Institute of Experimental Mineralogy Russian Academy of Sciences ------------------------------------------------- 142432, Chernogolovka, Moscow district A.V. Chichagov +7(496)52-22320 *** *** W W W - X R A Y P O L *** *********************** HOLTITE 2, DF [Si(2.43)Sb(0.36)As(0.21)]BO(3)Al(6)[Al(0.62)Ta(0.26)]O(15)(O,OH)(2.65) Orthorhombic P nma Z = 4 R =0.03 NR =1664 2 .6 .1905 Ref.Str.: S.S. Kazantsev, D.Yu. Puscharovsky, M. Pasero, S. Merlino et al. (2005) * Kristallogr., 50, 49-55 Reserv: N.A.D. Initial data from BDM-file Lattice parameters (cub. angs.,degr.): a = 4.695 alpha = 90.0 b = 11.906 beta = 90.0 c = 20.38 gamma = 90.0 Unit cell volume (cub. angs.) = 1139.21 Molar volume ( cub.cm/mol.) = 171.55 Co-ordinates, thermal parameters, occupation for atomic positions: NoP x/a y/b z/c B(j) atom / occupation 1 0.4014 0.75 0.2499 0.0 Al = 0.62, Ta = 0.26 2 0.5576 0.6105 0.4731 0.0 Al = 1.00 3 0.0593 0.4905 0.4318 0.0 Al = 0.98, Al = 0.0 4 0.0599 0.3597 0.2901 0.0 Al = 0.94, Al = 0.0 5 0.0889 0.75 0.4064 0.0 Si = 0.81, As = 0.09 6 0.114 0.75 0.3853 0.0 Sb = 0.1 , Sb = 0.0 7 0.5888 0.5231 0.3288 0.0 Si = 0.81, As = 0.06 8 0.6092 0.5636 0.3168 0.0 Sb = 0.13, Sb = 0.0 9 0.3784 0.75 0.4564 0.0 O = 1.00 10 0.1569 0.75 0.3304 0.0 O = 0.9 , O = 0.0 11 0.8928 0.6389 0.4551 0.0 O = 1.00 12 0.4029 0.4341 0.2822 0.0 O = 1.00 13 0.3957 0.5509 0.3944 0.0 O = 1.00 14 0.8831 0.4509 0.3512 0.0 O = 1.00 15 0.6593 0.6331 0.2886 0.0 O = 0.87, O = 0.0 16 0.1715 0.25 0.3493 0.0 O = 1.00 17 0.2536 0.3506 0.4476 0.0 O = 1.00 18 0.7567 0.25 0.2739 0.0 O = 1.00 19 0.7511 0.4669 0.4887 0.0 O = 1.00 20 0.231 0.25 0.4665 0.0 B = 1.00 Co-ordinates for all atomic positions : No NoP x/a y/b z/c 1 1 0.4014 0.75 0.2499 2 2 0.5576 0.6105 0.4731 3 3 0.0593 0.4905 0.4318 4 4 0.0599 0.3597 0.2901 5 5 0.0889 0.75 0.4064 6 6 0.114 0.75 0.3853 7 7 0.5888 0.5231 0.3288 8 8 0.6092 0.5636 0.3168 9 9 0.3784 0.75 0.4564 10 10 0.1569 0.75 0.3304 11 11 0.8928 0.6389 0.4551 12 12 0.4029 0.4341 0.2822 13 13 0.3957 0.5509 0.3944 14 14 0.8831 0.4509 0.3512 15 15 0.6593 0.6331 0.2886 16 16 0.1715 0.25 0.3493 17 17 0.2536 0.3506 0.4476 18 18 0.7567 0.25 0.2739 19 19 0.7511 0.4669 0.4887 20 20 0.231 0.25 0.4665 21 1 0.0986 0.25 0.7499 22 2 0.9424 0.3895 0.9731 23 3 0.4407 0.5095 0.9318 24 4 0.4401 0.6403 0.7901 25 5 0.4111 0.25 0.9064 26 6 0.386 0.25 0.8853 27 7 0.9112 0.4769 0.8288 28 8 0.8908 0.4364 0.8168 29 9 0.1216 0.25 0.9564 30 10 0.3431 0.25 0.8304 31 11 0.6072 0.3611 0.9551 32 12 0.0971 0.5659 0.7822 33 13 0.1043 0.4491 0.8944 34 14 0.6169 0.5491 0.8512 35 15 0.8407 0.3669 0.7886 36 16 0.3285 0.75 0.8493 37 17 0.2464 0.6494 0.9476 38 18 0.7433 0.75 0.7739 39 19 0.7489 0.5331 0.9887 40 20 0.269 0.75 0.9665 41 2 0.9424 0.1105 0.9731 42 3 0.4407 0.9905 0.9318 43 4 0.4401 0.8597 0.7901 44 7 0.9112 0.0231 0.8288 45 8 0.8908 0.0636 0.8168 46 11 0.6072 0.1389 0.9551 47 12 0.0971 0.9341 0.7822 48 13 0.1043 0.0509 0.8944 49 14 0.6169 0.9509 0.8512 50 15 0.8407 0.1331 0.7886 51 17 0.2464 0.8506 0.9476 52 19 0.7489 0.9669 0.9887 53 2 0.5576 0.8895 0.4731 54 3 0.0593 0.0095 0.4318 55 4 0.0599 0.1403 0.2901 56 7 0.5888 0.9769 0.3288 57 8 0.6092 0.9364 0.3168 58 11 0.8928 0.8611 0.4551 59 12 0.4029 0.0659 0.2822 60 13 0.3957 0.9491 0.3944 61 14 0.8831 0.0491 0.3512 62 15 0.6593 0.8669 0.2886 63 17 0.2536 0.1494 0.4476 64 19 0.7511 0.0331 0.4887 65 1 0.9014 0.75 0.2501 66 2 0.0576 0.6105 0.0269 67 3 0.5593 0.4905 0.0682 68 4 0.5599 0.3597 0.2099 69 5 0.5889 0.75 0.0936 70 6 0.614 0.75 0.1147 71 7 0.0888 0.5231 0.1712 72 8 0.1092 0.5636 0.1832 73 9 0.8784 0.75 0.0436 74 10 0.6569 0.75 0.1696 75 11 0.3928 0.6389 0.0449 76 12 0.9029 0.4341 0.2178 77 13 0.8957 0.5509 0.1056 78 14 0.3831 0.4509 0.1488 79 15 0.1593 0.6331 0.2114 80 16 0.6715 0.25 0.1507 81 17 0.7536 0.3506 0.0524 82 18 0.2567 0.25 0.2261 83 19 0.2511 0.4669 0.0113 84 20 0.731 0.25 0.0335 85 1 0.5986 0.25 0.7501 86 2 0.4424 0.3895 0.5269 87 3 0.9407 0.5095 0.5682 88 4 0.9401 0.6403 0.7099 89 5 0.9111 0.25 0.5936 90 6 0.886 0.25 0.6147 91 7 0.4112 0.4769 0.6712 92 8 0.3908 0.4364 0.6832 93 9 0.6216 0.25 0.5436 94 10 0.8431 0.25 0.6696 95 11 0.1072 0.3611 0.5449 96 12 0.5971 0.5659 0.7178 97 13 0.6043 0.4491 0.6056 98 14 0.1169 0.5491 0.6488 99 15 0.3407 0.3669 0.7114 100 16 0.8285 0.75 0.6507 101 17 0.7464 0.6494 0.5524 102 18 0.2433 0.75 0.7261 103 19 0.2489 0.5331 0.5113 104 20 0.769 0.75 0.5335 105 2 0.4424 0.1105 0.5269 106 3 0.9407 0.9905 0.5682 107 4 0.9401 0.8597 0.7099 108 7 0.4112 0.0231 0.6712 109 8 0.3908 0.0636 0.6832 110 11 0.1072 0.1389 0.5449 111 12 0.5971 0.9341 0.7178 112 13 0.6043 0.0509 0.6056 113 14 0.1169 0.9509 0.6488 114 15 0.3407 0.1331 0.7114 115 17 0.7464 0.8506 0.5524 116 19 0.2489 0.9669 0.5113 117 2 0.0576 0.8895 0.0269 118 3 0.5593 0.0095 0.0682 119 4 0.5599 0.1403 0.2099 120 7 0.0888 0.9769 0.1712 121 8 0.1092 0.9364 0.1832 122 11 0.3928 0.8611 0.0449 123 12 0.9029 0.0659 0.2178 124 13 0.8957 0.9491 0.1056 125 14 0.3831 0.0491 0.1488 126 15 0.1593 0.8669 0.2114 127 17 0.7536 0.1494 0.0524 128 19 0.2511 0.0331 0.0113 X-ray density (g/cm cub.) = 3.74 MU (1/cm) = 214.294 Mass attenuation coefficient (cm**2/g) = 57.298 Selected interatomic distances (cation-anion,anion-anion): NoP Atom Rad.sph. C.N. Distance NoP N. (angs.) (angs.) 1 Al ,Ta 2.424 6 2.0025 10 2.0064 15 2.0064 15 2.0289 10 1.9607 15 1.9607 15 2 Al 2.316 6 1.8931 9 1.651 11 1.9112 13 1.9616 19 1.9008 17 1.8856 19 3 Al ,Al 2.316 6 1.9894 11 1.8957 13 1.8994 14 1.9261 17 1.875 19 1.9163 19 4 Al ,Al 2.316 6 1.845 12 1.8491 14 1.8538 16 1.9599 18 1.8704 12 2.0641 18 5 Si ,As 2.46 4 1.6985 9 1.5818 10 1.8925 11 1.8925 11 6 Sb ,Sb 2.712 4 1.908 9 1.1368 10 2.2027 11 2.2027 11 7 Si ,As 2.46 4 1.6691 12 1.6493 13 1.6904 14 1.5794 15 8 Sb ,Sb 2.712 4 1.9523 12 1.8792 13 1.9867 14 1.0341 15 9 O 3.264 11 2.7705 10 2.7537 11 2.636 11 2.6874 13 2.7537 11 2.636 11 2.6874 13 2.8719 17 2.8793 19 2.8719 17 2.8793 19 10 O ,O 3.264 11 2.7705 9 3.1218 11 2.9287 13 2.8682 15 2.8497 15 3.1218 11 2.9287 13 2.8682 15 2.8497 15 2.7962 15 2.7962 15 11 O 3.264 10 2.636 9 2.7537 9 3.1218 10 2.8641 13 2.8417 13 3.0815 14 2.2595 19 2.6455 11 2.1024 17 2.3862 19 12 O 3.264 11 2.6765 13 2.6647 14 2.8237 14 2.6608 15 2.8026 16 2.7554 18 2.6895 12 2.6895 12 2.7276 14 3.0006 15 2.5657 18 13 O 3.264 11 2.6874 9 2.9287 10 2.8417 11 2.8641 11 2.6765 12 2.7257 14 2.8257 14 2.6718 15 2.7033 17 2.7346 19 2.4892 19 14 O 3.264 11 3.0815 11 2.8237 12 2.6647 12 2.8257 13 2.7257 13 2.7272 15 2.7489 16 2.883 17 2.9249 18 2.8763 19 2.7276 12 15 O ,O 3.264 10 2.8497 10 2.8682 10 2.6608 12 2.6718 13 2.7272 14 2.7836 15 2.7962 10 3.0006 12 2.826 15 2.826 15 16 O 3.264 9 2.8026 12 2.7489 14 2.3657 17 3.148 18 2.4807 18 2.8026 12 2.7488 14 2.3657 17 2.5425 18 17 O 3.264 9 2.7033 13 2.883 14 2.3657 16 2.8416 19 2.8609 19 2.3955 17 2.8719 9 2.1024 11 2.5312 19 18 O 3.264 11 2.7554 12 2.9249 14 2.4807 16 3.148 16 2.7554 12 2.9249 14 2.5657 12 2.5425 16 2.5416 18 2.5416 18 2.5657 12 19 O 3.264 11 2.2595 11 2.7346 13 2.8763 14 2.8609 17 2.8416 17 2.8793 9 2.3862 11 2.4892 13 2.5312 17 2.5091 19 2.5284 19 20 B 1.872 2 1.2626 17 1.2626 17 X-ray diffraction powder data (II), X-Ray W.L. = 1.54056(angs.): No H K L Theta 2*Theta S LPG MF F I int. ( degree ) *100 1 0 1 1 4.297 8.594 0.049 353.25 4 92.2 924.6 2 0 0 2 4.335 8.67 0.049 347.03 2 44.1 103.8 3 0 2 0 7.435 14.869 0.084 116.5 2 79.2 112.5 4 0 1 3 7.501 15.002 0.085 114.4 4 61.3 132.6 5 0 2 2 8.619 17.237 0.097 86.12 4 94.4 236.7 6 0 0 4 8.696 17.391 0.098 84.57 2 179.5 419.8 7 1 0 1 9.693 19.385 0.109 67.64 4 17.3 6.2 8 1 1 1 10.391 20.782 0.117 58.57 8 52.7 100.4 9 1 0 2 10.407 20.814 0.117 58.38 4 49.0 43.2 10 1 1 2 11.062 22.125 0.125 51.43 8 38.4 46.7 11 0 3 1 11.405 22.809 0.128 48.26 4 93.2 129.1 12 0 2 4 11.478 22.956 0.129 47.62 4 108.2 171.7 13 1 0 3 11.504 23.008 0.129 47.4 4 6.2 0.6 14 0 1 5 11.522 23.044 0.13 47.24 4 98.0 139.9 15 1 1 3 12.103 24.205 0.136 42.62 8 21.5 12.1 16 1 2 1 12.26 24.519 0.138 41.48 8 51.2 67.1 17 1 2 2 12.838 25.677 0.144 37.65 8 119.9 333.6 18 1 0 4 12.891 25.782 0.145 37.32 4 138.7 221.3 19 0 3 3 12.99 25.98 0.146 36.72 4 78.2 69.2 20 0 0 6 13.107 26.215 0.147 36.03 2 9.7 0.5 21 1 1 4 13.432 26.864 0.151 34.22 8 75.8 121.3 22 1 2 3 13.753 27.505 0.154 32.55 8 154.8 480.7 23 1 0 5 14.493 28.986 0.162 29.11 4 151.5 205.9 24 1 3 1 14.888 29.777 0.167 27.48 8 59.9 60.7 25 1 2 4 14.946 29.892 0.167 27.26 8 45.8 35.3 26 1 1 5 14.98 29.961 0.168 27.12 8 88.8 131.7 27 0 4 0 14.998 29.996 0.168 27.05 2 183.9 140.9 28 0 2 6 15.135 30.27 0.169 26.53 4 188.8 291.6 29 1 3 2 15.376 30.751 0.172 25.65 8 170.4 459.0 30 0 4 2 15.641 31.281 0.175 24.72 4 70.2 37.5 31 0 3 5 15.718 31.435 0.176 24.46 4 89.7 60.7 32 0 1 7 15.805 31.61 0.177 24.17 4 48.7 17.7 33 1 3 3 16.158 32.316 0.181 23.04 8 49.0 34.0 34 1 0 6 16.254 32.508 0.182 22.75 4 41.3 12.0 35 1 2 5 16.364 32.727 0.183 22.42 8 69.7 67.1 36 1 1 6 16.695 33.39 0.186 21.47 8 95.9 121.6 37 1 3 4 17.2 34.4 0.192 20.12 8 25.4 8.0 38 0 4 4 17.44 34.881 0.195 19.52 4 128.4 99.2 39 0 0 8 17.6 35.2 0.196 19.14 2 102.4 30.9 40 1 2 6 17.961 35.921 0.2 18.31 8 1.4 0.0 41 1 4 1 17.983 35.966 0.2 18.26 8 93.6 98.6 42 1 0 7 18.138 36.277 0.202 17.91 4 89.2 44.0 43 1 4 2 18.397 36.794 0.205 17.37 8 57.5 35.4 44 1 3 5 18.464 36.927 0.206 17.23 8 85.8 78.2 45 1 1 7 18.54 37.08 0.206 17.07 8 51.6 28.0 46 0 5 1 19.007 38.014 0.211 16.16 4 145.0 104.8 47 1 4 3 19.07 38.139 0.212 16.04 8 81.2 65.3 48 2 0 0 19.155 38.31 0.213 15.89 2 131.7 42.4 49 0 3 7 19.155 38.311 0.213 15.89 4 176.6 152.7 50 0 2 8 19.201 38.403 0.213 15.8 4 135.1 88.8 51 2 0 1 19.287 38.574 0.214 15.65 4 69.7 23.4 52 2 1 0 19.539 39.078 0.217 15.2 4 16.2 1.2 53 2 1 1 19.668 39.337 0.218 14.98 8 35.3 11.5 54 2 0 2 19.677 39.355 0.219 14.97 4 46.1 9.8 55 1 2 7 19.702 39.404 0.219 14.93 8 24.9 5.7 56 1 3 6 19.914 39.828 0.221 14.57 8 2.6 0.1 57 1 4 4 19.979 39.958 0.222 14.47 8 79.3 56.1 58 0 5 3 20.046 40.093 0.223 14.36 4 21.8 2.1 59 2 1 2 20.053 40.105 0.223 14.35 8 37.4 12.3 60 1 0 8 20.121 40.243 0.223 14.24 4 108.4 51.6 61 0 4 6 20.126 40.252 0.223 14.24 4 73.5 23.7 62 0 1 9 20.259 40.518 0.225 14.03 4 74.8 24.2 63 2 0 3 20.314 40.628 0.225 13.94 4 54.9 13.0 64 1 1 8 20.49 40.98 0.227 13.68 8 40.6 13.9 65 2 2 0 20.654 41.307 0.229 13.44 4 87.6 31.8 66 2 1 3 20.68 41.359 0.229 13.4 8 75.6 47.2 67 2 2 1 20.777 41.555 0.23 13.26 8 40.2 13.2 68 1 4 5 21.1 42.201 0.234 12.81 8 92.7 67.9 69 2 2 2 21.145 42.29 0.234 12.75 8 8.3 0.5 70 2 0 4 21.179 42.358 0.235 12.7 4 9.8 0.4 71 1 5 1 21.388 42.775 0.237 12.43 8 148.2 168.2 72 1 3 7 21.522 43.044 0.238 12.25 8 142.2 152.7 73 2 1 4 21.532 43.065 0.238 12.24 8 102.4 79.1 74 1 2 8 21.564 43.128 0.239 12.2 8 158.2 188.2 75 2 2 3 21.746 43.492 0.24 11.97 8 79.6 46.7 76 1 5 2 21.747 43.493 0.24 11.97 8 57.2 24.1 77 0 5 5 22.002 44.004 0.243 11.66 4 3.2 0.0 78 1 0 9 22.189 44.378 0.245 11.44 4 19.2 1.3 79 0 0 10 22.207 44.415 0.245 11.42 2 67.3 8.0 80 2 0 5 22.251 44.501 0.246 11.37 4 104.2 38.0 81 1 5 3 22.335 44.67 0.247 11.27 8 51.6 18.5 82 1 4 6 22.408 44.816 0.247 11.19 8 3.9 0.1 83 2 3 0 22.41 44.82 0.247 11.19 4 150.7 78.3 84 2 3 1 22.526 45.052 0.249 11.06 8 70.3 33.7 85 1 1 9 22.53 45.059 0.249 11.05 8 54.9 20.5 86 2 2 4 22.566 45.133 0.249 11.01 8 52.2 18.5 87 2 1 5 22.591 45.181 0.249 10.99 8 85.3 49.2 88 0 6 0 22.841 45.683 0.252 10.72 2 114.9 21.8 89 2 3 2 22.871 45.742 0.252 10.68 8 129.0 109.7 90 0 3 9 23.057 46.113 0.254 10.49 4 19.1 1.2 91 1 5 4 23.139 46.277 0.255 10.41 8 37.8 9.2 92 1 3 8 23.265 46.53 0.256 10.28 8 8.1 0.4 93 0 6 2 23.295 46.591 0.257 10.25 4 109.1 37.6 94 2 3 3 23.437 46.874 0.258 10.11 8 80.8 40.7 95 0 4 8 23.453 46.905 0.258 10.09 4 80.0 19.9 96 2 0 6 23.507 47.015 0.259 10.04 4 54.3 9.1 97 1 2 9 23.529 47.058 0.259 10.02 8 64.3 25.5 98 0 2 10 23.547 47.093 0.259 10.0 4 86.7 23.2 99 2 2 5 23.588 47.176 0.26 9.96 8 126.1 97.7 100 2 1 6 23.833 47.667 0.262 9.73 8 87.7 46.1 101 1 4 7 23.88 47.761 0.263 9.69 8 2.7 0.0 102 1 5 5 24.141 48.283 0.265 9.45 8 0.1 0.0 103 2 3 4 24.212 48.424 0.266 9.39 8 143.1 118.5 104 1 0 10 24.333 48.665 0.267 9.28 4 25.3 1.8 105 0 6 4 24.619 49.238 0.27 9.04 4 41.5 4.8 106 1 1 10 24.65 49.301 0.271 9.01 8 57.5 18.4 107 2 4 0 24.702 49.404 0.271 8.97 4 4.5 0.1 108 0 5 7 24.702 49.404 0.271 8.97 4 88.6 21.7 109 2 2 6 24.792 49.585 0.272 8.9 8 2.6 0.0 110 2 4 1 24.81 49.619 0.272 8.88 8 35.5 6.9 111 0 1 11 24.882 49.765 0.273 8.82 4 19.9 1.1 112 2 0 7 24.93 49.859 0.274 8.79 4 183.2 90.8 113 1 6 1 25.032 50.063 0.275 8.71 8 71.3 27.3 114 1 3 9 25.126 50.253 0.276 8.63 8 7.5 0.3 115 2 4 2 25.13 50.261 0.276 8.63 8 7.3 0.3 116 2 3 5 25.182 50.365 0.276 8.59 8 21.3 2.4 117 2 1 7 25.242 50.484 0.277 8.54 8 15.2 1.2 118 1 5 6 25.326 50.652 0.278 8.48 8 59.5 18.5 119 1 6 2 25.35 50.701 0.278 8.46 8 38.1 7.6 120 1 4 8 25.498 50.996 0.279 8.35 8 3.7 0.1 121 1 2 10 25.586 51.173 0.28 8.28 8 38.7 7.7 122 2 4 3 25.659 51.317 0.281 8.23 8 181.5 167.1 123 1 6 3 25.875 51.751 0.283 8.07 8 77.6 29.9 124 2 2 7 26.162 52.325 0.286 7.87 8 87.9 37.5 125 2 3 6 26.333 52.665 0.288 7.76 8 75.4 27.2 126 2 4 4 26.385 52.77 0.288 7.72 8 88.3 37.1 127 2 0 8 26.5 53.0 0.29 7.65 4 54.8 7.1 128 1 0 11 26.548 53.097 0.29 7.61 4 60.3 8.5 129 1 6 4 26.598 53.196 0.291 7.58 8 25.0 2.9 130 1 5 7 26.676 53.353 0.291 7.53 8 39.3 7.2 131 0 6 6 26.716 53.432 0.292 7.51 4 44.6 4.6 132 2 1 8 26.799 53.598 0.293 7.45 8 49.0 11.0 133 1 1 11 26.847 53.694 0.293 7.42 8 68.3 21.3 134 0 0 12 26.972 53.943 0.294 7.34 2 6.4 0.0 135 0 7 1 27.03 54.059 0.295 7.31 4 72.8 11.9 136 1 3 10 27.094 54.189 0.296 7.27 8 16.2 1.2 137 1 4 9 27.246 54.493 0.297 7.18 8 10.4 0.5 138 0 4 10 27.262 54.525 0.297 7.17 4 100.0 22.1 139 2 4 5 27.299 54.599 0.298 7.15 8 115.7 59.0 140 0 3 11 27.311 54.623 0.298 7.14 4 106.7 25.0 141 2 5 0 27.437 54.874 0.299 7.06 4 82.3 14.7 142 1 6 5 27.507 55.014 0.3 7.02 8 58.9 15.0 143 2 5 1 27.537 55.074 0.3 7.01 8 100.7 43.8 144 2 3 7 27.648 55.297 0.301 6.94 8 105.0 47.1 145 2 2 8 27.683 55.366 0.302 6.92 8 111.8 53.4 146 1 2 11 27.73 55.46 0.302 6.9 8 97.8 40.7 147 0 7 3 27.83 55.661 0.303 6.84 4 51.1 5.5 148 2 5 2 27.835 55.67 0.303 6.84 8 36.6 5.6 149 0 5 9 27.996 55.993 0.305 6.75 4 101.1 21.2 150 0 2 12 28.141 56.283 0.306 6.67 4 41.3 3.5 151 1 5 8 28.178 56.356 0.307 6.65 8 158.2 102.6 152 2 0 9 28.205 56.41 0.307 6.63 4 188.2 72.4 153 2 5 3 28.328 56.656 0.308 6.57 8 86.2 30.1 154 2 4 6 28.39 56.779 0.309 6.54 8 109.5 48.3 155 2 1 9 28.492 56.984 0.31 6.48 8 95.8 36.7 156 1 6 6 28.592 57.184 0.311 6.43 8 45.9 8.3 157 1 0 12 28.837 57.673 0.313 6.31 4 57.9 6.5 158 1 7 1 28.892 57.784 0.314 6.28 8 22.2 1.9 159 2 5 4 29.008 58.017 0.315 6.23 8 90.1 31.2 160 1 4 10 29.115 58.229 0.316 6.18 8 9.9 0.4 161 2 3 8 29.116 58.233 0.316 6.17 8 27.9 3.0 162 1 1 12 29.119 58.239 0.316 6.17 8 11.1 0.5 163 1 3 11 29.162 58.324 0.316 6.15 8 14.6 0.8 164 1 7 2 29.181 58.363 0.316 6.14 8 105.8 42.4 165 2 2 9 29.342 58.684 0.318 6.07 8 34.7 4.5 166 0 7 5 29.388 58.777 0.319 6.05 4 196.2 71.7 167 0 6 8 29.475 58.95 0.319 6.01 4 184.1 62.7 168 3 0 1 29.58 59.16 0.32 5.96 4 10.6 0.2 169 2 4 7 29.644 59.288 0.321 5.93 8 66.5 16.2 170 1 7 3 29.66 59.319 0.321 5.92 8 64.6 15.2 171 0 1 13 29.709 59.417 0.322 5.9 4 221.6 89.3 172 1 5 9 29.819 59.638 0.323 5.85 8 63.4 14.5 173 1 6 7 29.841 59.682 0.323 5.84 8 112.2 45.3 174 3 1 1 29.859 59.717 0.323 5.83 8 2.4 0.0 175 3 0 2 29.865 59.731 0.323 5.83 4 8.6 0.1 176 2 5 5 29.869 59.738 0.323 5.83 8 16.9 1.0 177 1 2 12 29.958 59.916 0.324 5.79 8 68.2 16.6 178 2 0 10 30.034 60.069 0.325 5.76 4 15.6 0.4 179 3 1 2 30.142 60.284 0.326 5.71 8 1.7 0.0 180 2 1 10 30.31 60.621 0.328 5.64 8 121.9 51.7 181 1 7 4 30.321 60.643 0.328 5.64 8 37.4 4.9 182 3 0 3 30.337 60.674 0.328 5.63 4 36.7 2.3 183 2 6 0 30.55 61.099 0.33 5.54 4 5.0 0.0 184 3 1 3 30.611 61.222 0.331 5.52 8 11.6 0.5 185 2 6 1 30.643 61.286 0.331 5.51 8 101.0 34.6 186 3 2 1 30.685 61.37 0.331 5.49 8 42.4 6.1 187 2 3 9 30.726 61.452 0.332 5.47 8 38.8 5.1 188 2 5 6 30.901 61.802 0.333 5.41 8 128.6 55.1 189 2 6 2 30.922 61.844 0.334 5.4 8 34.9 4.1 190 3 2 2 30.964 61.928 0.334 5.38 8 61.0 12.3 191 3 0 4 30.99 61.98 0.334 5.37 4 49.2 4.0 192 2 4 8 31.052 62.104 0.335 5.35 8 66.5 14.6 193 1 4 11 31.096 62.191 0.335 5.33 8 13.0 0.6 194 2 2 10 31.13 62.259 0.336 5.32 8 57.8 11.0 195 1 7 5 31.16 62.319 0.336 5.31 8 27.6 2.5 196 0 8 0 31.17 62.339 0.336 5.3 2 286.1 66.9 197 1 0 13 31.199 62.398 0.336 5.29 4 100.8 16.6 198 1 6 8 31.244 62.487 0.337 5.28 8 16.9 0.9 199 3 1 4 31.261 62.522 0.337 5.27 8 21.1 1.4 200 1 3 12 31.326 62.651 0.337 5.25 8 118.4 45.3 201 2 6 3 31.384 62.769 0.338 5.22 8 105.6 35.9 202 3 2 3 31.426 62.852 0.338 5.21 8 38.8 4.8 203 1 1 13 31.469 62.938 0.339 5.19 8 35.3 4.0 204 0 4 12 31.479 62.958 0.339 5.19 4 309.6 153.3 205 0 8 2 31.538 63.076 0.34 5.17 4 24.1 0.9 206 1 5 10 31.59 63.181 0.34 5.15 8 113.5 40.9 207 0 7 7 31.634 63.269 0.34 5.13 4 34.9 1.9 208 0 5 11 31.788 63.576 0.342 5.08 4 44.2 3.1 209 3 0 5 31.818 63.636 0.342 5.07 4 26.3 1.1 210 0 3 13 31.89 63.78 0.343 5.04 4 35.2 1.9 211 0 0 14 31.948 63.895 0.343 5.02 2 70.8 3.9 212 2 0 11 31.981 63.962 0.344 5.01 4 62.9 6.1 213 2 6 4 32.025 64.05 0.344 5.0 8 37.7 4.4 214 3 3 1 32.034 64.069 0.344 4.99 8 135.7 56.7 215 3 2 4 32.066 64.132 0.345 4.98 8 134.9 55.9 216 3 1 5 32.085 64.17 0.345 4.98 8 150.8 69.7 217 2 5 7 32.095 64.19 0.345 4.97 8 42.1 5.4 218 1 7 6 32.167 64.335 0.346 4.95 8 86.6 22.9 219 2 1 11 32.248 64.495 0.346 4.92 8 28.0 2.4 220 1 2 13 32.271 64.543 0.347 4.92 8 65.0 12.8 221 3 3 2 32.307 64.613 0.347 4.9 8 19.3 1.1 222 2 3 10 32.468 64.937 0.348 4.85 8 134.8 54.3 223 2 4 9 32.605 65.21 0.35 4.81 8 113.6 38.3 224 0 8 4 32.629 65.259 0.35 4.8 4 120.4 21.5 225 3 3 3 32.758 65.516 0.351 4.76 8 6.6 0.1 226 1 6 9 32.791 65.583 0.352 4.75 8 1.1 0.0 227 0 6 10 32.806 65.611 0.352 4.74 4 12.6 0.2 228 3 0 6 32.815 65.629 0.352 4.74 4 22.8 0.8 229 2 6 5 32.839 65.678 0.352 4.73 8 92.3 24.9 230 3 2 5 32.879 65.759 0.352 4.72 8 16.2 0.8 231 1 8 1 32.975 65.949 0.353 4.69 8 65.0 12.2 232 0 2 14 33.006 66.013 0.354 4.68 4 97.5 13.7 233 2 2 11 33.04 66.079 0.354 4.67 8 147.2 62.4 234 3 1 6 33.077 66.155 0.354 4.66 8 20.3 1.2 235 1 4 12 33.186 66.371 0.355 4.63 8 23.7 1.6 236 1 8 2 33.243 66.486 0.356 4.61 8 54.5 8.4 237 1 7 7 33.337 66.673 0.357 4.58 8 75.0 15.9 238 3 3 4 33.384 66.769 0.357 4.57 8 50.7 7.2 239 2 5 8 33.444 66.888 0.358 4.55 8 127.1 45.3 240 1 5 11 33.486 66.972 0.358 4.54 8 56.3 8.9 241 1 3 13 33.586 67.171 0.359 4.51 8 42.9 5.1 242 1 0 14 33.641 67.283 0.36 4.5 4 65.3 5.9 243 1 8 3 33.688 67.376 0.36 4.48 8 69.0 13.2 244 2 6 6 33.819 67.639 0.361 4.45 8 9.4 0.2 245 3 2 6 33.859 67.719 0.362 4.44 8 30.9 2.6 246 3 4 1 33.874 67.747 0.362 4.43 8 31.2 2.7 247 1 1 14 33.901 67.802 0.362 4.43 8 6.0 0.1 248 3 0 7 33.972 67.945 0.363 4.41 4 123.1 20.6 249 2 7 0 34.004 68.009 0.363 4.4 4 43.9 2.6 250 2 0 12 34.042 68.084 0.363 4.39 4 13.0 0.2 251 2 7 1 34.092 68.185 0.364 4.37 8 27.7 2.1 252 3 4 2 34.138 68.277 0.364 4.36 8 67.6 12.3 253 3 3 5 34.181 68.363 0.365 4.35 8 104.3 29.2 254 3 1 7 34.231 68.461 0.365 4.34 8 30.9 2.6 255 2 4 10 34.296 68.591 0.366 4.32 8 64.0 10.9 256 2 1 12 34.3 68.6 0.366 4.32 8 0.5 0.0 257 1 8 4 34.306 68.612 0.366 4.32 8 15.9 0.7 258 2 3 11 34.339 68.677 0.366 4.31 8 35.8 3.4 259 2 7 2 34.356 68.713 0.366 4.3 8 144.4 55.3 260 0 8 6 34.408 68.815 0.367 4.29 4 111.5 16.4 261 1 6 10 34.478 68.956 0.367 4.27 8 8.1 0.2 262 0 7 9 34.5 68.999 0.368 4.27 4 132.3 23.0 263 3 4 3 34.578 69.155 0.368 4.25 8 98.5 25.4 264 1 7 8 34.661 69.322 0.369 4.23 8 47.4 5.9 265 1 2 14 34.674 69.348 0.369 4.22 8 45.8 5.5 266 0 1 15 34.793 69.587 0.37 4.19 4 132.9 22.8 267 2 7 3 34.794 69.589 0.37 4.19 8 18.8 0.9 268 2 5 9 34.941 69.882 0.372 4.16 8 15.6 0.6 269 2 6 7 34.961 69.922 0.372 4.15 8 49.6 6.3 270 3 2 7 35.0 70.0 0.372 4.14 8 19.5 1.0 271 2 2 12 35.069 70.138 0.373 4.13 8 10.1 0.3 272 1 8 5 35.093 70.186 0.373 4.12 8 47.0 5.6 273 3 3 6 35.144 70.288 0.374 4.11 8 48.6 6.0 274 3 4 4 35.188 70.376 0.374 4.1 8 235.5 140.2 275 3 0 8 35.285 70.571 0.375 4.08 4 284.1 101.4 276 1 4 13 35.384 70.769 0.376 4.05 8 48.7 5.9 277 2 7 4 35.403 70.807 0.376 4.05 8 50.8 6.4 278 1 5 12 35.503 71.006 0.377 4.03 8 13.2 0.4 279 3 1 8 35.539 71.079 0.377 4.02 8 1.3 0.0 280 0 9 1 35.697 71.394 0.379 3.98 4 80.0 7.9 281 1 3 14 35.945 71.89 0.381 3.93 8 59.7 8.6 282 3 4 5 35.967 71.933 0.381 3.93 8 34.1 2.8 283 0 5 13 36.034 72.069 0.382 3.91 4 147.8 26.3 284 1 8 6 36.044 72.089 0.382 3.91 8 25.7 1.6 285 0 4 14 36.089 72.177 0.382 3.9 4 81.0 7.9 286 2 4 11 36.12 72.241 0.383 3.89 8 89.2 19.1 287 1 7 9 36.135 72.269 0.383 3.89 8 48.8 5.7 288 3 5 1 36.17 72.341 0.383 3.88 8 36.3 3.1 289 1 0 15 36.171 72.342 0.383 3.88 4 151.2 27.4 290 2 7 5 36.18 72.36 0.383 3.88 8 80.8 15.6 291 2 0 13 36.216 72.433 0.384 3.87 4 32.9 1.3 292 2 6 8 36.258 72.516 0.384 3.87 8 67.2 10.8 293 3 3 7 36.266 72.533 0.384 3.86 8 41.7 4.1 294 3 2 8 36.296 72.593 0.384 3.86 8 42.4 4.3 295 1 6 11 36.298 72.597 0.384 3.86 8 71.5 12.2 296 2 3 12 36.334 72.668 0.385 3.85 8 47.1 5.3 297 0 9 3 36.385 72.77 0.385 3.84 4 26.5 0.8 298 1 1 15 36.423 72.845 0.385 3.83 8 32.9 2.6 299 3 5 2 36.428 72.855 0.385 3.83 8 39.6 3.7 300 2 1 13 36.468 72.935 0.386 3.82 8 79.5 14.9 301 2 5 10 36.581 73.162 0.387 3.8 8 79.2 14.7 302 0 6 12 36.654 73.309 0.388 3.79 4 49.2 2.8 303 3 0 9 36.748 73.497 0.388 3.77 4 34.2 1.4 304 0 3 15 36.816 73.631 0.389 3.75 4 2.9 0.0 305 0 8 8 36.829 73.657 0.389 3.75 4 20.9 0.5 306 3 5 3 36.855 73.71 0.389 3.75 8 4.6 0.0 307 3 4 6 36.909 73.817 0.39 3.74 8 53.5 6.6 308 3 1 9 36.998 73.996 0.391 3.72 8 28.0 1.8 309 2 7 6 37.12 74.24 0.392 3.7 8 44.0 4.4 310 1 8 7 37.156 74.312 0.392 3.69 8 138.0 43.3 311 1 2 15 37.173 74.345 0.392 3.69 8 141.8 45.7 312 0 0 16 37.21 74.419 0.393 3.68 2 58.7 2.0 313 2 2 13 37.217 74.435 0.393 3.68 8 75.9 13.1 314 1 9 1 37.31 74.619 0.393 3.66 8 9.1 0.2 315 3 5 4 37.45 74.9 0.395 3.64 8 4.1 0.0 316 3 3 8 37.545 75.09 0.396 3.62 8 29.7 2.0 317 1 9 2 37.564 75.128 0.396 3.62 8 56.3 7.1 318 1 5 13 37.642 75.283 0.396 3.6 8 14.8 0.5 319 1 4 14 37.695 75.39 0.397 3.6 8 4.0 0.0 320 2 6 9 37.706 75.412 0.397 3.59 8 22.2 1.1 321 3 2 9 37.744 75.488 0.397 3.59 8 21.6 1.0 322 0 9 5 37.747 75.493 0.397 3.59 4 2.0 0.0 323 1 7 10 37.753 75.507 0.397 3.59 8 134.0 39.7 324 2 8 0 37.794 75.588 0.398 3.58 4 78.6 6.8 325 2 8 1 37.878 75.757 0.399 3.56 8 74.0 12.0 326 0 7 11 37.936 75.871 0.399 3.55 4 5.3 0.0 327 1 9 3 37.987 75.973 0.4 3.55 8 21.7 1.0 328 3 4 7 38.011 76.022 0.4 3.54 8 3.5 0.0 329 2 4 12 38.077 76.154 0.4 3.53 8 90.1 17.7 330 2 8 2 38.131 76.263 0.401 3.52 8 37.0 3.0 331 0 2 16 38.201 76.402 0.401 3.51 4 25.6 0.7 332 3 5 5 38.211 76.421 0.402 3.51 8 78.3 13.3 333 2 7 7 38.22 76.439 0.402 3.51 8 26.9 1.6 334 1 6 12 38.252 76.504 0.402 3.5 8 44.3 4.2 335 3 0 10 38.358 76.715 0.403 3.49 4 55.6 3.3 336 2 5 11 38.361 76.722 0.403 3.49 8 45.3 4.4 337 1 3 15 38.411 76.821 0.403 3.48 8 43.0 4.0 338 1 8 8 38.424 76.847 0.403 3.48 8 33.0 2.3 339 2 3 13 38.455 76.91 0.404 3.47 8 60.8 7.9 340 2 0 14 38.508 77.016 0.404 3.46 4 29.1 0.9 341 2 8 3 38.552 77.104 0.405 3.46 8 102.3 22.3 342 1 9 4 38.576 77.152 0.405 3.45 8 94.6 19.0 343 3 1 10 38.604 77.208 0.405 3.45 8 11.9 0.3 344 2 1 14 38.754 77.508 0.406 3.43 8 20.9 0.9 345 1 0 16 38.799 77.599 0.407 3.42 4 17.7 0.3 346 3 6 1 38.902 77.803 0.408 3.4 8 44.9 4.2 347 3 3 9 38.976 77.952 0.408 3.39 8 0.7 0.0 348 1 1 16 39.045 78.089 0.409 3.38 8 58.9 7.2 349 3 5 6 39.133 78.267 0.41 3.37 8 16.4 0.6 350 2 8 4 39.138 78.277 0.41 3.37 8 29.6 1.8 351 3 6 2 39.153 78.305 0.41 3.37 8 30.3 1.9 352 3 4 8 39.269 78.539 0.411 3.35 8 13.2 0.4 353 2 6 10 39.302 78.604 0.411 3.35 8 3.3 0.0 354 1 9 5 39.329 78.658 0.411 3.34 8 26.7 1.5 355 3 2 10 39.34 78.679 0.411 3.34 8 40.9 3.4 356 2 7 8 39.476 78.953 0.413 3.32 8 10.0 0.2 357 2 2 14 39.489 78.977 0.413 3.32 8 21.6 1.0 358 1 7 11 39.516 79.032 0.413 3.32 8 26.8 1.5 359 3 6 3 39.57 79.14 0.413 3.31 8 20.4 0.8 360 0 9 7 39.759 79.518 0.415 3.29 4 68.5 4.8 361 1 2 16 39.778 79.556 0.415 3.28 8 17.5 0.6 362 1 8 9 39.845 79.69 0.416 3.27 8 36.4 2.7 363 0 8 10 39.858 79.716 0.416 3.27 4 92.5 8.6 364 2 8 5 39.889 79.777 0.416 3.27 8 51.6 5.4 365 1 5 14 39.905 79.811 0.416 3.27 8 16.9 0.6 366 3 0 11 40.112 80.224 0.418 3.24 4 18.6 0.3 367 1 4 15 40.124 80.248 0.418 3.24 8 11.4 0.3 368 3 6 4 40.152 80.304 0.419 3.24 8 14.1 0.4 369 2 4 13 40.168 80.335 0.419 3.23 8 9.7 0.2 370 3 5 7 40.216 80.432 0.419 3.23 8 9.9 0.2 371 0 1 17 40.224 80.448 0.419 3.23 4 48.4 2.3 372 1 9 6 40.245 80.489 0.419 3.22 8 78.6 12.3 373 2 5 12 40.281 80.563 0.42 3.22 8 29.7 1.7 374 0 10 0 40.313 80.627 0.42 3.22 2 242.1 29.0 375 1 6 13 40.34 80.68 0.42 3.21 8 21.5 0.9 376 3 1 11 40.355 80.711 0.42 3.21 8 37.4 2.8 377 3 3 10 40.558 81.115 0.422 3.19 8 44.9 4.0 378 0 10 2 40.645 81.29 0.423 3.18 4 142.2 19.8 379 3 4 9 40.683 81.365 0.423 3.17 8 51.5 5.2 380 2 3 14 40.706 81.411 0.423 3.17 8 47.8 4.5 381 0 5 15 40.748 81.496 0.424 3.17 4 190.9 35.5 382 2 8 6 40.801 81.602 0.424 3.16 8 36.1 2.5 383 2 7 9 40.888 81.776 0.425 3.15 8 52.3 5.3 384 3 6 5 40.898 81.796 0.425 3.15 8 2.6 0.0 385 2 0 15 40.923 81.846 0.425 3.15 4 80.5 6.3 386 1 3 16 40.993 81.986 0.426 3.14 8 10.7 0.2 387 4 0 0 41.015 82.03 0.426 3.14 2 177.4 15.2 388 0 6 14 41.015 82.03 0.426 3.14 4 156.5 23.7 389 2 6 11 41.046 82.091 0.426 3.13 8 97.0 18.2 390 3 2 11 41.083 82.166 0.427 3.13 8 31.2 1.9 391 4 0 1 41.098 82.195 0.427 3.13 4 52.0 2.6 392 0 4 16 41.131 82.262 0.427 3.12 4 127.2 15.6 393 2 1 15 41.165 82.331 0.427 3.12 8 38.7 2.9 394 4 1 0 41.257 82.514 0.428 3.11 4 19.5 0.4 395 1 9 7 41.32 82.641 0.429 3.1 8 42.4 3.4 396 4 1 1 41.339 82.679 0.429 3.1 8 108.9 22.7 397 4 0 2 41.345 82.691 0.429 3.1 4 123.1 14.5 398 1 8 10 41.418 82.837 0.429 3.09 8 66.1 8.3 399 1 7 12 41.423 82.845 0.429 3.09 8 6.1 0.1 400 3 5 8 41.457 82.914 0.43 3.09 8 47.3 4.3 401 1 0 17 41.54 83.08 0.43 3.08 4 44.1 1.8 402 4 1 2 41.587 83.174 0.431 3.08 8 101.8 19.7 403 0 10 4 41.636 83.272 0.431 3.07 4 25.7 0.6 404 4 0 3 41.757 83.515 0.432 3.06 4 92.2 8.0 405 1 1 17 41.782 83.563 0.433 3.06 8 30.5 1.8 406 3 6 6 41.806 83.611 0.433 3.06 8 44.6 3.8 407 2 8 7 41.874 83.748 0.433 3.05 8 17.6 0.6 408 2 2 15 41.89 83.78 0.433 3.05 8 139.8 36.7 409 0 7 13 41.93 83.86 0.434 3.04 4 55.2 2.9 410 2 9 0 41.941 83.882 0.434 3.04 4 60.2 3.4 411 1 10 1 41.953 83.905 0.434 3.04 8 39.4 2.9 412 4 2 0 41.981 83.963 0.434 3.04 4 7.2 0.0 413 4 1 3 41.999 83.997 0.434 3.04 8 3.7 0.0 414 3 0 12 42.013 84.026 0.434 3.04 4 57.7 3.1 415 2 9 1 42.023 84.046 0.435 3.04 8 21.6 0.9 416 3 7 1 42.06 84.12 0.435 3.03 8 33.5 2.1 417 4 2 1 42.064 84.128 0.435 3.03 8 75.7 10.7 418 0 3 17 42.16 84.32 0.436 3.02 4 35.1 1.1 419 1 10 2 42.199 84.399 0.436 3.02 8 39.7 2.9 420 3 4 10 42.25 84.5 0.436 3.02 8 39.3 2.9 421 3 1 12 42.254 84.508 0.436 3.02 8 25.7 1.2 422 2 9 2 42.27 84.54 0.437 3.01 8 26.5 1.3 423 3 3 11 42.29 84.58 0.437 3.01 8 39.3 2.9 424 1 5 15 42.302 84.604 0.437 3.01 8 4.2 0.0 425 3 7 2 42.307 84.614 0.437 3.01 8 25.0 1.2 426 4 2 2 42.31 84.621 0.437 3.01 8 36.2 2.4 427 4 0 4 42.333 84.667 0.437 3.01 4 49.4 2.3 428 2 5 13 42.345 84.69 0.437 3.01 8 48.2 4.3 429 2 4 14 42.397 84.794 0.438 3.0 8 12.3 0.3 430 0 9 9 42.404 84.808 0.438 3.0 4 42.1 1.6 431 2 7 10 42.454 84.908 0.438 3.0 8 135.1 33.7 432 1 2 17 42.505 85.009 0.439 2.99 8 8.8 0.1 433 1 9 8 42.555 85.11 0.439 2.99 8 13.4 0.3 434 1 6 14 42.567 85.135 0.439 2.99 8 45.8 3.9 435 4 1 4 42.574 85.149 0.439 2.99 8 60.2 6.7 436 1 10 3 42.61 85.221 0.439 2.99 8 9.8 0.2 437 2 9 3 42.681 85.361 0.44 2.98 8 23.6 1.0 438 1 4 16 42.682 85.364 0.44 2.98 8 10.7 0.2 439 3 7 3 42.718 85.435 0.44 2.98 8 50.2 4.6 440 4 2 3 42.721 85.443 0.44 2.98 8 1.1 0.0 441 3 5 9 42.855 85.711 0.441 2.97 8 80.8 11.9 442 0 0 18 42.869 85.738 0.442 2.96 2 26.6 0.3 443 3 6 7 42.874 85.749 0.442 2.96 8 4.9 0.0 444 2 6 12 42.939 85.878 0.442 2.96 8 1.4 0.0 445 3 2 12 42.976 85.952 0.442 2.96 8 66.5 8.1 446 4 0 5 43.073 86.145 0.443 2.95 4 25.6 0.6 447 2 3 15 43.094 86.188 0.443 2.95 8 18.5 0.6 448 2 8 8 43.107 86.213 0.444 2.95 8 14.9 0.4 449 1 8 11 43.145 86.291 0.444 2.94 8 32.0 1.9 450 1 10 4 43.185 86.37 0.444 2.94 8 32.8 1.9 451 4 3 0 43.185 86.37 0.444 2.94 4 41.1 1.5 452 2 9 4 43.255 86.51 0.445 2.93 8 127.2 29.3 453 4 3 1 43.267 86.534 0.445 2.93 8 49.3 4.4 454 0 10 6 43.28 86.56 0.445 2.93 4 57.7 3.0 455 3 7 4 43.292 86.584 0.445 2.93 8 5.0 0.0 456 4 2 4 43.296 86.591 0.445 2.93 8 61.7 6.9 457 4 1 5 43.313 86.626 0.445 2.93 8 93.1 15.7 458 2 0 16 43.474 86.947 0.447 2.92 4 22.5 0.5 459 1 7 13 43.477 86.955 0.447 2.92 8 2.7 0.0 460 0 8 12 43.486 86.972 0.447 2.92 4 17.1 0.3 461 4 3 2 43.513 87.026 0.447 2.92 8 21.3 0.8 462 1 3 17 43.707 87.413 0.449 2.9 8 20.5 0.8 463 2 1 16 43.714 87.427 0.449 2.9 8 75.6 10.2 464 0 2 18 43.83 87.66 0.45 2.9 4 95.6 8.1 465 1 10 5 43.922 87.845 0.45 2.89 8 48.2 4.1 466 4 3 3 43.923 87.845 0.45 2.89 8 37.1 2.4 467 1 9 9 43.949 87.899 0.451 2.89 8 75.1 10.0 468 3 4 11 43.973 87.946 0.451 2.89 8 1.3 0.0 469 4 0 6 43.974 87.948 0.451 2.89 4 12.7 0.1 470 2 9 5 43.993 87.985 0.451 2.88 8 16.2 0.5 471 3 7 5 44.029 88.059 0.451 2.88 8 8.4 0.1 472 4 2 5 44.033 88.066 0.451 2.88 8 30.4 1.6 473 3 0 13 44.064 88.129 0.451 2.88 4 2.2 0.0 474 3 6 8 44.104 88.208 0.452 2.88 8 25.8 1.2 475 2 7 11 44.176 88.352 0.452 2.87 8 0.9 0.0 476 3 3 12 44.177 88.353 0.452 2.87 8 17.8 0.6 477 4 1 6 44.214 88.428 0.453 2.87 8 51.2 4.6 478 3 1 13 44.304 88.609 0.453 2.87 8 0.1 0.0 479 3 5 10 44.413 88.825 0.454 2.86 8 12.9 0.3 480 1 0 18 44.413 88.827 0.454 2.86 4 67.5 4.0 481 2 2 16 44.434 88.867 0.454 2.86 8 8.0 0.1 482 4 3 4 44.496 88.991 0.455 2.85 8 80.2 11.3 483 2 8 9 44.499 88.999 0.455 2.85 8 77.5 10.6 484 2 5 14 44.559 89.118 0.455 2.85 8 37.4 2.5 485 1 1 18 44.653 89.306 0.456 2.85 8 11.3 0.2 486 2 4 15 44.774 89.548 0.457 2.84 8 17.2 0.5 487 1 10 6 44.823 89.646 0.458 2.84 8 2.8 0.0 488 1 5 16 44.843 89.686 0.458 2.84 8 90.4 14.3 489 4 4 0 44.865 89.73 0.458 2.84 4 93.0 7.6 490 2 9 6 44.893 89.786 0.458 2.83 8 90.6 14.3 491 3 7 6 44.93 89.86 0.458 2.83 8 7.5 0.1 492 4 2 6 44.934 89.867 0.458 2.83 8 79.2 10.9 493 1 6 15 44.944 89.888 0.459 2.83 8 75.2 9.9 494 4 4 1 44.947 89.894 0.459 2.83 8 19.6 0.7 495 2 6 13 44.987 89.974 0.459 2.83 8 31.1 1.7 X-ray diffraction powder data (I)...X-Ray wave length = 1.54056 (angs.): No H K L Theta 2*Theta d I int I int.n. I p.h.n. H(Si) ( degree ) (angstrem) *100 *100 1 0 1 1 4.297 8.594 10.28027 924.6 100.0 100.0 5.6 2 0 0 2 4.335 8.67 10.19 103.8 11.2 11.2 5.6 3 0 2 0 7.435 14.869 5.953 112.5 12.2 12.1 5.6 4 0 1 3 7.501 15.002 5.90042 132.6 14.3 14.3 5.6 5 0 2 2 8.619 17.237 5.14014 236.7 25.6 25.5 5.6 6 0 0 4 8.696 17.391 5.095 419.8 45.4 45.2 5.6 7 1 1 1 10.391 20.782 4.2707 143.7 15.5 15.4 5.6 8 1 1 2 11.062 22.125 4.01445 46.7 5.1 5.0 5.6 9 0 3 1 11.405 22.809 3.89549 129.1 14.0 13.8 5.6 10 0 2 4 11.478 22.956 3.87084 172.2 18.6 18.5 5.6 11 0 1 5 11.522 23.044 3.85628 139.9 15.1 15.0 5.6 12 1 1 3 12.103 24.205 3.67386 12.1 1.3 1.3 5.6 13 1 2 1 12.26 24.519 3.62758 67.1 7.3 7.2 5.6 14 1 2 2 12.838 25.677 3.46657 333.6 36.1 35.7 5.6 15 1 0 4 12.891 25.782 3.45263 221.3 23.9 23.7 5.6 16 0 3 3 12.99 25.98 3.42676 69.2 7.5 7.4 5.6 17 1 1 4 13.432 26.864 3.31601 121.3 13.1 13.0 5.6 18 1 2 3 13.753 27.505 3.24012 480.7 52.0 51.3 5.6 19 1 0 5 14.493 28.986 3.07792 205.9 22.3 22.0 5.6 20 1 3 1 14.888 29.777 2.99793 60.7 6.6 6.5 5.6 21 1 2 4 14.946 29.892 2.98666 35.3 3.8 3.8 5.6 22 0 4 0 14.998 29.996 2.9765 272.6 29.5 29.1 5.6 23 0 2 6 15.135 30.27 2.95021 291.6 31.5 31.1 5.6 24 1 3 2 15.376 30.751 2.90512 459.0 49.6 48.9 5.6 25 0 4 2 15.641 31.281 2.85711 37.5 4.1 4.0 5.6 26 0 3 5 15.718 31.435 2.84346 60.7 6.6 6.5 5.6 27 0 1 7 15.805 31.61 2.8281 17.7 1.9 1.9 5.6 28 1 3 3 16.158 32.316 2.76791 34.0 3.7 3.6 5.6 29 1 0 6 16.254 32.508 2.75198 12.0 1.3 1.3 5.6 30 1 2 5 16.364 32.727 2.73409 67.1 7.3 7.1 5.6 31 1 1 6 16.695 33.39 2.68129 121.6 13.2 12.9 5.7 32 0 4 4 17.44 34.881 2.57007 99.2 10.7 10.5 5.7 33 0 0 8 17.6 35.2 2.5475 30.9 3.3 3.3 5.7 34 1 4 1 17.983 35.966 2.49497 98.6 10.7 10.5 5.7 35 1 0 7 18.138 36.277 2.47431 44.0 4.8 4.7 5.7 36 1 4 2 18.397 36.794 2.4407 35.4 3.8 3.7 5.7 37 1 3 5 18.464 36.927 2.43218 78.2 8.5 8.3 5.7 38 1 1 7 18.54 37.08 2.42255 28.0 3.0 3.0 5.7 39 0 5 1 19.007 38.014 2.36511 104.8 11.3 11.1 5.7 40 1 4 3 19.07 38.139 2.35763 65.3 7.1 6.9 5.7 41 0 3 7 19.155 38.311 2.34749 195.1 21.1 20.6 5.7 42 0 2 8 19.201 38.403 2.34206 88.8 9.6 9.4 5.7 43 2 0 1 19.287 38.574 2.33208 23.4 2.5 2.5 5.7 44 2 1 1 19.668 39.337 2.28859 21.3 2.3 2.3 5.7 45 1 4 4 19.979 39.958 2.2544 56.1 6.1 5.9 5.7 46 2 1 2 20.053 40.105 2.24649 14.4 1.6 1.5 5.7 47 1 0 8 20.121 40.243 2.23912 75.3 8.1 8.0 5.7 48 0 1 9 20.259 40.518 2.22457 24.2 2.6 2.6 5.7 49 2 0 3 20.314 40.628 2.21876 13.0 1.4 1.4 5.7 50 1 1 8 20.49 40.98 2.20054 13.9 1.5 1.5 5.7 51 2 1 3 20.68 41.359 2.18121 79.0 8.5 8.3 5.7 52 2 2 1 20.777 41.555 2.17141 13.2 1.4 1.4 5.7 53 1 4 5 21.1 42.201 2.13966 67.9 7.3 7.2 5.7 54 1 5 1 21.388 42.775 2.11224 168.2 18.2 17.7 5.7 55 1 3 7 21.522 43.044 2.09966 231.8 25.1 24.4 5.7 56 1 2 8 21.564 43.128 2.09577 188.2 20.3 19.8 5.7 57 2 2 3 21.746 43.492 2.07905 70.9 7.7 7.5 5.7 58 0 0 10 22.207 44.415 2.038 9.3 1.0 1.0 5.7 59 2 0 5 22.251 44.501 2.03424 38.0 4.1 4.0 5.7 60 1 5 3 22.335 44.67 2.02694 18.5 2.0 1.9 5.7 61 2 3 0 22.41 44.82 2.02049 78.3 8.5 8.2 5.7 62 2 3 1 22.526 45.052 2.01064 54.2 5.9 5.7 5.7 63 2 1 5 22.591 45.181 2.00518 67.8 7.3 7.1 5.7 64 0 6 0 22.841 45.683 1.98433 21.8 2.4 2.3 5.7 65 2 3 2 22.871 45.742 1.98191 109.7 11.9 11.5 5.7 66 0 6 2 23.295 46.591 1.94775 37.6 4.1 3.9 5.7 67 2 3 3 23.437 46.874 1.93665 60.6 6.6 6.4 5.7 68 1 2 9 23.529 47.058 1.9295 57.8 6.3 6.1 5.7 69 2 2 5 23.588 47.176 1.92496 97.7 10.6 10.2 5.7 70 2 1 6 23.833 47.667 1.90626 46.1 5.0 4.8 5.7 71 2 3 4 24.212 48.424 1.8782 118.5 12.8 12.4 5.7 72 1 1 10 24.65 49.301 1.84684 18.4 2.0 1.9 5.7 73 0 5 7 24.702 49.404 1.84322 21.7 2.3 2.3 5.7 74 2 0 7 24.93 49.859 1.82746 90.8 9.8 9.5 5.7 75 1 6 1 25.032 50.063 1.82048 27.3 3.0 2.9 5.7 76 1 5 6 25.326 50.652 1.80069 26.1 2.8 2.7 5.8 77 2 4 3 25.659 51.317 1.77891 167.1 18.1 17.4 5.8 78 1 6 3 25.875 51.751 1.76502 29.9 3.2 3.1 5.8 79 2 2 7 26.162 52.325 1.74699 37.5 4.1 3.9 5.8 80 2 3 6 26.333 52.665 1.7365 27.2 2.9 2.8 5.8 81 2 4 4 26.385 52.77 1.73329 37.1 4.0 3.9 5.8 82 2 1 8 26.799 53.598 1.70845 11.0 1.2 1.1 5.8 83 1 1 11 26.847 53.694 1.70562 21.3 2.3 2.2 5.8 84 0 7 1 27.03 54.059 1.69496 11.9 1.3 1.2 5.8 85 0 4 10 27.262 54.525 1.6816 22.1 2.4 2.3 5.8 86 2 4 5 27.299 54.599 1.67948 84.0 9.1 8.7 5.8 87 2 5 0 27.437 54.874 1.67172 14.7 1.6 1.5 5.8 88 1 6 5 27.507 55.014 1.66778 15.0 1.6 1.6 5.8 89 2 5 1 27.537 55.074 1.66612 43.8 4.7 4.5 5.8 90 2 3 7 27.648 55.297 1.65993 47.1 5.1 4.9 5.8 91 2 2 8 27.683 55.366 1.65801 53.4 5.8 5.5 5.8 92 1 2 11 27.73 55.46 1.65542 40.7 4.4 4.2 5.8 93 2 5 2 27.835 55.67 1.64967 11.1 1.2 1.2 5.8 94 0 5 9 27.996 55.993 1.64093 21.2 2.3 2.2 5.8 95 1 5 8 28.178 56.356 1.63121 175.0 18.9 18.1 5.8 96 2 5 3 28.328 56.656 1.62329 30.1 3.3 3.1 5.8 97 2 4 6 28.39 56.779 1.62006 48.3 5.2 5.0 5.8 98 2 1 9 28.492 56.984 1.61472 36.7 4.0 3.8 5.8 99 2 5 4 29.008 58.017 1.58841 31.2 3.4 3.2 5.8 100 1 7 2 29.181 58.363 1.57982 42.4 4.6 4.4 5.8 101 0 7 5 29.388 58.777 1.56968 71.7 7.8 7.4 5.8 102 0 6 8 29.475 58.95 1.56546 62.7 6.8 6.5 5.8 103 2 4 7 29.644 59.288 1.55736 31.4 3.4 3.2 5.8 104 0 1 13 29.709 59.417 1.55428 89.3 9.7 9.2 5.8 105 1 6 7 29.841 59.682 1.54801 60.8 6.6 6.3 5.8 106 1 2 12 29.958 59.916 1.54251 16.6 1.8 1.7 5.8 107 2 1 10 30.31 60.621 1.52626 58.9 6.4 6.1 5.8 108 2 6 1 30.643 61.286 1.51128 34.6 3.7 3.6 5.8 109 2 5 6 30.901 61.802 1.4999 59.1 6.4 6.1 5.8 110 3 2 2 30.964 61.928 1.49715 16.4 1.8 1.7 5.8 111 2 4 8 31.052 62.104 1.49333 14.6 1.6 1.5 5.8 112 2 2 10 31.13 62.259 1.48997 11.0 1.2 1.1 5.8 113 0 8 0 31.17 62.339 1.48825 69.4 7.5 7.1 5.8 114 1 0 13 31.199 62.398 1.48699 16.6 1.8 1.7 5.8 115 1 3 12 31.326 62.651 1.48159 45.3 4.9 4.7 5.8 116 2 6 3 31.384 62.769 1.4791 35.9 3.9 3.7 5.9 117 0 4 12 31.479 62.958 1.4751 157.3 17.0 16.1 5.9 118 1 5 10 31.59 63.181 1.47044 40.9 4.4 4.2 5.9 119 3 3 1 32.034 64.069 1.45219 61.1 6.6 6.3 5.9 120 3 1 5 32.085 64.17 1.45013 131.1 14.2 13.4 5.9 121 1 7 6 32.167 64.335 1.44683 22.9 2.5 2.3 5.9 122 1 2 13 32.271 64.543 1.44266 15.2 1.6 1.6 5.9 123 2 3 10 32.468 64.937 1.43485 54.3 5.9 5.6 5.9 124 2 4 9 32.605 65.21 1.42951 59.7 6.5 6.1 5.9 125 2 6 5 32.839 65.678 1.42045 24.9 2.7 2.5 5.9 126 1 8 1 32.975 65.949 1.41526 12.2 1.3 1.2 5.9 127 0 2 14 33.006 66.013 1.41405 13.7 1.5 1.4 5.9 128 2 2 11 33.04 66.079 1.41279 62.4 6.8 6.4 5.9 129 1 7 7 33.337 66.673 1.40164 15.9 1.7 1.6 5.9 130 2 5 8 33.444 66.888 1.39766 45.3 4.9 4.6 5.9 131 1 8 3 33.688 67.376 1.38872 13.2 1.4 1.3 5.9 132 3 0 7 33.972 67.945 1.37847 20.6 2.2 2.1 5.9 133 3 4 2 34.138 68.277 1.37258 12.3 1.3 1.3 5.9 134 3 3 5 34.181 68.363 1.37105 29.2 3.2 3.0 5.9 135 2 4 10 34.296 68.591 1.36704 11.6 1.3 1.2 5.9 136 2 7 2 34.356 68.713 1.36492 58.7 6.4 6.0 5.9 137 0 8 6 34.408 68.815 1.36315 16.4 1.8 1.7 5.9 138 0 7 9 34.5 68.999 1.35996 23.0 2.5 2.3 5.9 139 3 4 3 34.578 69.155 1.35727 25.4 2.8 2.6 5.9 140 1 7 8 34.661 69.322 1.35441 11.3 1.2 1.1 5.9 141 0 1 15 34.793 69.587 1.34991 23.7 2.6 2.4 5.9 142 3 4 4 35.188 70.376 1.33668 140.2 15.2 14.2 5.9 143 3 0 8 35.285 70.571 1.33347 101.4 11.0 10.3 5.9 144 2 7 4 35.403 70.807 1.32961 12.4 1.3 1.3 5.9 145 1 3 14 35.945 71.89 1.31221 11.5 1.2 1.2 5.9 146 0 5 13 36.034 72.069 1.3094 27.9 3.0 2.8 5.9 147 2 4 11 36.12 72.241 1.3067 24.8 2.7 2.5 5.9 148 2 7 5 36.18 72.36 1.30485 46.2 5.0 4.7 5.9 149 2 6 8 36.258 72.516 1.30242 14.9 1.6 1.5 5.9 150 1 6 11 36.298 72.597 1.30117 16.4 1.8 1.7 6.0 151 2 1 13 36.468 72.935 1.29596 14.9 1.6 1.5 6.0 152 2 5 10 36.581 73.162 1.29251 14.7 1.6 1.5 6.0 153 1 2 15 37.173 74.345 1.27484 89.0 9.6 9.0 6.0 154 2 2 13 37.217 74.435 1.27353 15.0 1.6 1.5 6.0 155 1 7 10 37.753 75.507 1.25808 40.7 4.4 4.1 6.0 156 2 8 1 37.878 75.757 1.25456 12.0 1.3 1.2 6.0 157 2 4 12 38.077 76.154 1.24899 17.7 1.9 1.8 6.0 158 3 5 5 38.211 76.421 1.24529 14.9 1.6 1.5 6.0 159 2 8 3 38.552 77.104 1.23596 41.3 4.5 4.1 6.0 160 0 8 10 39.858 79.716 1.2019 11.3 1.2 1.1 6.0 161 1 9 6 40.245 80.489 1.19229 14.6 1.6 1.5 6.0 162 0 10 0 40.313 80.627 1.1906 30.0 3.2 3.0 6.1 163 0 10 2 40.645 81.29 1.18256 19.8 2.1 2.0 6.1 164 3 4 9 40.683 81.365 1.18165 9.7 1.0 1.0 6.1 165 0 5 15 40.748 81.496 1.18008 35.5 3.8 3.5 6.1 166 0 6 14 41.015 82.03 1.17374 38.9 4.2 3.8 6.1 167 2 6 11 41.046 82.091 1.17302 18.2 2.0 1.8 6.1 168 0 4 16 41.131 82.262 1.17103 15.6 1.7 1.5 6.1 169 4 0 2 41.345 82.691 1.16604 40.6 4.4 4.0 6.1 170 4 1 2 41.587 83.174 1.16049 19.7 2.1 1.9 6.1 171 4 0 3 41.757 83.515 1.15661 9.8 1.1 1.0 6.1 172 2 2 15 41.89 83.78 1.15362 36.7 4.0 3.6 6.1 173 4 2 1 42.064 84.128 1.14975 12.8 1.4 1.3 6.1 174 2 7 10 42.454 84.908 1.14116 33.7 3.6 3.3 6.1 175 4 1 4 42.574 85.149 1.13855 10.5 1.1 1.0 6.1 176 3 5 9 42.855 85.711 1.13251 12.3 1.3 1.2 6.1 177 2 9 4 43.255 86.51 1.12409 36.7 4.0 3.6 6.1 178 4 1 5 43.313 86.626 1.12289 22.5 2.4 2.2 6.1 179 2 1 16 43.714 87.427 1.11464 10.2 1.1 1.0 6.2 180 1 9 9 43.949 87.899 1.10988 16.6 1.8 1.6 6.2 181 4 3 4 44.496 88.991 1.09906 21.9 2.4 2.1 6.2 182 1 5 16 44.843 89.686 1.09234 21.8 2.4 2.1 6.2 183 2 9 6 44.893 89.786 1.09138 14.3 1.6 1.4 6.2 184 4 2 6 44.934 89.867 1.09061 21.5 2.3 2.1 6.2 Reference: Chichagov A.V. et al. Information-Calculating System on Crystal Structure Data of Minerals (MINCRYST) - Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian) |