 3 2 23.309 46.619 0.257 10.23 8 17.1 2.5 75 0 6 2 23.338 46.677 0.257 10.21 4 168.1 119.6 76 3 7 1 23.348 46.697 0.257 10.2 8 63.5 34.1 77 2 8 1 23.364 46.729 0.257 10.18 8 214.2 387.2 78 2 5 2 23.464 46.928 0.258 10.08 8 15.6 2.0 79 5 2 1 23.712 47.423 0.261 9.85 8 61.6 31.0 80 1 6 2 23.749 47.498 0.261 9.81 8 28.9 6.8 81 2 9 0 23.882 47.764 0.263 9.69 4 70.5 20.0 82 0 9 1 24.063 48.127 0.265 9.52 4 22.2 1.9 83 3 4 2 24.268 48.536 0.267 9.34 8 38.4 11.4 84 4 7 0 24.386 48.773 0.268 9.24 4 26.9 2.8 85 5 3 1 24.391 48.781 0.268 9.23 8 55.1 23.2 86 4 6 1 24.419 48.837 0.268 9.21 8 40.1 12.3 87 1 9 1 24.465 48.93 0.269 9.17 8 25.5 4.9 88 0 10 0 24.836 49.672 0.273 8.86 2 87.3 14.0 89 4 0 2 24.914 49.829 0.273 8.8 4 258.6 243.8 90 2 6 2 24.951 49.902 0.274 8.77 8 115.2 96.4 91 4 1 2 25.046 50.093 0.275 8.69 8 32.6 7.7 92 5 4 1 25.318 50.637 0.278 8.48 8 45.5 14.6 93 3 8 1 25.367 50.733 0.278 8.45 8 6.9 0.3 94 4 2 2 25.439 50.879 0.279 8.39 8 45.2 14.2 95 3 5 2 25.46 50.921 0.279 8.37 8 6.1 0.3 96 1 7 2 25.484 50.969 0.279 8.36 8 16.9 2.0 97 2 9 1 25.642 51.283 0.281 8.24 8 90.8 56.3 98 6 0 0 25.774 51.547 0.282 8.14 2 12.0 0.2 99 6 1 0 25.903 51.805 0.284 8.05 4 26.6 2.4 100 4 3 2 26.085 52.17 0.285 7.93 8 4.5 0.1 101 4 7 1 26.121 52.242 0.286 7.9 8 5.1 0.2 102 6 2 0 26.286 52.573 0.287 7.79 4 142.1 65.2 103 4 8 0 26.345 52.69 0.288 7.75 4 69.5 15.5 104 2 10 0 26.38 52.761 0.288 7.72 4 98.2 30.9 105 5 5 1 26.476 52.952 0.289 7.66 8 84.7 45.6 106 2 7 2 26.628 53.257 0.291 7.56 8 36.7 8.4 107 3 6 2 26.865 53.731 0.293 7.41 8 94.1 54.4 108 6 3 0 26.918 53.835 0.294 7.38 4 103.3 32.6 109 1 10 1 26.924 53.847 0.294 7.37 8 18.1 2.0 110 4 4 2 26.97 53.941 0.294 7.35 8 142.8 124.2 111 0 8 2 27.017 54.033 0.295 7.32 4 82.5 20.7 112 1 8 2 27.387 54.773 0.299 7.09 8 153.3 138.1 113 0 1 3 27.414 54.828 0.299 7.08 4 27.6 2.2 114 6 0 1 27.445 54.89 0.299 7.06 4 90.9 24.2 115 3 9 1 27.522 55.044 0.3 7.01 8 103.9 62.8 116 6 1 1 27.568 55.137 0.3 6.99 8 45.4 11.9 117 1 0 3 27.658 55.316 0.301 6.94 4 102.6 30.2 118 1 1 3 27.781 55.561 0.303 6.87 8 11.7 0.8 119 6 4 0 27.785 55.569 0.303 6.86 4 42.0 5.0 120 5 6 1 27.845 55.69 0.303 6.83 8 39.3 8.7 121 6 2 1 27.936 55.872 0.304 6.78 8 86.5 42.0 122 4 8 1 27.993 55.985 0.305 6.75 8 94.3 49.8 123 2 10 1 28.026 56.053 0.305 6.73 8 89.8 45.0 124 4 5 2 28.08 56.161 0.306 6.7 8 12.8 0.9 125 1 2 3 28.147 56.294 0.306 6.67 8 82.5 37.6 126 5 0 2 28.298 56.596 0.308 6.59 4 44.9 5.5 127 0 3 3 28.392 56.784 0.309 6.54 4 157.5 67.2 128 5 1 2 28.419 56.838 0.309 6.52 8 7.7 0.3 129 4 9 0 28.449 56.897 0.309 6.51 4 75.1 15.2 130 3 7 2 28.463 56.927 0.309 6.5 8 47.4 12.1 131 2 8 2 28.477 56.955 0.31 6.49 8 27.0 3.9 132 6 3 1 28.542 57.085 0.31 6.46 8 8.7 0.4 133 2 0 3 28.742 57.484 0.312 6.36 4 18.8 0.9 134 1 3 3 28.75 57.5 0.312 6.35 8 24.2 3.1 135 5 2 2 28.78 57.559 0.313 6.34 8 140.2 103.3 136 2 1 3 28.862 57.723 0.313 6.3 8 76.3 30.4 137 6 5 0 28.874 57.747 0.313 6.29 4 51.9 7.0 138 2 11 0 28.962 57.924 0.314 6.25 4 11.5 0.3 139 0 11 1 29.12 58.241 0.316 6.17 4 4.4 0.0 140 2 2 3 29.219 58.438 0.317 6.13 8 58.2 17.2 141 5 3 2 29.375 58.749 0.318 6.05 8 52.4 13.8 142 6 4 1 29.378 58.755 0.318 6.05 8 212.3 226.1 143 4 6 2 29.399 58.798 0.319 6.04 8 54.2 14.7 144 5 7 1 29.408 58.815 0.319 6.04 8 74.4 27.7 145 1 9 2 29.44 58.88 0.319 6.02 8 37.9 7.2 146 1 11 1 29.473 58.946 0.319 6.01 8 85.1 36.1 147 1 4 3 29.581 59.163 0.32 5.96 8 53.0 13.9 148 3 10 1 29.804 59.608 0.323 5.86 8 27.6 3.7 149 2 3 3 29.808 59.617 0.323 5.86 8 45.3 10.0 150 4 9 1 30.019 60.038 0.325 5.77 8 51.0 12.4 151 6 6 0 30.17 60.34 0.326 5.7 4 267.2 168.7 152 5 4 2 30.195 60.39 0.326 5.69 8 34.4 5.6 153 3 8 2 30.238 60.476 0.327 5.67 8 34.9 5.7 154 0 12 0 30.267 60.534 0.327 5.66 2 375.0 164.9 155 0 5 3 30.285 60.571 0.327 5.65 4 102.6 24.6 156 6 5 1 30.43 60.86 0.329 5.59 8 0.2 0.0 157 2 9 2 30.483 60.966 0.329 5.57 8 36.1 6.0 158 3 0 3 30.493 60.986 0.329 5.57 4 124.9 36.0 159 2 11 1 30.516 61.031 0.33 5.56 8 11.8 0.6 160 3 1 3 30.608 61.217 0.331 5.52 8 14.9 1.0 161 2 4 3 30.622 61.244 0.331 5.52 8 188.1 161.8 162 1 5 3 30.63 61.26 0.331 5.51 8 49.1 11.0 163 4 10 0 30.687 61.373 0.331 5.49 4 224.0 114.1 164 4 7 2 30.912 61.824 0.333 5.4 8 47.4 10.1 165 3 2 3 30.953 61.907 0.334 5.39 8 74.4 24.7 166 5 8 1 31.149 62.298 0.336 5.31 8 65.4 18.8 167 5 5 2 31.231 62.462 0.337 5.28 8 29.7 3.9 168 0 10 2 31.297 62.594 0.337 5.26 4 192.8 81.0 169 3 3 3 31.523 63.047 0.339 5.17 8 39.7 6.8 170 2 12 0 31.631 63.263 0.34 5.13 4 44.0 4.1 171 1 10 2 31.635 63.27 0.34 5.13 8 50.4 10.8 172 2 5 3 31.65 63.299 0.341 5.13 8 78.0 25.8 173 6 7 0 31.661 63.322 0.341 5.12 4 19.1 0.8 174 6 6 1 31.688 63.376 0.341 5.11 8 96.8 39.7 175 1 6 3 31.883 63.767 0.343 5.05 8 90.2 34.0 176 7 0 1 31.993 63.985 0.344 5.01 4 91.1 17.2 177 7 1 1 32.105 64.21 0.345 4.97 8 46.7 9.0 178 6 0 2 32.107 64.215 0.345 4.97 4 100.6 20.8 179 1 12 1 32.117 64.234 0.345 4.97 8 6.2 0.2 180 3 9 2 32.177 64.354 0.346 4.95 8 24.4 2.4 181 4 10 1 32.19 64.381 0.346 4.94 8 129.3 68.5 182 3 11 1 32.209 64.417 0.346 4.94 8 51.4 10.8 183 6 1 2 32.219 64.439 0.346 4.93 8 68.0 18.9 184 3 4 3 32.312 64.623 0.347 4.9 8 95.2 36.8 185 7 2 1 32.441 64.882 0.348 4.86 8 7.8 0.2 186 5 6 2 32.471 64.943 0.348 4.85 8 110.1 48.7 187 6 2 2 32.555 65.109 0.349 4.82 8 27.4 3.0 188 4 8 2 32.606 65.212 0.35 4.81 8 156.1 97.0 189 2 10 2 32.637 65.274 0.35 4.8 8 47.4 8.9 190 4 0 3 32.851 65.701 0.352 4.73 4 122.4 29.4 191 2 6 3 32.881 65.763 0.352 4.72 8 136.6 73.0 192 4 1 3 32.961 65.923 0.353 4.7 8 114.7 51.2 193 7 3 1 32.997 65.993 0.354 4.69 8 15.4 0.9 194 0 7 3 33.002 66.005 0.354 4.68 4 47.2 4.3 195 4 11 0 33.054 66.108 0.354 4.67 4 12.0 0.3 196 5 9 1 33.058 66.116 0.354 4.67 8 47.5 8.7 197 6 3 2 33.109 66.219 0.355 4.65 8 0.0 0.0 198 2 12 1 33.111 66.223 0.355 4.65 8 91.3 32.1 199 6 7 1 33.14 66.28 0.355 4.64 8 58.7 13.3 200 4 2 3 33.293 66.585 0.356 4.6 8 63.1 15.2 201 3 5 3 33.31 66.621 0.356 4.59 8 32.9 4.1 202 1 7 3 33.331 66.662 0.357 4.59 8 4.1 0.1 203 6 8 0 33.334 66.669 0.357 4.59 4 22.6 1.0 204 7 4 1 33.767 67.533 0.361 4.46 8 48.5 8.7 205 4 3 3 33.841 67.682 0.361 4.44 8 36.2 4.8 206 6 4 2 33.878 67.756 0.362 4.43 8 115.6 49.1 207 5 7 2 33.906 67.812 0.362 4.42 8 10.6 0.4 208 1 11 2 33.966 67.933 0.363 4.41 8 12.6 0.6 209 3 10 2 34.273 68.545 0.366 4.33 8 96.5 33.4 210 2 7 3 34.307 68.614 0.366 4.32 8 70.4 17.7 211 2 13 0 34.398 68.796 0.367 4.29 4 72.4 9.3 212 4 9 2 34.472 68.944 0.367 4.28 8 6.4 0.1 213 4 11 1 34.502 69.005 0.368 4.27 8 60.2 12.8 214 3 6 3 34.511 69.023 0.368 4.27 8 161.4 92.1 215 0 13 1 34.542 69.085 0.368 4.26 4 101.6 18.2 216 4 4 3 34.602 69.204 0.369 4.24 8 34.4 4.2 217 3 12 1 34.736 69.472 0.37 4.21 8 8.7 0.3 218 7 5 1 34.744 69.489 0.37 4.21 8 68.3 16.2 219 6 8 1 34.777 69.553 0.37 4.2 8 150.6 79.0 220 6 5 2 34.854 69.709 0.371 4.18 8 9.5 0.3 221 1 13 1 34.864 69.728 0.371 4.18 8 75.7 19.8 222 2 11 2 34.934 69.868 0.372 4.16 8 11.2 0.4 223 1 8 3 34.963 69.926 0.372 4.15 8 9.6 0.3 224 5 10 1 35.127 70.254 0.373 4.11 8 13.2 0.6 225 6 9 0 35.181 70.363 0.374 4.1 4 141.7 34.1 226 8 0 0 35.433 70.867 0.376 4.04 2 187.5 29.4 227 5 8 2 35.525 71.051 0.377 4.02 8 44.3 6.5 228 8 1 0 35.54 71.081 0.377 4.02 4 111.6 20.8 229 4 12 0 35.552 71.104 0.377 4.02 4 162.2 43.8 230 4 5 3 35.569 71.138 0.378 4.01 8 60.4 12.1 231 5 0 3 35.76 71.521 0.379 3.97 4 65.1 7.0 232 2 13 1 35.82 71.641 0.38 3.96 8 6.9 0.2 233 8 2 0 35.86 71.721 0.38 3.95 4 8.1 0.1 234 5 1 3 35.867 71.734 0.38 3.95 8 8.1 0.2 235 3 7 3 35.906 71.812 0.381 3.94 8 20.4 1.4 236 2 8 3 35.918 71.837 0.381 3.94 8 136.7 61.0 237 7 6 1 35.923 71.845 0.381 3.94 8 0.2 0.0 238 0 14 0 36.017 72.035 0.382 3.92 2 10.4 0.1 239 6 6 2 36.031 72.062 0.382 3.91 8 93.6 28.4 240 0 12 2 36.119 72.239 0.383 3.89 4 146.7 34.7 241 5 2 3 36.186 72.371 0.383 3.88 8 6.9 0.2 242 7 0 2 36.318 72.635 0.384 3.85 4 44.3 3.1 243 8 3 0 36.391 72.782 0.385 3.84 4 69.8 7.8 244 7 1 2 36.423 72.847 0.385 3.83 8 23.7 1.8 245 1 12 2 36.435 72.87 0.386 3.83 8 91.7 26.7 246 0 9 3 36.459 72.917 0.386 3.82 4 155.7 38.4 247 4 10 2 36.504 73.008 0.386 3.82 8 88.8 24.9 248 3 11 2 36.521 73.042 0.386 3.81 8 52.0 8.5 249 6 9 1 36.59 73.181 0.387 3.8 8 6.8 0.1 250 5 3 3 36.714 73.429 0.388 3.77 8 19.6 1.2 251 4 6 3 36.736 73.473 0.388 3.77 8 31.6 3.1 252 7 2 2 36.74 73.481 0.388 3.77 8 40.3 5.1 253 1 9 3 36.773 73.546 0.389 3.76 8 44.9 6.3 254 8 0 1 36.839 73.677 0.389 3.75 4 137.9 29.5 255 8 1 1 36.944 73.888 0.39 3.73 8 56.7 9.9 256 4 12 1 36.955 73.911 0.39 3.73 8 34.9 3.8 257 8 4 0 37.129 74.258 0.392 3.7 4 107.1 17.6 258 6 10 0 37.197 74.394 0.392 3.68 4 84.3 10.8 259 8 2 1 37.259 74.518 0.393 3.67 8 146.2 65.1 260 7 3 2 37.266 74.532 0.393 3.67 8 28.5 2.5 261 2 14 0 37.274 74.549 0.393 3.67 4 78.0 9.2 262 7 7 1 37.295 74.591 0.393 3.67 8 53.7 8.8 263 5 9 2 37.324 74.648 0.394 3.66 8 5.7 0.1 264 5 11 1 37.353 74.707 0.394 3.66 8 59.4 10.7 265 2 12 2 37.375 74.75 0.394 3.65 8 23.9 1.7 266 3 13 1 37.392 74.784 0.394 3.65 8 50.3 7.7 267 6 7 2 37.402 74.805 0.394 3.65 8 46.4 6.5 268 5 4 3 37.45 74.9 0.395 3.64 8 20.0 1.2 269 3 8 3 37.489 74.977 0.395 3.63 8 55.3 9.2 270 0 0 4 37.686 75.372 0.397 3.6 2 52.1 2.0 271 2 9 3 37.71 75.419 0.397 3.59 8 57.0 9.7 272 1 14 1 37.725 75.45 0.397 3.59 8 22.1 1.4 273 8 3 1 37.782 75.564 0.398 3.58 8 4.5 0.1 274 1 0 4 37.997 75.993 0.4 3.54 4 17.1 0.4 275 7 4 2 37.998 75.995 0.4 3.54 8 33.5 3.3 276 8 5 0 38.07 76.14 0.4 3.53 4 90.8 12.1 277 4 7 3 38.098 76.196 0.401 3.53 8 69.2 14.0 278 1 1 4 38.101 76.201 0.401 3.53 8 17.1 0.9 279 0 2 4 38.103 76.206 0.401 3.53 4 59.4 5.2 280 4 13 0 38.185 76.37 0.401 3.51 4 35.4 1.8 281 5 5 3 38.388 76.776 0.403 3.48 8 7.7 0.2 282 1 2 4 38.413 76.825 0.403 3.48 8 179.1 92.5 283 8 4 1 38.511 77.021 0.404 3.46 8 74.8 16.0 284 6 10 1 38.578 77.155 0.405 3.45 8 11.4 0.4 285 2 14 1 38.654 77.308 0.405 3.44 8 180.2 92.6 286 4 11 2 38.7 77.4 0.406 3.43 8 3.0 0.0 287 1 10 3 38.757 77.513 0.406 3.43 8 39.9 4.5 288 7 8 1 38.857 77.714 0.407 3.41 8 49.6 6.9 289 2 0 4 38.923 77.847 0.408 3.4 4 17.0 0.4 290 3 12 2 38.924 77.847 0.408 3.4 8 43.8 5.4 291 1 3 4 38.931 77.861 0.408 3.4 8 35.7 3.6 292 7 5 2 38.932 77.863 0.408 3.4 8 16.5 0.8 293 6 8 2 38.963 77.925 0.408 3.39 8 63.5 11.3 294 2 1 4 39.027 78.053 0.409 3.39 8 65.2 11.9 295 1 13 2 39.046 78.092 0.409 3.38 8 22.3 1.4 296 6 0 3 39.19 78.38 0.41 3.36 4 27.7 1.1 297 8 6 0 39.21 78.42 0.41 3.36 4 19.9 0.6 298 3 9 3 39.254 78.508 0.411 3.35 8 7.9 0.2 299 6 1 3 39.293 78.586 0.411 3.35 8 37.2 3.8 300 5 10 2 39.299 78.597 0.411 3.35 8 118.6 39.0 301 2 2 4 39.336 78.673 0.411 3.34 8 24.1 1.6 302 0 4 4 39.346 78.692 0.412 3.34 4 7.2 0.1 303 6 11 0 39.38 78.759 0.412 3.34 4 3.9 0.0 304 8 5 1 39.441 78.882 0.412 3.33 8 2.7 0.0 305 5 6 3 39.525 79.051 0.413 3.32 8 64.0 11.3 306 4 13 1 39.555 79.11 0.413 3.31 8 38.3 4.0 307 6 2 3 39.602 79.204 0.414 3.31 8 76.1 15.9 308 4 8 3 39.65 79.299 0.414 3.3 8 40.9 4.6 309 1 4 4 39.652 79.305 0.414 3.3 8 4.7 0.1 310 2 10 3 39.678 79.356 0.414 3.3 8 3.6 0.0 311 5 12 1 39.739 79.479 0.415 3.29 8 3.1 0.0 312 2 3 4 39.851 79.702 0.416 3.27 8 19.8 1.1 313 2 13 2 39.966 79.932 0.417 3.26 8 56.5 8.6 314 7 6 2 40.064 80.129 0.418 3.25 8 10.0 0.3 315 6 3 3 40.116 80.232 0.418 3.24 8 128.0 44.0 316 3 14 1 40.188 80.376 0.419 3.23 8 9.0 0.2 317 2 15 0 40.278 80.555 0.42 3.22 4 8.5 0.1 318 0 15 1 40.414 80.828 0.421 3.2 4 6.0 0.0 319 3 0 4 40.454 80.909 0.421 3.2 4 148.2 29.1 320 8 7 0 40.545 81.091 0.422 3.19 4 83.0 9.1 321 3 1 4 40.557 81.113 0.422 3.19 8 1.2 0.0 322 2 4 4 40.568 81.137 0.422 3.19 8 10.3 0.3 323 8 6 1 40.57 81.14 0.422 3.19 8 2.2 0.0 324 1 5 4 40.576 81.151 0.422 3.19 8 5.5 0.1 325 7 9 1 40.605 81.211 0.422 3.18 8 35.0 3.2 326 0 11 3 40.611 81.221 0.423 3.18 4 68.8 6.2 327 6 9 2 40.71 81.419 0.423 3.17 8 16.7 0.7 328 1 15 1 40.719 81.437 0.423 3.17 8 22.7 1.4 329 6 11 1 40.738 81.476 0.424 3.17 8 10.1 0.3 330 6 4 3 40.832 81.665 0.424 3.16 8 71.7 13.5 331 5 7 3 40.858 81.716 0.425 3.15 8 4.1 0.0 332 3 2 4 40.863 81.727 0.425 3.15 8 33.1 2.9 333 1 11 3 40.915 81.83 0.425 3.15 8 10.9 0.3 334 8 0 2 40.95 81.9 0.425 3.14 4 77.2 7.8 335 4 14 0 40.965 81.93 0.426 3.14 4 97.8 12.4 336 8 1 2 41.052 82.104 0.426 3.13 8 6.6 0.1 337 4 12 2 41.063 82.126 0.426 3.13 8 185.8 89.6 338 3 10 3 41.202 82.404 0.428 3.12 8 46.6 5.6 339 8 2 2 41.358 82.716 0.429 3.1 8 82.2 17.4 340 3 3 4 41.373 82.747 0.429 3.1 8 34.1 3.0 341 4 9 3 41.389 82.779 0.429 3.1 8 20.8 1.1 342 7 7 2 41.393 82.787 0.429 3.1 8 44.3 5.0 343 0 6 4 41.395 82.789 0.429 3.1 4 49.8 3.2 344 5 11 2 41.45 82.9 0.43 3.09 8 30.5 2.4 345 2 5 4 41.487 82.974 0.43 3.09 8 6.2 0.1 346 3 13 2 41.487 82.975 0.43 3.09 8 36.6 3.4 347 0 14 2 41.509 83.017 0.43 3.09 4 64.5 5.3 348 2 15 1 41.629 83.259 0.431 3.07 8 54.0 7.4 349 1 6 4 41.698 83.395 0.432 3.07 8 82.5 17.3 350 6 12 0 41.733 83.467 0.432 3.06 4 0.3 0.0 351 6 5 3 41.75 83.499 0.432 3.06 8 24.6 1.5 352 1 14 2 41.812 83.623 0.433 3.06 8 35.3 3.2 353 2 11 3 41.825 83.65 0.433 3.05 8 42.8 4.6 354 8 3 2 41.867 83.734 0.433 3.05 8 62.3 9.8 355 8 7 1 41.895 83.791 0.433 3.05 8 33.8 2.9 356 9 0 1 42.059 84.118 0.435 3.03 4 79.9 8.0 357 8 8 0 42.074 84.149 0.435 3.03 4 130.8 21.5 358 3 4 4 42.086 84.171 0.435 3.03 8 64.6 10.5 359 9 1 1 42.16 84.321 0.436 3.02 8 34.6 3.0 360 0 16 0 42.224 84.449 0.436 3.02 2 120.1 9.0 361 5 13 1 42.292 84.584 0.437 3.01 8 43.7 4.8 362 4 14 1 42.313 84.626 0.437 3.01 8 72.9 13.2 363 5 8 3 42.385 84.77 0.438 3.0 8 19.1 0.9 364 9 2 1 42.465 84.93 0.438 3.0 8 35.1 3.1 365 7 10 1 42.54 85.08 0.439 2.99 8 14.2 0.5 366 4 0 4 42.577 85.154 0.439 2.99 4 131.6 21.4 367 8 4 2 42.578 85.156 0.439 2.99 8 23.6 1.4 368 2 6 4 42.605 85.21 0.439 2.99 8 16.3 0.7 369 6 10 2 42.644 85.287 0.44 2.98 8 2.2 0.0 370 4 1 4 42.678 85.357 0.44 2.98 8 20.1 1.0 371 2 14 2 42.718 85.437 0.44 2.98 8 58.0 8.3 372 6 6 3 42.867 85.733 0.442 2.96 8 108.9 29.1 373 7 8 2 42.917 85.835 0.442 2.96 8 33.9 2.8 374 9 3 1 42.972 85.944 0.442 2.96 8 27.5 1.9 375 4 2 4 42.982 85.965 0.443 2.96 8 60.7 9.0 376 3 5 4 42.999 85.997 0.443 2.95 8 12.1 0.4 377 1 7 4 43.017 86.035 0.443 2.95 8 31.6 2.4 378 6 12 1 43.077 86.155 0.443 2.95 8 51.4 6.5 379 7 0 3 43.14 86.28 0.444 2.94 4 98.0 11.7 380 3 15 1 43.14 86.281 0.444 2.94 8 80.9 16.0 381 7 1 3 43.241 86.483 0.445 2.94 8 28.4 2.0 382 1 12 3 43.252 86.505 0.445 2.94 8 64.8 10.2 383 4 10 3 43.319 86.637 0.445 2.93 8 41.5 4.2 384 3 11 3 43.335 86.67 0.445 2.93 8 7.0 0.1 385 8 8 1 43.417 86.834 0.446 2.92 8 101.6 25.0 386 2 16 0 43.432 86.863 0.446 2.92 4 85.2 8.8 387 4 3 4 43.489 86.977 0.447 2.92 8 37.2 3.4 388 8 5 2 43.49 86.98 0.447 2.92 8 6.3 0.1 389 7 2 3 43.545 87.09 0.447 2.91 8 71.2 12.2 390 4 13 2 43.602 87.204 0.448 2.91 8 47.3 5.4 391 9 4 1 43.681 87.362 0.448 2.91 8 32.5 2.5 392 5 12 2 43.783 87.567 0.449 2.9 8 25.6 1.6 393 8 9 0 43.797 87.595 0.449 2.9 4 31.0 1.2 394 1 16 1 43.868 87.735 0.45 2.89 8 15.7 0.6 395 4 15 0 43.91 87.819 0.45 2.89 4 51.1 3.1 396 2 7 4 43.922 87.843 0.45 2.89 8 47.1 5.3 397 7 3 3 44.051 88.102 0.451 2.88 8 29.8 2.1 398 5 9 3 44.107 88.214 0.452 2.88 8 20.5 1.0 399 3 6 4 44.112 88.224 0.452 2.88 8 63.2 9.5 400 2 12 3 44.156 88.312 0.452 2.87 8 17.9 0.8 401 6 7 3 44.183 88.365 0.452 2.87 8 6.6 0.1 402 4 4 4 44.197 88.394 0.453 2.87 8 31.8 2.4 403 3 14 2 44.225 88.451 0.453 2.87 8 60.3 8.6 404 0 8 4 44.234 88.469 0.453 2.87 4 69.7 5.8 405 6 13 0 44.267 88.535 0.453 2.87 4 29.9 1.1 406 1 8 4 44.535 89.07 0.455 2.85 8 30.9 2.3 407 9 5 1 44.591 89.182 0.456 2.85 8 52.4 6.5 408 8 6 2 44.602 89.205 0.456 2.85 8 67.9 10.9 409 7 9 2 44.637 89.275 0.456 2.85 8 6.0 0.1 410 7 11 1 44.666 89.331 0.456 2.85 8 28.0 1.8 411 1 15 2 44.749 89.499 0.457 2.84 8 33.6 2.7 412 7 4 3 44.759 89.518 0.457 2.84 8 48.2 5.5 413 6 11 2 44.769 89.538 0.457 2.84 8 25.0 1.5 414 2 16 1 44.771 89.541 0.457 2.84 8 183.0 78.8 X-ray diffraction powder data (I)...X-Ray wave length = 1.54056 (angs.): No H K L Theta 2*Theta d I int I int.n. I p.h.n. H(Si) ( degree ) (angstrem) *100 *100 1 0 2 0 4.819 9.638 9.1695 1028.1 58.1 59.0 5.6 2 2 0 0 8.334 16.668 5.3145 281.9 15.9 16.1 5.6 3 2 1 0 8.679 17.358 5.10448 402.2 22.7 23.0 5.6 4 0 1 1 9.12 18.24 4.85981 499.4 28.2 28.5 5.6 5 2 2 0 9.644 19.288 4.59804 154.1 8.7 8.8 5.6 6 0 4 0 9.672 19.344 4.58475 684.4 38.7 39.0 5.6 7 1 0 1 9.738 19.476 4.55398 35.6 2.0 2.0 5.6 8 1 1 1 10.037 20.074 4.41974 634.1 35.8 36.1 5.6 9 1 2 1 10.886 21.772 4.07866 82.0 4.6 4.7 5.6 10 2 3 0 11.073 22.145 4.01073 348.2 19.7 19.8 5.6 11 0 3 1 11.425 22.849 3.88873 201.3 11.4 11.5 5.6 12 1 3 1 12.176 24.353 3.65199 175.4 9.9 10.0 5.6 13 2 4 0 12.82 25.64 3.47147 503.6 28.5 28.6 5.6 14 2 2 1 13.107 26.213 3.39683 694.6 39.2 39.4 5.6 15 2 3 1 14.208 28.416 3.1383 155.8 8.8 8.8 5.6 16 2 5 0 14.784 29.567 3.01868 65.5 3.7 3.7 5.6 17 0 5 1 15.054 30.109 2.96563 134.9 7.6 7.6 5.6 18 2 4 1 15.63 31.261 2.85892 1769.8 100.0 100.0 5.6 19 3 2 1 16.183 32.367 2.76369 49.2 2.8 2.8 5.6 20 4 0 0 16.851 33.701 2.65725 287.6 16.3 16.2 5.7 21 2 6 0 16.901 33.802 2.64956 42.7 2.4 2.4 5.7 22 3 3 1 17.104 34.209 2.61899 496.6 28.1 28.0 5.7 23 2 5 1 17.304 34.608 2.5897 62.3 3.5 3.5 5.7 24 4 2 0 17.566 35.132 2.55224 273.4 15.4 15.4 5.7 25 1 6 1 17.669 35.338 2.53787 110.9 6.3 6.2 5.7 26 0 0 2 17.798 35.597 2.52 274.2 15.5 15.4 5.7 27 3 4 1 18.325 36.65 2.44995 25.2 1.4 1.4 5.7 28 0 2 2 18.482 36.963 2.42991 209.4 11.8 11.8 5.7 29 2 7 0 19.135 38.271 2.34985 30.9 1.7 1.7 5.7 30 2 6 1 19.174 38.349 2.34523 155.7 8.8 8.7 5.7 31 0 7 1 19.352 38.703 2.32456 23.1 1.3 1.3 5.7 32 0 8 0 19.634 39.269 2.29238 93.6 5.3 5.3 5.7 33 3 5 1 19.799 39.598 2.27411 224.5 12.7 12.6 5.7 34 1 7 1 19.828 39.656 2.27089 127.5 7.2 7.2 5.7 35 2 1 2 19.931 39.862 2.25964 35.2 2.0 2.0 5.7 36 2 2 2 20.399 40.799 2.20987 95.7 5.4 5.4 5.7 37 4 3 1 20.554 41.108 2.19396 42.5 2.4 2.4 5.7 38 1 4 2 20.87 41.74 2.16222 147.0 8.3 8.2 5.7 39 4 5 0 20.975 41.95 2.15187 25.1 1.4 1.4 5.7 40 3 6 1 21.484 42.968 2.10318 263.9 14.9 14.7 5.7 41 3 1 2 22.175 44.351 2.04079 44.0 2.5 2.5 5.7 42 3 2 2 22.606 45.212 2.0039 352.6 19.9 19.7 5.7 43 4 5 1 22.906 45.812 1.97903 37.8 2.1 2.1 5.7 44 5 1 1 23.297 46.594 1.94762 44.8 2.5 2.5 5.7 45 2 8 1 23.364 46.729 1.94232 540.8 30.6 30.1 5.7 46 5 2 1 23.712 47.423 1.91548 31.0 1.8 1.7 5.7 47 2 9 0 23.882 47.764 1.90261 20.0 1.1 1.1 5.7 48 5 3 1 24.391 48.781 1.86529 38.3 2.2 2.1 5.7 49 4 0 2 24.914 49.829 1.82851 243.8 13.8 13.5 5.7 50 2 6 2 24.951 49.902 1.82599 96.4 5.4 5.3 5.7 51 2 9 1 25.642 51.283 1.78 56.3 3.2 3.1 5.8 52 6 2 0 26.286 52.573 1.73934 65.2 3.7 3.6 5.8 53 2 10 0 26.38 52.761 1.73359 30.9 1.7 1.7 5.8 54 5 5 1 26.476 52.952 1.72777 45.6 2.6 2.5 5.8 55 3 6 2 26.865 53.731 1.70455 54.4 3.1 3.0 5.8 56 6 3 0 26.918 53.835 1.70149 34.6 2.0 1.9 5.8 57 4 4 2 26.97 53.941 1.69841 124.2 7.0 6.9 5.8 58 0 8 2 27.017 54.033 1.69573 20.7 1.2 1.1 5.8 59 1 8 2 27.387 54.773 1.67455 140.4 7.9 7.7 5.8 60 6 0 1 27.445 54.89 1.67127 24.2 1.4 1.3 5.8 61 3 9 1 27.522 55.044 1.66696 62.8 3.5 3.5 5.8 62 1 0 3 27.658 55.316 1.6594 30.2 1.7 1.7 5.8 63 6 2 1 27.936 55.872 1.64418 42.0 2.4 2.3 5.8 64 4 8 1 27.993 55.985 1.64114 49.8 2.8 2.7 5.8 65 2 10 1 28.026 56.053 1.63932 45.0 2.5 2.5 5.8 66 1 2 3 28.147 56.294 1.63288 37.6 2.1 2.1 5.8 67 0 3 3 28.392 56.784 1.61994 67.5 3.8 3.7 5.8 68 4 9 0 28.449 56.897 1.61698 31.3 1.8 1.7 5.8 69 5 2 2 28.78 57.559 1.59995 103.3 5.8 5.7 5.8 70 2 1 3 28.862 57.723 1.59579 37.4 2.1 2.1 5.8 71 4 6 2 29.399 58.798 1.56915 282.3 16.0 15.5 5.8 72 1 11 1 29.473 58.946 1.56557 36.1 2.0 2.0 5.8 73 6 6 0 30.17 60.34 1.53268 174.3 9.8 9.5 5.8 74 0 12 0 30.267 60.534 1.52825 195.3 11.0 10.7 5.8 75 3 0 3 30.493 60.986 1.51799 42.0 2.4 2.3 5.8 76 1 5 3 30.63 61.26 1.51187 173.8 9.8 9.5 5.8 77 4 10 0 30.687 61.373 1.50934 114.1 6.4 6.2 5.8 78 3 2 3 30.953 61.907 1.49761 24.7 1.4 1.3 5.8 79 5 8 1 31.149 62.298 1.48914 18.8 1.1 1.0 5.8 80 0 10 2 31.297 62.594 1.48281 81.0 4.6 4.4 5.8 81 2 5 3 31.65 63.299 1.46797 40.8 2.3 2.2 5.9 82 6 6 1 31.688 63.376 1.46637 39.7 2.2 2.2 5.9 83 1 6 3 31.883 63.767 1.45834 34.0 1.9 1.8 5.9 84 6 0 2 32.107 64.215 1.44924 30.0 1.7 1.6 5.9 85 4 10 1 32.19 64.381 1.4459 100.6 5.7 5.5 5.9 86 3 4 3 32.312 64.623 1.44106 36.8 2.1 2.0 5.9 87 5 6 2 32.471 64.943 1.43474 48.7 2.8 2.6 5.9 88 4 8 2 32.606 65.212 1.42946 97.0 5.5 5.3 5.9 89 4 0 3 32.851 65.701 1.42 29.4 1.7 1.6 5.9 90 2 6 3 32.881 65.763 1.41882 73.0 4.1 4.0 5.9 91 4 1 3 32.961 65.923 1.41576 51.2 2.9 2.8 5.9 92 2 12 1 33.111 66.223 1.41008 45.4 2.6 2.5 5.9 93 4 2 3 33.293 66.585 1.40328 19.3 1.1 1.0 5.9 94 6 4 2 33.878 67.756 1.38185 49.5 2.8 2.7 5.9 95 3 10 2 34.273 68.545 1.36785 33.4 1.9 1.8 5.9 96 2 7 3 34.307 68.614 1.36665 17.7 1.0 1.0 5.9 97 3 6 3 34.511 69.023 1.35955 104.9 5.9 5.7 5.9 98 0 13 1 34.542 69.085 1.35848 18.2 1.0 1.0 5.9 99 6 8 1 34.777 69.553 1.35047 79.0 4.5 4.3 5.9 100 1 13 1 34.864 69.728 1.34752 19.8 1.1 1.1 5.9 101 6 9 0 35.181 70.363 1.33691 34.1 1.9 1.8 5.9 102 8 0 0 35.433 70.867 1.32862 29.4 1.7 1.6 5.9 103 4 12 0 35.552 71.104 1.32478 83.2 4.7 4.5 5.9 104 2 8 3 35.918 71.837 1.31305 62.4 3.5 3.3 5.9 105 6 6 2 36.031 72.062 1.3095 28.4 1.6 1.5 5.9 106 0 12 2 36.119 72.239 1.30673 34.7 2.0 1.9 5.9 107 0 9 3 36.459 72.917 1.29624 66.9 3.8 3.6 6.0 108 4 10 2 36.504 73.008 1.29485 33.5 1.9 1.8 6.0 109 8 0 1 36.839 73.677 1.28473 29.5 1.7 1.6 6.0 110 8 2 1 37.259 74.518 1.27231 76.8 4.3 4.1 6.0 111 4 7 3 38.098 76.196 1.24841 31.2 1.8 1.7 6.0 112 1 2 4 38.413 76.825 1.23975 92.5 5.2 4.9 6.0 113 2 14 1 38.654 77.308 1.2332 92.6 5.2 4.9 6.0 114 5 10 2 39.299 78.597 1.21618 42.8 2.4 2.3 6.0 115 6 3 3 40.116 80.232 1.19547 44.0 2.5 2.3 6.0 116 3 0 4 40.454 80.909 1.18716 29.1 1.6 1.5 6.1 117 4 14 0 40.965 81.93 1.17492 20.2 1.1 1.1 6.1 118 4 12 2 41.063 82.126 1.17262 89.6 5.1 4.7 6.1 119 8 2 2 41.358 82.716 1.16574 20.4 1.1 1.1 6.1 120 3 4 4 42.086 84.171 1.14926 40.0 2.3 2.1 6.1 121 4 14 1 42.313 84.626 1.14424 18.0 1.0 0.9 6.1 122 4 0 4 42.577 85.154 1.13849 23.5 1.3 1.2 6.1 123 6 6 3 42.867 85.733 1.13228 29.1 1.6 1.5 6.1 124 3 15 1 43.14 86.281 1.12649 27.7 1.6 1.4 6.1 125 8 8 1 43.417 86.834 1.12073 33.8 1.9 1.8 6.1 126 2 16 1 44.771 89.541 1.09373 88.4 5.0 4.6 6.2 Reference: Chichagov A.V. et al. Information-Calculating System on Crystal Structure Data of Minerals (MINCRYST) - Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian) |