Institute of Experimental Mineralogy Russian Academy of Sciences ------------------------------------------------- 142432, Chernogolovka, Moscow district A.V. Chichagov +7(496)52-22320 *** *** W W W - X R A Y P O L *** *********************** GAIDONNAYITE 1, t-catapleiite, f-catapleiite Na(2)ZrSi(3)O(9).2H(2)O Orthorhombic * P2(1)nb Z = 4 R =0.039 NR =1211 1 .2 .1990 Ref.Str.: G.Y.Chao (1985) * Canad. Mineral., 23, 11-15 Reserv: See U(ij) in the original Initial data from BDM-file Lattice parameters (cub. angs.,degr.): a = 11.74 alpha = 90.0 b = 12.82 beta = 90.0 c = 6.691 gamma = 90.0 Unit cell volume (cub. angs.) = 1007.04 Molar volume ( cub.cm/mol.) = 151.64 Co-ordinates, thermal parameters, occupation for atomic positions: NoP x/a y/b z/c B(j) atom / occupation 1 0.7466 0.1567 0.4307 0.0 Na = 1.00 2 0.9959 0.3876 0.3316 0.0 Na = 1.00 3 0.25 0.0531 0.151 0.0 Zr = 1.00 4 0.2809 0.2883 0.3927 0.0 Si = 1.00 5 0.4981 0.418 0.3911 0.0 Si = 1.00 6 0.7144 0.3918 0.1501 0.0 Si = 1.00 7 0.2116 0.3958 0.3644 0.0 O = 1.00 8 0.4173 0.3155 0.4186 0.0 O = 1.00 9 0.7417 0.2699 0.1017 0.0 O = 1.00 10 0.2654 0.2096 0.2065 0.0 O = 1.00 11 0.4225 0.0194 0.1562 0.0 O = 1.00 12 0.5759 0.394 0.196 0.0 O = 1.00 13 0.0743 0.0706 0.0898 0.0 O = 1.00 14 0.2398 0.0361 0.4583 0.0 O = 1.00 15 0.7817 0.4258 0.3474 0.0 O = 1.00 16 0.5397 0.1326 0.4739 0.0 O = 1.00 17 0.9558 0.1991 0.3821 0.0 O = 1.00 Co-ordinates for all atomic positions : No NoP x/a y/b z/c 1 1 0.7466 0.1567 0.4307 2 2 0.9959 0.3876 0.3316 3 3 0.25 0.0531 0.151 4 4 0.2809 0.2883 0.3927 5 5 0.4981 0.418 0.3911 6 6 0.7144 0.3918 0.1501 7 7 0.2116 0.3958 0.3644 8 8 0.4173 0.3155 0.4186 9 9 0.7417 0.2699 0.1017 10 10 0.2654 0.2096 0.2065 11 11 0.4225 0.0194 0.1562 12 12 0.5759 0.394 0.196 13 13 0.0743 0.0706 0.0898 14 14 0.2398 0.0361 0.4583 15 15 0.7817 0.4258 0.3474 16 16 0.5397 0.1326 0.4739 17 17 0.9558 0.1991 0.3821 18 1 0.7466 0.6567 0.0693 19 2 0.9959 0.8876 0.1684 20 3 0.25 0.5531 0.349 21 4 0.2809 0.7883 0.1073 22 5 0.4981 0.918 0.1089 23 6 0.7144 0.8918 0.3499 24 7 0.2116 0.8958 0.1356 25 8 0.4173 0.8155 0.0814 26 9 0.7417 0.7699 0.3983 27 10 0.2654 0.7096 0.2935 28 11 0.4225 0.5194 0.3438 29 12 0.5759 0.894 0.304 30 13 0.0743 0.5706 0.4102 31 14 0.2398 0.5361 0.0417 32 15 0.7817 0.9258 0.1526 33 16 0.5397 0.6326 0.0261 34 17 0.9558 0.6991 0.1179 35 1 0.2466 0.3433 0.9307 36 2 0.4959 0.1124 0.8316 37 3 0.75 0.4469 0.651 38 4 0.7809 0.2117 0.8927 39 5 0.9981 0.082 0.8911 40 6 0.2144 0.1082 0.6501 41 7 0.7116 0.1042 0.8644 42 8 0.9173 0.1845 0.9186 43 9 0.2417 0.2301 0.6017 44 10 0.7654 0.2904 0.7065 45 11 0.9225 0.4806 0.6562 46 12 0.0759 0.106 0.696 47 13 0.5743 0.4294 0.5898 48 14 0.7398 0.4639 0.9583 49 15 0.2817 0.0742 0.8474 50 16 0.0397 0.3674 0.9739 51 17 0.4558 0.3009 0.8821 52 1 0.2466 0.8433 0.5693 53 2 0.4959 0.6124 0.6684 54 3 0.75 0.9469 0.849 55 4 0.7809 0.7117 0.6073 56 5 0.9981 0.582 0.6089 57 6 0.2144 0.6082 0.8499 58 7 0.7116 0.6042 0.6356 59 8 0.9173 0.6845 0.5814 60 9 0.2417 0.7301 0.8983 61 10 0.7654 0.7904 0.7935 62 11 0.9225 0.9806 0.8438 63 12 0.0759 0.606 0.804 64 13 0.5743 0.9294 0.9102 65 14 0.7398 0.9639 0.5417 66 15 0.2817 0.5742 0.6526 67 16 0.0397 0.8674 0.5261 68 17 0.4558 0.8009 0.6179 X-ray density (g/cm cub.) = 2.62 MU (1/cm) = 142.147 Mass attenuation coefficient (cm**2/g) = 54.242 Selected interatomic distances (cation-anion,anion-anion): NoP Atom Rad.sph. C.N. Distance NoP N. (angs.) (angs.) 1 Na 2.808 5 2.6373 9 2.4656 16 2.5364 17 2.5282 10 2.5821 14 2 Na 2.808 6 2.544 7 2.5641 15 2.4851 17 2.5744 13 2.6232 11 2.4616 16 3 Zr 2.616 6 2.0484 10 2.071 11 2.1149 13 2.0711 14 2.0689 7 2.0828 15 4 Si 2.1 4 1.6115 7 1.648 8 1.6135 10 1.6505 9 5 Si 2.1 4 1.6311 8 1.6227 12 1.6055 11 1.6091 13 6 Si 2.1 4 1.6278 9 1.655 12 1.5991 15 1.6094 14 7 O 3.264 7 2.6501 8 2.6858 10 2.9428 11 2.7774 13 2.8296 14 2.6755 9 3.1027 15 8 O 3.264 8 2.6501 7 2.6528 10 2.5881 12 2.7748 16 2.6622 11 2.6362 9 2.6157 13 3.1396 17 9 O 3.264 6 2.5919 12 2.6302 15 2.6755 7 2.6362 8 2.6718 10 2.6658 14 10 O 3.264 7 2.6858 7 2.6528 8 3.0758 11 2.9696 13 2.8065 14 2.6718 9 2.9703 15 11 O 3.264 8 3.0758 10 2.955 14 2.9186 16 2.9428 7 2.6622 8 2.6088 12 2.7377 15 2.6864 13 12 O 3.264 7 2.5881 8 2.5919 9 2.6514 15 2.6088 11 2.6738 13 2.6524 14 2.7971 17 13 O 3.264 8 2.9696 10 3.1702 14 2.9111 17 2.7774 7 2.6157 8 2.6738 12 2.926 15 2.6864 11 14 O 3.264 8 2.8065 10 2.955 11 3.1702 13 2.8296 7 2.6658 9 2.6524 12 2.6942 15 3.2252 16 15 O 3.264 7 2.6302 9 2.6514 12 2.9703 10 2.7377 11 2.926 13 2.6942 14 3.1027 7 16 O 3.264 3 2.7748 8 2.9186 11 3.2252 14 17 O 3.264 3 2.9111 13 3.1396 8 2.7971 12 X-ray diffraction powder data (II), X-Ray W.L. = 1.54056(angs.): No H K L Theta 2*Theta S LPG MF F I int. ( degree ) *100 1 0 2 0 6.902 13.804 0.078 135.54 2 104.4 291.2 2 0 1 1 7.461 14.923 0.084 115.65 4 113.9 591.9 3 2 0 0 7.54 15.081 0.085 113.19 2 214.1 1023.1 4 1 0 1 7.614 15.229 0.086 110.96 4 121.6 647.2 5 1 2 0 7.869 15.739 0.089 103.75 4 126.0 650.0 6 1 1 1 8.366 16.732 0.094 91.54 8 34.8 87.5 7 0 2 1 9.579 19.159 0.108 69.3 4 55.7 84.7 8 2 2 0 10.249 20.499 0.115 60.26 4 55.5 73.1 9 1 2 1 10.305 20.609 0.116 59.59 8 69.0 223.7 10 2 1 1 10.639 21.277 0.12 55.78 8 33.3 48.8 11 2 2 1 12.235 24.471 0.138 41.66 8 73.2 176.2 12 0 3 1 12.35 24.699 0.139 40.85 4 72.9 85.6 13 1 3 1 12.927 25.855 0.145 37.1 8 90.9 241.6 14 3 0 1 13.181 26.362 0.148 35.61 4 99.6 139.3 15 0 0 2 13.311 26.623 0.149 34.88 2 16.4 1.9 16 3 2 0 13.333 26.667 0.15 34.75 4 90.0 110.9 17 3 1 1 13.639 27.279 0.153 33.12 8 25.4 16.8 18 0 1 2 13.766 27.532 0.154 32.48 4 58.2 43.4 19 0 4 0 13.906 27.813 0.156 31.79 2 67.0 28.2 20 1 1 2 14.29 28.581 0.16 30.0 8 200.2 948.3 21 1 4 0 14.426 28.852 0.162 29.4 4 245.4 698.2 22 2 3 1 14.532 29.065 0.163 28.94 8 32.5 24.2 23 3 2 1 14.937 29.874 0.167 27.29 8 57.4 70.9 24 0 2 2 15.053 30.106 0.169 26.84 4 46.1 22.5 25 4 0 0 15.215 30.431 0.17 26.23 2 389.6 785.2 26 2 0 2 15.368 30.735 0.172 25.68 4 33.8 11.6 27 0 4 1 15.455 30.911 0.173 25.36 4 36.7 13.5 28 1 2 2 15.538 31.076 0.174 25.08 8 83.2 136.9 29 2 1 2 15.768 31.535 0.176 24.29 8 96.8 179.6 30 2 4 0 15.892 31.784 0.178 23.89 4 121.0 138.0 31 1 4 1 15.929 31.858 0.178 23.77 8 89.7 150.9 32 4 2 0 16.777 33.554 0.187 21.24 4 68.5 39.3 33 3 3 1 16.898 33.796 0.189 20.91 8 89.2 131.3 34 2 2 2 16.917 33.834 0.189 20.86 8 24.0 9.5 35 0 3 2 17.002 34.005 0.19 20.63 4 71.9 42.1 36 4 1 1 17.027 34.053 0.19 20.57 8 57.2 53.0 37 2 4 1 17.28 34.56 0.193 19.92 8 98.0 150.9 38 1 3 2 17.438 34.877 0.195 19.53 8 48.5 36.2 39 3 1 2 17.988 35.976 0.2 18.25 8 94.0 127.2 40 3 4 0 18.099 36.197 0.202 18.0 4 105.0 78.2 41 4 2 1 18.105 36.21 0.202 17.99 8 13.5 2.6 42 2 3 2 18.693 37.387 0.208 16.77 8 108.0 154.1 43 0 5 1 18.767 37.534 0.209 16.62 4 22.1 3.2 44 3 2 2 19.019 38.038 0.212 16.14 8 22.9 6.7 45 1 5 1 19.168 38.337 0.213 15.86 8 25.9 8.4 46 3 4 1 19.348 38.695 0.215 15.54 8 31.8 12.4 47 0 4 2 19.44 38.881 0.216 15.37 4 1.7 0.0 48 4 3 1 19.789 39.578 0.22 14.78 8 54.2 34.3 49 1 4 2 19.83 39.66 0.22 14.71 8 10.2 1.2 50 2 5 1 20.332 40.664 0.226 13.92 8 36.1 14.3 51 5 0 1 20.345 40.69 0.226 13.9 4 82.8 37.6 52 4 0 2 20.434 40.868 0.227 13.76 4 16.7 1.5 53 5 2 0 20.449 40.898 0.227 13.74 4 72.0 28.1 54 0 1 3 20.521 41.042 0.228 13.63 4 194.2 202.8 55 1 0 3 20.582 41.163 0.228 13.54 4 41.8 9.3 56 3 3 2 20.64 41.279 0.229 13.46 8 14.4 2.2 57 5 1 1 20.66 41.32 0.229 13.43 8 36.7 14.2 58 4 1 2 20.748 41.496 0.23 13.3 8 27.7 8.0 59 4 4 0 20.846 41.693 0.231 13.16 4 30.4 4.8 60 1 1 3 20.894 41.788 0.232 13.09 8 56.0 32.4 61 2 4 2 20.963 41.926 0.232 13.0 8 13.0 1.7 62 0 6 0 21.131 42.262 0.234 12.77 2 131.5 43.6 63 0 2 3 21.449 42.898 0.237 12.35 4 6.5 0.2 64 1 6 0 21.495 42.991 0.238 12.29 4 138.8 93.4 65 5 2 1 21.583 43.166 0.239 12.18 8 88.5 75.2 66 4 2 2 21.668 43.336 0.24 12.07 8 22.3 4.8 67 1 2 3 21.809 43.618 0.241 11.89 8 55.5 28.9 68 4 4 1 21.964 43.928 0.243 11.71 8 26.7 6.6 69 2 1 3 21.982 43.963 0.243 11.68 8 88.3 71.9 70 3 5 1 22.158 44.316 0.245 11.48 8 12.8 1.5 71 0 6 1 22.237 44.474 0.246 11.38 4 159.5 114.3 72 0 5 2 22.241 44.482 0.246 11.38 4 136.8 84.0 73 2 6 0 22.56 45.119 0.249 11.02 4 69.0 20.7 74 1 6 1 22.587 45.174 0.249 10.99 8 14.7 1.9 75 1 5 2 22.591 45.182 0.249 10.99 8 84.6 62.0 76 3 4 2 22.748 45.496 0.251 10.82 8 20.0 3.4 77 2 2 3 22.862 45.723 0.252 10.69 8 33.5 9.4 78 0 3 3 22.928 45.856 0.253 10.62 4 62.9 16.6 79 5 3 1 23.055 46.111 0.254 10.49 8 87.6 63.5 80 4 3 2 23.136 46.272 0.255 10.41 8 8.0 0.5 81 6 0 0 23.183 46.366 0.256 10.36 2 237.0 114.8 82 1 3 3 23.27 46.54 0.256 10.27 8 85.9 59.8 83 3 0 3 23.423 46.846 0.258 10.12 4 28.5 3.2 84 2 6 1 23.612 47.225 0.26 9.94 8 60.2 28.4 85 2 5 2 23.616 47.232 0.26 9.94 8 97.8 74.9 86 3 1 3 23.705 47.411 0.261 9.85 8 16.1 2.0 87 5 1 2 23.908 47.816 0.263 9.66 8 166.6 211.5 88 5 4 0 23.996 47.992 0.264 9.58 4 206.6 161.4 89 3 6 0 24.251 48.503 0.267 9.36 4 138.8 71.1 90 2 3 3 24.273 48.546 0.267 9.34 8 61.3 27.6 91 6 2 0 24.306 48.611 0.267 9.31 4 72.7 19.4 92 6 1 1 24.49 48.98 0.269 9.15 8 47.7 16.4 93 4 5 1 24.531 49.063 0.27 9.11 8 52.2 19.6 94 3 2 3 24.537 49.075 0.27 9.11 8 54.2 21.1 95 5 2 2 24.735 49.47 0.272 8.94 8 78.7 43.7 96 0 4 3 24.883 49.765 0.273 8.82 4 50.8 9.0 97 5 4 1 25.002 50.005 0.274 8.73 8 69.8 33.5 98 4 4 2 25.078 50.156 0.275 8.67 8 9.9 0.7 99 1 4 3 25.204 50.408 0.276 8.57 8 33.0 7.3 100 3 6 1 25.25 50.5 0.277 8.53 8 45.0 13.6 101 3 5 2 25.254 50.507 0.277 8.53 8 45.4 13.8 102 6 2 1 25.303 50.605 0.277 8.49 8 93.4 58.5 103 0 6 2 25.325 50.651 0.278 8.48 4 55.3 10.2 104 1 6 2 25.643 51.286 0.281 8.24 8 36.6 8.7 105 0 7 1 25.853 51.706 0.283 8.09 4 137.2 60.1 106 3 3 3 25.879 51.759 0.283 8.07 8 99.5 63.0 107 4 1 3 25.971 51.941 0.284 8.0 8 158.2 158.1 108 5 3 2 26.069 52.139 0.285 7.94 8 25.2 4.0 109 2 4 3 26.152 52.303 0.286 7.88 8 67.2 28.1 110 1 7 1 26.166 52.331 0.286 7.87 8 80.2 39.9 111 4 6 0 26.482 52.964 0.289 7.66 4 113.8 39.1 112 2 6 2 26.579 53.158 0.29 7.59 8 37.1 8.2 113 6 3 1 26.617 53.233 0.291 7.57 8 57.5 19.8 114 4 2 3 26.751 53.501 0.292 7.48 8 29.6 5.2 115 2 7 1 27.089 54.178 0.296 7.27 8 62.9 22.7 116 6 0 2 27.133 54.266 0.296 7.25 4 21.1 1.3 117 0 5 3 27.242 54.483 0.297 7.18 4 6.4 0.1 118 5 5 1 27.354 54.708 0.298 7.11 8 21.1 2.5 119 6 1 2 27.387 54.774 0.299 7.09 8 83.6 39.1 120 0 0 4 27.419 54.837 0.299 7.07 2 248.9 86.4 121 4 6 1 27.422 54.844 0.299 7.07 8 112.7 70.9 122 4 5 2 27.425 54.85 0.299 7.07 8 95.4 50.8 123 6 4 0 27.467 54.934 0.299 7.05 4 109.1 33.1 124 1 5 3 27.544 55.087 0.3 7.0 8 146.5 118.5 125 0 1 4 27.671 55.342 0.301 6.93 4 92.0 23.1 126 3 4 3 27.679 55.359 0.302 6.92 8 48.1 12.6 127 5 4 2 27.861 55.722 0.303 6.82 8 11.8 0.7 128 1 1 4 27.97 55.939 0.304 6.76 8 74.1 29.3 129 4 3 3 28.017 56.034 0.305 6.74 8 49.4 13.0 130 3 6 2 28.091 56.182 0.306 6.7 8 39.6 8.3 131 6 2 2 28.14 56.279 0.306 6.67 8 32.4 5.5 132 7 0 1 28.261 56.522 0.307 6.61 4 119.7 37.3 133 7 2 0 28.343 56.685 0.308 6.56 4 93.8 22.8 134 6 4 1 28.384 56.769 0.309 6.54 8 111.2 63.8 135 0 2 4 28.419 56.837 0.309 6.52 4 58.8 8.9 136 2 5 3 28.436 56.873 0.309 6.51 8 62.8 20.3 137 5 0 3 28.447 56.893 0.309 6.51 4 54.0 7.5 138 7 1 1 28.508 57.017 0.31 6.48 8 4.4 0.1 139 3 7 1 28.583 57.165 0.311 6.44 8 78.6 31.4 140 2 0 4 28.608 57.217 0.311 6.42 4 106.4 28.7 141 0 7 2 28.652 57.304 0.311 6.4 4 44.5 5.0 142 5 1 3 28.693 57.386 0.312 6.38 8 37.2 7.0 143 1 2 4 28.712 57.424 0.312 6.37 8 68.7 23.7 144 0 8 0 28.729 57.459 0.312 6.36 2 98.9 12.3 145 2 1 4 28.854 57.707 0.313 6.3 8 60.2 18.0 146 1 7 2 28.944 57.888 0.314 6.26 8 102.3 51.6 147 1 8 0 29.021 58.042 0.315 6.22 4 60.0 8.8 148 5 6 0 29.172 58.343 0.316 6.15 4 125.0 37.9 149 7 2 1 29.242 58.484 0.317 6.11 8 69.0 23.0 150 6 3 2 29.366 58.732 0.318 6.06 8 149.6 106.9 151 5 2 3 29.424 58.847 0.319 6.03 8 65.3 20.3 152 2 2 4 29.582 59.164 0.32 5.96 8 29.2 4.0 153 0 8 1 29.621 59.243 0.321 5.94 4 149.2 52.2 154 0 3 4 29.637 59.275 0.321 5.93 4 56.1 7.4 155 4 4 3 29.729 59.458 0.322 5.89 8 36.1 6.1 156 2 7 2 29.81 59.619 0.323 5.86 8 9.8 0.4 157 2 8 0 29.885 59.77 0.323 5.82 4 97.6 21.9 158 3 5 3 29.886 59.771 0.323 5.82 8 110.0 55.6 159 1 8 1 29.908 59.815 0.324 5.81 8 102.1 47.8 160 1 3 4 29.923 59.847 0.324 5.81 8 80.0 29.3 161 0 6 3 29.95 59.9 0.324 5.8 4 12.6 0.4 162 5 6 1 30.055 60.111 0.325 5.75 8 31.5 4.5 163 5 5 2 30.059 60.117 0.325 5.75 8 49.0 10.9 164 4 6 2 30.123 60.245 0.326 5.72 8 37.0 6.2 165 1 6 3 30.234 60.468 0.327 5.67 8 26.7 3.2 166 3 1 4 30.29 60.581 0.327 5.65 8 64.4 18.5 167 7 3 1 30.44 60.88 0.329 5.59 8 86.7 33.1 168 6 5 1 30.558 61.116 0.33 5.54 8 37.7 6.2 169 4 7 1 30.594 61.187 0.33 5.53 8 115.1 57.8 170 5 3 3 30.617 61.235 0.331 5.52 8 83.5 30.4 171 2 8 1 30.756 61.513 0.332 5.46 8 61.8 16.4 172 2 3 4 30.772 61.544 0.332 5.46 8 64.5 17.9 173 3 2 4 30.998 61.996 0.334 5.37 8 49.4 10.3 174 6 4 2 31.031 62.063 0.335 5.36 8 14.9 0.9 175 2 6 3 31.078 62.155 0.335 5.34 8 18.4 1.4 176 7 1 2 31.149 62.298 0.336 5.31 8 110.9 51.5 177 3 7 2 31.219 62.439 0.336 5.28 8 74.9 23.4 178 7 4 0 31.223 62.445 0.336 5.28 4 125.6 32.9 179 3 8 0 31.293 62.586 0.337 5.26 4 26.2 1.4 180 0 4 4 31.294 62.588 0.337 5.26 4 4.4 0.0 181 1 4 4 31.571 63.143 0.34 5.16 8 125.1 63.6 182 8 0 0 31.661 63.322 0.341 5.12 2 151.9 23.3 183 6 1 3 31.812 63.623 0.342 5.07 8 83.6 28.0 184 7 2 2 31.845 63.691 0.342 5.06 8 28.6 3.3 185 4 5 3 31.846 63.693 0.343 5.06 8 34.4 4.7 186 4 0 4 32.007 64.014 0.344 5.0 4 173.2 59.2 187 7 4 1 32.073 64.145 0.345 4.98 8 34.5 4.7 188 3 8 1 32.142 64.284 0.345 4.96 8 83.2 27.1 189 3 3 4 32.157 64.314 0.345 4.95 8 40.2 6.3 190 0 8 2 32.207 64.413 0.346 4.94 4 1.9 0.0 191 4 1 4 32.237 64.474 0.346 4.93 8 48.6 9.2 192 5 4 3 32.245 64.489 0.346 4.92 8 26.4 2.7 193 6 6 0 32.262 64.525 0.346 4.92 4 18.0 0.6 194 2 4 4 32.395 64.79 0.348 4.87 8 22.4 1.9 195 3 6 3 32.455 64.911 0.348 4.86 8 29.5 3.3 196 1 8 2 32.479 64.959 0.349 4.85 8 9.6 0.4 197 6 2 3 32.5 65.0 0.349 4.84 8 60.0 13.7 198 8 2 0 32.58 65.159 0.35 4.82 4 77.7 11.5 199 5 6 2 32.62 65.241 0.35 4.8 8 6.5 0.2 200 8 1 1 32.732 65.465 0.351 4.77 8 59.0 13.1 201 4 2 4 32.921 65.841 0.353 4.71 8 50.0 9.3 202 0 7 3 32.971 65.942 0.353 4.69 4 78.7 11.5 203 7 3 2 32.988 65.976 0.353 4.69 8 27.3 2.8 204 5 7 1 33.071 66.143 0.354 4.66 8 61.6 13.9 205 6 6 1 33.098 66.196 0.354 4.66 8 79.6 23.3 206 6 5 2 33.101 66.202 0.354 4.65 8 139.4 71.4 207 4 7 2 33.135 66.27 0.355 4.64 8 69.1 17.5 208 4 8 0 33.206 66.413 0.355 4.62 4 82.8 12.5 209 1 7 3 33.241 66.482 0.356 4.61 8 132.9 64.3 210 2 8 2 33.291 66.582 0.356 4.6 8 43.3 6.8 211 0 5 4 33.355 66.709 0.357 4.58 4 34.9 2.2 212 8 2 1 33.411 66.822 0.357 4.56 8 43.5 6.8 213 0 9 1 33.565 67.129 0.359 4.52 4 44.7 3.6 214 1 5 4 33.623 67.245 0.359 4.5 8 44.2 6.9 215 6 3 3 33.631 67.262 0.36 4.5 8 78.9 22.1 216 3 4 4 33.744 67.487 0.361 4.47 8 85.2 25.6 217 1 9 1 33.832 67.664 0.361 4.44 8 31.9 3.6 218 4 8 1 34.03 68.06 0.363 4.39 8 102.0 36.0 219 2 7 3 34.043 68.086 0.363 4.39 8 105.1 38.2 220 4 3 4 34.045 68.089 0.363 4.39 8 55.8 10.8 221 7 5 1 34.108 68.216 0.364 4.37 8 41.1 5.8 222 5 5 3 34.275 68.55 0.366 4.33 8 130.8 58.4 223 4 6 3 34.334 68.669 0.366 4.31 8 41.5 5.9 224 2 5 4 34.42 68.841 0.367 4.29 8 39.0 5.1 225 8 3 1 34.527 69.054 0.368 4.26 8 36.0 4.4 226 7 4 2 34.555 69.11 0.368 4.25 8 18.3 1.1 227 3 8 2 34.622 69.244 0.369 4.24 8 11.4 0.4 228 2 9 1 34.627 69.255 0.369 4.24 8 33.8 3.8 229 5 1 4 34.651 69.302 0.369 4.23 8 73.6 18.1 230 8 0 2 34.972 69.943 0.372 4.15 4 21.1 0.7 231 7 0 3 35.075 70.149 0.373 4.13 4 26.1 1.1 232 6 4 3 35.184 70.368 0.374 4.1 8 89.6 25.9 233 8 1 2 35.192 70.383 0.374 4.1 8 45.5 6.7 234 8 4 0 35.261 70.522 0.375 4.08 4 58.8 5.6 235 7 1 3 35.294 70.589 0.375 4.08 8 40.2 5.2 236 5 2 4 35.312 70.623 0.375 4.07 8 56.4 10.2 237 3 7 3 35.361 70.721 0.376 4.06 8 79.4 20.2 238 0 1 5 35.362 70.723 0.376 4.06 4 40.7 2.7 239 1 0 5 35.404 70.808 0.376 4.05 4 76.5 9.3 240 5 7 2 35.519 71.038 0.377 4.02 8 107.6 36.8 241 6 6 2 35.545 71.089 0.377 4.02 8 34.5 3.8 242 5 8 0 35.588 71.176 0.378 4.01 4 25.2 1.0 243 4 4 4 35.589 71.178 0.378 4.01 8 36.6 4.2 244 1 1 5 35.623 71.245 0.378 4.0 8 55.5 9.7 245 7 6 0 35.723 71.446 0.379 3.98 4 119.3 22.3 246 3 5 4 35.732 71.463 0.379 3.98 8 20.3 1.3 247 0 6 4 35.79 71.58 0.38 3.96 4 99.1 15.4 248 8 2 2 35.848 71.695 0.38 3.95 8 13.9 0.6 249 3 9 1 35.935 71.87 0.381 3.93 8 10.4 0.3 250 7 2 3 35.95 71.899 0.381 3.93 8 67.5 14.1 251 6 7 1 35.978 71.956 0.381 3.92 8 52.0 8.4 252 0 9 2 35.996 71.993 0.382 3.92 4 71.3 7.9 253 0 2 5 36.017 72.033 0.382 3.92 4 48.5 3.6 254 1 6 4 36.05 72.1 0.382 3.91 8 34.4 3.7 255 8 4 1 36.062 72.125 0.382 3.91 8 53.3 8.8 256 1 9 2 36.255 72.511 0.384 3.87 8 28.5 2.5 257 1 2 5 36.275 72.551 0.384 3.86 8 55.8 9.5 258 0 8 3 36.291 72.581 0.384 3.86 4 110.8 18.7 259 5 8 1 36.387 72.773 0.385 3.84 8 91.6 25.4 260 2 1 5 36.401 72.801 0.385 3.84 8 38.7 4.5 261 5 3 4 36.401 72.802 0.385 3.84 8 72.6 16.0 262 4 8 2 36.447 72.895 0.386 3.83 8 32.8 3.2 263 7 6 1 36.521 73.041 0.386 3.81 8 30.8 2.8 264 7 5 2 36.523 73.047 0.386 3.81 8 122.0 44.8 265 1 8 3 36.549 73.098 0.387 3.81 8 46.5 6.5 266 5 6 3 36.683 73.365 0.388 3.78 8 58.8 10.3 267 2 6 4 36.824 73.648 0.389 3.75 8 46.0 6.3 268 0 10 0 36.93 73.861 0.39 3.73 2 0.6 0.0 269 8 3 2 36.93 73.861 0.39 3.73 8 16.1 0.8 270 9 0 1 36.986 73.972 0.391 3.72 4 65.4 6.3 271 2 9 2 37.028 74.056 0.391 3.71 8 46.5 6.3 272 7 3 3 37.031 74.063 0.391 3.71 8 106.8 33.4 273 2 2 5 37.048 74.096 0.391 3.71 8 33.4 3.3 274 9 2 0 37.057 74.114 0.391 3.71 4 22.4 0.7 275 0 3 5 37.097 74.195 0.392 3.7 4 0.4 0.0 276 6 5 3 37.138 74.277 0.392 3.69 8 60.7 10.7 277 4 7 3 37.171 74.342 0.392 3.69 8 87.9 22.5 278 1 10 0 37.187 74.373 0.392 3.69 4 71.3 7.4 279 9 1 1 37.201 74.402 0.392 3.68 8 57.3 9.5 280 6 0 4 37.288 74.576 0.393 3.67 4 84.6 10.3 281 2 8 3 37.319 74.638 0.394 3.66 8 84.1 20.4 282 1 3 5 37.353 74.707 0.394 3.66 8 70.4 14.3 283 3 0 5 37.469 74.938 0.395 3.63 4 82.9 9.9 284 6 1 4 37.503 75.005 0.395 3.63 8 69.1 13.7 285 4 5 4 37.535 75.07 0.395 3.62 8 54.1 8.4 286 3 1 5 37.683 75.366 0.397 3.6 8 44.1 5.5 287 0 10 1 37.718 75.435 0.397 3.59 4 24.6 0.9 288 4 9 1 37.735 75.469 0.397 3.59 8 23.6 1.6 289 9 2 1 37.843 75.687 0.398 3.57 8 76.3 16.4 290 5 4 4 37.905 75.81 0.399 3.56 8 108.4 33.0 291 2 10 0 37.952 75.905 0.399 3.55 4 104.9 15.4 292 1 10 1 37.972 75.945 0.399 3.55 8 59.0 9.7 293 8 5 1 37.999 75.998 0.4 3.54 8 68.0 12.9 294 3 6 4 38.101 76.203 0.401 3.53 8 43.5 5.3 295 2 3 5 38.118 76.236 0.401 3.52 8 8.1 0.2 296 6 2 4 38.143 76.286 0.401 3.52 8 41.2 4.7 297 3 9 2 38.303 76.606 0.402 3.49 8 32.3 2.9 298 3 2 5 38.323 76.645 0.403 3.49 8 29.6 2.4 299 6 7 2 38.345 76.689 0.403 3.49 8 19.2 1.0 300 6 8 0 38.412 76.823 0.403 3.48 4 118.1 19.1 301 8 4 2 38.427 76.854 0.403 3.48 8 31.8 2.8 302 7 4 3 38.527 77.053 0.404 3.46 8 33.0 3.0 303 0 7 4 38.583 77.167 0.405 3.45 4 74.8 7.6 304 3 8 3 38.591 77.182 0.405 3.45 8 20.3 1.1 305 0 4 5 38.592 77.184 0.405 3.45 4 49.7 3.4 306 2 10 1 38.733 77.465 0.406 3.43 8 45.9 5.7 307 5 8 2 38.744 77.488 0.406 3.43 8 27.3 2.0 308 1 7 4 38.836 77.672 0.407 3.41 8 38.9 4.1 309 1 4 5 38.845 77.689 0.407 3.41 8 38.6 4.0 310 7 6 2 38.875 77.751 0.407 3.41 8 63.0 10.7 311 9 3 1 38.906 77.812 0.408 3.4 8 60.4 9.8 312 8 1 3 39.138 78.276 0.41 3.37 8 126.4 42.5 313 6 8 1 39.189 78.378 0.41 3.36 8 46.2 5.7 314 6 3 4 39.203 78.406 0.41 3.36 8 73.2 14.2 315 3 10 0 39.217 78.434 0.41 3.36 4 80.0 8.5 316 7 7 1 39.295 78.59 0.411 3.35 8 53.3 7.5 317 3 3 5 39.381 78.762 0.412 3.34 8 60.1 9.5 318 5 7 3 39.453 78.907 0.412 3.33 8 118.4 36.8 319 4 1 5 39.454 78.909 0.412 3.33 8 24.7 1.6 320 6 6 3 39.478 78.956 0.413 3.32 8 27.3 2.0 321 9 1 2 39.542 79.084 0.413 3.31 8 52.8 7.3 322 8 6 0 39.551 79.103 0.413 3.31 4 68.2 6.1 323 2 7 4 39.592 79.183 0.414 3.31 8 54.5 7.8 324 2 4 5 39.6 79.2 0.414 3.31 8 93.7 22.9 325 9 4 0 39.609 79.217 0.414 3.31 4 67.6 6.0 326 8 2 3 39.77 79.541 0.415 3.28 8 20.1 1.0 327 5 5 4 39.811 79.621 0.416 3.28 8 43.2 4.8 328 4 6 4 39.867 79.734 0.416 3.27 8 90.7 21.2 329 0 9 3 39.914 79.828 0.416 3.27 4 88.4 10.1 330 3 10 1 39.99 79.981 0.417 3.26 8 49.7 6.3 331 5 9 1 40.007 80.014 0.417 3.25 8 16.6 0.7 332 0 10 2 40.049 80.099 0.418 3.25 4 21.5 0.6 333 4 9 2 40.066 80.132 0.418 3.25 8 48.1 5.9 334 4 2 5 40.085 80.171 0.418 3.24 8 28.2 2.0 335 1 9 3 40.164 80.329 0.419 3.23 8 26.8 1.8 336 9 2 2 40.173 80.346 0.419 3.23 8 37.8 3.7 337 1 10 2 40.3 80.599 0.42 3.22 8 15.8 0.6 338 8 6 1 40.323 80.646 0.42 3.22 8 82.6 17.3 339 8 5 2 40.326 80.651 0.42 3.21 8 85.1 18.4 340 4 8 3 40.35 80.701 0.42 3.21 8 104.8 27.8 341 9 4 1 40.38 80.759 0.421 3.21 8 17.4 0.8 342 7 5 3 40.424 80.848 0.421 3.2 8 94.2 22.4 343 0 5 5 40.488 80.976 0.421 3.2 4 34.4 1.5 344 6 4 4 40.674 81.348 0.423 3.17 8 55.1 7.6 345 1 5 5 40.738 81.475 0.424 3.17 8 36.2 3.3 346 7 1 4 40.779 81.558 0.424 3.16 8 58.1 8.4 347 8 3 3 40.819 81.637 0.424 3.16 8 33.7 2.8 348 3 7 4 40.842 81.685 0.425 3.16 8 56.4 7.9 349 3 4 5 40.851 81.701 0.425 3.15 8 27.2 1.8 350 2 9 3 40.913 81.827 0.425 3.15 8 123.9 38.1 351 4 10 0 40.97 81.939 0.426 3.14 4 56.4 3.9 352 10 0 0 41.004 82.009 0.426 3.14 2 58.7 2.1 353 2 10 2 41.048 82.096 0.426 3.13 8 20.7 1.1 354 4 3 5 41.132 82.264 0.427 3.12 8 27.2 1.8 355 9 3 2 41.219 82.438 0.428 3.11 8 29.1 2.1 356 7 2 4 41.405 82.811 0.429 3.1 8 37.9 3.5 357 2 5 5 41.485 82.969 0.43 3.09 8 43.7 4.7 358 5 0 5 41.493 82.986 0.43 3.09 4 83.3 8.4 359 6 8 2 41.498 82.997 0.43 3.09 8 21.1 1.1 360 7 7 2 41.603 83.206 0.431 3.08 8 58.5 8.3 361 7 8 0 41.669 83.337 0.432 3.07 4 42.2 2.2 362 5 1 5 41.702 83.403 0.432 3.07 8 33.3 2.7 363 0 8 4 41.733 83.465 0.432 3.06 4 82.9 8.3 364 4 10 1 41.735 83.471 0.432 3.06 8 25.6 1.6 365 10 2 0 41.838 83.676 0.433 3.05 4 40.1 1.9 366 10 1 1 41.978 83.956 0.434 3.04 8 31.0 2.3 367 1 8 4 41.981 83.961 0.434 3.04 8 47.9 5.5 368 5 6 4 42.109 84.219 0.435 3.03 8 34.9 2.9 369 0 11 1 42.135 84.27 0.435 3.03 4 2.0 0.0 370 3 9 3 42.156 84.312 0.436 3.02 8 29.7 2.1 371 6 7 3 42.197 84.393 0.436 3.02 8 60.6 8.8 372 9 5 1 42.257 84.514 0.437 3.02 8 15.4 0.6 373 8 4 3 42.277 84.555 0.437 3.01 8 37.2 3.3 374 3 10 2 42.29 84.579 0.437 3.01 8 26.9 1.7 375 5 9 2 42.306 84.612 0.437 3.01 8 56.0 7.4 376 5 2 5 42.325 84.651 0.437 3.01 8 60.5 8.7 377 1 11 1 42.383 84.765 0.438 3.0 8 102.0 24.7 378 7 8 1 42.432 84.864 0.438 3.0 8 90.7 19.5 379 7 3 4 42.446 84.891 0.438 3.0 8 53.2 6.7 380 6 5 4 42.549 85.098 0.439 2.99 8 24.2 1.4 381 4 7 4 42.581 85.161 0.439 2.99 8 69.6 11.4 382 5 8 3 42.588 85.175 0.439 2.99 8 40.3 3.8 383 4 4 5 42.589 85.178 0.439 2.99 8 68.5 11.1 384 10 2 1 42.601 85.202 0.439 2.99 8 120.8 34.4 385 8 6 2 42.619 85.238 0.44 2.98 8 19.1 0.9 386 9 4 2 42.675 85.35 0.44 2.98 8 10.9 0.3 387 7 6 3 42.716 85.432 0.44 2.98 8 46.3 5.0 388 2 8 4 42.724 85.448 0.44 2.98 8 26.5 1.6 389 3 5 5 42.724 85.449 0.44 2.98 8 46.3 5.0 390 6 9 1 42.743 85.486 0.441 2.97 8 61.0 8.7 391 0 6 5 42.78 85.56 0.441 2.97 4 131.6 20.3 392 1 6 5 43.027 86.054 0.443 2.95 8 5.1 0.1 393 8 7 1 43.031 86.062 0.443 2.95 8 67.3 10.5 394 2 11 1 43.125 86.25 0.444 2.94 8 65.1 9.8 395 9 0 3 43.164 86.327 0.444 2.94 4 70.6 5.8 396 5 10 0 43.202 86.403 0.444 2.94 4 15.5 0.3 397 5 3 5 43.363 86.725 0.446 2.93 8 30.6 2.2 398 9 1 3 43.371 86.742 0.446 2.93 8 43.9 4.4 399 10 3 1 43.638 87.275 0.448 2.91 8 65.2 9.7 400 0 0 6 43.688 87.376 0.448 2.9 2 67.6 2.6 401 2 6 5 43.768 87.537 0.449 2.9 8 59.4 8.1 402 9 6 0 43.777 87.554 0.449 2.9 4 120.8 16.7 403 0 10 3 43.87 87.741 0.45 2.89 4 11.0 0.1 404 4 9 3 43.887 87.773 0.45 2.89 8 76.0 13.2 405 0 1 6 43.895 87.79 0.45 2.89 4 13.6 0.2 406 7 4 4 43.897 87.794 0.45 2.89 8 88.7 17.9 407 3 8 4 43.959 87.919 0.451 2.89 8 17.9 0.7 408 5 10 1 43.962 87.924 0.451 2.89 8 64.4 9.4 409 9 2 3 43.992 87.984 0.451 2.88 8 56.7 7.3 410 4 10 2 44.02 88.04 0.451 2.88 8 6.3 0.1 411 10 0 2 44.054 88.109 0.451 2.88 4 20.8 0.5 412 1 10 3 44.117 88.234 0.452 2.88 8 8.6 0.2 413 1 1 6 44.142 88.284 0.452 2.88 8 75.5 12.9 414 8 5 3 44.143 88.286 0.452 2.88 8 38.3 3.3 415 10 1 2 44.261 88.523 0.453 2.87 8 54.6 6.8 416 8 0 4 44.287 88.574 0.453 2.87 4 85.6 8.3 417 10 4 0 44.327 88.653 0.454 2.86 4 68.9 5.4 418 3 11 1 44.359 88.719 0.454 2.86 8 86.2 16.8 419 0 11 2 44.418 88.835 0.454 2.86 4 32.8 1.2 420 6 1 5 44.422 88.844 0.454 2.86 8 13.5 0.4 421 4 5 5 44.453 88.906 0.455 2.86 8 17.4 0.7 422 8 1 4 44.494 88.988 0.455 2.86 8 24.5 1.4 423 0 2 6 44.516 89.032 0.455 2.85 4 105.0 12.4 424 9 6 1 44.537 89.073 0.455 2.85 8 52.2 6.1 425 9 5 2 44.539 89.079 0.455 2.85 8 42.0 4.0 426 1 11 2 44.664 89.329 0.456 2.85 8 78.3 13.8 427 2 0 6 44.675 89.35 0.456 2.85 4 62.3 4.4 428 7 8 2 44.713 89.427 0.457 2.84 8 15.7 0.6 429 1 2 6 44.762 89.525 0.457 2.84 8 107.0 25.6 430 5 7 4 44.803 89.607 0.457 2.84 8 43.9 4.3 431 5 4 5 44.811 89.623 0.457 2.84 8 14.0 0.4 432 6 6 4 44.827 89.655 0.458 2.84 8 19.2 0.8 433 2 10 3 44.857 89.714 0.458 2.84 8 66.0 9.7 434 2 1 6 44.882 89.764 0.458 2.83 8 26.6 1.6 435 10 2 2 44.882 89.764 0.458 2.83 8 15.8 0.6 X-ray diffraction powder data (I)...X-Ray wave length = 1.54056 (angs.): No H K L Theta 2*Theta d I int I int.n. I p.h.n. H(Si) ( degree ) (angstrem) *100 *100 1 0 2 0 6.902 13.804 6.41 291.2 28.5 28.5 5.6 2 0 1 1 7.461 14.923 5.9317 591.9 57.9 57.9 5.6 3 2 0 0 7.54 15.081 5.87 1023.1 100.0 100.0 5.6 4 1 0 1 7.614 15.229 5.81316 647.2 63.3 63.3 5.6 5 1 2 0 7.869 15.739 5.62603 650.0 63.5 63.5 5.6 6 1 1 1 8.366 16.732 5.2943 87.5 8.5 8.5 5.6 7 0 2 1 9.579 19.159 4.62871 84.7 8.3 8.3 5.6 8 2 2 0 10.249 20.499 4.32906 73.1 7.1 7.1 5.6 9 1 2 1 10.305 20.609 4.30611 223.7 21.9 21.8 5.6 10 2 1 1 10.639 21.277 4.17236 48.8 4.8 4.7 5.6 11 2 2 1 12.235 24.471 3.63465 176.2 17.2 17.1 5.6 12 0 3 1 12.35 24.699 3.60148 85.6 8.4 8.3 5.6 13 1 3 1 12.927 25.855 3.44311 241.6 23.6 23.4 5.6 14 3 0 1 13.181 26.362 3.378 139.3 13.6 13.5 5.6 15 3 2 0 13.333 26.667 3.34008 112.8 11.0 10.9 5.6 16 3 1 1 13.639 27.279 3.26651 16.8 1.6 1.6 5.6 17 0 1 2 13.766 27.532 3.23709 43.4 4.2 4.2 5.6 18 0 4 0 13.906 27.813 3.205 28.2 2.8 2.7 5.6 19 1 1 2 14.29 28.581 3.12064 948.3 92.7 91.8 5.6 20 1 4 0 14.426 28.852 3.09186 698.2 68.2 67.6 5.6 21 2 3 1 14.532 29.065 3.06976 24.2 2.4 2.3 5.6 22 3 2 1 14.937 29.874 2.98842 70.9 6.9 6.9 5.6 23 0 2 2 15.053 30.106 2.96585 22.5 2.2 2.2 5.6 24 4 0 0 15.215 30.431 2.935 785.2 76.8 75.9 5.6 25 2 0 2 15.368 30.735 2.90658 11.6 1.1 1.1 5.6 26 0 4 1 15.455 30.911 2.89051 13.5 1.3 1.3 5.6 27 1 2 2 15.538 31.076 2.87551 136.9 13.4 13.2 5.6 28 2 1 2 15.768 31.535 2.83464 179.6 17.6 17.3 5.6 29 2 4 0 15.892 31.784 2.81301 138.0 13.5 13.3 5.6 30 1 4 1 15.929 31.858 2.80669 150.9 14.7 14.6 5.6 31 4 2 0 16.777 33.554 2.66856 39.3 3.8 3.8 5.7 32 3 3 1 16.898 33.796 2.65003 140.8 13.8 13.6 5.7 33 4 1 1 17.027 34.053 2.63059 95.1 9.3 9.2 5.7 34 2 4 1 17.28 34.56 2.59316 150.9 14.7 14.5 5.7 35 1 3 2 17.438 34.877 2.57034 36.2 3.5 3.5 5.7 36 3 1 2 17.988 35.976 2.49432 127.2 12.4 12.2 5.7 37 3 4 0 18.099 36.197 2.47954 80.8 7.9 7.8 5.7 38 2 3 2 18.693 37.387 2.40334 154.1 15.1 14.8 5.7 39 3 4 1 19.348 38.695 2.32503 12.4 1.2 1.2 5.7 40 4 3 1 19.789 39.578 2.27517 34.3 3.4 3.3 5.7 41 5 0 1 20.345 40.69 2.21554 51.9 5.1 5.0 5.7 42 5 2 0 20.449 40.898 2.20474 29.6 2.9 2.8 5.7 43 0 1 3 20.521 41.042 2.19733 202.8 19.8 19.4 5.7 44 5 1 1 20.66 41.32 2.18318 16.5 1.6 1.6 5.7 45 1 1 3 20.894 41.788 2.15982 32.4 3.2 3.1 5.7 46 0 6 0 21.131 42.262 2.13667 43.6 4.3 4.2 5.7 47 1 6 0 21.495 42.991 2.10214 93.4 9.1 8.9 5.7 48 5 2 1 21.583 43.166 2.09399 75.2 7.4 7.2 5.7 49 1 2 3 21.809 43.618 2.07335 28.9 2.8 2.8 5.7 50 2 1 3 21.982 43.963 2.05787 78.5 7.7 7.5 5.7 51 0 6 1 22.237 44.474 2.03541 198.4 19.4 18.9 5.7 52 2 6 0 22.56 45.119 2.00779 22.5 2.2 2.1 5.7 53 1 5 2 22.591 45.182 2.00516 62.0 6.1 5.9 5.7 54 0 3 3 22.928 45.856 1.97723 16.6 1.6 1.6 5.7 55 5 3 1 23.055 46.111 1.96691 63.5 6.2 6.0 5.7 56 6 0 0 23.183 46.366 1.95667 114.8 11.2 10.9 5.7 57 1 3 3 23.27 46.54 1.94977 59.8 5.8 5.7 5.7 58 2 5 2 23.616 47.232 1.92279 103.3 10.1 9.8 5.7 59 5 1 2 23.908 47.816 1.90066 211.5 20.7 20.1 5.7 60 5 4 0 23.996 47.992 1.8941 161.4 15.8 15.3 5.7 61 3 6 0 24.251 48.503 1.87534 98.7 9.7 9.4 5.7 62 6 2 0 24.306 48.611 1.87142 19.4 1.9 1.8 5.7 63 6 1 1 24.49 48.98 1.85818 16.4 1.6 1.6 5.7 64 3 2 3 24.537 49.075 1.85482 40.7 4.0 3.9 5.7 65 5 2 2 24.735 49.47 1.84093 43.7 4.3 4.1 5.7 66 5 4 1 25.002 50.005 1.82248 33.5 3.3 3.2 5.7 67 3 5 2 25.254 50.507 1.80552 27.5 2.7 2.6 5.8 68 6 2 1 25.303 50.605 1.80225 68.7 6.7 6.5 5.8 69 3 3 3 25.879 51.759 1.76477 123.0 12.0 11.6 5.8 70 4 1 3 25.971 51.941 1.75899 158.1 15.5 14.9 5.8 71 1 7 1 26.166 52.331 1.74679 68.0 6.6 6.4 5.8 72 4 6 0 26.482 52.964 1.72741 39.1 3.8 3.7 5.8 73 6 3 1 26.617 53.233 1.71931 19.8 1.9 1.9 5.8 74 2 7 1 27.089 54.178 1.69152 22.7 2.2 2.1 5.8 75 6 1 2 27.387 54.774 1.67453 39.1 3.8 3.7 5.8 76 0 0 4 27.419 54.837 1.67275 208.2 20.3 19.6 5.8 77 6 4 0 27.467 54.934 1.67004 33.1 3.2 3.1 5.8 78 1 5 3 27.544 55.087 1.66575 118.5 11.6 11.2 5.8 79 0 1 4 27.671 55.342 1.65869 35.8 3.5 3.4 5.8 80 1 1 4 27.97 55.939 1.64238 29.3 2.9 2.8 5.8 81 4 3 3 28.017 56.034 1.63984 13.0 1.3 1.2 5.8 82 7 0 1 28.261 56.522 1.62682 37.3 3.6 3.5 5.8 83 7 2 0 28.343 56.685 1.62252 22.8 2.2 2.1 5.8 84 6 4 1 28.384 56.769 1.62033 63.8 6.2 6.0 5.8 85 2 5 3 28.436 56.873 1.61762 36.6 3.6 3.4 5.8 86 3 7 1 28.583 57.165 1.61003 60.1 5.9 5.6 5.8 87 1 2 4 28.712 57.424 1.60338 43.0 4.2 4.0 5.8 88 2 1 4 28.854 57.707 1.59619 18.0 1.8 1.7 5.8 89 1 7 2 28.944 57.888 1.59163 51.6 5.0 4.8 5.8 90 5 6 0 29.172 58.343 1.58029 37.9 3.7 3.6 5.8 91 7 2 1 29.242 58.484 1.57683 23.0 2.2 2.2 5.8 92 6 3 2 29.366 58.732 1.57076 106.9 10.5 10.0 5.8 93 5 2 3 29.424 58.847 1.56796 20.3 2.0 1.9 5.8 94 0 8 1 29.621 59.243 1.55843 59.5 5.8 5.6 5.8 95 1 8 1 29.908 59.815 1.54488 154.9 15.1 14.5 5.8 96 5 5 2 30.059 60.117 1.53783 15.4 1.5 1.4 5.8 97 3 1 4 30.29 60.581 1.52717 18.5 1.8 1.7 5.8 98 7 3 1 30.44 60.88 1.52037 33.1 3.2 3.1 5.8 99 4 7 1 30.594 61.187 1.51348 88.2 8.6 8.2 5.8 100 2 3 4 30.772 61.544 1.50556 34.4 3.4 3.2 5.8 101 3 2 4 30.998 61.996 1.49567 10.3 1.0 1.0 5.8 102 7 1 2 31.149 62.298 1.48914 51.5 5.0 4.8 5.8 103 7 4 0 31.223 62.445 1.48598 56.3 5.5 5.2 5.8 104 1 4 4 31.571 63.143 1.47123 63.6 6.2 5.9 5.9 105 8 0 0 31.661 63.322 1.4675 23.3 2.3 2.2 5.9 106 6 1 3 31.812 63.623 1.46128 28.0 2.7 2.6 5.9 107 4 0 4 32.007 64.014 1.45329 59.2 5.8 5.5 5.9 108 3 8 1 32.142 64.284 1.44784 33.4 3.3 3.1 5.9 109 4 1 4 32.237 64.474 1.44404 12.5 1.2 1.2 5.9 110 6 2 3 32.5 65.0 1.43361 13.7 1.3 1.3 5.9 111 8 2 0 32.58 65.159 1.43049 11.5 1.1 1.1 5.9 112 8 1 1 32.732 65.465 1.42455 13.1 1.3 1.2 5.9 113 0 7 3 32.971 65.942 1.41539 14.2 1.4 1.3 5.9 114 6 5 2 33.101 66.202 1.41047 108.6 10.6 10.1 5.9 115 4 7 2 33.135 66.27 1.40919 17.5 1.7 1.6 5.9 116 4 8 0 33.206 66.413 1.40651 12.5 1.2 1.2 5.9 117 1 7 3 33.241 66.482 1.40521 64.3 6.3 6.0 5.9 118 6 3 3 33.631 67.262 1.39079 29.0 2.8 2.7 5.9 119 3 4 4 33.744 67.487 1.3867 25.6 2.5 2.4 5.9 120 2 7 3 34.043 68.086 1.37596 85.0 8.3 7.8 5.9 121 5 5 3 34.275 68.55 1.36778 58.4 5.7 5.4 5.9 122 5 1 4 34.651 69.302 1.35475 21.9 2.1 2.0 5.9 123 6 4 3 35.184 70.368 1.33681 32.6 3.2 3.0 5.9 124 5 2 4 35.312 70.623 1.33261 15.4 1.5 1.4 5.9 125 3 7 3 35.361 70.721 1.33101 22.8 2.2 2.1 5.9 126 5 7 2 35.519 71.038 1.32584 40.5 4.0 3.7 5.9 127 7 6 0 35.723 71.446 1.31927 23.6 2.3 2.2 5.9 128 0 6 4 35.79 71.58 1.31713 15.4 1.5 1.4 5.9 129 7 2 3 35.95 71.899 1.31206 22.5 2.2 2.1 5.9 130 0 9 2 35.996 71.993 1.31059 11.5 1.1 1.1 5.9 131 8 4 1 36.062 72.125 1.30852 12.4 1.2 1.1 5.9 132 0 8 3 36.291 72.581 1.30141 30.7 3.0 2.8 6.0 133 5 8 1 36.387 72.773 1.29845 45.9 4.5 4.2 6.0 134 1 8 3 36.549 73.098 1.29348 54.1 5.3 5.0 6.0 135 5 6 3 36.683 73.365 1.28943 10.3 1.0 0.9 6.0 136 7 3 3 37.031 74.063 1.279 43.7 4.3 4.0 6.0 137 6 5 3 37.138 74.277 1.27584 10.7 1.0 1.0 6.0 138 4 7 3 37.171 74.342 1.27489 29.9 2.9 2.7 6.0 139 6 0 4 37.288 74.576 1.27146 10.3 1.0 0.9 6.0 140 2 8 3 37.319 74.638 1.27056 20.4 2.0 1.9 6.0 141 1 3 5 37.353 74.707 1.26956 14.3 1.4 1.3 6.0 142 6 1 4 37.503 75.005 1.26525 13.7 1.3 1.2 6.0 143 9 2 1 37.843 75.687 1.25554 16.4 1.6 1.5 6.0 144 5 4 4 37.905 75.81 1.2538 33.0 3.2 3.0 6.0 145 2 10 0 37.952 75.905 1.25248 25.2 2.5 2.3 6.0 146 8 5 1 37.999 75.998 1.25118 12.9 1.3 1.2 6.0 147 6 8 0 38.412 76.823 1.23977 21.9 2.1 2.0 6.0 148 0 7 4 38.583 77.167 1.23511 12.1 1.2 1.1 6.0 149 7 6 2 38.875 77.751 1.22729 10.7 1.0 1.0 6.0 150 8 1 3 39.138 78.276 1.22036 42.5 4.2 3.8 6.0 151 3 10 0 39.217 78.434 1.21829 28.3 2.8 2.6 6.0 152 5 7 3 39.453 78.907 1.21218 40.3 3.9 3.6 6.0 153 9 1 2 39.542 79.084 1.2099 13.4 1.3 1.2 6.0 154 2 4 5 39.6 79.2 1.20843 36.6 3.6 3.3 6.0 155 4 6 4 39.867 79.734 1.20167 21.2 2.1 1.9 6.0 156 4 8 3 40.35 80.701 1.1897 63.5 6.2 5.7 6.1 157 7 5 3 40.424 80.848 1.1879 22.4 2.2 2.0 6.1 158 3 7 4 40.842 81.685 1.17784 12.6 1.2 1.1 6.1 159 2 9 3 40.913 81.827 1.17615 38.1 3.7 3.4 6.1 160 5 0 5 41.493 82.986 1.16263 14.2 1.4 1.3 6.1 161 5 9 2 42.306 84.612 1.14439 21.2 2.1 1.9 6.1 162 1 11 1 42.383 84.765 1.14272 24.7 2.4 2.2 6.1 163 7 8 1 42.432 84.864 1.14164 26.1 2.6 2.3 6.1 164 10 2 1 42.601 85.202 1.13797 60.6 5.9 5.4 6.1 165 6 9 1 42.743 85.486 1.13492 20.5 2.0 1.8 6.1 166 0 6 5 42.78 85.56 1.13413 20.3 2.0 1.8 6.1 167 8 7 1 43.031 86.062 1.12879 10.5 1.0 0.9 6.1 168 9 6 0 43.777 87.554 1.11336 24.7 2.4 2.2 6.2 169 7 4 4 43.897 87.794 1.11094 31.3 3.1 2.8 6.2 170 5 10 1 43.962 87.924 1.10962 16.8 1.6 1.5 6.2 171 1 1 6 44.142 88.284 1.10603 16.3 1.6 1.4 6.2 172 8 0 4 44.287 88.574 1.10315 15.0 1.5 1.3 6.2 173 3 11 1 44.359 88.719 1.10173 16.8 1.6 1.5 6.2 174 0 2 6 44.516 89.032 1.09866 23.9 2.3 2.1 6.2 175 1 11 2 44.664 89.329 1.09578 18.1 1.8 1.6 6.2 176 1 2 6 44.762 89.525 1.09388 25.6 2.5 2.3 6.2 177 2 10 3 44.857 89.714 1.09206 11.9 1.2 1.0 6.2 Reference: Chichagov A.V. et al. Information-Calculating System on Crystal Structure Data of Minerals (MINCRYST) - Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian) |