Institute of Experimental Mineralogy Russian Academy of Sciences ------------------------------------------------- 142432, Chernogolovka, Moscow district A.V. Chichagov +7(496)52-22320 *** *** W W W - X R A Y P O L *** *********************** BURPALITE 1, t-cuspidine, f-baghdadite Na(2)CaZrSi(2)O(7)F(2) Monoclinic P 2(1)/a Z = 4 R =0.067 NR =1419 12 .12 .1991 Ref.Str.: Merlino S.,Perchiazzi N.,Khomyakhov A.P.,Pushcarovskii D.Y., Kulikova I.M.,Kuzmin V.I.(1990) * Eur. J. Mineral., 2, 177-185 Reserv: [Na(1.55)Ca(0.45)]CaZrSi(2)O(7)[F(1.55)O(0.45)] Initial data from BDM-file Lattice parameters (cub. angs.,degr.): a = 10.1173 alpha = 90.0 b = 10.4446 beta = 90.04 c = 7.2555 gamma = 90.0 Unit cell volume (cub. angs.) = 766.7 Molar volume ( cub.cm/mol.) = 115.45 Co-ordinates, thermal parameters, occupation for atomic positions: NoP x/a y/b z/c B(j) atom / occupation 1 0.107 0.8003 0.6247 1.21 Zr = 1.00 2 0.1052 0.8001 0.126 1.29 Ca = 1.00 3 0.3769 0.9257 0.8769 1.57 Na = 0.8 , Ca = 0.2 4 0.3744 0.9292 0.3759 1.39 Na = 0.75, Ca = 0.25 5 0.1671 0.1204 0.6521 1.07 Si = 1.00 6 0.1702 0.1215 0.0995 1.04 Si = 1.00 7 0.1681 0.1468 0.8794 3.23 O = 1.00 8 0.2658 0.2316 0.583 1.9 O = 1.00 9 0.266 0.2391 0.1652 2.24 O = 1.00 10 0.0189 0.1499 0.5909 2.25 O = 1.00 11 0.0171 0.1469 0.1584 2.49 O = 1.00 12 0.2148 0.9739 0.6158 1.43 O = 1.00 13 0.2243 0.9827 0.1381 1.98 O = 1.00 14 0.4894 0.111 0.8728 2.08 F = 1.00 15 0.4837 0.1203 0.3745 1.72 F = 0.55, O = 0.45 Co-ordinates for all atomic positions : No NoP x/a y/b z/c 1 1 0.107 0.8003 0.6247 2 2 0.1052 0.8001 0.126 3 3 0.3769 0.9257 0.8769 4 4 0.3744 0.9292 0.3759 5 5 0.1671 0.1204 0.6521 6 6 0.1702 0.1215 0.0995 7 7 0.1681 0.1468 0.8794 8 8 0.2658 0.2316 0.583 9 9 0.266 0.2391 0.1652 10 10 0.0189 0.1499 0.5909 11 11 0.0171 0.1469 0.1584 12 12 0.2148 0.9739 0.6158 13 13 0.2243 0.9827 0.1381 14 14 0.4894 0.111 0.8728 15 15 0.4837 0.1203 0.3745 16 1 0.893 0.1997 0.3753 17 2 0.8948 0.1999 0.874 18 3 0.6231 0.0743 0.1231 19 4 0.6256 0.0708 0.6241 20 5 0.8329 0.8796 0.3479 21 6 0.8298 0.8785 0.9005 22 7 0.8319 0.8532 0.1206 23 8 0.7342 0.7684 0.417 24 9 0.734 0.7609 0.8348 25 10 0.9811 0.8501 0.4091 26 11 0.9829 0.8531 0.8416 27 12 0.7852 0.0261 0.3842 28 13 0.7757 0.0173 0.8619 29 14 0.5106 0.889 0.1272 30 15 0.5163 0.8797 0.6255 31 1 0.607 0.6997 0.6247 32 2 0.6052 0.6999 0.126 33 3 0.8769 0.5743 0.8769 34 4 0.8744 0.5708 0.3759 35 5 0.6671 0.3796 0.6521 36 6 0.6702 0.3785 0.0995 37 7 0.6681 0.3532 0.8794 38 8 0.7658 0.2684 0.583 39 9 0.766 0.2609 0.1652 40 10 0.5189 0.3501 0.5909 41 11 0.5171 0.3531 0.1584 42 12 0.7148 0.5261 0.6158 43 13 0.7243 0.5173 0.1381 44 14 0.9894 0.389 0.8728 45 15 0.9837 0.3797 0.3745 46 1 0.393 0.3003 0.3753 47 2 0.3948 0.3001 0.874 48 3 0.1231 0.4257 0.1231 49 4 0.1256 0.4292 0.6241 50 5 0.3329 0.6204 0.3479 51 6 0.3298 0.6215 0.9005 52 7 0.3319 0.6468 0.1206 53 8 0.2342 0.7316 0.417 54 9 0.234 0.7391 0.8348 55 10 0.4811 0.6499 0.4091 56 11 0.4829 0.6469 0.8416 57 12 0.2852 0.4739 0.3842 58 13 0.2757 0.4827 0.8619 59 14 0.0106 0.611 0.1272 60 15 0.0163 0.6203 0.6255 X-ray density (g/cm cub.) = 3.38 MU (1/cm) = 249.332 Mass attenuation coefficient (cm**2/g) = 73.861 Selected interatomic distances (cation-anion,anion-anion): NoP Atom Rad.sph. C.N. Distance NoP N. (angs.) (angs.) 1 Zr 2.616 6 2.1169 12 2.0826 10 2.088 11 2.1082 8 2.093 9 2.092 15 2 Ca 2.88 8 2.2576 13 2.8204 7 2.4641 10 2.4682 11 2.7975 7 2.5825 8 2.5635 9 2.1948 14 3 Na ,Ca 2.88 6 2.5549 12 2.5167 13 2.2455 14 2.2959 14 2.356 15 2.4457 9 4 Na ,Ca 2.88 6 2.4205 12 2.3647 13 2.2818 15 2.3097 14 2.3674 15 2.5221 8 5 Si 2.1 4 1.6721 7 1.6119 8 1.5935 10 1.626 12 6 Si 2.1 4 1.6188 7 1.6355 9 1.6289 11 1.5746 13 7 O 3.264 7 2.5277 8 2.4915 9 2.5801 10 2.5369 11 2.6727 12 2.6043 13 3.1097 14 8 O 3.264 7 2.5277 7 3.0324 9 2.6404 10 2.7509 12 2.9162 15 2.8447 10 2.9196 12 9 O 3.264 7 2.4915 7 3.0324 8 2.6965 11 2.7181 13 2.9483 15 2.8061 11 2.9285 12 10 O 3.264 8 2.5801 7 2.6404 8 3.1382 11 2.7092 12 3.0833 12 2.8447 8 3.2419 14 2.89 15 11 O 3.264 7 2.5369 7 2.6965 9 3.1382 10 2.7125 13 3.1282 12 2.8061 9 2.913 15 12 O 3.264 8 2.6727 7 2.7509 8 2.7092 10 3.0833 10 3.1282 11 3.2058 15 2.9196 8 2.9285 9 13 O 3.264 4 2.6043 7 2.7181 9 2.7125 11 3.0585 14 14 F 3.228 4 3.0585 13 2.9713 14 3.0217 15 3.1097 7 15 F ,O 3.264 7 2.9162 8 2.9483 9 3.2058 12 3.0217 14 3.1208 15 2.89 10 2.913 11 X-ray diffraction powder data (II), X-Ray W.L. = 1.54056(angs.): No H K L Theta 2*Theta S LPG MF F I int. ( degree ) *100 1 1 1 0 6.085 12.169 0.069 175.04 4 35.6 150.6 2 0 0 1 6.094 12.189 0.069 174.48 2 42.5 107.3 3 0 1 1 7.427 14.854 0.084 116.74 4 43.7 151.4 4 0 2 0 8.482 16.964 0.096 88.99 2 128.9 503.4 5 1 1 -1 8.626 17.252 0.097 85.97 4 32.4 61.4 6 1 1 1 8.63 17.261 0.097 85.88 4 11.8 8.1 7 2 0 0 8.758 17.517 0.099 83.32 2 6.6 1.2 8 1 2 0 9.555 19.109 0.108 69.67 4 13.3 8.4 9 2 1 0 9.741 19.481 0.11 66.95 4 89.2 362.1 10 0 2 1 10.471 20.941 0.118 57.65 4 46.8 85.8 11 2 0 -1 10.694 21.388 0.12 55.18 2 99.6 186.2 12 2 0 1 10.701 21.402 0.121 55.1 2 57.3 61.6 13 1 2 -1 11.362 22.724 0.128 48.64 4 24.2 19.4 14 1 2 1 11.365 22.731 0.128 48.61 4 59.5 117.1 15 2 1 -1 11.519 23.037 0.13 47.27 4 51.2 84.4 16 2 1 1 11.525 23.05 0.13 47.21 4 83.2 222.5 17 2 2 0 12.239 24.479 0.138 41.63 4 39.6 44.4 18 0 0 2 12.259 24.518 0.138 41.49 2 0.4 0.0 19 0 1 2 12.99 25.979 0.146 36.73 4 75.2 141.5 20 1 3 0 13.532 27.063 0.152 33.69 4 176.6 715.1 21 2 2 -1 13.712 27.425 0.154 32.75 4 47.9 51.2 22 2 2 1 13.718 27.435 0.154 32.72 4 30.7 20.9 23 1 1 -2 13.726 27.451 0.154 32.68 4 73.9 121.4 24 1 1 2 13.731 27.462 0.154 32.66 4 74.7 124.2 25 3 1 0 13.887 27.775 0.156 31.88 4 87.4 165.7 26 0 3 1 14.206 28.411 0.159 30.38 4 48.6 48.7 27 1 3 -1 14.887 29.775 0.167 27.49 4 68.4 87.5 28 1 3 1 14.89 29.78 0.167 27.48 4 21.0 8.3 29 0 2 2 14.983 29.966 0.168 27.11 4 1.6 0.0 30 2 0 -2 15.141 30.283 0.17 26.51 2 333.7 1004.1 31 2 0 2 15.151 30.303 0.17 26.47 2 335.3 1012.7 32 3 1 -1 15.212 30.423 0.17 26.25 4 28.1 14.1 33 3 1 1 15.219 30.438 0.17 26.22 4 1.0 0.0 34 2 3 0 15.58 31.16 0.174 24.93 4 238.9 967.9 35 1 2 -2 15.633 31.266 0.175 24.75 4 15.1 3.8 36 1 2 2 15.638 31.275 0.175 24.73 4 13.1 2.9 37 2 1 -2 15.748 31.497 0.176 24.36 4 94.6 148.3 38 2 1 2 15.758 31.516 0.176 24.33 4 91.9 139.9 39 3 2 0 15.777 31.554 0.176 24.26 4 116.2 222.9 40 2 3 -1 16.784 33.568 0.187 21.22 4 23.5 8.0 41 2 3 1 16.789 33.577 0.187 21.21 4 7.9 0.9 42 3 2 -1 16.967 33.935 0.189 20.73 4 1.9 0.1 43 3 2 1 16.974 33.948 0.19 20.71 4 34.0 16.3 44 0 4 0 17.157 34.315 0.191 20.23 2 66.4 30.4 45 2 2 -2 17.456 34.912 0.195 19.48 4 62.1 51.1 46 2 2 2 17.465 34.929 0.195 19.46 4 64.6 55.3 47 4 0 0 17.73 35.461 0.198 18.83 2 122.6 96.4 48 1 4 0 17.738 35.476 0.198 18.81 4 11.6 1.7 49 0 3 2 17.857 35.715 0.199 18.54 4 143.8 260.7 50 4 1 0 18.261 36.522 0.203 17.65 4 109.8 144.9 51 0 4 1 18.271 36.543 0.204 17.63 4 38.2 17.5 52 1 3 -2 18.417 36.833 0.205 17.32 4 97.2 111.3 53 1 3 2 18.421 36.842 0.205 17.32 4 95.3 106.9 54 3 3 0 18.542 37.083 0.206 17.07 4 102.7 122.5 55 0 0 3 18.572 37.144 0.207 17.01 2 12.1 0.9 56 3 1 -2 18.684 37.368 0.208 16.78 4 37.0 15.7 57 3 1 2 18.697 37.393 0.208 16.76 4 40.1 18.4 58 4 0 -1 18.811 37.622 0.209 16.54 2 29.7 4.9 59 4 0 1 18.819 37.638 0.209 16.52 2 15.9 1.4 60 1 4 -1 18.821 37.642 0.209 16.52 4 4.3 0.2 61 1 4 1 18.823 37.646 0.209 16.51 4 47.8 25.7 62 0 1 3 19.082 38.164 0.212 16.02 4 18.0 3.5 63 4 1 -1 19.316 38.631 0.215 15.6 4 15.6 2.6 64 4 1 1 19.324 38.647 0.215 15.58 4 21.8 5.0 65 2 4 0 19.389 38.778 0.215 15.47 4 84.3 74.8 66 3 3 -1 19.585 39.169 0.218 15.12 4 35.0 12.6 67 3 3 1 19.591 39.181 0.218 15.11 4 18.5 3.5 68 1 1 -3 19.61 39.221 0.218 15.08 4 1.7 0.0 69 1 1 3 19.616 39.233 0.218 15.07 4 15.1 2.3 70 4 2 0 19.778 39.556 0.22 14.8 4 64.9 42.4 71 2 3 -2 20.018 40.035 0.222 14.41 4 19.4 3.7 72 2 3 2 20.026 40.051 0.222 14.39 4 20.5 4.1 73 3 2 -2 20.174 40.349 0.224 14.16 4 112.2 121.3 74 3 2 2 20.186 40.372 0.224 14.14 4 108.0 112.2 75 2 4 -1 20.396 40.792 0.226 13.82 4 18.2 3.1 76 2 4 1 20.4 40.8 0.226 13.81 4 16.6 2.6 77 0 2 3 20.548 41.096 0.228 13.59 4 11.6 1.2 78 2 0 -3 20.667 41.333 0.229 13.42 2 30.3 4.2 79 2 0 3 20.678 41.356 0.229 13.4 2 47.7 10.4 80 4 2 -1 20.768 41.535 0.23 13.27 4 7.3 0.5 81 4 2 1 20.775 41.551 0.23 13.26 4 28.6 7.4 82 1 2 -3 21.045 42.091 0.233 12.88 4 20.5 3.7 83 1 2 3 21.051 42.102 0.233 12.88 4 3.2 0.1 84 2 1 -3 21.134 42.268 0.234 12.76 4 40.7 14.4 85 2 1 3 21.145 42.291 0.234 12.75 4 21.8 4.1 86 0 4 2 21.313 42.626 0.236 12.52 4 0.9 0.0 87 4 0 -2 21.786 43.571 0.241 11.92 2 42.3 7.3 88 1 4 -2 21.797 43.595 0.241 11.91 4 73.9 44.2 89 4 0 2 21.8 43.6 0.241 11.9 2 45.2 8.3 90 1 4 2 21.801 43.602 0.241 11.9 4 66.8 36.1 91 3 4 0 21.906 43.812 0.242 11.78 4 114.3 104.8 92 4 3 0 22.112 44.225 0.244 11.53 4 18.2 2.6 93 1 5 0 22.118 44.237 0.244 11.52 4 165.3 214.2 94 4 1 -2 22.234 44.468 0.246 11.39 4 111.4 96.1 95 4 1 2 22.248 44.497 0.246 11.37 4 111.8 96.8 96 3 3 -2 22.475 44.95 0.248 11.11 4 146.7 162.8 97 3 3 2 22.486 44.971 0.248 11.1 4 146.3 161.7 98 2 2 -3 22.489 44.979 0.248 11.1 4 11.4 1.0 99 2 2 3 22.5 45.0 0.248 11.09 4 49.4 18.4 100 0 5 1 22.565 45.129 0.249 11.02 4 12.4 1.1 101 5 1 0 22.815 45.629 0.252 10.74 4 43.1 13.6 102 0 3 3 22.818 45.635 0.252 10.74 4 2.2 0.0 103 3 4 -1 22.821 45.642 0.252 10.74 4 50.5 18.7 104 3 4 1 22.826 45.652 0.252 10.73 4 27.9 5.7 105 4 3 -1 23.02 46.04 0.254 10.53 4 40.1 11.5 106 4 3 1 23.027 46.054 0.254 10.52 4 4.4 0.1 107 1 5 -1 23.029 46.057 0.254 10.52 4 47.2 15.9 108 1 5 1 23.03 46.061 0.254 10.52 4 16.8 2.0 109 2 4 -2 23.205 46.409 0.256 10.34 4 18.0 2.3 110 2 4 2 23.212 46.423 0.256 10.33 4 22.3 3.5 111 1 3 -3 23.276 46.552 0.257 10.27 4 5.6 0.2 112 1 3 3 23.281 46.563 0.257 10.26 4 36.5 9.3 113 3 1 -3 23.496 46.992 0.259 10.05 4 29.6 6.0 114 3 1 3 23.511 47.023 0.259 10.04 4 10.3 0.7 115 2 5 0 23.512 47.025 0.259 10.04 4 16.0 1.8 116 4 2 -2 23.539 47.078 0.259 10.01 4 99.0 66.8 117 4 2 2 23.553 47.105 0.259 10.0 4 94.6 60.9 118 5 1 -1 23.7 47.401 0.261 9.86 4 32.0 6.8 119 5 1 1 23.709 47.418 0.261 9.85 4 4.5 0.1 120 5 2 0 24.095 48.19 0.265 9.49 4 17.2 1.9 121 2 5 -1 24.381 48.762 0.268 9.24 4 8.0 0.4 122 2 5 1 24.385 48.769 0.268 9.24 4 33.5 7.1 123 2 3 -3 24.617 49.233 0.27 9.04 4 64.0 25.2 124 2 3 3 24.627 49.253 0.27 9.03 4 4.6 0.1 125 3 2 -3 24.749 49.498 0.272 8.93 4 16.7 1.7 126 3 2 3 24.764 49.528 0.272 8.92 4 57.3 19.9 127 5 2 -1 24.946 49.892 0.274 8.77 4 4.8 0.1 128 5 2 1 24.954 49.909 0.274 8.77 4 49.2 14.4 129 4 4 0 25.087 50.173 0.275 8.66 4 0.2 0.0 130 0 0 4 25.129 50.258 0.276 8.63 2 376.0 415.1 131 0 5 2 25.183 50.366 0.276 8.59 4 17.8 1.9 132 3 4 -2 25.417 50.833 0.279 8.41 4 31.0 5.5 133 3 4 2 25.426 50.853 0.279 8.4 4 30.8 5.4 134 0 1 4 25.532 51.064 0.28 8.32 4 1.3 0.0 135 4 3 -2 25.599 51.199 0.28 8.27 4 205.3 237.1 136 1 5 -2 25.61 51.22 0.281 8.26 4 114.7 74.0 137 4 3 2 25.612 51.225 0.281 8.26 4 204.7 235.6 138 1 5 2 25.613 51.226 0.281 8.26 4 113.7 72.6 139 3 5 0 25.706 51.412 0.282 8.19 4 16.6 1.5 140 0 4 3 25.729 51.459 0.282 8.18 4 8.7 0.4 141 4 4 -1 25.914 51.829 0.284 8.04 4 2.4 0.0 142 4 4 1 25.921 51.842 0.284 8.04 4 32.4 5.7 143 1 1 -4 25.953 51.907 0.284 8.02 4 12.5 0.9 144 1 1 4 25.96 51.919 0.284 8.01 4 6.1 0.2 145 5 3 0 26.123 52.246 0.286 7.9 4 115.0 71.1 146 4 0 -3 26.137 52.273 0.286 7.89 2 106.4 30.4 147 1 4 -3 26.149 52.298 0.286 7.88 4 46.7 11.7 148 1 4 3 26.154 52.308 0.286 7.88 4 16.8 1.5 149 4 0 3 26.156 52.311 0.286 7.88 2 39.9 4.3 150 5 1 -2 26.229 52.458 0.287 7.83 4 16.3 1.4 151 5 1 2 26.245 52.489 0.287 7.82 4 13.6 1.0 152 0 6 0 26.263 52.526 0.287 7.8 2 3.2 0.0 153 3 5 -1 26.521 53.041 0.29 7.63 4 10.8 0.6 154 3 5 1 26.525 53.051 0.29 7.63 4 60.8 19.2 155 4 1 -3 26.529 53.057 0.29 7.63 4 26.2 3.6 156 4 1 3 26.547 53.095 0.29 7.61 4 88.6 40.7 157 1 6 0 26.679 53.359 0.291 7.53 4 172.5 152.5 158 0 2 4 26.715 53.429 0.292 7.51 4 68.3 23.8 159 3 3 -3 26.741 53.482 0.292 7.49 4 64.3 21.0 160 3 3 3 26.755 53.51 0.292 7.48 4 2.3 0.0 161 2 0 -4 26.81 53.62 0.293 7.45 2 12.6 0.4 162 2 0 4 26.823 53.646 0.293 7.44 2 11.2 0.3 163 2 5 -2 26.865 53.729 0.293 7.41 4 0.9 0.0 164 2 5 2 26.871 53.742 0.293 7.41 4 0.8 0.0 165 5 3 -1 26.927 53.854 0.294 7.37 4 61.5 19.0 166 5 3 1 26.935 53.87 0.294 7.37 4 20.4 2.1 167 0 6 1 27.068 54.137 0.295 7.28 4 10.1 0.5 168 1 2 -4 27.123 54.246 0.296 7.25 4 33.9 5.7 169 1 2 4 27.129 54.258 0.296 7.25 4 26.8 3.5 170 6 0 0 27.181 54.363 0.297 7.22 2 1.5 0.0 171 2 1 -4 27.195 54.391 0.297 7.21 4 70.9 24.6 172 2 1 4 27.208 54.416 0.297 7.2 4 72.9 26.1 173 2 4 -3 27.386 54.772 0.299 7.09 4 15.8 1.2 174 5 2 -2 27.39 54.78 0.299 7.09 4 178.9 154.4 175 2 4 3 27.395 54.79 0.299 7.09 4 56.1 15.2 176 5 2 2 27.406 54.811 0.299 7.08 4 182.5 160.5 177 1 6 -1 27.475 54.951 0.299 7.04 4 22.1 2.3 178 1 6 1 27.477 54.954 0.299 7.04 4 46.0 10.2 179 6 1 0 27.563 55.126 0.3 6.99 4 63.8 19.4 180 4 2 -3 27.681 55.362 0.302 6.92 4 55.0 14.2 181 4 2 3 27.7 55.399 0.302 6.91 4 11.3 0.6 182 2 6 0 27.902 55.804 0.304 6.8 4 23.5 2.6 183 6 0 -1 27.964 55.928 0.304 6.77 2 66.2 10.1 184 6 0 1 27.973 55.946 0.304 6.76 2 7.2 0.1 185 4 4 -2 28.3 56.601 0.308 6.58 4 33.6 5.1 186 4 4 2 28.312 56.625 0.308 6.58 4 34.6 5.4 187 2 2 -4 28.33 56.659 0.308 6.57 4 37.6 6.3 188 6 1 -1 28.338 56.677 0.308 6.56 4 10.5 0.5 189 2 2 4 28.342 56.683 0.308 6.56 4 35.0 5.5 190 6 1 1 28.347 56.695 0.308 6.56 4 58.1 15.1 191 4 5 0 28.571 57.142 0.31 6.44 4 59.4 15.5 192 0 3 4 28.61 57.219 0.311 6.42 4 0.5 0.0 193 2 6 -1 28.674 57.349 0.311 6.39 4 31.1 4.2 194 2 6 1 28.677 57.355 0.311 6.39 4 3.8 0.1 195 6 2 0 28.688 57.375 0.312 6.38 4 78.0 26.4 196 5 4 0 28.79 57.58 0.313 6.33 4 9.7 0.4 197 3 5 -2 28.873 57.746 0.313 6.29 4 128.9 71.1 198 3 5 2 28.882 57.763 0.314 6.29 4 129.6 71.8 199 1 3 -4 29.0 58.0 0.315 6.23 4 104.9 46.7 200 1 3 4 29.006 58.012 0.315 6.23 4 108.9 50.3 201 0 5 3 29.16 58.32 0.316 6.15 4 4.7 0.1 202 3 1 -4 29.187 58.374 0.317 6.14 4 49.9 10.4 203 3 1 4 29.205 58.409 0.317 6.13 4 51.8 11.2 204 5 3 -2 29.256 58.512 0.317 6.11 4 54.6 12.4 205 5 3 2 29.271 58.541 0.317 6.1 4 56.3 13.2 206 4 5 -1 29.33 58.66 0.318 6.07 4 13.1 0.7 207 4 5 1 29.336 58.672 0.318 6.07 4 4.4 0.1 208 3 4 -3 29.37 58.739 0.318 6.06 4 11.3 0.5 209 3 4 3 29.383 58.766 0.318 6.05 4 42.9 7.6 210 0 6 2 29.393 58.786 0.319 6.04 4 0.5 0.0 211 6 2 -1 29.443 58.887 0.319 6.02 4 44.3 8.1 212 6 2 1 29.452 58.905 0.319 6.02 4 4.5 0.1 213 4 3 -3 29.535 59.07 0.32 5.98 4 23.9 2.3 214 5 4 -1 29.545 59.09 0.32 5.97 4 21.8 1.9 215 1 5 -3 29.546 59.093 0.32 5.97 4 26.6 2.9 216 1 5 3 29.551 59.102 0.32 5.97 4 62.7 16.0 217 5 4 1 29.552 59.104 0.32 5.97 4 54.3 12.0 218 4 3 3 29.552 59.105 0.32 5.97 4 23.6 2.3 219 1 6 -2 29.779 59.557 0.322 5.87 4 184.5 135.9 220 1 6 2 29.781 59.563 0.322 5.87 4 181.4 131.4 221 3 6 0 29.866 59.731 0.323 5.83 4 135.0 72.3 222 5 1 -3 30.107 60.215 0.326 5.73 4 19.8 1.5 223 5 1 3 30.129 60.259 0.326 5.72 4 0.6 0.0 224 2 3 -4 30.158 60.315 0.326 5.71 4 156.3 94.9 225 2 3 4 30.169 60.338 0.326 5.7 4 154.2 92.3 226 6 0 -2 30.239 60.479 0.327 5.67 2 110.8 23.7 227 6 0 2 30.257 60.514 0.327 5.66 2 110.7 23.6 228 3 2 -4 30.272 60.545 0.327 5.66 4 83.5 26.8 229 3 2 4 30.29 60.58 0.327 5.65 4 88.7 30.3 230 6 3 0 30.502 61.004 0.329 5.56 4 108.2 44.3 231 6 1 -2 30.596 61.193 0.33 5.53 4 88.1 29.2 232 3 6 -1 30.606 61.211 0.33 5.52 4 70.2 18.5 233 3 6 1 30.61 61.22 0.331 5.52 4 4.6 0.1 234 6 1 2 30.614 61.227 0.331 5.52 4 89.1 29.8 235 2 5 -3 30.692 61.384 0.331 5.49 4 13.1 0.6 236 2 5 3 30.701 61.401 0.331 5.48 4 19.2 1.4 237 2 6 -2 30.92 61.839 0.334 5.4 4 9.1 0.3 238 2 6 2 30.925 61.851 0.334 5.4 4 10.2 0.4 239 0 4 4 31.136 62.272 0.336 5.32 4 36.8 4.9 240 5 2 -3 31.174 62.347 0.336 5.3 4 6.2 0.1 241 5 2 3 31.195 62.39 0.336 5.29 4 24.1 2.1 242 6 3 -1 31.231 62.462 0.337 5.28 4 14.6 0.8 243 6 3 1 31.239 62.479 0.337 5.28 4 25.4 2.3 244 1 7 0 31.455 62.91 0.339 5.2 4 7.8 0.2 245 4 0 -4 31.494 62.987 0.339 5.18 2 123.8 27.0 246 1 4 -4 31.507 63.014 0.339 5.18 4 21.0 1.6 247 1 4 4 31.513 63.025 0.339 5.18 4 25.9 2.4 248 4 0 4 31.516 63.032 0.339 5.18 2 120.8 25.7 249 4 5 -2 31.546 63.091 0.34 5.17 4 29.5 3.1 250 4 5 2 31.557 63.114 0.34 5.16 4 28.6 2.9 251 6 2 -2 31.653 63.305 0.341 5.13 4 77.2 20.8 252 6 2 2 31.67 63.339 0.341 5.12 4 76.3 20.3 253 5 4 -2 31.751 63.501 0.342 5.09 4 86.9 26.1 254 5 4 2 31.765 63.529 0.342 5.09 4 87.0 26.2 255 0 7 1 31.806 63.612 0.342 5.07 4 21.6 1.6 256 4 1 -4 31.842 63.685 0.342 5.06 4 80.2 22.2 257 4 1 4 31.865 63.73 0.343 5.05 4 83.9 24.2 258 5 5 0 32.005 64.009 0.344 5.0 4 140.8 67.5 259 4 4 -3 32.017 64.033 0.344 5.0 4 2.5 0.0 260 3 3 -4 32.032 64.065 0.344 5.0 4 75.7 19.5 261 4 4 3 32.033 64.067 0.344 4.99 4 20.3 1.4 262 3 3 4 32.049 64.099 0.344 4.99 4 81.0 22.3 263 0 0 5 32.061 64.122 0.345 4.99 2 33.5 1.9 264 1 7 -1 32.175 64.35 0.346 4.95 4 38.1 4.9 265 1 7 1 32.176 64.353 0.346 4.95 4 15.2 0.8 266 0 1 5 32.407 64.813 0.348 4.87 4 32.5 3.5 267 4 6 0 32.491 64.982 0.349 4.84 4 10.6 0.4 268 7 1 0 32.549 65.098 0.349 4.82 4 40.0 5.3 269 3 5 -3 32.55 65.1 0.349 4.82 4 25.1 2.1 270 3 5 3 32.563 65.125 0.349 4.82 4 20.5 1.4 271 2 7 0 32.563 65.127 0.349 4.82 4 110.4 40.0 272 2 4 -4 32.612 65.223 0.35 4.81 4 29.9 2.9 273 2 4 4 32.623 65.245 0.35 4.8 4 27.6 2.5 274 5 5 -1 32.715 65.431 0.351 4.77 4 34.9 3.9 275 5 5 1 32.722 65.444 0.351 4.77 4 25.6 2.1 276 1 1 -5 32.769 65.538 0.351 4.76 4 24.3 1.9 277 3 6 -2 32.771 65.542 0.351 4.75 4 86.4 24.2 278 1 1 5 32.776 65.552 0.351 4.75 4 13.9 0.6 279 3 6 2 32.779 65.559 0.351 4.75 4 84.3 23.0 280 4 2 -4 32.876 65.752 0.352 4.72 4 63.5 13.0 281 4 2 4 32.898 65.797 0.353 4.72 4 63.1 12.8 282 5 3 -3 32.906 65.812 0.353 4.71 4 32.3 3.3 283 5 3 3 32.927 65.854 0.353 4.71 4 27.3 2.4 284 6 4 0 32.941 65.883 0.353 4.7 4 146.9 69.0 285 0 6 3 33.038 66.076 0.354 4.67 4 5.8 0.1 286 4 6 -1 33.197 66.393 0.355 4.63 4 0.7 0.0 287 4 6 1 33.202 66.404 0.355 4.62 4 11.0 0.4 288 7 1 -1 33.252 66.505 0.356 4.61 4 5.4 0.1 289 7 1 1 33.262 66.524 0.356 4.61 4 0.2 0.0 290 2 7 -1 33.27 66.54 0.356 4.6 4 8.4 0.2 291 2 7 1 33.273 66.545 0.356 4.6 4 22.8 1.6 292 6 3 -2 33.372 66.744 0.357 4.57 4 6.5 0.1 293 6 3 2 33.388 66.777 0.357 4.57 4 6.4 0.1 294 1 6 -3 33.398 66.797 0.357 4.57 4 65.5 13.3 295 1 6 3 33.403 66.805 0.357 4.57 4 8.9 0.2 296 0 2 5 33.431 66.863 0.358 4.56 4 39.7 4.9 297 2 0 -5 33.513 67.027 0.358 4.53 2 81.1 10.1 298 2 0 5 33.527 67.054 0.359 4.53 2 42.6 2.8 299 7 2 0 33.572 67.143 0.359 4.52 4 182.2 102.0 300 6 4 -1 33.641 67.282 0.36 4.5 4 2.4 0.0 301 6 4 1 33.649 67.299 0.36 4.5 4 10.0 0.3 302 1 2 -5 33.788 67.576 0.361 4.46 4 31.2 3.0 303 1 2 5 33.795 67.59 0.361 4.45 4 54.0 8.8 304 6 0 -3 33.828 67.656 0.361 4.45 2 23.9 0.9 305 2 1 -5 33.851 67.702 0.362 4.44 4 42.2 5.4 306 6 0 3 33.853 67.705 0.362 4.44 2 27.3 1.1 307 2 1 5 33.865 67.73 0.362 4.44 4 69.9 14.7 308 0 7 2 33.932 67.863 0.362 4.42 4 121.7 44.5 309 6 1 -3 34.164 68.328 0.365 4.36 4 34.4 3.5 310 6 1 3 34.189 68.377 0.365 4.35 4 15.3 0.7 311 0 5 4 34.223 68.446 0.365 4.34 4 1.0 0.0 312 7 2 -1 34.264 68.528 0.365 4.33 4 7.1 0.1 313 7 2 1 34.274 68.547 0.366 4.33 4 11.5 0.4 314 1 7 -2 34.288 68.576 0.366 4.32 4 5.1 0.1 315 1 7 2 34.291 68.581 0.366 4.32 4 7.3 0.2 316 3 7 0 34.369 68.737 0.366 4.3 4 32.0 3.0 317 3 4 -4 34.413 68.826 0.367 4.29 4 81.8 19.6 318 3 4 4 34.429 68.858 0.367 4.29 4 81.5 19.4 319 2 6 -3 34.472 68.944 0.367 4.28 4 22.9 1.5 320 2 6 3 34.48 68.96 0.367 4.27 4 19.7 1.1 321 4 3 -4 34.564 69.127 0.368 4.25 4 2.3 0.0 322 1 5 -4 34.576 69.153 0.368 4.25 4 118.2 40.4 323 1 5 4 34.582 69.164 0.368 4.25 4 122.9 43.7 324 4 3 4 34.585 69.171 0.368 4.25 4 2.7 0.0 325 5 5 -2 34.809 69.618 0.371 4.19 4 11.2 0.4 326 5 5 2 34.822 69.645 0.371 4.19 4 14.0 0.6 327 2 2 -5 34.855 69.709 0.371 4.18 4 29.1 2.4 328 2 2 5 34.868 69.736 0.371 4.18 4 23.6 1.6 329 3 7 -1 35.056 70.113 0.373 4.13 4 2.2 0.0 330 3 7 1 35.06 70.121 0.373 4.13 4 41.6 4.9 331 4 5 -3 35.063 70.126 0.373 4.13 4 1.6 0.0 332 4 5 3 35.079 70.158 0.373 4.13 4 8.7 0.2 333 5 1 -4 35.09 70.18 0.373 4.12 4 16.6 0.8 334 0 3 5 35.106 70.212 0.373 4.12 4 53.3 8.0 335 5 1 4 35.117 70.234 0.373 4.12 4 21.4 1.3 336 6 2 -3 35.163 70.327 0.374 4.11 4 13.5 0.5 337 6 2 3 35.187 70.375 0.374 4.1 4 42.8 5.1 338 7 3 0 35.243 70.486 0.375 4.09 4 44.3 5.5 339 5 4 -3 35.257 70.514 0.375 4.08 4 46.7 6.1 340 5 4 3 35.277 70.554 0.375 4.08 4 35.0 3.4 341 4 6 -2 35.277 70.554 0.375 4.08 4 17.1 0.8 342 4 6 2 35.288 70.576 0.375 4.08 4 16.0 0.7 343 7 1 -2 35.329 70.658 0.375 4.07 4 13.0 0.5 344 7 1 2 35.348 70.696 0.376 4.06 4 14.3 0.6 345 2 7 -2 35.349 70.699 0.376 4.06 4 59.5 9.8 346 2 7 2 35.355 70.71 0.376 4.06 4 60.7 10.2 347 1 3 -5 35.455 70.909 0.377 4.04 4 53.7 7.9 348 1 3 5 35.461 70.923 0.377 4.04 4 17.1 0.8 349 3 1 -5 35.621 71.242 0.378 4.0 4 34.0 3.1 350 2 5 -4 35.633 71.265 0.378 4.0 4 1.6 0.0 351 3 1 5 35.641 71.282 0.378 4.0 4 13.1 0.5 352 2 5 4 35.643 71.287 0.378 4.0 4 0.7 0.0 353 6 4 -2 35.708 71.416 0.379 3.98 4 31.2 2.6 354 5 6 0 35.712 71.424 0.379 3.98 4 68.0 12.5 355 6 4 2 35.724 71.448 0.379 3.98 4 33.5 3.0 356 7 3 -1 35.921 71.841 0.381 3.94 4 21.4 1.2 357 7 3 1 35.93 71.86 0.381 3.93 4 29.2 2.3 358 6 5 0 35.949 71.898 0.381 3.93 4 64.3 11.1 359 5 2 -4 36.078 72.156 0.382 3.9 4 11.1 0.3 360 5 2 4 36.104 72.209 0.382 3.9 4 11.4 0.3 361 0 8 0 36.157 72.313 0.383 3.89 2 27.2 1.0 362 3 6 -3 36.23 72.46 0.384 3.87 4 22.4 1.3 363 3 6 3 36.242 72.483 0.384 3.87 4 26.9 1.9 364 7 2 -2 36.314 72.628 0.384 3.85 4 32.1 2.7 365 7 2 2 36.333 72.665 0.385 3.85 4 33.0 2.8 366 5 6 -1 36.387 72.774 0.385 3.84 4 24.1 1.5 367 5 6 1 36.394 72.787 0.385 3.84 4 29.5 2.3 368 2 3 -5 36.499 72.999 0.386 3.82 4 23.9 1.5 369 1 8 0 36.504 73.009 0.386 3.82 4 24.2 1.5 370 2 3 5 36.512 73.025 0.386 3.81 4 21.9 1.2 371 3 2 -5 36.603 73.206 0.387 3.8 4 21.4 1.2 372 6 5 -1 36.622 73.244 0.387 3.79 4 2.4 0.0 373 3 2 5 36.623 73.246 0.387 3.79 4 44.4 5.1 374 6 5 1 36.63 73.26 0.387 3.79 4 7.5 0.1 375 6 3 -3 36.802 73.604 0.389 3.76 4 34.5 3.0 376 4 7 0 36.825 73.651 0.389 3.75 4 20.2 1.0 377 6 3 3 36.826 73.652 0.389 3.75 4 13.8 0.5 378 0 8 1 36.832 73.664 0.389 3.75 4 36.5 3.4 379 4 4 -4 36.866 73.731 0.389 3.75 4 7.4 0.1 380 4 4 4 36.887 73.773 0.39 3.74 4 8.6 0.2 381 3 7 -2 37.09 74.18 0.391 3.7 4 49.9 6.3 382 3 7 2 37.098 74.196 0.392 3.7 4 47.7 5.7 383 1 8 -1 37.177 74.353 0.392 3.69 4 14.7 0.5 384 1 8 1 37.178 74.356 0.392 3.69 4 14.8 0.5 385 0 7 3 37.343 74.686 0.394 3.66 4 11.4 0.3 386 3 5 -4 37.367 74.734 0.394 3.65 4 22.1 1.2 387 3 5 4 37.382 74.765 0.394 3.65 4 21.3 1.1 388 0 4 5 37.394 74.787 0.394 3.65 4 49.0 6.0 389 4 7 -1 37.493 74.987 0.395 3.63 4 27.7 1.9 390 4 7 1 37.499 74.997 0.395 3.63 4 11.6 0.3 391 8 0 0 37.523 75.046 0.395 3.63 2 115.1 16.3 392 7 4 0 37.527 75.055 0.395 3.62 4 72.1 12.8 393 2 8 0 37.541 75.082 0.396 3.62 4 44.3 4.8 394 1 7 -3 37.685 75.37 0.397 3.6 4 0.6 0.0 395 1 7 3 37.689 75.378 0.397 3.6 4 52.5 6.7 396 5 3 -4 37.701 75.402 0.397 3.59 4 96.5 22.8 397 4 0 -5 37.72 75.44 0.397 3.59 2 15.1 0.3 398 5 3 4 37.727 75.454 0.397 3.59 4 88.6 19.2 399 1 4 -5 37.734 75.468 0.397 3.59 4 14.5 0.5 400 1 4 5 37.741 75.481 0.397 3.59 4 35.1 3.0 401 4 0 5 37.746 75.492 0.397 3.59 2 28.8 1.0 402 0 6 4 37.829 75.657 0.398 3.57 4 1.4 0.0 403 8 1 0 37.845 75.69 0.398 3.57 4 133.2 43.1 404 7 3 -2 37.933 75.867 0.399 3.55 4 69.3 11.6 405 7 3 2 37.952 75.903 0.399 3.55 4 69.1 11.5 406 4 1 -5 38.041 76.083 0.4 3.54 4 18.7 0.8 407 4 1 5 38.067 76.135 0.4 3.53 4 13.7 0.5 408 1 6 -4 38.168 76.336 0.401 3.52 4 123.6 36.6 409 1 6 4 38.173 76.347 0.401 3.52 4 126.2 38.1 410 5 5 -3 38.184 76.368 0.401 3.51 4 22.4 1.2 411 8 0 -1 38.184 76.368 0.401 3.51 2 17.0 0.3 412 7 4 -1 38.189 76.379 0.401 3.51 4 28.8 2.0 413 8 0 1 38.195 76.389 0.401 3.51 2 42.6 2.2 414 7 4 1 38.198 76.397 0.401 3.51 4 29.8 2.1 415 5 5 3 38.204 76.407 0.401 3.51 4 49.4 5.8 416 2 8 -1 38.206 76.412 0.401 3.51 4 17.3 0.7 417 2 8 1 38.208 76.417 0.401 3.51 4 22.0 1.2 418 3 3 -5 38.218 76.435 0.402 3.51 4 40.2 3.9 419 3 3 5 38.237 76.474 0.402 3.51 4 4.9 0.1 420 5 6 -2 38.392 76.784 0.403 3.48 4 47.8 5.4 421 5 6 2 38.405 76.81 0.403 3.48 4 49.9 5.9 422 8 1 -1 38.504 77.009 0.404 3.46 4 45.4 4.9 423 8 1 1 38.515 77.03 0.404 3.46 4 3.5 0.0 424 6 0 -4 38.572 77.144 0.405 3.45 2 11.8 0.2 425 6 0 4 38.603 77.206 0.405 3.45 2 11.5 0.2 426 6 5 -2 38.622 77.244 0.405 3.45 4 31.2 2.3 427 4 6 -3 38.637 77.274 0.405 3.44 4 2.1 0.0 428 6 5 2 38.638 77.275 0.405 3.44 4 34.4 2.8 429 4 6 3 38.652 77.305 0.405 3.44 4 3.9 0.0 430 7 1 -3 38.685 77.37 0.406 3.44 4 19.3 0.9 431 2 7 -3 38.708 77.416 0.406 3.43 4 32.1 2.4 432 7 1 3 38.712 77.425 0.406 3.43 4 12.9 0.4 433 2 7 3 38.716 77.432 0.406 3.43 4 28.9 1.9 434 2 4 -5 38.756 77.511 0.406 3.43 4 48.9 5.6 435 2 4 5 38.768 77.537 0.406 3.42 4 24.0 1.3 436 8 2 0 38.806 77.612 0.407 3.42 4 39.3 3.6 437 0 8 2 38.832 77.664 0.407 3.41 4 2.7 0.0 438 6 1 -4 38.891 77.782 0.408 3.41 4 52.9 6.5 439 6 1 4 38.922 77.844 0.408 3.4 4 55.8 7.2 440 4 2 -5 39.001 78.001 0.409 3.39 4 7.9 0.1 441 4 2 5 39.026 78.053 0.409 3.39 4 14.8 0.5 442 6 4 -3 39.052 78.105 0.409 3.38 4 9.3 0.2 443 6 4 3 39.076 78.151 0.409 3.38 4 16.0 0.6 444 1 8 -2 39.17 78.34 0.41 3.37 4 57.1 7.5 445 1 8 2 39.173 78.345 0.41 3.36 4 56.4 7.3 446 2 6 -4 39.187 78.374 0.41 3.36 4 6.6 0.1 447 2 6 4 39.197 78.394 0.41 3.36 4 4.2 0.0 448 3 8 0 39.247 78.493 0.411 3.35 4 96.3 21.2 449 8 2 -1 39.46 78.921 0.413 3.33 4 1.5 0.0 450 8 2 1 39.471 78.941 0.413 3.32 4 43.3 4.2 451 4 7 -2 39.48 78.959 0.413 3.32 4 76.5 13.2 452 4 7 2 39.49 78.98 0.413 3.32 4 77.0 13.4 453 6 6 0 39.493 78.986 0.413 3.32 4 13.6 0.4 454 0 0 6 39.568 79.135 0.413 3.31 2 1.1 0.0 455 7 2 -3 39.64 79.28 0.414 3.3 4 25.7 1.5 456 7 2 3 39.667 79.334 0.414 3.3 4 23.2 1.2 457 4 5 -4 39.75 79.499 0.415 3.29 4 34.3 2.6 458 4 5 4 39.77 79.541 0.415 3.28 4 39.3 3.5 459 6 2 -4 39.844 79.689 0.416 3.27 4 55.8 6.9 460 6 2 4 39.875 79.75 0.416 3.27 4 53.3 6.3 461 0 1 6 39.885 79.769 0.416 3.27 4 81.2 14.7 462 5 7 0 39.898 79.796 0.416 3.27 4 92.1 18.8 463 3 8 -1 39.902 79.805 0.416 3.27 4 26.4 1.6 464 3 8 1 39.906 79.812 0.416 3.27 4 14.6 0.5 465 5 4 -4 39.935 79.869 0.417 3.26 4 1.7 0.0 466 5 4 4 39.96 79.92 0.417 3.26 4 3.8 0.0 467 6 6 -1 40.146 80.291 0.419 3.24 4 13.1 0.4 468 6 6 1 40.153 80.307 0.419 3.24 4 6.3 0.1 469 8 0 -2 40.158 80.315 0.419 3.24 2 37.8 1.6 470 7 4 -2 40.163 80.326 0.419 3.23 4 22.0 1.1 471 8 0 2 40.178 80.356 0.419 3.23 2 35.8 1.4 472 7 4 2 40.181 80.362 0.419 3.23 4 21.4 1.0 473 2 8 -2 40.183 80.365 0.419 3.23 4 76.4 12.8 474 2 8 2 40.188 80.376 0.419 3.23 4 77.4 13.2 475 1 1 -6 40.218 80.436 0.419 3.23 4 22.3 1.1 476 1 1 6 40.226 80.451 0.419 3.23 4 23.8 1.2 477 0 5 5 40.266 80.532 0.42 3.22 4 14.5 0.5 478 8 3 0 40.392 80.785 0.421 3.21 4 28.6 1.8 479 7 5 0 40.397 80.793 0.421 3.21 4 3.7 0.0 480 3 7 -3 40.398 80.795 0.421 3.21 4 12.6 0.3 481 3 7 3 40.409 80.818 0.421 3.2 4 14.9 0.5 482 3 4 -5 40.443 80.886 0.421 3.2 4 38.5 3.2 483 3 4 5 40.462 80.924 0.421 3.2 4 23.5 1.2 484 8 1 -2 40.473 80.947 0.421 3.2 4 50.9 5.6 485 8 1 2 40.494 80.988 0.422 3.19 4 50.7 5.6 486 5 7 -1 40.55 81.099 0.422 3.19 4 12.9 0.4 487 5 7 1 40.556 81.112 0.422 3.19 4 24.6 1.3 488 4 3 -5 40.585 81.17 0.422 3.18 4 42.1 3.8 489 1 5 -5 40.599 81.198 0.422 3.18 4 25.5 1.4 490 1 5 5 40.605 81.211 0.422 3.18 4 39.8 3.4 491 4 3 5 40.611 81.221 0.423 3.18 4 7.5 0.1 492 0 2 6 40.832 81.664 0.424 3.16 4 0.8 0.0 493 3 6 -4 40.87 81.741 0.425 3.15 4 98.0 20.6 494 3 6 4 40.886 81.771 0.425 3.15 4 99.8 21.4 495 2 0 -6 40.907 81.814 0.425 3.15 2 164.3 28.9 496 2 0 6 40.923 81.845 0.425 3.15 2 166.6 29.7 497 8 3 -1 41.04 82.081 0.426 3.13 4 30.0 1.9 498 7 5 -1 41.045 82.091 0.426 3.13 4 27.4 1.6 499 8 3 1 41.051 82.101 0.426 3.13 4 1.2 0.0 500 7 5 1 41.054 82.109 0.426 3.13 4 31.0 2.1 501 5 1 -5 41.083 82.166 0.427 3.13 4 38.0 3.1 502 5 1 5 41.115 82.23 0.427 3.13 4 12.4 0.3 503 1 2 -6 41.164 82.327 0.427 3.12 4 37.1 2.9 504 1 2 6 41.171 82.343 0.427 3.12 4 36.7 2.9 505 7 3 -3 41.218 82.437 0.428 3.11 4 31.2 2.1 506 2 1 -6 41.222 82.444 0.428 3.11 4 38.1 3.1 507 2 1 6 41.237 82.474 0.428 3.11 4 35.2 2.6 508 7 3 3 41.245 82.49 0.428 3.11 4 32.6 2.2 509 8 2 -2 41.418 82.836 0.429 3.09 4 41.8 3.7 510 6 3 -4 41.421 82.842 0.429 3.09 4 87.9 16.3 511 8 2 2 41.438 82.876 0.43 3.09 4 42.5 3.8 512 6 3 4 41.452 82.903 0.43 3.09 4 86.5 15.7 513 2 5 -5 41.602 83.203 0.431 3.08 4 13.6 0.4 514 4 8 0 41.602 83.204 0.431 3.08 4 120.6 30.4 515 2 5 5 41.614 83.228 0.431 3.07 4 41.6 3.6 516 5 6 -3 41.669 83.337 0.432 3.07 4 46.9 4.6 517 5 6 3 41.688 83.375 0.432 3.07 4 8.7 0.2 518 3 8 -2 41.858 83.717 0.433 3.05 4 15.9 0.5 519 3 8 2 41.866 83.732 0.433 3.05 4 12.7 0.3 520 6 5 -3 41.894 83.787 0.433 3.05 4 4.0 0.0 521 6 5 3 41.916 83.833 0.434 3.05 4 9.0 0.2 522 1 9 0 41.92 83.84 0.434 3.05 4 31.9 2.1 523 0 7 4 41.949 83.897 0.434 3.04 4 1.8 0.0 524 5 2 -5 42.025 84.05 0.435 3.04 4 13.4 0.4 525 5 2 5 42.057 84.113 0.435 3.03 4 58.9 7.2 526 6 6 -2 42.098 84.195 0.435 3.03 4 29.2 1.8 527 0 8 3 42.103 84.207 0.435 3.03 4 23.3 1.1 528 6 6 2 42.113 84.225 0.435 3.03 4 26.7 1.5 529 2 2 -6 42.163 84.326 0.436 3.02 4 47.2 4.6 530 2 2 6 42.178 84.356 0.436 3.02 4 49.5 5.0 531 0 9 1 42.235 84.471 0.436 3.02 4 24.7 1.3 532 4 8 -1 42.249 84.498 0.436 3.02 4 12.7 0.3 533 4 8 1 42.254 84.509 0.436 3.02 4 40.6 3.4 534 1 7 -4 42.28 84.56 0.437 3.01 4 17.2 0.6 535 1 7 4 42.285 84.57 0.437 3.01 4 21.7 1.0 536 0 3 6 42.401 84.803 0.438 3.0 4 91.8 17.2 537 1 8 -3 42.435 84.87 0.438 3.0 4 29.5 1.8 538 1 8 3 42.439 84.878 0.438 3.0 4 16.3 0.5 539 5 7 -2 42.498 84.997 0.439 2.99 4 22.5 1.0 540 5 7 2 42.511 85.022 0.439 2.99 4 23.2 1.1 541 1 9 -1 42.568 85.137 0.439 2.99 4 12.5 0.3 542 1 9 1 42.57 85.139 0.439 2.99 4 1.0 0.0 543 8 4 0 42.591 85.182 0.439 2.99 4 28.0 1.6 544 1 3 -6 42.731 85.462 0.44 2.98 4 52.6 5.6 545 4 7 -3 42.738 85.476 0.441 2.97 4 11.0 0.2 546 1 3 6 42.738 85.477 0.441 2.97 4 50.5 5.2 547 4 7 3 42.753 85.506 0.441 2.97 4 4.9 0.0 548 5 5 -4 42.763 85.527 0.441 2.97 4 107.4 23.3 549 4 4 -5 42.782 85.563 0.441 2.97 4 8.3 0.1 550 5 5 4 42.789 85.577 0.441 2.97 4 110.0 24.5 551 4 4 5 42.807 85.614 0.441 2.97 4 44.2 3.9 552 3 1 -6 42.888 85.775 0.442 2.96 4 8.4 0.1 553 3 1 6 42.91 85.821 0.442 2.96 4 12.4 0.3 554 2 9 0 42.921 85.841 0.442 2.96 4 82.0 13.6 555 8 3 -2 42.984 85.967 0.443 2.96 4 35.3 2.5 556 7 5 -2 42.989 85.978 0.443 2.95 4 143.3 41.3 557 8 3 2 43.004 86.008 0.443 2.95 4 33.9 2.3 558 7 5 2 43.007 86.014 0.443 2.95 4 147.3 43.6 559 4 6 -4 43.206 86.412 0.444 2.94 4 6.6 0.1 560 4 6 4 43.226 86.452 0.445 2.94 4 8.3 0.1 561 8 4 -1 43.233 86.466 0.445 2.94 4 17.4 0.6 562 8 4 1 43.243 86.487 0.445 2.94 4 15.7 0.5 563 7 1 -4 43.251 86.502 0.445 2.94 4 33.2 2.2 564 3 5 -5 43.266 86.532 0.445 2.93 4 2.5 0.0 565 2 7 -4 43.277 86.554 0.445 2.93 4 84.0 14.1 566 3 5 5 43.285 86.57 0.445 2.93 4 65.9 8.7 567 7 1 4 43.287 86.573 0.445 2.93 4 29.6 1.7 568 2 7 4 43.287 86.574 0.445 2.93 4 82.8 13.7 569 8 0 -3 43.404 86.807 0.446 2.92 2 22.0 0.5 570 7 4 -3 43.41 86.82 0.446 2.92 4 29.0 1.7 571 2 8 -3 43.432 86.864 0.446 2.92 4 32.5 2.1 572 8 0 3 43.434 86.868 0.446 2.92 2 17.2 0.3 573 7 4 3 43.436 86.873 0.446 2.92 4 19.5 0.8 574 2 8 3 43.44 86.88 0.446 2.92 4 39.9 3.2 575 9 1 0 43.565 87.129 0.447 2.91 4 21.9 0.9 576 2 9 -1 43.566 87.133 0.447 2.91 4 17.9 0.6 577 2 9 1 43.569 87.138 0.447 2.91 4 21.7 0.9 578 6 7 0 43.577 87.155 0.447 2.91 4 48.3 4.6 579 5 3 -5 43.588 87.176 0.448 2.91 4 60.8 7.3 580 6 4 -4 43.611 87.222 0.448 2.91 4 88.5 15.5 581 5 3 5 43.619 87.239 0.448 2.91 4 8.4 0.1 582 6 4 4 43.641 87.283 0.448 2.91 4 91.6 16.6 583 0 6 5 43.715 87.43 0.449 2.9 4 12.2 0.3 584 8 1 -3 43.716 87.431 0.449 2.9 4 13.6 0.4 585 2 3 -6 43.725 87.451 0.449 2.9 4 3.6 0.0 586 2 3 6 43.741 87.481 0.449 2.9 4 1.8 0.0 587 8 1 3 43.746 87.492 0.449 2.9 4 22.3 1.0 588 3 2 -6 43.824 87.648 0.449 2.9 4 49.3 4.8 589 7 6 0 43.844 87.688 0.45 2.89 4 39.8 3.1 590 3 2 6 43.847 87.694 0.45 2.89 4 44.1 3.8 591 1 6 -5 44.044 88.088 0.451 2.88 4 33.1 2.1 592 1 6 5 44.05 88.101 0.451 2.88 4 23.0 1.0 593 0 9 2 44.177 88.354 0.452 2.87 4 81.5 13.0 594 7 2 -4 44.187 88.374 0.452 2.87 4 125.8 30.9 595 4 8 -2 44.188 88.376 0.452 2.87 4 64.9 8.2 596 4 8 2 44.198 88.396 0.453 2.87 4 63.9 8.0 597 9 1 -1 44.205 88.41 0.453 2.87 4 11.0 0.2 598 9 1 1 44.217 88.433 0.453 2.87 4 23.3 1.1 599 6 7 -1 44.22 88.44 0.453 2.87 4 11.9 0.3 600 7 2 4 44.222 88.445 0.453 2.87 4 131.5 33.8 601 6 7 1 44.228 88.455 0.453 2.87 4 14.3 0.4 602 6 0 -5 44.434 88.868 0.454 2.86 2 69.0 4.6 603 6 0 5 44.472 88.943 0.455 2.86 2 23.3 0.5 604 7 6 -1 44.486 88.972 0.455 2.86 4 35.5 2.5 605 7 6 1 44.495 88.989 0.455 2.86 4 25.1 1.2 606 9 2 0 44.5 89.0 0.455 2.85 4 15.1 0.4 607 1 9 -2 44.508 89.016 0.455 2.85 4 75.5 11.1 608 1 9 2 44.51 89.021 0.455 2.85 4 76.7 11.4 609 3 9 0 44.583 89.166 0.456 2.85 4 82.2 13.1 610 0 4 6 44.586 89.173 0.456 2.85 4 0.9 0.0 611 5 8 0 44.599 89.198 0.456 2.85 4 30.6 1.8 612 8 2 -3 44.651 89.302 0.456 2.85 4 20.0 0.8 613 8 2 3 44.681 89.363 0.456 2.84 4 4.5 0.0 614 6 1 -5 44.746 89.491 0.457 2.84 4 19.2 0.7 615 6 1 5 44.783 89.567 0.457 2.84 4 53.5 5.5 616 4 0 -6 44.899 89.798 0.458 2.83 2 22.8 0.5 617 1 4 -6 44.915 89.829 0.458 2.83 4 54.5 5.7 618 1 4 6 44.922 89.844 0.458 2.83 4 46.6 4.2 619 4 0 6 44.929 89.858 0.458 2.83 2 25.8 0.6 620 3 7 -4 44.936 89.872 0.458 2.83 4 23.6 1.1 621 3 7 4 44.951 89.902 0.459 2.83 4 16.6 0.5 X-ray diffraction powder data (I)...X-Ray wave length = 1.54056 (angs.): No H K L Theta 2*Theta d I int I int.n. I p.h.n. H(Si) ( degree ) (angstrem) *100 *100 1 1 1 0 6.085 12.169 7.26697 257.9 12.8 13.0 5.6 2 0 1 1 7.427 14.854 5.95883 151.4 7.5 7.6 5.6 3 0 2 0 8.482 16.964 5.2223 503.4 25.0 25.2 5.6 4 1 1 -1 8.626 17.252 5.13572 69.5 3.4 3.5 5.6 5 2 1 0 9.741 19.481 4.55277 362.1 18.0 18.1 5.6 6 0 2 1 10.471 20.941 4.23854 85.8 4.3 4.3 5.6 7 2 0 -1 10.694 21.388 4.15095 247.8 12.3 12.4 5.6 8 1 2 1 11.365 22.731 3.90878 136.5 6.8 6.8 5.6 9 2 1 1 11.525 23.05 3.85535 306.8 15.2 15.3 5.6 10 2 2 0 12.239 24.479 3.63348 44.4 2.2 2.2 5.6 11 0 1 2 12.99 25.979 3.42692 141.5 7.0 7.0 5.6 12 1 3 0 13.532 27.063 3.29207 715.1 35.5 35.6 5.6 13 1 1 2 13.731 27.462 3.24515 317.7 15.8 15.8 5.6 14 3 1 0 13.887 27.775 3.20929 165.7 8.2 8.2 5.6 15 0 3 1 14.206 28.411 3.13887 48.7 2.4 2.4 5.6 16 1 3 -1 14.887 29.775 2.99815 95.8 4.7 4.8 5.6 17 2 0 2 15.151 30.303 2.94709 2016.8 100.0 100.0 5.6 18 2 3 0 15.58 31.16 2.86795 967.9 48.0 48.0 5.6 19 2 1 -2 15.748 31.497 2.83804 288.2 14.3 14.3 5.6 20 3 2 0 15.777 31.554 2.83305 222.9 11.1 11.0 5.6 21 0 4 0 17.157 34.315 2.61115 30.4 1.5 1.5 5.7 22 2 2 2 17.465 34.929 2.5666 106.5 5.3 5.3 5.7 23 4 0 0 17.73 35.461 2.52932 98.1 4.9 4.8 5.7 24 0 3 2 17.857 35.715 2.51192 260.7 12.9 12.9 5.7 25 4 1 0 18.261 36.522 2.45827 162.4 8.1 8.0 5.7 26 1 3 -2 18.417 36.833 2.43817 218.2 10.8 10.8 5.7 27 3 3 0 18.542 37.083 2.42232 122.5 6.1 6.0 5.7 28 3 1 2 18.697 37.393 2.40293 34.1 1.7 1.7 5.7 29 1 4 1 18.823 37.646 2.38737 32.2 1.6 1.6 5.7 30 2 4 0 19.389 38.778 2.32028 74.8 3.7 3.7 5.7 31 4 2 0 19.778 39.556 2.27638 42.4 2.1 2.1 5.7 32 3 2 -2 20.174 40.349 2.23347 233.5 11.6 11.5 5.7 33 1 4 2 21.801 43.602 2.07408 95.9 4.8 4.7 5.7 34 3 4 0 21.906 43.812 2.06463 104.8 5.2 5.1 5.7 35 1 5 0 22.118 44.237 2.04577 216.8 10.8 10.6 5.7 36 4 1 2 22.248 44.497 2.03442 192.9 9.6 9.4 5.7 37 3 3 -2 22.475 44.95 2.01497 344.0 17.1 16.8 5.7 38 3 4 -1 22.821 45.642 1.98601 38.0 1.9 1.9 5.7 39 1 5 -1 23.029 46.057 1.96907 29.6 1.5 1.4 5.7 40 4 2 -2 23.539 47.078 1.92874 127.7 6.3 6.2 5.7 41 2 3 -3 24.617 49.233 1.84921 25.3 1.3 1.2 5.7 42 3 2 3 24.764 49.528 1.83889 21.6 1.1 1.1 5.7 43 0 0 4 25.129 50.258 1.81387 415.1 20.6 20.2 5.8 44 4 3 -2 25.599 51.199 1.78274 619.4 30.7 30.1 5.8 45 5 3 0 26.123 52.246 1.74945 113.2 5.6 5.5 5.8 46 4 1 3 26.547 53.095 1.72346 63.4 3.1 3.1 5.8 47 1 6 0 26.679 53.359 1.71556 152.5 7.6 7.4 5.8 48 0 2 4 26.715 53.429 1.71346 44.8 2.2 2.2 5.8 49 5 3 -1 26.927 53.854 1.70093 21.1 1.0 1.0 5.8 50 2 1 4 27.208 54.416 1.68471 50.7 2.5 2.5 5.8 51 5 2 2 27.406 54.811 1.67348 331.3 16.4 16.0 5.8 52 6 1 1 28.347 56.695 1.62227 27.4 1.4 1.3 5.8 53 6 2 0 28.688 57.375 1.60464 30.7 1.5 1.5 5.8 54 3 5 2 28.882 57.763 1.59477 142.9 7.1 6.9 5.8 55 1 3 4 29.006 58.012 1.58854 97.0 4.8 4.7 5.8 56 3 1 4 29.205 58.409 1.57867 21.6 1.1 1.0 5.8 57 5 3 2 29.271 58.541 1.57542 25.6 1.3 1.2 5.8 58 5 4 1 29.552 59.104 1.56175 37.3 1.9 1.8 5.8 59 1 6 -2 29.779 59.557 1.55095 267.3 13.3 12.8 5.8 60 3 6 0 29.866 59.731 1.54685 72.3 3.6 3.5 5.8 61 2 3 -4 30.158 60.315 1.53326 187.1 9.3 9.0 5.8 62 6 0 -2 30.239 60.479 1.5295 47.3 2.3 2.3 5.8 63 3 2 4 30.29 60.58 1.5272 57.1 2.8 2.7 5.8 64 6 3 0 30.502 61.004 1.51759 44.3 2.2 2.1 5.8 65 6 1 2 30.614 61.227 1.51259 77.6 3.8 3.7 5.8 66 4 0 -4 31.494 62.987 1.47449 56.6 2.8 2.7 5.9 67 6 2 -2 31.653 63.305 1.46784 41.1 2.0 2.0 5.9 68 5 4 2 31.765 63.529 1.46321 52.4 2.6 2.5 5.9 69 4 1 4 31.865 63.73 1.45909 46.4 2.3 2.2 5.9 70 5 5 0 32.005 64.009 1.45339 88.4 4.4 4.2 5.9 71 3 3 4 32.049 64.099 1.45158 24.2 1.2 1.2 5.9 72 2 7 0 32.563 65.127 1.43113 48.7 2.4 2.3 5.9 73 3 6 2 32.779 65.559 1.42274 49.7 2.5 2.4 5.9 74 4 2 -4 32.876 65.752 1.41902 25.7 1.3 1.2 5.9 75 6 4 0 32.941 65.883 1.41653 69.0 3.4 3.3 5.9 76 7 2 0 33.572 67.143 1.39296 102.0 5.1 4.8 5.9 77 2 1 5 33.865 67.73 1.38233 21.3 1.1 1.0 5.9 78 0 7 2 33.932 67.863 1.37993 44.5 2.2 2.1 5.9 79 3 4 -4 34.413 68.826 1.36296 38.9 1.9 1.8 5.9 80 1 5 4 34.582 69.164 1.35712 84.1 4.2 4.0 5.9 81 8 0 0 37.523 75.046 1.26466 36.2 1.8 1.7 6.0 82 5 3 -4 37.701 75.402 1.25958 53.2 2.6 2.5 6.0 83 8 1 0 37.845 75.69 1.25549 43.1 2.1 2.0 6.0 84 7 3 -2 37.933 75.867 1.25301 23.2 1.1 1.1 6.0 85 1 6 4 38.173 76.347 1.24632 80.4 4.0 3.7 6.0 86 3 8 0 39.247 78.493 1.21752 21.2 1.0 1.0 6.0 87 4 7 2 39.49 78.98 1.21124 31.3 1.6 1.5 6.0 88 5 7 0 39.898 79.796 1.2009 41.4 2.1 1.9 6.0 89 2 8 2 40.188 80.376 1.19369 31.1 1.5 1.4 6.0 90 3 6 4 40.886 81.771 1.1768 41.9 2.1 1.9 6.1 91 2 0 6 40.923 81.845 1.17593 58.6 2.9 2.7 6.1 92 8 2 2 41.438 82.876 1.1639 39.5 2.0 1.8 6.1 93 4 8 0 41.602 83.204 1.16014 34.1 1.7 1.6 6.1 94 5 5 4 42.789 85.577 1.13394 51.9 2.6 2.4 6.1 95 7 5 2 43.007 86.014 1.1293 89.7 4.4 4.1 6.1 96 2 7 4 43.287 86.574 1.12343 40.4 2.0 1.8 6.1 97 6 4 4 43.641 87.283 1.11612 32.2 1.6 1.5 6.2 98 7 2 -4 44.187 88.374 1.10513 60.4 3.0 2.7 6.2 99 7 2 4 44.222 88.445 1.10443 35.5 1.8 1.6 6.2 100 1 9 2 44.51 89.021 1.09877 26.6 1.3 1.2 6.2 Reference: Chichagov A.V. et al. Information-Calculating System on Crystal Structure Data of Minerals (MINCRYST) - Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian) |