Institute of Experimental Mineralogy
                 Russian Academy of Sciences
     -------------------------------------------------
           142432, Chernogolovka, Moscow district
             A.V. Chichagov  +7(496)52-22320

                            ***

          ***      W W W - X R A Y P O L       ***
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HILAIRITE

7, K-analogue

K(1.48)Na(0.09)H(0.1)ZrSi(3)O(9)


Hexagonal  R 3  Z = 6

R =0.0526          NR =1765

28 .11 .11

Ref.Str.:

         Pekov I.V., Grigoryeva N.V., Zubkova N.V., Turchkova A.G.,

         Pushcharovsky D.Y., (2010) * Kristallogr., 55, 1091-1100

         R: Sample was synthesized by cation exchange at 150 C.

         Sample locality Kirovskii  mine, Khibiny alkaline complex,

         Kola Peninsula, Russia.  N.A.D.

                   Initial data from BDM-file 

   Lattice parameters (cub. angs.,degr.):

             a =  10.3804   alpha =   90.0 
             b =  10.3804   beta  =   90.0 
             c =  14.9541   gamma =  120.0 

    Unit cell volume (cub. angs.) =  1395.47

    Molar volume ( cub.cm/mol.) =   140.09

  Co-ordinates, thermal parameters, occupation for atomic positions:

NoP   x/a     y/b     z/c    B(j)   atom  / occupation

   1 0.0     0.0     0.9241   0.0    K     = 1.0 , K     = 0.0 
   2 0.3354  0.8962  0.0871   0.0    K     = 0.87, Na    = 0.06
   3 0.0     0.0     0.1895   0.0    Zr    = 1.00
   4 0.3333  0.6667  0.3352   0.0    Zr    = 1.00
   5 0.3184  0.2124  0.0759   0.0    Si    = 1.00
   6 0.0634  0.7211  0.2465   0.0    Si    = 1.00
   7 0.1839  0.0573  0.1076   0.0    O     = 1.00
   8 0.2206  0.7394  0.2563   0.0    O     = 1.00
   9 0.1274  0.1858  0.2673   0.0    O     = 1.00
  10 0.4072  0.8575  0.4145   0.0    O     = 1.00
  11 0.9497  0.5858  0.3074   0.0    O     = 1.00
  12 0.3289  0.3495  0.14     0.0    O     = 1.00


  Co-ordinates for all atomic positions :

   No       NoP      x/a        y/b       z/c 

     1       1     0.0        0.0        0.9241
     2       2     0.3354     0.8962     0.0871
     3       3     0.0        0.0        0.1895
     4       4     0.3333     0.6667     0.3352
     5       5     0.3184     0.2124     0.0759
     6       6     0.0634     0.7211     0.2465
     7       7     0.1839     0.0573     0.1076
     8       8     0.2206     0.7394     0.2563
     9       9     0.1274     0.1858     0.2673
    10      10     0.4072     0.8575     0.4145
    11      11     0.9497     0.5858     0.3074
    12      12     0.3289     0.3495     0.14  
    13       2     0.1038     0.4392     0.0871
    14       2     0.5608     0.6646     0.0871
    15       5     0.7876     0.106      0.0759
    16       5     0.894      0.6816     0.0759
    17       6     0.2789     0.3423     0.2465
    18       6     0.6577     0.9366     0.2465
    19       7     0.9427     0.1266     0.1076
    20       7     0.8734     0.8161     0.1076
    21       8     0.2606     0.4812     0.2563
    22       8     0.5188     0.7794     0.2563
    23       9     0.8142     0.9416     0.2673
    24       9     0.0584     0.8726     0.2673
    25      10     0.1425     0.5497     0.4145
    26      10     0.4503     0.5928     0.4145
    27      11     0.4142     0.3639     0.3074
    28      11     0.6361     0.0503     0.3074
    29      12     0.6505     0.9794     0.14  
    30      12     0.0206     0.6711     0.14  
    31       1     0.6667     0.3333     0.2574
    32       1     0.3333     0.6667     0.5908
    33       2     0.7705     0.7725     0.4204
    34       2     0.8941     0.3313     0.7538
    35       3     0.6667     0.3333     0.5228
    36       3     0.3333     0.6667     0.8561
    37       4     0.0        0.0        0.6685
    38       4     0.6667     0.3333     0.0018
    39       5     0.4543     0.4393     0.4092
    40       5     0.2273     0.3483     0.7426
    41       6     0.9456     0.6756     0.5798
    42       6     0.991      0.6033     0.9132
    43       7     0.6094     0.4599     0.4409
    44       7     0.2067     0.4828     0.7743
    45       8     0.9273     0.8145     0.5896
    46       8     0.8521     0.4461     0.923 
    47       9     0.4809     0.2749     0.6006
    48       9     0.3917     0.5393     0.934 
    49      10     0.8092     0.883      0.7478
    50      10     0.7836     0.2595     0.0812
    51      11     0.0809     0.6972     0.6407
    52      11     0.9694     0.717      0.9741
    53      12     0.3172     0.3127     0.4733
    54      12     0.3539     0.3378     0.8067
    55       2     0.2275     0.9979     0.4204
    56       2     0.6687     0.5629     0.7538
    57       2     0.0021     0.2295     0.4204
    58       2     0.4371     0.1058     0.7538
    59       5     0.5607     0.0149     0.4092
    60       5     0.6517     0.8791     0.7426
    61       5     0.9851     0.5457     0.4092
    62       5     0.1209     0.7727     0.7426
    63       6     0.3244     0.2699     0.5798
    64       6     0.3967     0.3878     0.9132
    65       6     0.7301     0.0544     0.5798
    66       6     0.6122     0.0089     0.9132
    67       7     0.5401     0.1494     0.4409
    68       7     0.5172     0.724      0.7743
    69       7     0.8506     0.3906     0.4409
    70       7     0.276      0.7932     0.7743
    71       8     0.1855     0.1127     0.5896
    72       8     0.5539     0.4061     0.923 
    73       8     0.8873     0.0727     0.5896
    74       8     0.5939     0.1478     0.923 
    75       9     0.7251     0.2059     0.6006
    76       9     0.4607     0.8525     0.934 
    77       9     0.7941     0.5191     0.6006
    78       9     0.1475     0.6082     0.934 
    79      10     0.117      0.9261     0.7478
    80      10     0.7405     0.5242     0.0812
    81      10     0.0739     0.1908     0.7478
    82      10     0.4758     0.2164     0.0812
    83      11     0.3028     0.3836     0.6407
    84      11     0.283      0.2525     0.9741
    85      11     0.6164     0.9191     0.6407
    86      11     0.7475     0.0305     0.9741
    87      12     0.6873     0.0044     0.4733
    88      12     0.6622     0.0162     0.8067
    89      12     0.9956     0.6828     0.4733
    90      12     0.9838     0.646      0.8067


X-ray density (g/cm cub.)   =      2.8 

MU (1/cm) =     213.999    Mass attenuation coefficient (cm**2/g) =     76.435

 Selected interatomic distances (cation-anion,anion-anion):

 NoP    Atom              Rad.sph.      C.N.    Distance     NoP N.
                           (angs.)               (angs.)

    1   K    ,K              3.228        9
                                                 3.2237       7
                                                 3.2237       7
                                                 3.2237       7
                                                 3.153       10
                                                 2.8912      11
                                                 3.153       10
                                                 3.153       10
                                                 2.891       11
                                                 2.8911      11
    2   K    ,Na             3.228        6
                                                 2.8273       7
                                                 2.9209       8
                                                 3.0406      12
                                                 3.0212      12
                                                 2.7809       9
                                                 2.8866      10
    3    Zr                  2.616        6
                                                 2.0884       7
                                                 2.0671       9
                                                 2.0883       7
                                                 2.0884       7
                                                 2.067        9
                                                 2.0671       9
    4    Zr                  2.616        6
                                                 2.0528       8
                                                 2.0976      10
                                                 2.053        8
                                                 2.053        8
                                                 2.0976      10
                                                 2.0978      10
    5    Si                  2.1          4
                                                 1.5869       7
                                                 1.6736      12
                                                 1.6159      10
                                                 1.6673      11
    6    Si                  2.1          4
                                                 1.5525       8
                                                 1.5929      11
                                                 1.6291       9
                                                 1.6651      12
    7    O                   3.264        7
                                                 2.9341       9
                                                 2.6711      12
                                                 2.9303       7
                                                 2.9303       7
                                                 2.9289       9
                                                 2.6574      10
                                                 2.6582      11
    8    O                   3.264        7
                                                 2.9115      10
                                                 2.5593      11
                                                 2.9102       8
                                                 2.9102       8
                                                 2.6648       9
                                                 2.9216      10
                                                 2.5229      12
    9    O                   3.264        7
                                                 2.9341       7
                                                 2.7078      12
                                                 2.9289       7
                                                 2.6648       8
                                                 2.9588       9
                                                 2.9588       9
                                                 2.6714      11
   10    O                   3.264        7
                                                 2.9115       8
                                                 2.9216       8
                                                 2.9966      10
                                                 2.9966      10
                                                 2.7315      11
                                                 2.6575       7
                                                 2.668       12
   11    O                   3.264        6
                                                 2.5593       8
                                                 2.6714       9
                                                 2.7315      10
                                                 2.6345      12
                                                 2.6581       7
                                                 2.6304      12
   12    O                   3.264        6
                                                 2.6711       7
                                                 2.7078       9
                                                 2.5229       8
                                                 2.6345      11
                                                 2.668       10
                                                 2.6305      11

  X-ray diffraction powder data (II),  X-Ray W.L. =   1.54056(angs.):

  No   H   K   L   Theta 2*Theta    S       LPG   MF        F          I int.
                    ( degree )                                         *100

    1   1   0   1  5.738  11.476   0.065  197.13    6        6.5        2.5
    2   1   0  -2  7.701  15.401   0.087  108.44    6      254.8     2170.0
    3   1   1   0  8.535  17.07    0.096   87.86    6      205.6     1144.6
    4   0   0   3  8.889  17.779   0.1     80.82    2       48.3       19.3
    5   2   0  -1 10.308  20.616   0.116   59.55    6       22.9        9.6
    6   2   0   2 11.534  23.068   0.13    47.14    6       62.4       56.5
    7   1   1  -3 12.372  24.744   0.139   40.7     6      187.0      438.3
    8   1   1   3 12.372  24.744   0.139   40.7     6      163.9      336.8
    9   1   0   4 12.894  25.788   0.145   37.31    6      184.4      390.7
   10   1   2  -1 13.443  26.886   0.151   34.16    6      118.6      148.1
   11   2   1   1 13.443  26.886   0.151   34.16    6      136.2      195.3
   12   1   2   2 14.419  28.838   0.162   29.43    6      238.6      516.3
   13   2   1  -2 14.419  28.838   0.162   29.43    6      355.2     1143.9
   14   3   0   0 14.895  29.791   0.167   27.45    6      294.2      732.3
   15   2   0  -4 15.545  31.09    0.174   25.05    6      354.2      968.2
   16   1   0  -5 15.749  31.498   0.176   24.36    6       32.9        8.1
   17   2   2   0 17.267  34.534   0.193   19.95    6      193.6      230.4
   18   3   0  -3 17.453  34.906   0.195   19.49    6      131.9      104.5
   19   3   0   3 17.453  34.906   0.195   19.49    6      104.4       65.4
   20   1   2  -4 17.839  35.678   0.199   18.58    6      133.8      102.5
   21   2   1   4 17.839  35.678   0.199   18.58    6      255.4      373.3
   22   0   0   6 18.002  36.005   0.201   18.21    2      302.2      170.8
   23   2   0   5 18.02   36.04    0.201   18.17    6       11.8        0.8
   24   1   3   1 18.253  36.505   0.203   17.67    6       38.6        8.1
   25   3   1  -1 18.253  36.505   0.203   17.67    6        0.9        0.0
   26   1   3  -2 19.006  38.012   0.211   16.16    6      139.4       96.8
   27   3   1   2 19.006  38.012   0.211   16.16    6      111.8       62.3
   28   2   2  -3 19.55   39.101   0.217   15.18    6      126.7       75.1
   29   2   2   3 19.55   39.101   0.217   15.18    6      118.5       65.7
   30   1   1  -6 20.05   40.101   0.223   14.36    6      201.0      178.6
   31   1   1   6 20.05   40.101   0.223   14.36    6      134.4       79.9
   32   1   2   5 20.066  40.133   0.223   14.33    6       67.1       19.9
   33   2   1  -5 20.066  40.133   0.223   14.33    6       19.7        1.7
   34   4   0   1 20.279  40.558   0.225   14.0     6      108.2       50.5
   35   4   0  -2 20.97   41.941   0.232   12.99    6       58.1       13.5
   36   1   0   7 21.753  43.506   0.241   11.96    6       36.3        4.8
   37   1   3   4 21.799  43.597   0.241   11.91    6      258.3      244.8
   38   3   1  -4 21.799  43.597   0.241   11.91    6      342.1      429.4
   39   2   3  -1 22.15   44.299   0.245   11.49    6      125.2       55.5
   40   3   2   1 22.15   44.299   0.245   11.49    6      121.5       52.2
   41   2   3   2 22.795  45.59    0.251   10.76    6      189.5      119.1
   42   3   2  -2 22.795  45.59    0.251   10.76    6      105.7       37.1
   43   1   4   0 23.12   46.24    0.255   10.43    6      227.6      166.3
   44   4   1   0 23.12   46.24    0.255   10.43    6      170.5       93.4
   45   2   0  -7 23.529  47.059   0.259   10.02    6      114.1       40.2
   46   4   0   4 23.572  47.144   0.26     9.98    6      238.6      175.0
   47   3   0  -6 23.702  47.405   0.261    9.85    6      163.3       81.0
   48   3   0   6 23.702  47.405   0.261    9.85    6      135.9       56.0
   49   1   3  -5 23.717  47.433   0.261    9.84    6       48.7        7.2
   50   3   1   5 23.717  47.433   0.261    9.84    6       45.6        6.3
   51   1   0  -8 24.891  49.782   0.273    8.82    6      121.2       39.9
   52   1   4  -3 24.959  49.918   0.274    8.76    6       78.6       16.7
   53   1   4   3 24.959  49.918   0.274    8.76    6        2.8        0.0
   54   4   1  -3 24.959  49.918   0.274    8.76    6      102.4       28.3
   55   4   1   3 24.959  49.918   0.274    8.76    6       49.7        6.7
   56   1   2  -7 25.208  50.417   0.276    8.57    6      195.6      101.0
   57   2   1   7 25.208  50.417   0.276    8.57    6      189.9       95.2
   58   2   3  -4 25.249  50.498   0.277    8.54    6      173.1       78.8
   59   3   2   4 25.249  50.498   0.277    8.54    6      171.8       77.7
   60   2   2  -6 25.373  50.746   0.278    8.44    6      199.8      103.8
   61   2   2   6 25.373  50.746   0.278    8.44    6      181.9       86.1
   62   4   0  -5 25.386  50.773   0.278    8.43    6      191.7       95.5
   63   5   0  -1 25.563  51.127   0.28     8.3     6       18.4        0.9
   64   5   0   2 26.144  52.289   0.286    7.88    6      102.6       25.5
   65   3   3   0 26.438  52.876   0.289    7.69    6      275.4      179.6
   66   2   0   8 26.506  53.012   0.29     7.64    6      275.6      178.8
   67   2   3   5 26.98   53.96    0.294    7.34    6       38.8        3.4
   68   3   2  -5 26.98   53.96    0.294    7.34    6      124.7       35.1
   69   2   4   1 27.15   54.3     0.296    7.24    6       12.0        0.3
   70   4   2  -1 27.15   54.3     0.296    7.24    6       43.3        4.2
   71   0   0   9 27.619  55.238   0.301    6.96    2      118.3       10.0
   72   2   4  -2 27.707  55.415   0.302    6.91    6      241.8      124.4
   73   4   2   2 27.707  55.415   0.302    6.91    6      187.1       74.5
   74   1   2   8 28.055  56.11    0.305    6.72    6      230.8      110.3
   75   2   1  -8 28.055  56.11    0.305    6.72    6       93.1       17.9
   76   3   3  -3 28.118  56.236   0.306    6.68    6      182.4       68.5
   77   3   3   3 28.118  56.236   0.306    6.68    6      156.3       50.3
   78   1   3   7 28.348  56.695   0.308    6.56    6       90.5       16.6
   79   3   1  -7 28.348  56.695   0.308    6.56    6       96.8       18.9
   80   5   0  -4 28.385  56.77    0.309    6.54    6      365.9      269.7
   81   1   5  -1 28.675  57.351   0.311    6.39    6       84.5       14.1
   82   5   1   1 28.675  57.351   0.311    6.39    6       70.0        9.6
   83   1   1  -9 29.128  58.256   0.316    6.17    6       71.3        9.7
   84   1   1   9 29.128  58.256   0.316    6.17    6      133.5       33.9
   85   1   5   2 29.214  58.428   0.317    6.13    6      165.0       51.4
   86   5   1  -2 29.214  58.428   0.317    6.13    6      196.9       73.2
   87   4   0   7 29.833  59.666   0.323    5.85    6       79.7       11.4
   88   2   4   4 29.869  59.738   0.323    5.83    6      185.6       61.9
   89   4   2  -4 29.869  59.738   0.323    5.83    6      105.9       20.1
   90   1   4  -6 29.98   59.96    0.324    5.78    6      133.5       31.7
   91   1   4   6 29.98   59.96    0.324    5.78    6       60.7        6.6
   92   4   1  -6 29.98   59.96    0.324    5.78    6      169.4       51.1
   93   4   1   6 29.98   59.96    0.324    5.78    6       57.9        6.0
   94   5   0   5 29.992  59.984   0.324    5.78    6       20.6        0.8
   95   6   0   0 30.938  61.876   0.334    5.39    6      186.6       57.8
   96   1   3  -8 30.999  61.998   0.334    5.37    6      313.1      162.2
   97   3   1   8 30.999  61.998   0.334    5.37    6      144.5       34.5
   98   2   3  -7 31.274  62.549   0.337    5.26    6      181.8       53.6
   99   3   2   7 31.274  62.549   0.337    5.26    6      140.4       32.0
  100   1   5  -4 31.31   62.619   0.337    5.25    6      160.6       41.7
  101   5   1   4 31.31   62.619   0.337    5.25    6      168.5       46.0
  102   2   4  -5 31.429  62.858   0.338    5.21    6       62.6        6.3
  103   4   2   5 31.429  62.858   0.338    5.21    6       36.1        2.1
  104   1   0  10 31.478  62.956   0.339    5.19    6      115.5       21.3
  105   3   4  -1 31.583  63.167   0.34     5.15    6       19.3        0.6
  106   4   3   1 31.583  63.167   0.34     5.15    6       40.8        2.6
  107   3   0  -9 32.011  64.022   0.344    5.0     6       57.1        5.0
  108   3   0   9 32.011  64.022   0.344    5.0     6       78.8        9.6
  109   3   4   2 32.092  64.185   0.345    4.97    6      123.2       23.3
  110   4   3  -2 32.092  64.185   0.345    4.97    6      169.8       44.2
  111   2   5   0 32.351  64.702   0.347    4.89    6      200.1       60.3
  112   5   2   0 32.351  64.702   0.347    4.89    6      293.1      129.4
  113   4   0  -8 32.411  64.821   0.348    4.87    6      191.4       55.0
  114   6   0  -3 32.468  64.936   0.348    4.85    6       33.5        1.7
  115   6   0   3 32.468  64.936   0.348    4.85    6       71.6        7.7
  116   3   3  -6 32.819  65.638   0.352    4.74    6      177.6       46.1
  117   3   3   6 32.819  65.638   0.352    4.74    6      215.3       67.7
  118   1   5   5 32.83   65.661   0.352    4.74    6       42.2        2.6
  119   5   1  -5 32.83   65.661   0.352    4.74    6       88.8       11.5
  120   2   0 -10 32.878  65.756   0.352    4.72    6      103.0       15.4
  121   2   2  -9 33.399  66.798   0.357    4.57    6      108.6       16.6
  122   2   2   9 33.399  66.798   0.357    4.57    6       39.8        2.2
  123   2   3   8 33.79   67.58    0.361    4.46    6      151.6       31.6
  124   3   2  -8 33.79   67.58    0.361    4.46    6      220.8       66.9
  125   2   5  -3 33.846  67.693   0.362    4.44    6       96.8       12.8
  126   2   5   3 33.846  67.693   0.362    4.44    6      115.8       18.3
  127   5   2  -3 33.846  67.693   0.362    4.44    6       81.6        9.1
  128   5   2   3 33.846  67.693   0.362    4.44    6      114.8       18.0
  129   5   0  -7 34.053  68.106   0.363    4.38    6       58.5        4.6
  130   3   4  -4 34.087  68.174   0.364    4.38    6      186.8       47.0
  131   4   3   4 34.087  68.174   0.364    4.38    6      116.0       18.1
  132   1   2 -10 34.248  68.496   0.365    4.33    6      236.2       74.5
  133   2   1  10 34.248  68.496   0.365    4.33    6      157.6       33.2
  134   1   6   1 34.349  68.698   0.366    4.31    6      187.6       46.7
  135   6   1  -1 34.349  68.698   0.366    4.31    6      246.5       80.7
  136   1   6  -2 34.837  69.673   0.371    4.18    6      202.5       52.9
  137   6   1   2 34.837  69.673   0.371    4.18    6      261.9       88.5
  138   1   0 -11 34.963  69.926   0.372    4.15    6      117.6       17.7
  139   2   4   7 35.401  70.802   0.376    4.05    6      108.8       14.8
  140   4   2  -7 35.401  70.802   0.376    4.05    6       51.6        3.3
  141   3   4   5 35.546  71.093   0.377    4.02    6       24.3        0.7
  142   4   3  -5 35.546  71.093   0.377    4.02    6       48.0        2.8
  143   2   0  11 36.296  72.592   0.384    3.86    6      167.0       33.2
  144   4   4   0 36.416  72.832   0.385    3.83    6      248.3       72.8
  145   5   0   8 36.472  72.945   0.386    3.82    6      318.9      119.8
  146   1   5  -7 36.727  73.454   0.388    3.77    6      105.7       13.0
  147   5   1   7 36.727  73.454   0.388    3.77    6      133.8       20.8
  148   1   6   4 36.76   73.519   0.388    3.77    6       83.5        8.1
  149   6   1  -4 36.76   73.519   0.388    3.77    6       34.3        1.4
  150   6   0  -6 36.859  73.719   0.389    3.75    6      123.6       17.6
  151   6   0   6 36.859  73.719   0.389    3.75    6      130.0       19.5
  152   1   3  10 36.916  73.832   0.39     3.74    6      137.4       21.7
  153   3   1 -10 36.916  73.832   0.39     3.74    6       48.3        2.7
  154   3   5   1 37.013  74.027   0.391    3.72    6       98.7       11.1
  155   5   3  -1 37.013  74.027   0.391    3.72    6       77.1        6.8
  156   7   0   1 37.013  74.027   0.391    3.72    6        6.9        0.1
  157   1   4  -9 37.411  74.822   0.394    3.64    6      125.9       17.8
  158   1   4   9 37.411  74.822   0.394    3.64    6      134.7       20.4
  159   4   1  -9 37.411  74.822   0.394    3.64    6       55.3        3.4
  160   4   1   9 37.411  74.822   0.394    3.64    6      178.9       35.9
  161   3   5  -2 37.487  74.973   0.395    3.63    6      102.1       11.7
  162   5   3   2 37.487  74.973   0.395    3.63    6      114.5       14.7
  163   7   0  -2 37.487  74.973   0.395    3.63    6       22.9        0.6
  164   1   2  11 37.609  75.219   0.396    3.61    6      106.2       12.5
  165   2   1 -11 37.609  75.219   0.396    3.61    6      168.1       31.4
  166   2   4  -8 37.784  75.567   0.398    3.58    6       47.8        2.5
  167   4   2   8 37.784  75.567   0.398    3.58    6      117.4       15.2
  168   4   4  -3 37.838  75.675   0.398    3.57    6       23.7        0.6
  169   4   4   3 37.838  75.675   0.398    3.57    6       56.3        3.5
  170   2   5  -6 38.166  76.332   0.401    3.52    6      155.2       26.1
  171   2   5   6 38.166  76.332   0.401    3.52    6       54.0        3.2
  172   5   2  -6 38.166  76.332   0.401    3.52    6       74.4        6.0
  173   5   2   6 38.166  76.332   0.401    3.52    6       30.3        1.0
  174   1   6  -5 38.177  76.353   0.401    3.52    6      164.1       29.2
  175   6   1   5 38.177  76.353   0.401    3.52    6      236.0       60.3
  176   0   0  12 38.179  76.357   0.401    3.51    2      317.0       36.3
  177   4   0  10 38.222  76.443   0.402    3.51    6      125.7       17.1
  178   2   6  -1 38.318  76.636   0.402    3.49    6       92.9        9.3
  179   6   2   1 38.318  76.636   0.402    3.49    6       77.7        6.5
  180   2   6   2 38.786  77.572   0.407    3.42    6      178.9       33.7
  181   6   2  -2 38.786  77.572   0.407    3.42    6      153.6       24.9
  182   1   5   8 39.08   78.159   0.409    3.38    6      130.1       17.6
  183   5   1  -8 39.08   78.159   0.409    3.38    6      128.7       17.2
  184   3   4  -7 39.328  78.657   0.411    3.34    6       61.9        3.9
  185   4   3   7 39.328  78.657   0.411    3.34    6       20.9        0.5
  186   3   5   4 39.36   78.721   0.412    3.34    6      128.7       17.0
  187   5   3  -4 39.36   78.721   0.412    3.34    6      180.0       33.3
  188   7   0   4 39.36   78.721   0.412    3.34    6      270.0       75.0
  189   1   1 -12 39.471  78.941   0.413    3.32    6      190.8       37.3
  190   1   1  12 39.471  78.941   0.413    3.32    6      133.4       18.2
  191   2   3 -10 39.513  79.026   0.413    3.32    6       94.1        9.1
  192   3   2  10 39.513  79.026   0.413    3.32    6      130.0       17.3
  193   3   3  -9 39.998  79.996   0.417    3.25    6      126.7       16.1
  194   3   3   9 39.998  79.996   0.417    3.25    6       87.3        7.6
  195   1   3 -11 40.193  80.385   0.419    3.23    6       92.3        8.5
  196   3   1  11 40.193  80.385   0.419    3.23    6      108.0       11.6
  197   1   7   0 40.309  80.617   0.42     3.22    6      133.7       17.7
  198   7   1   0 40.309  80.617   0.42     3.22    6      101.1       10.1
  199   2   6  -4 40.642  81.284   0.423    3.18    6      148.4       21.6
  200   6   2   4 40.642  81.284   0.423    3.18    6      149.8       22.0
  201   3   5  -5 40.749  81.499   0.424    3.17    6       21.6        0.5
  202   5   3   5 40.749  81.499   0.424    3.17    6       46.7        2.1
  203   7   0  -5 40.749  81.499   0.424    3.17    6       21.9        0.5
  204   4   0 -11 41.468  82.936   0.43     3.09    6       75.6        5.4
  205   3   4   8 41.638  83.276   0.431    3.07    6      108.3       11.1
  206   4   3  -8 41.638  83.276   0.431    3.07    6      106.6       10.8
  207   1   7  -3 41.691  83.381   0.432    3.07    6      128.2       15.5
  208   1   7   3 41.691  83.381   0.432    3.07    6      134.1       17.0
  209   7   1  -3 41.691  83.381   0.432    3.07    6      112.8       12.0
  210   7   1   3 41.691  83.381   0.432    3.07    6       93.8        8.3
  211   1   6   7 41.883  83.767   0.433    3.05    6      132.1       16.4
  212   6   1  -7 41.883  83.767   0.433    3.05    6      237.5       53.0
  213   4   4  -6 42.011  84.022   0.434    3.04    6       98.5        9.1
  214   4   4   6 42.011  84.022   0.434    3.04    6       42.3        1.7
  215   2   6   5 42.022  84.043   0.435    3.04    6       58.4        3.2
  216   6   2  -5 42.022  84.043   0.435    3.04    6       50.0        2.3
  217   3   0 -12 42.023  84.047   0.435    3.04    6       86.3        7.0
  218   3   0  12 42.023  84.047   0.435    3.04    6       93.0        8.1
  219   5   0 -10 42.065  84.131   0.435    3.03    6      132.5       16.4
  220   4   5  -1 42.16   84.319   0.436    3.02    6       78.0        5.7
  221   5   4   1 42.16   84.319   0.436    3.02    6      121.9       13.8
  222   1   0  13 42.461  84.921   0.438    3.0     6      151.4       21.2
  223   4   5   2 42.618  85.235   0.44     2.98    6       73.1        4.9
  224   5   4  -2 42.618  85.235   0.44     2.98    6       38.2        1.3
  225   2   3  11 42.737  85.473   0.441    2.97    6      117.2       12.6
  226   3   2 -11 42.737  85.473   0.441    2.97    6      156.5       22.5
  227   3   6   0 42.852  85.703   0.441    2.97    6      152.7       21.3
  228   6   3   0 42.852  85.703   0.441    2.97    6      126.7       14.7
  229   2   2 -12 43.29   86.58    0.445    2.93    6       40.2        1.5
  230   2   2  12 43.29   86.58    0.445    2.93    6      144.5       18.9
  231   2   4  10 43.332  86.663   0.445    2.93    6       72.1        4.7
  232   4   2 -10 43.332  86.663   0.445    2.93    6      142.7       18.4
  233   8   0  -1 43.426  86.851   0.446    2.92    6       52.0        2.4
  234   2   0 -13 43.726  87.451   0.449    2.9     6       44.2        1.7
  235   6   0  -9 43.809  87.618   0.449    2.9     6       64.9        3.8
  236   6   0   9 43.809  87.618   0.449    2.9     6       13.8        0.2
  237   8   0   2 43.882  87.764   0.45     2.89    6       54.6        2.7
  238   1   6  -8 44.17   88.339   0.452    2.87    6       61.0        3.3
  239   6   1   8 44.17   88.339   0.452    2.87    6      109.3       10.6
  240   3   6  -3 44.222  88.443   0.453    2.87    6       38.8        1.3
  241   3   6   3 44.222  88.443   0.453    2.87    6       29.2        0.8
  242   6   3  -3 44.222  88.443   0.453    2.87    6       47.9        2.0
  243   6   3   3 44.222  88.443   0.453    2.87    6       71.7        4.5
  244   3   5   7 44.413  88.827   0.454    2.86    6      173.0       26.4
  245   5   3  -7 44.413  88.827   0.454    2.86    6       57.2        2.9
  246   7   0   7 44.413  88.827   0.454    2.86    6       82.3        6.0
  247   4   5  -4 44.445  88.889   0.455    2.86    6      195.1       33.5
  248   5   4   4 44.445  88.889   0.455    2.86    6      266.8       62.7
  249   1   5 -10 44.594  89.189   0.456    2.85    6       35.4        1.1
  250   5   1  10 44.594  89.189   0.456    2.85    6       85.6        6.4
  251   2   7   1 44.688  89.377   0.456    2.84    6       44.2        1.7
  252   7   2  -1 44.688  89.377   0.456    2.84    6       58.5        3.0
  253   1   2 -13 44.988  89.976   0.459    2.83    6       20.5        0.4
  254   2   1  13 44.988  89.976   0.459    2.83    6       88.5        6.8


  X-ray diffraction powder data (I)...X-Ray wave length =  1.54056 (angs.):

  No   H   K   L   Theta 2*Theta    d           I int   I int.n.  I p.h.n.   H(Si)
                    ( degree )   (angstrem)     *100                         *100

    1   1   0   2   7.701  15.401  5.74854     2170.0    100.0    100.0     5.6
    2   1   1   0   8.535  17.07   5.1902      1144.6     52.7     52.7     5.6
    3   2   0   2  11.534  23.068  3.85234       56.5      2.6      2.6     5.6
    4   1   1   3  12.372  24.744  3.59517      775.1     35.7     35.5     5.6
    5   1   0   4  12.894  25.788  3.45192      390.7     18.0     17.9     5.6
    6   2   1   1  13.443  26.886  3.31333      343.4     15.8     15.7     5.6
    7   2   1   2  14.419  28.838  3.09336     1660.3     76.5     75.8     5.6
    8   3   0   0  14.895  29.791  2.99656      732.3     33.7     33.4     5.6
    9   2   0   4  15.545  31.09   2.87427      968.2     44.6     44.1     5.6
   10   2   2   0  17.267  34.534  2.5951       230.4     10.6     10.5     5.7
   11   3   0   3  17.453  34.906  2.56823      169.9      7.8      7.7     5.7
   12   2   1   4  17.839  35.678  2.51445      475.9     21.9     21.6     5.7
   13   0   0   6  18.002  36.005  2.49235      171.6      7.9      7.8     5.7
   14   1   3   2  19.006  38.012  2.36525      159.1      7.3      7.2     5.7
   15   2   2   3  19.55   39.101  2.30184      140.8      6.5      6.4     5.7
   16   1   1   6  20.05   40.101  2.24673      280.1     12.9     12.7     5.7
   17   4   0   1  20.279  40.558  2.22246       50.5      2.3      2.3     5.7
   18   3   1   4  21.799  43.597  2.0743       674.3     31.1     30.4     5.7
   19   2   3   1  22.15   44.299  2.04304      107.8      5.0      4.8     5.7
   20   2   3   2  22.795  45.59   1.98813      156.2      7.2      7.0     5.7
   21   1   4   0  23.12   46.24   1.96171      259.7     12.0     11.7     5.7
   22   2   0   7  23.529  47.059  1.92946       40.2      1.9      1.8     5.7
   23   4   0   4  23.572  47.144  1.92617      175.0      8.1      7.8     5.7
   24   3   0   6  23.702  47.405  1.91618      150.5      6.9      6.7     5.7
   25   1   0   8  24.891  49.782  1.83012       39.9      1.8      1.8     5.7
   26   4   1   3  24.959  49.918  1.82544       51.6      2.4      2.3     5.7
   27   1   2   7  25.208  50.417  1.80854      196.2      9.0      8.8     5.8
   28   2   3   4  25.249  50.498  1.80582      156.4      7.2      7.0     5.8
   29   2   2   6  25.373  50.746  1.79758      285.4     13.2     12.7     5.8
   30   5   0   2  26.144  52.289  1.74811       25.5      1.2      1.1     5.8
   31   3   3   0  26.438  52.876  1.73007      179.6      8.3      8.0     5.8
   32   2   0   8  26.506  53.012  1.72596      178.8      8.2      8.0     5.8
   33   3   2   5  26.98   53.96   1.69784       38.6      1.8      1.7     5.8
   34   2   4   2  27.707  55.415  1.65667      198.9      9.2      8.8     5.8
   35   1   2   8  28.055  56.11   1.63778      128.2      5.9      5.7     5.8
   36   3   3   3  28.118  56.236  1.63442      118.8      5.5      5.3     5.8
   37   3   1   7  28.348  56.695  1.62226       35.5      1.6      1.6     5.8
   38   5   0   4  28.385  56.77   1.6203       269.7     12.4     11.9     5.8
   39   1   5   1  28.675  57.351  1.60527       23.7      1.1      1.0     5.8
   40   1   1   9  29.128  58.256  1.58245       43.5      2.0      1.9     5.8
   41   5   1   2  29.214  58.428  1.57822      124.6      5.7      5.5     5.8
   42   2   4   4  29.869  59.738  1.54668       82.0      3.8      3.6     5.8
   43   4   1   6  29.98   59.96   1.5415        96.2      4.4      4.2     5.8
   44   6   0   0  30.938  61.876  1.49828       57.8      2.7      2.5     5.8
   45   1   3   8  30.999  61.998  1.49561      196.7      9.1      8.6     5.8
   46   2   3   7  31.274  62.549  1.48377       85.5      3.9      3.8     5.8
   47   5   1   4  31.31   62.619  1.48227       87.7      4.0      3.9     5.8
   48   4   3   2  32.092  64.185  1.44985       67.5      3.1      3.0     5.9
   49   5   2   0  32.351  64.702  1.4395       189.7      8.7      8.3     5.9
   50   4   0   8  32.411  64.821  1.43714       55.0      2.5      2.4     5.9
   51   3   3   6  32.819  65.638  1.42122      127.9      5.9      5.6     5.9
   52   3   2   8  33.79   67.58   1.38502       98.5      4.5      4.3     5.9
   53   5   2   3  33.846  67.693  1.38299       58.3      2.7      2.5     5.9
   54   3   4   4  34.087  68.174  1.3744        65.2      3.0      2.8     5.9
   55   1   2  10  34.248  68.496  1.36871      107.6      5.0      4.7     5.9
   56   6   1   1  34.349  68.698  1.36519      127.4      5.9      5.5     5.9
   57   6   1   2  34.837  69.673  1.34844      141.3      6.5      6.1     5.9
   58   2   0  11  36.296  72.592  1.30125       33.2      1.5      1.4     6.0
   59   4   4   0  36.416  72.832  1.29755       72.8      3.4      3.1     6.0
   60   5   0   8  36.472  72.945  1.29582      119.8      5.5      5.2     6.0
   61   5   1   7  36.727  73.454  1.28809       33.8      1.6      1.5     6.0
   62   6   0   6  36.859  73.719  1.28411       37.2      1.7      1.6     6.0
   63   1   3  10  36.916  73.832  1.28243       24.4      1.1      1.1     6.0
   64   4   1   9  37.411  74.822  1.26789       77.6      3.6      3.3     6.0
   65   5   3   2  37.487  74.973  1.26571       26.9      1.2      1.2     6.0
   66   2   1  11  37.609  75.219  1.26219       44.0      2.0      1.9     6.0
   67   0   0  12  38.179  76.357  1.24617      162.0      7.5      6.9     6.0
   68   2   6   2  38.786  77.572  1.22967       58.6      2.7      2.5     6.0
   69   1   5   8  39.08   78.159  1.22189       34.9      1.6      1.5     6.0
   70   7   0   4  39.36   78.721  1.21458      125.4      5.8      5.3     6.0
   71   1   1  12  39.471  78.941  1.21174       55.5      2.6      2.4     6.0
   72   3   2  10  39.513  79.026  1.21065       26.3      1.2      1.1     6.0
   73   3   3   9  39.998  79.996  1.19839       23.7      1.1      1.0     6.0
   74   1   7   0  40.309  80.617  1.19071       27.9      1.3      1.2     6.1
   75   6   2   4  40.642  81.284  1.18263       43.5      2.0      1.8     6.1
   76   3   4   8  41.638  83.276  1.15932       21.9      1.0      0.9     6.1
   77   1   7   3  41.691  83.381  1.15813       52.9      2.4      2.2     6.1
   78   6   1   7  41.883  83.767  1.15378       69.4      3.2      2.9     6.1
   79   4   4   6  42.011  84.022  1.15092       31.3      1.4      1.3     6.1
   80   3   2  11  42.737  85.473  1.13505       35.0      1.6      1.5     6.1
   81   3   6   0  42.852  85.703  1.13259       36.0      1.7      1.5     6.1
   82   4   2  10  43.332  86.663  1.1225        23.1      1.1      1.0     6.1
   83   3   5   7  44.413  88.827  1.10067       35.2      1.6      1.5     6.2
   84   5   4   4  44.445  88.889  1.10006       96.2      4.4      4.0     6.2

Reference:
Chichagov A.V. et al.
Information-Calculating System on Crystal Structure Data of Minerals
(MINCRYST)
- Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian)