Institute of Experimental Mineralogy Russian Academy of Sciences ------------------------------------------------- 142432, Chernogolovka, Moscow district A.V. Chichagov +7(496)52-22320 *** *** W W W - X R A Y P O L *** *********************** BORAX 1, f-borax Na(2)B(4)O(7).10H(2)O Monoclinic C 2/c Z = 4 R =0.22 NR =1800 8 .6 .1988 Ref.Str.: Morimoto N. (1956) * Mineral. J. (Japan), 2, 1-18 Initial data from BDM-file Lattice parameters (cub. angs.,degr.): a = 11.858 alpha = 90.0 b = 10.67 beta = 106.69 c = 12.197 gamma = 90.0 Unit cell volume (cub. angs.) = 1478.21 Molar volume ( cub.cm/mol.) = 222.6 Co-ordinates, thermal parameters, occupation for atomic positions: NoP x/a y/b z/c B(j) atom / occupation 1 0.0 0.0 0.0 0.0 Na = 1.00 2 0.0 0.845 0.25 0.0 Na = 1.00 3 0.0 0.265 0.25 0.0 O = 1.00 4 0.085 0.345 0.217 0.0 B = 1.00 5 0.095 0.454 0.39 0.0 B = 1.00 6 0.154 0.419 0.314 0.0 O = 1.00 7 0.018 0.435 0.123 0.0 O = 1.00 8 0.161 0.269 0.167 0.0 O = 1.00 9 0.163 0.511 0.491 0.0 O = 1.00 10 0.123 0.846 0.45 0.0 O = 1.00 11 0.125 0.002 0.196 0.0 O = 1.00 12 0.119 0.165 0.459 0.0 O = 1.00 13 0.116 0.707 0.171 0.0 O = 1.00 Co-ordinates for all atomic positions : No NoP x/a y/b z/c 1 1 0.0 0.0 0.0 2 2 0.0 0.845 0.25 3 3 0.0 0.265 0.25 4 4 0.085 0.345 0.217 5 5 0.095 0.454 0.39 6 6 0.154 0.419 0.314 7 7 0.018 0.435 0.123 8 8 0.161 0.269 0.167 9 9 0.163 0.511 0.491 10 10 0.123 0.846 0.45 11 11 0.125 0.002 0.196 12 12 0.119 0.165 0.459 13 13 0.116 0.707 0.171 14 2 0.0 0.155 0.75 15 3 0.0 0.735 0.75 16 4 0.915 0.655 0.783 17 5 0.905 0.546 0.61 18 6 0.846 0.581 0.686 19 7 0.982 0.565 0.877 20 8 0.839 0.731 0.833 21 9 0.837 0.489 0.509 22 10 0.877 0.154 0.55 23 11 0.875 0.998 0.804 24 12 0.881 0.835 0.541 25 13 0.884 0.293 0.829 26 1 0.0 0.0 0.5 27 4 0.085 0.655 0.717 28 5 0.095 0.546 0.89 29 6 0.154 0.581 0.814 30 7 0.018 0.565 0.623 31 8 0.161 0.731 0.667 32 9 0.163 0.489 0.991 33 10 0.123 0.154 0.95 34 11 0.125 0.998 0.696 35 12 0.119 0.835 0.959 36 13 0.116 0.293 0.671 37 4 0.915 0.345 0.283 38 5 0.905 0.454 0.11 39 6 0.846 0.419 0.186 40 7 0.982 0.435 0.377 41 8 0.839 0.269 0.333 42 9 0.837 0.511 0.009 43 10 0.877 0.846 0.05 44 11 0.875 0.002 0.304 45 12 0.881 0.165 0.041 46 13 0.884 0.707 0.329 47 1 0.5 0.5 0.5 48 2 0.5 0.655 0.75 49 3 0.5 0.235 0.75 50 4 0.585 0.155 0.717 51 5 0.595 0.046 0.89 52 6 0.654 0.081 0.814 53 7 0.518 0.065 0.623 54 8 0.661 0.231 0.667 55 9 0.663 0.989 0.991 56 10 0.623 0.654 0.95 57 11 0.625 0.498 0.696 58 12 0.619 0.335 0.959 59 13 0.616 0.793 0.671 60 2 0.5 0.345 0.25 61 3 0.5 0.765 0.25 62 4 0.415 0.845 0.283 63 5 0.405 0.954 0.11 64 6 0.346 0.919 0.186 65 7 0.482 0.935 0.377 66 8 0.339 0.769 0.333 67 9 0.337 0.011 0.009 68 10 0.377 0.346 0.05 69 11 0.375 0.502 0.304 70 12 0.381 0.665 0.041 71 13 0.384 0.207 0.329 72 1 0.5 0.5 0.0 73 4 0.585 0.845 0.217 74 5 0.595 0.954 0.39 75 6 0.654 0.919 0.314 76 7 0.518 0.935 0.123 77 8 0.661 0.769 0.167 78 9 0.663 0.011 0.491 79 10 0.623 0.346 0.45 80 11 0.625 0.502 0.196 81 12 0.619 0.665 0.459 82 13 0.616 0.207 0.171 83 4 0.415 0.155 0.783 84 5 0.405 0.046 0.61 85 6 0.346 0.081 0.686 86 7 0.482 0.065 0.877 87 8 0.339 0.231 0.833 88 9 0.337 0.989 0.509 89 10 0.377 0.654 0.55 90 11 0.375 0.498 0.804 91 12 0.381 0.335 0.541 92 13 0.384 0.793 0.829 X-ray density (g/cm cub.) = 1.62 MU (1/cm) = 20.731 Mass attenuation coefficient (cm**2/g) = 12.777 Selected interatomic distances (cation-anion,anion-anion): NoP Atom Rad.sph. C.N. Distance NoP N. (angs.) (angs.) 1 Na 2.808 6 2.4243 11 2.4243 11 2.3896 10 2.3971 12 2.3896 10 2.3971 12 2 Na 2.808 6 2.4565 10 2.4491 11 2.3979 13 2.4565 10 2.4491 11 2.3979 13 3 O 3.264 8 2.4136 6 2.4342 7 2.4045 8 2.7499 12 2.4136 6 2.4342 7 2.4045 8 2.7499 12 4 B 1.872 4 1.4627 3 1.4617 6 1.5312 7 1.4688 8 5 B 1.872 3 1.3641 6 1.4025 9 1.319 7 6 O 3.264 6 2.4136 3 2.4288 7 2.4225 8 2.3459 9 2.3832 7 2.8019 11 7 O 3.264 9 2.4342 3 2.4288 6 2.4037 8 3.1186 13 3.2208 7 2.7332 9 2.3832 6 3.2465 7 2.3417 9 8 O 3.264 7 2.4045 3 2.4225 6 2.4037 7 2.9172 11 3.1856 9 2.8335 10 2.8867 13 9 O 3.264 6 2.3459 6 2.7332 7 3.1856 8 2.3417 7 2.8699 10 3.1105 12 10 O 3.264 3 2.8335 8 3.1634 13 2.8699 9 11 O 3.264 3 2.9172 8 3.1612 13 2.8019 6 12 O 3.264 3 2.7499 3 2.9335 13 3.1105 9 13 O 3.264 5 3.1186 7 3.1612 11 2.9335 12 3.1634 10 2.8867 8 X-ray diffraction powder data (II), X-Ray W.L. = 1.54056(angs.): No H K L Theta 2*Theta S LPG MF F I int. ( degree ) *100 1 1 1 0 5.684 11.369 0.064 200.89 4 27.4 27.6 2 1 1 -1 6.18 12.36 0.07 169.61 4 46.8 68.1 3 1 1 1 7.431 14.861 0.084 116.62 4 46.4 46.0 4 0 0 2 7.577 15.154 0.086 112.07 2 44.3 20.2 5 2 0 0 7.795 15.59 0.088 105.77 2 135.5 177.8 6 0 2 0 8.302 16.603 0.094 93.0 2 43.3 16.0 7 1 1 -2 8.542 17.084 0.096 87.72 4 64.9 67.7 8 0 2 1 9.133 18.266 0.103 76.46 4 145.1 294.8 9 2 0 -2 9.191 18.381 0.104 75.47 2 20.2 2.8 10 1 1 2 10.359 20.718 0.117 58.94 4 0.9 0.0 11 0 2 2 11.276 22.552 0.127 49.42 4 99.5 89.5 12 2 2 -1 11.309 22.617 0.127 49.12 4 81.8 60.1 13 2 2 0 11.426 22.851 0.129 48.08 4 17.6 2.7 14 1 1 -3 11.715 23.43 0.132 45.63 4 2.9 0.1 15 3 1 -1 12.002 24.005 0.135 43.37 4 13.7 1.5 16 2 0 2 12.392 24.785 0.139 40.55 2 51.0 9.7 17 2 2 -2 12.434 24.867 0.14 40.27 4 5.8 0.2 18 3 1 0 12.467 24.934 0.14 40.05 4 53.3 20.8 19 3 1 -2 12.733 25.466 0.143 38.31 4 30.7 6.6 20 2 2 1 12.752 25.505 0.143 38.18 4 38.6 10.4 21 1 3 0 13.117 26.234 0.147 35.98 4 29.1 5.6 22 1 3 -1 13.346 26.692 0.15 34.69 4 57.0 20.6 23 1 1 3 13.768 27.535 0.154 32.47 4 6.4 0.2 24 1 3 1 13.987 27.974 0.157 31.4 4 29.3 4.9 25 3 1 1 14.016 28.031 0.157 31.26 4 50.8 14.8 26 0 2 3 14.175 28.35 0.159 30.52 4 24.8 3.4 27 3 1 -3 14.491 28.981 0.162 29.12 4 9.1 0.4 28 2 2 -3 14.531 29.063 0.163 28.95 4 63.7 21.5 29 1 3 -2 14.625 29.251 0.164 28.55 4 20.0 2.1 30 2 2 2 14.99 29.98 0.168 27.08 4 110.1 60.1 31 2 0 -4 15.047 30.095 0.169 26.86 2 173.1 73.7 32 1 1 -4 15.239 30.478 0.171 26.14 4 41.3 8.2 33 0 0 4 15.291 30.582 0.171 25.95 2 93.2 20.7 34 4 0 -2 15.389 30.779 0.172 25.6 2 7.6 0.1 35 4 0 0 15.739 31.479 0.176 24.39 2 178.8 71.4 36 1 3 2 15.788 31.576 0.177 24.23 4 192.5 164.3 37 3 1 2 16.366 32.733 0.183 22.42 4 27.6 3.1 38 1 3 -3 16.736 33.472 0.187 21.36 4 9.8 0.4 39 0 4 0 16.784 33.568 0.187 21.22 2 95.7 17.8 40 3 3 -1 16.944 33.888 0.189 20.79 4 34.6 4.6 41 3 1 -4 16.985 33.97 0.19 20.68 4 56.5 12.1 42 0 4 1 17.229 34.459 0.192 20.05 4 51.6 9.8 43 2 2 -4 17.281 34.563 0.193 19.92 4 3.6 0.0 44 3 3 0 17.286 34.572 0.193 19.9 4 33.3 4.1 45 4 2 -1 17.307 34.615 0.193 19.85 4 16.8 1.0 46 1 1 4 17.421 34.842 0.194 19.57 4 173.6 107.9 47 3 3 -2 17.485 34.97 0.195 19.41 4 298.4 316.4 48 0 2 4 17.497 34.994 0.195 19.38 4 19.6 1.4 49 4 2 -2 17.584 35.169 0.196 19.17 4 122.3 52.5 50 2 2 3 17.832 35.664 0.199 18.6 4 35.5 4.3 51 4 2 0 17.896 35.792 0.199 18.45 4 32.0 3.5 52 1 3 3 18.275 36.55 0.204 17.62 4 110.4 39.3 53 3 3 1 18.468 36.936 0.206 17.22 4 9.8 0.3 54 0 4 2 18.509 37.017 0.206 17.14 4 4.3 0.1 55 2 4 -1 18.529 37.059 0.206 17.09 4 8.7 0.2 56 2 4 0 18.604 37.209 0.207 16.94 4 7.3 0.2 57 4 0 -4 18.629 37.258 0.207 16.89 2 8.0 0.1 58 4 2 -3 18.694 37.389 0.208 16.76 4 16.3 0.8 59 3 3 -3 18.842 37.684 0.21 16.47 4 89.7 24.3 60 1 1 -5 18.967 37.934 0.211 16.24 4 1.5 0.0 61 2 0 4 19.231 38.462 0.214 15.75 2 218.5 68.8 62 3 1 3 19.263 38.526 0.214 15.69 4 44.2 5.6 63 2 4 -2 19.268 38.537 0.214 15.68 4 125.5 45.2 64 4 2 1 19.282 38.565 0.214 15.65 4 35.3 3.6 65 1 3 -4 19.441 38.882 0.216 15.37 4 16.1 0.7 66 2 4 1 19.485 38.97 0.217 15.3 4 16.0 0.7 67 4 0 2 19.508 39.016 0.217 15.26 2 28.9 1.2 68 5 1 -1 19.524 39.048 0.217 15.23 4 32.9 3.0 69 5 1 -2 19.542 39.084 0.217 15.2 4 61.7 10.6 70 3 1 -5 19.98 39.96 0.222 14.47 4 27.2 2.0 71 5 1 0 20.284 40.568 0.225 13.99 4 33.7 2.9 72 5 1 -3 20.337 40.674 0.226 13.91 4 29.8 2.3 73 3 3 2 20.364 40.728 0.226 13.87 4 93.3 22.1 74 2 2 -5 20.464 40.928 0.227 13.72 4 34.2 2.9 75 0 4 3 20.488 40.976 0.227 13.68 4 72.1 13.0 76 4 2 -4 20.521 41.043 0.228 13.63 4 78.2 15.2 77 2 4 -3 20.748 41.495 0.23 13.3 4 52.0 6.6 78 3 3 -4 20.88 41.76 0.231 13.11 4 79.4 15.1 79 2 2 4 21.078 42.156 0.233 12.84 4 125.9 37.3 80 2 4 2 21.087 42.173 0.234 12.83 4 69.4 11.3 81 0 2 5 21.093 42.186 0.234 12.82 4 15.5 0.6 82 1 1 5 21.247 42.493 0.235 12.61 4 20.0 0.9 83 1 3 4 21.247 42.494 0.235 12.61 4 5.3 0.1 84 4 2 2 21.335 42.669 0.236 12.5 4 40.7 3.8 85 1 5 0 21.547 43.095 0.238 12.22 4 44.5 4.4 86 1 5 -1 21.696 43.392 0.24 12.03 4 86.7 16.6 87 5 1 1 21.755 43.51 0.241 11.96 4 30.0 2.0 88 5 1 -4 21.838 43.676 0.241 11.86 4 103.0 23.0 89 1 5 1 22.121 44.242 0.244 11.52 4 97.7 20.1 90 2 0 -6 22.306 44.613 0.246 11.3 2 119.3 14.7 91 3 1 4 22.542 45.085 0.249 11.04 4 133.9 36.2 92 1 5 -2 22.556 45.112 0.249 11.02 4 21.0 0.9 93 1 3 -5 22.572 45.144 0.249 11.01 4 46.6 4.4 94 3 3 3 22.829 45.658 0.252 10.73 4 58.3 6.7 95 2 4 -4 22.849 45.699 0.252 10.71 4 43.0 3.6 96 1 1 -6 22.858 45.715 0.252 10.7 4 8.7 0.1 97 4 4 -1 22.87 45.74 0.252 10.69 4 55.4 6.0 98 4 2 -5 22.926 45.851 0.253 10.63 4 9.9 0.2 99 6 0 -2 22.957 45.914 0.253 10.59 2 11.3 0.1 100 0 4 4 23.021 46.042 0.254 10.53 4 14.3 0.4 101 5 3 -1 23.057 46.113 0.254 10.49 4 67.3 8.7 102 5 3 -2 23.073 46.145 0.254 10.47 4 68.0 8.9 103 4 4 -2 23.091 46.181 0.255 10.46 4 56.1 6.0 104 2 4 3 23.289 46.577 0.257 10.26 4 93.7 16.5 105 0 0 6 23.302 46.605 0.257 10.24 2 108.9 11.1 106 3 1 -6 23.332 46.664 0.257 10.21 4 64.4 7.8 107 4 4 0 23.34 46.681 0.257 10.2 4 10.6 0.2 108 1 5 2 23.375 46.751 0.258 10.17 4 59.4 6.6 109 3 3 -5 23.456 46.913 0.258 10.09 4 52.6 5.1 110 5 3 0 23.725 47.449 0.261 9.83 4 11.1 0.2 111 5 3 -3 23.771 47.542 0.262 9.79 4 119.8 25.7 112 5 1 2 23.831 47.663 0.262 9.73 4 27.7 1.4 113 4 2 3 23.918 47.835 0.263 9.65 4 34.5 2.1 114 5 1 -5 23.94 47.879 0.263 9.63 4 71.1 8.9 115 2 2 -6 23.96 47.919 0.264 9.62 4 82.6 12.0 116 4 4 -3 23.987 47.975 0.264 9.59 4 98.5 17.0 117 6 0 0 24.01 48.02 0.264 9.57 2 157.4 21.7 118 1 5 -3 24.067 48.134 0.265 9.52 4 11.9 0.2 119 3 5 -1 24.222 48.444 0.266 9.38 4 33.1 1.9 120 4 0 -6 24.23 48.461 0.266 9.37 2 88.3 6.7 121 4 4 1 24.471 48.942 0.269 9.17 4 36.6 2.2 122 3 5 0 24.478 48.956 0.269 9.16 4 49.2 4.1 123 6 2 -2 24.576 49.153 0.27 9.08 4 111.8 20.8 124 1 3 5 24.579 49.158 0.27 9.07 4 81.8 11.1 125 6 0 -4 24.614 49.228 0.27 9.04 2 196.4 31.9 126 2 2 5 24.623 49.246 0.27 9.04 4 20.1 0.7 127 3 5 -2 24.628 49.256 0.271 9.03 4 58.4 5.6 128 6 2 -1 24.755 49.511 0.272 8.93 4 33.7 1.9 129 0 2 6 24.905 49.809 0.273 8.81 4 52.8 4.5 130 5 3 1 25.034 50.069 0.275 8.7 4 15.3 0.4 131 6 2 -3 25.052 50.104 0.275 8.69 4 26.2 1.1 132 5 3 -4 25.109 50.218 0.275 8.64 4 3.9 0.0 133 1 1 6 25.231 50.462 0.277 8.55 4 20.3 0.6 134 1 5 3 25.232 50.463 0.277 8.55 4 12.9 0.3 135 3 5 1 25.381 50.762 0.278 8.43 4 10.5 0.2 136 4 0 4 25.418 50.835 0.279 8.41 2 39.4 1.2 137 2 4 -5 25.458 50.916 0.279 8.38 4 37.2 2.1 138 4 4 -4 25.506 51.013 0.28 8.34 4 86.5 11.4 139 6 2 0 25.579 51.157 0.28 8.29 4 45.8 3.2 140 0 6 0 25.667 51.335 0.281 8.22 2 99.8 7.5 141 3 5 -3 25.673 51.345 0.281 8.22 4 42.2 2.7 142 3 3 4 25.744 51.488 0.282 8.17 4 77.9 9.1 143 4 2 -6 25.789 51.579 0.282 8.13 4 74.1 8.2 144 2 4 4 25.979 51.957 0.284 8.0 4 58.0 4.9 145 0 6 1 25.985 51.97 0.284 7.99 4 0.4 0.0 146 0 4 5 25.992 51.984 0.284 7.99 4 80.8 9.5 147 1 3 -6 26.03 52.06 0.285 7.96 4 164.5 39.5 148 3 1 5 26.118 52.236 0.286 7.9 4 3.6 0.0 149 1 5 -4 26.145 52.29 0.286 7.88 4 50.6 3.7 150 6 2 -4 26.156 52.312 0.286 7.88 4 17.1 0.4 151 4 4 2 26.198 52.396 0.287 7.85 4 111.3 17.8 152 5 1 3 26.409 52.819 0.289 7.71 4 9.3 0.1 153 3 3 -6 26.461 52.923 0.289 7.67 4 127.2 22.7 154 5 1 -6 26.538 53.077 0.29 7.62 4 28.7 1.2 155 3 5 2 26.884 53.769 0.294 7.4 4 86.0 10.0 156 1 1 -7 26.909 53.819 0.294 7.38 4 2.6 0.0 157 5 3 2 26.918 53.835 0.294 7.38 4 188.3 47.9 158 0 6 2 26.922 53.844 0.294 7.38 4 95.8 12.4 159 4 2 4 26.926 53.853 0.294 7.37 4 24.2 0.8 160 2 6 -1 26.937 53.875 0.294 7.37 4 8.0 0.1 161 3 1 -7 26.969 53.938 0.294 7.35 4 6.6 0.1 162 2 0 6 26.971 53.942 0.294 7.34 2 17.6 0.2 163 2 6 0 26.993 53.987 0.295 7.33 4 33.0 1.5 164 6 2 1 27.004 54.008 0.295 7.32 4 86.6 10.1 165 5 3 -5 27.017 54.034 0.295 7.32 4 32.0 1.4 166 3 5 -4 27.304 54.607 0.298 7.14 4 14.3 0.3 167 7 1 -2 27.415 54.829 0.299 7.08 4 7.4 0.1 168 2 6 -2 27.494 54.988 0.3 7.03 4 25.3 0.8 169 6 0 2 27.539 55.078 0.3 7.0 2 31.5 0.6 170 4 4 -5 27.574 55.149 0.3 6.98 4 28.6 1.0 171 1 5 4 27.605 55.209 0.301 6.97 4 9.1 0.1 172 2 6 1 27.659 55.319 0.301 6.94 4 6.9 0.1 173 7 1 -3 27.677 55.354 0.302 6.93 4 53.6 3.6 174 2 2 -7 27.714 55.429 0.302 6.9 4 77.6 7.6 175 7 1 -1 27.759 55.519 0.302 6.88 4 28.2 1.0 176 6 2 -5 27.836 55.672 0.303 6.84 4 4.6 0.0 177 1 3 6 28.207 56.413 0.307 6.63 4 4.6 0.0 178 2 2 6 28.422 56.845 0.309 6.52 4 11.6 0.2 179 0 6 3 28.436 56.871 0.309 6.51 4 27.0 0.9 180 4 4 3 28.447 56.894 0.309 6.51 4 4.2 0.0 181 2 4 -6 28.484 56.969 0.31 6.49 4 80.3 7.7 182 7 1 -4 28.536 57.071 0.31 6.46 4 82.0 8.0 183 6 0 -6 28.631 57.261 0.311 6.41 2 79.6 3.7 184 2 6 -3 28.639 57.279 0.311 6.41 4 16.1 0.3 185 7 1 0 28.696 57.393 0.312 6.38 4 27.2 0.9 186 1 5 -5 28.707 57.414 0.312 6.38 4 9.4 0.1 187 2 6 2 28.907 57.815 0.314 6.28 4 5.3 0.0 188 0 2 7 28.919 57.838 0.314 6.27 4 44.8 2.3 189 3 5 3 28.924 57.848 0.314 6.27 4 3.1 0.0 190 6 2 2 28.971 57.942 0.314 6.24 4 61.9 4.4 191 3 3 5 29.03 58.061 0.315 6.22 4 24.9 0.7 192 6 4 -2 29.032 58.064 0.315 6.21 4 7.9 0.1 193 4 2 -7 29.032 58.064 0.315 6.21 4 21.4 0.5 194 2 4 5 29.074 58.148 0.315 6.19 4 66.0 4.9 195 5 5 -1 29.117 58.233 0.316 6.17 4 75.2 6.4 196 5 5 -2 29.13 58.26 0.316 6.17 4 49.1 2.7 197 6 4 -1 29.192 58.384 0.317 6.14 4 21.5 0.5 198 5 3 3 29.302 58.604 0.318 6.09 4 28.9 0.9 199 0 4 6 29.325 58.651 0.318 6.08 4 113.7 14.4 200 1 1 7 29.386 58.773 0.319 6.05 4 2.5 0.0 201 5 1 4 29.407 58.815 0.319 6.04 4 30.4 1.0 202 5 3 -6 29.422 58.845 0.319 6.03 4 52.7 3.1 203 3 5 -5 29.456 58.913 0.319 6.02 4 52.8 3.1 204 6 4 -3 29.457 58.915 0.319 6.01 4 12.1 0.2 205 5 1 -7 29.554 59.109 0.32 5.97 4 44.5 2.2 206 5 5 0 29.686 59.371 0.321 5.91 4 15.7 0.3 207 5 5 -3 29.725 59.451 0.322 5.89 4 43.4 2.0 208 1 3 -7 29.769 59.539 0.322 5.87 4 0.6 0.0 209 3 3 -7 29.825 59.65 0.323 5.85 4 12.3 0.2 210 6 4 0 29.93 59.861 0.324 5.8 4 69.8 5.2 211 3 1 6 29.955 59.909 0.324 5.79 4 75.3 6.0 212 7 1 -5 29.957 59.913 0.324 5.79 4 49.2 2.6 213 6 2 -6 30.029 60.058 0.325 5.76 4 13.9 0.2 214 4 4 -6 30.12 60.24 0.326 5.72 4 25.6 0.7 215 7 1 1 30.19 60.381 0.326 5.69 4 40.6 1.7 216 7 3 -2 30.243 60.487 0.327 5.67 4 77.6 6.3 217 4 2 5 30.294 60.589 0.327 5.65 4 26.5 0.7 218 2 6 -4 30.331 60.662 0.328 5.63 4 57.4 3.4 219 4 6 -1 30.348 60.695 0.328 5.63 4 48.1 2.4 220 2 0 -8 30.363 60.726 0.328 5.62 2 72.3 2.7 221 1 5 5 30.422 60.843 0.329 5.6 4 10.2 0.1 222 6 4 -4 30.452 60.904 0.329 5.58 4 74.3 5.6 223 0 6 4 30.472 60.944 0.329 5.58 4 141.0 20.3 224 7 3 -3 30.49 60.98 0.329 5.57 4 20.6 0.4 225 4 6 -2 30.529 61.059 0.33 5.55 4 43.1 1.9 226 7 3 -1 30.567 61.135 0.33 5.54 4 3.9 0.0 227 1 7 0 30.655 61.31 0.331 5.5 4 168.4 28.6 228 2 6 3 30.693 61.385 0.331 5.49 4 65.9 4.4 229 4 6 0 30.736 61.471 0.332 5.47 4 56.0 3.1 230 1 7 -1 30.771 61.542 0.332 5.46 4 18.6 0.3 231 5 5 1 30.817 61.634 0.333 5.44 4 67.8 4.6 232 3 1 -8 30.864 61.727 0.333 5.42 4 14.9 0.2 233 5 5 -4 30.882 61.764 0.333 5.41 4 43.9 1.9 234 1 7 1 31.105 62.21 0.335 5.33 4 30.8 0.9 235 1 1 -8 31.143 62.285 0.336 5.31 4 43.1 1.8 236 4 4 4 31.152 62.304 0.336 5.31 4 1.3 0.0 237 6 4 1 31.223 62.445 0.336 5.28 4 12.5 0.1 238 4 6 -3 31.274 62.549 0.337 5.26 4 1.6 0.0 239 4 0 -8 31.281 62.561 0.337 5.26 2 171.0 14.1 240 7 3 -4 31.3 62.599 0.337 5.25 4 38.0 1.4 241 8 0 -2 31.347 62.694 0.338 5.24 2 21.9 0.2 242 6 2 3 31.42 62.839 0.338 5.21 4 53.3 2.7 243 3 5 4 31.438 62.877 0.339 5.2 4 14.0 0.2 244 1 7 -2 31.449 62.899 0.339 5.2 4 13.4 0.2 245 7 3 0 31.452 62.903 0.339 5.2 4 25.5 0.6 246 4 6 1 31.681 63.361 0.341 5.12 4 2.1 0.0 247 1 5 -6 31.69 63.38 0.341 5.11 4 0.6 0.0 248 2 2 -8 31.715 63.429 0.341 5.1 4 19.4 0.4 249 0 0 8 31.833 63.666 0.342 5.06 2 3.1 0.0 250 2 4 -7 31.873 63.746 0.343 5.05 4 24.5 0.6 251 7 1 -6 31.896 63.792 0.343 5.04 4 31.3 0.9 252 6 4 -5 31.985 63.969 0.344 5.01 4 12.7 0.1 253 8 0 -4 32.057 64.113 0.345 4.99 2 91.1 3.8 254 3 5 -6 32.072 64.143 0.345 4.98 4 49.2 2.2 255 1 3 7 32.106 64.212 0.345 4.97 4 4.2 0.0 256 1 7 2 32.107 64.213 0.345 4.97 4 36.4 1.2 257 5 3 4 32.126 64.252 0.345 4.96 4 8.0 0.1 258 7 1 2 32.196 64.393 0.346 4.94 4 19.3 0.3 259 5 3 -7 32.265 64.531 0.347 4.92 4 11.7 0.1 260 2 2 7 32.468 64.937 0.348 4.85 4 48.8 2.1 261 5 5 2 32.477 64.955 0.349 4.85 4 29.9 0.8 262 2 6 -5 32.52 65.039 0.349 4.83 4 8.0 0.1 263 2 4 6 32.525 65.05 0.349 4.83 4 46.0 1.9 264 4 6 -4 32.561 65.122 0.349 4.82 4 4.5 0.0 265 5 5 -5 32.566 65.131 0.349 4.82 4 42.8 1.6 266 4 2 -8 32.611 65.222 0.35 4.81 4 32.4 0.9 267 3 3 6 32.646 65.293 0.35 4.79 4 35.0 1.1 268 7 3 -5 32.648 65.297 0.35 4.79 4 17.1 0.3 269 1 7 -3 32.67 65.34 0.35 4.79 4 21.6 0.4 270 8 2 -2 32.676 65.352 0.35 4.78 4 2.1 0.0 271 6 2 -7 32.68 65.36 0.35 4.78 4 4.3 0.0 272 4 0 6 32.69 65.381 0.351 4.78 2 111.3 5.4 273 8 2 -3 32.751 65.501 0.351 4.76 4 7.8 0.1 274 5 1 5 32.776 65.551 0.351 4.75 4 37.3 1.2 275 3 7 -1 32.797 65.594 0.352 4.75 4 25.2 0.6 276 8 0 0 32.856 65.711 0.352 4.73 2 171.8 12.8 277 7 3 1 32.871 65.742 0.352 4.72 4 2.1 0.0 278 5 1 -8 32.939 65.878 0.353 4.7 4 65.3 3.7 279 2 6 4 32.967 65.934 0.353 4.69 4 145.4 18.2 280 0 6 5 32.978 65.957 0.353 4.69 4 31.3 0.8 281 0 4 7 32.984 65.969 0.353 4.69 4 28.8 0.7 282 6 0 4 33.007 66.015 0.354 4.68 2 41.5 0.7 283 3 7 0 33.008 66.016 0.354 4.68 4 3.0 0.0 284 6 4 2 33.033 66.065 0.354 4.67 4 102.3 8.9 285 4 4 -7 33.089 66.179 0.354 4.66 4 37.4 1.2 286 3 7 -2 33.132 66.264 0.355 4.65 4 58.1 2.9 287 8 2 -1 33.147 66.294 0.355 4.64 4 9.5 0.1 288 0 2 8 33.151 66.302 0.355 4.64 4 59.6 3.0 289 4 6 2 33.157 66.313 0.355 4.64 4 34.2 1.0 290 8 2 -4 33.37 66.74 0.357 4.57 4 3.1 0.0 291 3 3 -8 33.514 67.028 0.358 4.53 4 44.5 1.6 292 1 5 6 33.634 67.267 0.36 4.5 4 9.6 0.1 293 1 7 3 33.634 67.268 0.36 4.5 4 55.2 2.5 294 1 1 8 33.744 67.487 0.361 4.47 4 3.6 0.0 295 3 7 1 33.759 67.519 0.361 4.46 4 8.1 0.1 296 1 3 -8 33.781 67.562 0.361 4.46 4 7.1 0.0 297 4 2 6 33.991 67.982 0.363 4.4 4 40.5 1.3 298 3 7 -3 34.004 68.009 0.363 4.4 4 23.2 0.4 299 6 4 -6 34.018 68.035 0.363 4.39 4 1.8 0.0 300 3 1 7 34.051 68.103 0.363 4.38 4 42.8 1.5 301 8 2 0 34.153 68.306 0.364 4.36 4 0.5 0.0 302 4 4 5 34.266 68.531 0.365 4.33 4 6.7 0.0 303 6 2 4 34.302 68.604 0.366 4.32 4 59.7 2.8 304 7 1 -7 34.31 68.619 0.366 4.32 4 16.5 0.2 305 4 6 -5 34.358 68.716 0.366 4.3 4 12.0 0.1 306 3 5 5 34.381 68.761 0.367 4.3 4 40.7 1.3 307 1 7 -4 34.403 68.807 0.367 4.29 4 39.9 1.2 308 6 0 -8 34.48 68.96 0.367 4.27 2 95.8 3.6 309 7 3 -6 34.504 69.007 0.368 4.27 4 7.2 0.0 310 8 2 -5 34.519 69.038 0.368 4.26 4 69.2 3.7 311 5 5 3 34.628 69.256 0.369 4.24 4 52.9 2.2 312 7 1 3 34.671 69.343 0.369 4.22 4 23.1 0.4 313 5 5 -6 34.738 69.477 0.37 4.21 4 19.8 0.3 314 7 3 2 34.793 69.585 0.37 4.19 4 50.8 2.0 315 8 0 -6 34.912 69.824 0.372 4.17 2 59.2 1.3 316 3 1 -9 35.022 70.045 0.373 4.14 4 22.7 0.4 317 3 7 2 35.034 70.069 0.373 4.14 4 37.4 1.1 318 1 5 -7 35.056 70.112 0.373 4.13 4 84.6 5.4 319 3 5 -7 35.107 70.214 0.373 4.12 4 101.0 7.7 320 4 6 3 35.131 70.262 0.374 4.11 4 22.2 0.4 321 2 6 -6 35.164 70.328 0.374 4.11 4 16.1 0.2 322 0 8 0 35.277 70.554 0.375 4.08 2 25.4 0.2 323 6 4 3 35.323 70.646 0.375 4.07 4 6.0 0.0 324 5 3 5 35.351 70.701 0.376 4.06 4 9.6 0.1 325 3 7 -4 35.395 70.791 0.376 4.05 4 3.8 0.0 326 7 5 -2 35.491 70.982 0.377 4.03 4 6.8 0.0 327 5 3 -8 35.508 71.016 0.377 4.03 4 50.1 1.8 328 2 0 8 35.528 71.057 0.377 4.02 2 115.5 4.9 329 0 8 1 35.541 71.081 0.377 4.02 4 12.6 0.1 330 1 1 -9 35.596 71.191 0.378 4.01 4 0.4 0.0 331 2 4 -8 35.601 71.203 0.378 4.01 4 52.8 2.0 332 6 6 -2 35.653 71.307 0.378 3.99 4 57.8 2.4 333 1 7 4 35.656 71.311 0.378 3.99 4 49.0 1.8 334 8 2 1 35.673 71.346 0.379 3.99 4 29.7 0.6 335 2 6 5 35.691 71.381 0.379 3.99 4 5.0 0.0 336 7 5 -3 35.719 71.437 0.379 3.98 4 8.3 0.1 337 6 2 -8 35.749 71.499 0.379 3.97 4 36.3 1.0 338 7 5 -1 35.79 71.58 0.38 3.96 4 42.9 1.3 339 6 6 -1 35.796 71.593 0.38 3.96 4 15.6 0.2 340 0 6 6 35.916 71.833 0.381 3.94 4 1.8 0.0 341 2 2 -9 35.977 71.954 0.381 3.92 4 6.6 0.0 342 6 6 -3 36.035 72.07 0.382 3.91 4 34.5 0.9 343 9 1 -3 36.121 72.243 0.383 3.89 4 11.2 0.1 344 8 2 -6 36.175 72.349 0.383 3.88 4 3.2 0.0 345 9 1 -2 36.204 72.409 0.383 3.88 4 15.8 0.2 346 1 3 8 36.286 72.572 0.384 3.86 4 59.9 2.5 347 2 4 7 36.315 72.63 0.384 3.85 4 20.2 0.3 348 0 8 2 36.327 72.654 0.385 3.85 4 14.9 0.2 349 2 8 -1 36.34 72.68 0.385 3.85 4 25.9 0.5 350 2 8 0 36.387 72.775 0.385 3.84 4 7.0 0.0 351 8 0 2 36.44 72.88 0.386 3.83 2 29.7 0.3 352 4 4 -8 36.45 72.901 0.386 3.83 4 17.0 0.2 353 6 6 0 36.462 72.924 0.386 3.82 4 18.3 0.2 354 7 5 -4 36.468 72.936 0.386 3.82 4 43.4 1.3 355 5 1 6 36.494 72.988 0.386 3.82 4 6.1 0.0 356 8 4 -2 36.512 73.024 0.386 3.81 4 7.6 0.0 357 4 2 -9 36.515 73.031 0.386 3.81 4 48.3 1.6 358 6 4 -7 36.516 73.032 0.386 3.81 4 6.7 0.0 359 9 1 -4 36.56 73.121 0.387 3.8 4 40.0 1.1 360 8 4 -3 36.583 73.166 0.387 3.8 4 1.0 0.0 361 3 3 7 36.584 73.169 0.387 3.8 4 2.0 0.0 362 7 5 0 36.609 73.218 0.387 3.79 4 41.5 1.2 363 1 7 -5 36.619 73.237 0.387 3.79 4 20.7 0.3 364 4 6 -6 36.634 73.268 0.387 3.79 4 30.1 0.6 365 5 1 -9 36.674 73.347 0.388 3.78 4 31.8 0.7 366 2 2 8 36.782 73.564 0.389 3.76 4 41.9 1.2 367 9 1 -1 36.808 73.616 0.389 3.76 4 57.2 2.2 368 3 7 3 36.81 73.619 0.389 3.76 4 19.6 0.3 369 2 8 -2 36.813 73.626 0.389 3.76 4 30.8 0.7 370 7 3 -7 36.835 73.669 0.389 3.75 4 8.7 0.1 371 6 6 -4 36.935 73.87 0.39 3.73 4 143.1 14.0 372 2 8 1 36.955 73.909 0.39 3.73 4 49.4 1.7 373 8 4 -1 36.961 73.921 0.39 3.73 4 1.4 0.0 374 0 4 8 36.964 73.929 0.39 3.73 4 33.4 0.8 375 5 7 -1 36.98 73.96 0.39 3.72 4 34.9 0.8 376 5 7 -2 36.992 73.984 0.391 3.72 4 26.5 0.5 377 7 1 -8 37.164 74.329 0.392 3.69 4 44.6 1.3 378 8 4 -4 37.173 74.346 0.392 3.69 4 35.3 0.8 379 7 3 3 37.186 74.372 0.392 3.69 4 45.7 1.4 380 1 5 7 37.219 74.438 0.393 3.68 4 18.4 0.2 381 5 5 4 37.238 74.476 0.393 3.68 4 7.9 0.0 382 3 7 -5 37.281 74.563 0.393 3.67 4 58.9 2.3 383 5 5 -7 37.368 74.737 0.394 3.65 4 10.4 0.1 384 5 7 0 37.485 74.97 0.395 3.63 4 8.8 0.1 385 9 1 -5 37.514 75.029 0.395 3.63 4 63.1 2.6 386 5 7 -3 37.521 75.041 0.395 3.63 4 34.1 0.8 387 3 3 -9 37.527 75.055 0.395 3.62 4 37.2 0.9 388 4 6 4 37.574 75.148 0.396 3.62 4 4.9 0.0 389 7 1 4 37.585 75.169 0.396 3.61 4 26.5 0.5 390 6 2 5 37.591 75.182 0.396 3.61 4 6.9 0.0 391 0 8 3 37.623 75.246 0.396 3.61 4 9.7 0.1 392 6 6 1 37.639 75.278 0.396 3.6 4 37.1 0.9 393 0 2 9 37.639 75.279 0.396 3.6 4 4.9 0.0 394 8 2 2 37.682 75.364 0.397 3.6 4 4.1 0.0 395 3 5 6 37.725 75.451 0.397 3.59 4 59.2 2.3 396 7 5 -5 37.727 75.454 0.397 3.59 4 30.4 0.6 397 4 4 6 37.767 75.533 0.398 3.58 4 20.3 0.3 398 2 8 -3 37.8 75.599 0.398 3.58 4 14.4 0.1 399 8 4 0 37.922 75.844 0.399 3.56 4 11.0 0.1 400 9 1 0 37.922 75.845 0.399 3.56 4 89.6 5.2 401 7 5 1 37.936 75.873 0.399 3.55 4 108.9 7.7 402 4 2 7 38.017 76.035 0.4 3.54 4 48.6 1.5 403 2 8 2 38.033 76.066 0.4 3.54 4 28.7 0.5 404 6 4 4 38.065 76.129 0.4 3.53 4 30.3 0.6 405 1 3 -9 38.085 76.171 0.4 3.53 4 37.4 0.9 406 1 7 5 38.144 76.288 0.401 3.52 4 6.1 0.0 407 2 6 -7 38.237 76.474 0.402 3.51 4 29.4 0.6 408 8 4 -5 38.273 76.545 0.402 3.5 4 1.1 0.0 409 8 2 -7 38.314 76.627 0.402 3.49 4 77.6 3.9 410 6 6 -5 38.34 76.68 0.403 3.49 4 28.9 0.5 411 1 1 9 38.353 76.705 0.403 3.49 4 1.8 0.0 412 3 1 8 38.436 76.872 0.404 3.47 4 63.7 2.6 413 5 7 1 38.5 77.0 0.404 3.46 4 33.6 0.7 414 3 5 -8 38.542 77.084 0.404 3.46 4 44.3 1.2 415 5 7 -4 38.559 77.118 0.405 3.46 4 63.1 2.5 416 9 3 -3 38.599 77.197 0.405 3.45 4 28.5 0.5 417 9 3 -2 38.68 77.359 0.406 3.44 4 21.2 0.3 418 1 5 -8 38.795 77.589 0.407 3.42 4 25.9 0.4 419 2 6 6 38.84 77.68 0.407 3.41 4 18.8 0.2 420 5 3 6 38.963 77.926 0.408 3.39 4 50.0 1.6 421 9 1 -6 38.97 77.94 0.408 3.39 4 97.6 5.9 422 9 3 -4 39.028 78.055 0.409 3.39 4 26.8 0.4 423 3 7 4 39.063 78.127 0.409 3.38 4 97.4 5.9 424 5 3 -9 39.138 78.277 0.41 3.37 4 14.3 0.1 425 6 2 -9 39.221 78.442 0.41 3.36 4 30.3 0.6 426 0 6 7 39.267 78.535 0.411 3.35 4 40.2 1.0 427 9 3 -1 39.27 78.539 0.411 3.35 4 4.4 0.0 428 2 8 -4 39.287 78.573 0.411 3.35 4 21.4 0.3 429 1 7 -6 39.293 78.585 0.411 3.35 4 5.9 0.0 430 4 8 -1 39.302 78.603 0.411 3.35 4 14.8 0.1 431 6 6 2 39.312 78.625 0.411 3.35 4 71.1 3.1 432 2 0 -10 39.332 78.664 0.411 3.34 2 60.3 1.1 433 4 6 -7 39.365 78.73 0.412 3.34 4 32.1 0.6 434 8 4 1 39.384 78.768 0.412 3.34 4 32.0 0.6 435 0 8 4 39.412 78.824 0.412 3.33 4 83.5 4.3 436 6 4 -8 39.458 78.916 0.413 3.33 4 6.5 0.0 437 4 8 -2 39.463 78.926 0.413 3.32 4 3.8 0.0 438 3 1 -10 39.479 78.959 0.413 3.32 4 26.9 0.4 439 7 5 -6 39.481 78.961 0.413 3.32 4 5.1 0.0 440 9 1 1 39.535 79.069 0.413 3.32 4 39.6 1.0 441 4 0 -10 39.555 79.111 0.413 3.31 2 12.2 0.0 442 2 8 3 39.609 79.218 0.414 3.31 4 26.3 0.4 443 7 3 -8 39.619 79.238 0.414 3.3 4 22.2 0.3 444 3 7 -6 39.641 79.283 0.414 3.3 4 58.0 2.0 445 4 8 0 39.647 79.295 0.414 3.3 4 3.9 0.0 446 2 4 -9 39.678 79.356 0.414 3.3 4 17.1 0.2 447 8 0 -8 39.708 79.417 0.415 3.29 2 7.8 0.0 448 7 5 2 39.756 79.511 0.415 3.29 4 7.8 0.0 449 8 4 -6 39.869 79.739 0.416 3.27 4 36.4 0.8 450 9 3 -5 39.962 79.924 0.417 3.26 4 13.1 0.1 451 5 7 2 40.014 80.027 0.417 3.25 4 26.0 0.4 452 7 3 4 40.031 80.062 0.418 3.25 4 25.7 0.4 453 6 0 6 40.077 80.154 0.418 3.25 2 42.0 0.5 454 5 7 -5 40.095 80.19 0.418 3.24 4 26.2 0.4 455 4 8 -3 40.131 80.262 0.418 3.24 4 5.2 0.0 456 8 2 3 40.161 80.321 0.419 3.23 4 3.6 0.0 457 4 4 -9 40.2 80.399 0.419 3.23 4 33.0 0.6 458 6 6 -6 40.235 80.469 0.419 3.23 4 29.5 0.5 459 5 5 5 40.288 80.577 0.42 3.22 4 0.1 0.0 460 1 1 -10 40.328 80.656 0.42 3.21 4 26.3 0.4 461 9 3 0 40.363 80.726 0.42 3.21 4 4.9 0.0 462 5 5 -8 40.439 80.879 0.421 3.2 4 53.2 1.7 463 7 1 -9 40.447 80.893 0.421 3.2 4 24.6 0.4 464 2 4 8 40.459 80.917 0.421 3.2 4 30.5 0.5 465 4 6 5 40.468 80.936 0.421 3.2 4 21.5 0.3 466 4 8 1 40.498 80.995 0.422 3.19 4 0.2 0.0 467 2 2 -10 40.545 81.091 0.422 3.19 4 58.2 2.0 468 5 1 7 40.574 81.149 0.422 3.19 4 17.9 0.2 469 10 0 -2 40.74 81.48 0.424 3.17 2 16.3 0.1 470 4 2 -10 40.767 81.534 0.424 3.16 4 38.6 0.9 471 5 1 -10 40.771 81.543 0.424 3.16 4 7.0 0.0 472 1 3 9 40.786 81.571 0.424 3.16 4 5.7 0.0 473 10 0 -4 40.786 81.572 0.424 3.16 2 26.6 0.2 474 1 9 0 40.787 81.574 0.424 3.16 4 9.1 0.0 475 3 3 8 40.868 81.736 0.425 3.15 4 11.4 0.1 476 1 9 -1 40.89 81.78 0.425 3.15 4 35.1 0.7 477 9 1 -7 40.914 81.828 0.425 3.15 4 55.8 1.8 478 8 2 -8 40.919 81.838 0.425 3.15 4 35.0 0.7 479 7 1 5 40.925 81.85 0.425 3.15 4 19.9 0.2 480 1 7 6 41.084 82.168 0.427 3.13 4 37.7 0.8 481 1 5 8 41.186 82.372 0.427 3.12 4 29.8 0.5 482 1 9 1 41.187 82.374 0.427 3.12 4 34.5 0.7 483 4 0 8 41.205 82.411 0.428 3.12 2 156.1 6.9 484 6 4 5 41.246 82.492 0.428 3.11 4 32.2 0.6 485 0 0 10 41.247 82.494 0.428 3.11 2 5.6 0.0 486 2 8 -5 41.261 82.522 0.428 3.11 4 44.5 1.1 487 6 2 6 41.285 82.571 0.428 3.11 4 100.5 5.7 488 0 4 9 41.293 82.586 0.428 3.11 4 17.8 0.2 489 4 8 -4 41.299 82.598 0.428 3.11 4 58.0 1.9 490 8 4 2 41.334 82.669 0.429 3.1 4 51.2 1.5 491 9 3 -6 41.394 82.788 0.429 3.1 4 121.8 8.4 492 2 2 9 41.413 82.827 0.429 3.09 4 66.1 2.5 493 6 6 3 41.469 82.938 0.43 3.09 4 41.8 1.0 494 3 5 7 41.474 82.947 0.43 3.09 4 43.6 1.1 495 1 9 -2 41.495 82.991 0.43 3.09 4 3.9 0.0 496 9 1 2 41.631 83.263 0.431 3.07 4 41.0 0.9 497 4 4 7 41.662 83.324 0.431 3.07 4 10.4 0.1 498 2 8 4 41.671 83.342 0.432 3.07 4 78.6 3.5 499 0 8 5 41.682 83.363 0.432 3.07 4 27.1 0.4 500 7 5 -7 41.715 83.43 0.432 3.07 4 28.5 0.5 501 10 2 -3 41.717 83.433 0.432 3.06 4 14.0 0.1 502 2 6 -8 41.734 83.468 0.432 3.06 4 79.8 3.6 503 3 7 5 41.782 83.564 0.433 3.06 4 32.7 0.6 504 4 8 2 41.846 83.691 0.433 3.05 4 34.1 0.6 505 3 3 -10 41.896 83.793 0.433 3.05 4 27.6 0.4 506 8 0 4 41.904 83.807 0.434 3.05 2 14.4 0.1 507 6 0 -10 41.909 83.818 0.434 3.05 2 55.8 0.9 508 10 2 -2 41.944 83.888 0.434 3.04 4 74.4 3.1 509 9 3 1 41.951 83.901 0.434 3.04 4 26.3 0.4 510 8 4 -7 41.952 83.903 0.434 3.04 4 24.7 0.3 511 10 2 -4 41.99 83.98 0.434 3.04 4 39.9 0.9 512 5 7 3 42.014 84.029 0.434 3.04 4 3.5 0.0 513 7 5 3 42.055 84.11 0.435 3.03 4 62.2 2.2 514 1 9 2 42.088 84.176 0.435 3.03 4 4.2 0.0 515 5 7 -6 42.118 84.236 0.435 3.03 4 31.0 0.5 516 3 5 -9 42.386 84.771 0.438 3.0 4 72.3 2.9 517 4 2 8 42.407 84.814 0.438 3.0 4 33.5 0.6 518 2 6 7 42.416 84.832 0.438 3.0 4 11.2 0.1 519 1 7 -7 42.417 84.835 0.438 3.0 4 1.5 0.0 520 0 2 10 42.449 84.898 0.438 3.0 4 126.5 8.8 521 3 7 -7 42.465 84.931 0.438 3.0 4 51.3 1.4 522 4 6 -8 42.546 85.092 0.439 2.99 4 34.7 0.7 523 1 9 -3 42.6 85.199 0.439 2.99 4 12.6 0.1 524 8 6 -2 42.605 85.21 0.439 2.99 4 8.9 0.0 525 6 6 -7 42.609 85.217 0.439 2.99 4 8.7 0.0 526 10 2 -1 42.672 85.343 0.44 2.98 4 9.4 0.0 527 8 6 -3 42.673 85.347 0.44 2.98 4 34.1 0.6 528 10 0 0 42.7 85.399 0.44 2.98 2 50.5 0.7 529 3 9 -1 42.715 85.431 0.44 2.98 4 23.0 0.3 530 1 3 -10 42.735 85.47 0.44 2.97 4 70.1 2.7 531 10 2 -5 42.763 85.527 0.441 2.97 4 52.6 1.5 532 7 7 -2 42.829 85.658 0.441 2.97 4 28.2 0.4 533 10 0 -6 42.837 85.675 0.441 2.97 2 99.4 2.7 534 6 4 -9 42.841 85.683 0.441 2.97 4 57.2 1.8 535 7 3 -9 42.853 85.705 0.441 2.97 4 83.7 3.8 536 3 9 0 42.908 85.817 0.442 2.96 4 62.8 2.1 537 1 5 -9 42.928 85.856 0.442 2.96 4 38.7 0.8 538 4 8 -5 42.96 85.921 0.442 2.96 4 3.2 0.0 539 5 3 7 42.979 85.958 0.443 2.96 4 1.3 0.0 540 3 9 -2 43.022 86.044 0.443 2.95 4 96.0 5.0 541 8 6 -1 43.036 86.072 0.443 2.95 4 55.2 1.6 542 0 6 8 43.04 86.08 0.443 2.95 4 11.7 0.1 543 7 7 -3 43.045 86.09 0.443 2.95 4 13.5 0.1 544 8 2 4 43.103 86.205 0.444 2.95 4 27.3 0.4 545 6 2 -10 43.108 86.216 0.444 2.95 4 53.3 1.5 546 7 7 -1 43.113 86.226 0.444 2.95 4 66.7 2.4 547 3 1 9 43.167 86.335 0.444 2.94 4 24.0 0.3 548 5 3 -10 43.174 86.348 0.444 2.94 4 10.5 0.1 549 8 6 -4 43.241 86.482 0.445 2.94 4 51.2 1.4 550 1 1 10 43.29 86.581 0.445 2.93 4 13.6 0.1 551 9 3 -7 43.316 86.632 0.445 2.93 4 1.3 0.0 552 7 3 5 43.327 86.653 0.445 2.93 4 70.7 2.7 553 9 1 -8 43.339 86.677 0.445 2.93 4 17.4 0.2 554 9 5 -3 43.428 86.857 0.446 2.92 4 13.2 0.1 555 1 9 3 43.485 86.969 0.447 2.92 4 31.3 0.5 556 9 5 -2 43.508 87.015 0.447 2.92 4 52.2 1.5 557 3 9 1 43.6 87.2 0.448 2.91 4 2.8 0.0 558 4 8 3 43.685 87.371 0.448 2.9 4 39.1 0.8 559 2 8 -6 43.716 87.433 0.449 2.9 4 28.1 0.4 560 7 7 -4 43.76 87.519 0.449 2.9 4 82.6 3.6 561 8 4 3 43.766 87.533 0.449 2.9 4 46.7 1.2 562 5 5 6 43.785 87.569 0.449 2.9 4 26.8 0.4 563 4 6 6 43.815 87.63 0.449 2.9 4 12.0 0.1 564 3 9 -3 43.827 87.654 0.45 2.9 4 13.6 0.1 565 9 5 -4 43.848 87.696 0.45 2.89 4 44.1 1.0 566 7 7 0 43.895 87.79 0.45 2.89 4 121.8 7.8 567 10 2 0 43.896 87.793 0.45 2.89 4 8.2 0.0 568 5 5 -9 43.957 87.913 0.451 2.89 4 43.0 1.0 569 8 6 0 43.966 87.931 0.451 2.89 4 70.2 2.6 570 8 2 -9 43.99 87.979 0.451 2.89 4 13.3 0.1 571 9 3 2 44.028 88.055 0.451 2.88 4 2.7 0.0 572 10 2 -6 44.034 88.067 0.451 2.88 4 45.5 1.1 573 9 5 -1 44.085 88.171 0.452 2.88 4 3.1 0.0 574 6 6 4 44.104 88.208 0.452 2.88 4 8.0 0.0 575 2 4 -10 44.146 88.293 0.452 2.88 4 28.1 0.4 576 7 1 -10 44.168 88.335 0.452 2.87 4 11.4 0.1 577 6 8 -2 44.179 88.358 0.452 2.87 4 1.7 0.0 578 1 9 -4 44.199 88.397 0.453 2.87 4 2.4 0.0 579 9 1 3 44.209 88.417 0.453 2.87 4 21.4 0.2 580 2 8 5 44.214 88.429 0.453 2.87 4 54.6 1.6 581 3 1 -11 44.302 88.604 0.453 2.87 4 34.2 0.6 582 8 6 -5 44.306 88.613 0.453 2.87 4 0.0 0.0 583 6 8 -1 44.315 88.629 0.453 2.87 4 34.4 0.6 584 4 4 -10 44.366 88.731 0.454 2.86 4 3.8 0.0 585 7 5 -8 44.428 88.856 0.454 2.86 4 17.6 0.2 586 0 8 6 44.429 88.857 0.454 2.86 4 33.4 0.6 587 1 7 7 44.481 88.962 0.455 2.86 4 14.2 0.1 588 5 7 4 44.499 88.998 0.455 2.85 4 12.4 0.1 589 8 4 -8 44.516 89.032 0.455 2.85 4 6.9 0.0 590 6 8 -3 44.541 89.083 0.455 2.85 4 20.7 0.2 591 5 7 -7 44.625 89.25 0.456 2.85 4 12.9 0.1 592 7 1 6 44.708 89.417 0.457 2.84 4 61.9 2.0 593 9 5 -5 44.766 89.531 0.457 2.84 4 53.8 1.5 594 3 9 2 44.789 89.579 0.457 2.84 4 67.7 2.4 595 7 5 4 44.834 89.667 0.458 2.84 4 12.1 0.1 596 6 4 6 44.879 89.758 0.458 2.83 4 99.6 5.1 597 6 8 0 44.949 89.897 0.459 2.83 4 43.3 1.0 598 3 7 6 44.97 89.939 0.459 2.83 4 9.4 0.0 599 7 7 -5 44.971 89.943 0.459 2.83 4 4.9 0.0 X-ray diffraction powder data (I)...X-Ray wave length = 1.54056 (angs.): No H K L Theta 2*Theta d I int I int.n. I p.h.n. H(Si) ( degree ) (angstrem) *100 *100 1 1 1 0 5.684 11.369 7.77683 27.6 8.7 8.8 5.6 2 1 1 -1 6.18 12.36 7.15519 68.1 21.4 21.8 5.6 3 1 1 1 7.431 14.861 5.95605 46.0 14.5 14.7 5.6 4 0 0 2 7.577 15.154 5.84159 20.2 6.3 6.4 5.6 5 2 0 0 7.795 15.59 5.67923 177.8 55.9 56.8 5.6 6 0 2 0 8.302 16.603 5.335 16.0 5.0 5.1 5.6 7 1 1 -2 8.542 17.084 5.18597 67.7 21.3 21.6 5.6 8 0 2 1 9.133 18.266 4.85297 294.8 92.8 94.0 5.6 9 0 2 2 11.276 22.552 3.93936 89.5 28.2 28.4 5.6 10 2 2 -1 11.309 22.617 3.92813 60.1 18.9 19.1 5.6 11 2 0 2 12.392 24.785 3.58927 9.7 3.0 3.1 5.6 12 3 1 0 12.467 24.934 3.56817 20.8 6.6 6.6 5.6 13 2 2 1 12.752 25.505 3.48957 17.1 5.4 5.4 5.6 14 1 3 0 13.117 26.234 3.39416 5.6 1.8 1.8 5.6 15 1 3 -1 13.346 26.692 3.33702 20.6 6.5 6.5 5.6 16 1 3 1 13.987 27.974 3.18695 4.9 1.6 1.6 5.6 17 3 1 1 14.016 28.031 3.18055 14.8 4.7 4.7 5.6 18 0 2 3 14.175 28.35 3.14549 3.4 1.1 1.1 5.6 19 2 2 -3 14.531 29.063 3.06997 21.5 6.8 6.8 5.6 20 2 2 2 14.99 29.98 2.97803 60.1 18.9 19.0 5.6 21 2 0 -4 15.047 30.095 2.967 73.7 23.2 23.3 5.6 22 1 1 -4 15.239 30.478 2.93055 8.2 2.6 2.6 5.6 23 0 0 4 15.291 30.582 2.92079 20.7 6.5 6.5 5.6 24 4 0 0 15.739 31.479 2.83961 71.4 22.5 22.5 5.6 25 1 3 2 15.788 31.576 2.83109 164.3 51.7 51.9 5.6 26 0 4 0 16.784 33.568 2.6675 17.8 5.6 5.6 5.7 27 3 3 -1 16.944 33.888 2.64302 4.6 1.4 1.4 5.7 28 3 1 -4 16.985 33.97 2.63686 12.1 3.8 3.8 5.7 29 0 4 1 17.229 34.459 2.60058 9.8 3.1 3.1 5.7 30 3 3 0 17.286 34.572 2.59228 5.1 1.6 1.6 5.7 31 1 1 4 17.421 34.842 2.57285 107.9 34.0 34.0 5.7 32 3 3 -2 17.485 34.97 2.56371 317.8 100.0 100.0 5.7 33 4 2 -2 17.584 35.169 2.54965 52.5 16.5 16.5 5.7 34 2 2 3 17.832 35.664 2.51542 4.3 1.3 1.3 5.7 35 4 2 0 17.896 35.792 2.50666 3.5 1.1 1.1 5.7 36 1 3 3 18.275 36.55 2.45645 39.3 12.4 12.4 5.7 37 3 3 -3 18.842 37.684 2.38507 24.3 7.6 7.6 5.7 38 2 0 4 19.231 38.462 2.33858 68.8 21.6 21.6 5.7 39 2 4 -2 19.268 38.537 2.33423 54.4 17.1 17.1 5.7 40 5 1 -2 19.542 39.084 2.30277 14.8 4.6 4.6 5.7 41 3 3 2 20.364 40.728 2.21357 24.3 7.7 7.6 5.7 42 0 4 3 20.488 40.976 2.20074 16.0 5.0 5.0 5.7 43 4 2 -4 20.521 41.043 2.19732 15.2 4.8 4.8 5.7 44 2 4 -3 20.748 41.495 2.17439 6.6 2.1 2.1 5.7 45 3 3 -4 20.88 41.76 2.16123 15.1 4.8 4.7 5.7 46 2 2 4 21.078 42.156 2.14184 49.1 15.5 15.3 5.7 47 4 2 2 21.335 42.669 2.11722 3.8 1.2 1.2 5.7 48 1 5 0 21.547 43.095 2.09731 4.4 1.4 1.4 5.7 49 1 5 -1 21.696 43.392 2.08361 16.6 5.2 5.2 5.7 50 5 1 -4 21.838 43.676 2.07074 23.0 7.3 7.2 5.7 51 1 5 1 22.121 44.242 2.04553 20.1 6.3 6.3 5.7 52 2 0 -6 22.306 44.613 2.02941 14.7 4.6 4.6 5.7 53 3 1 4 22.542 45.085 2.00925 37.1 11.7 11.6 5.7 54 1 3 -5 22.572 45.144 2.00677 4.4 1.4 1.4 5.7 55 3 3 3 22.829 45.658 1.98535 10.3 3.2 3.2 5.7 56 4 4 -1 22.87 45.74 1.98198 6.0 1.9 1.9 5.7 57 5 3 -2 23.073 46.145 1.96551 23.6 7.4 7.3 5.7 58 2 4 3 23.289 46.577 1.94829 27.6 8.7 8.6 5.7 59 3 1 -6 23.332 46.664 1.94486 8.0 2.5 2.5 5.7 60 1 5 2 23.375 46.751 1.94147 6.6 2.1 2.0 5.7 61 3 3 -5 23.456 46.913 1.93513 5.1 1.6 1.6 5.7 62 5 3 -3 23.771 47.542 1.91096 25.7 8.1 8.0 5.7 63 5 1 -5 23.94 47.879 1.8983 11.0 3.5 3.4 5.7 64 4 4 -3 23.987 47.975 1.89474 50.7 16.0 15.8 5.7 65 4 0 -6 24.23 48.461 1.87687 8.6 2.7 2.7 5.7 66 3 5 0 24.478 48.956 1.85904 6.3 2.0 2.0 5.7 67 6 2 -2 24.576 49.153 1.85205 31.9 10.0 9.9 5.7 68 6 0 -4 24.614 49.228 1.84939 38.2 12.0 11.9 5.7 69 0 2 6 24.905 49.809 1.82917 4.5 1.4 1.4 5.7 70 4 4 -4 25.506 51.013 1.7888 11.4 3.6 3.5 5.8 71 6 2 0 25.579 51.157 1.78409 3.2 1.0 1.0 5.8 72 0 6 0 25.667 51.335 1.77833 10.2 3.2 3.2 5.8 73 3 3 4 25.744 51.488 1.7734 9.1 2.9 2.8 5.8 74 4 2 -6 25.789 51.579 1.7705 8.2 2.6 2.5 5.8 75 0 4 5 25.992 51.984 1.75766 14.5 4.6 4.5 5.8 76 1 3 -6 26.03 52.06 1.75526 39.5 12.4 12.2 5.8 77 1 5 -4 26.145 52.29 1.74809 4.1 1.3 1.3 5.8 78 4 4 2 26.198 52.396 1.74478 17.8 5.6 5.5 5.8 79 3 3 -6 26.461 52.923 1.72866 22.7 7.1 7.0 5.8 80 3 5 2 26.884 53.769 1.70344 10.0 3.2 3.1 5.8 81 5 3 2 26.918 53.835 1.70148 61.2 19.2 18.9 5.8 82 6 2 1 27.004 54.008 1.69645 12.9 4.1 4.0 5.8 83 7 1 -3 27.677 55.354 1.65834 3.6 1.1 1.1 5.8 84 2 2 -7 27.714 55.429 1.65629 7.6 2.4 2.3 5.8 85 2 4 -6 28.484 56.969 1.61512 7.7 2.4 2.4 5.8 86 7 1 -4 28.536 57.071 1.61246 8.0 2.5 2.4 5.8 87 6 0 -6 28.631 57.261 1.60756 4.0 1.3 1.2 5.8 88 6 2 2 28.971 57.942 1.59027 4.4 1.4 1.3 5.8 89 2 4 5 29.074 58.148 1.58515 4.9 1.6 1.5 5.8 90 5 5 -1 29.117 58.233 1.58302 9.1 2.9 2.8 5.8 91 0 4 6 29.325 58.651 1.57275 14.4 4.5 4.4 5.8 92 5 3 -6 29.422 58.845 1.56802 4.1 1.3 1.3 5.8 93 3 5 -5 29.456 58.913 1.56637 3.2 1.0 1.0 5.8 94 3 1 6 29.955 59.909 1.54267 13.8 4.3 4.2 5.8 95 7 3 -2 30.243 60.487 1.52933 6.3 2.0 1.9 5.8 96 2 6 -4 30.331 60.662 1.52533 5.8 1.8 1.8 5.8 97 0 6 4 30.472 60.944 1.51894 25.9 8.2 7.9 5.8 98 1 7 0 30.655 61.31 1.51074 28.6 9.0 8.7 5.8 99 2 6 3 30.693 61.385 1.50907 4.4 1.4 1.3 5.8 100 5 5 1 30.817 61.634 1.50357 4.6 1.4 1.4 5.8 101 4 0 -8 31.281 62.561 1.4835 15.5 4.9 4.7 5.8 102 8 0 -4 32.057 64.113 1.45129 6.0 1.9 1.8 5.9 103 4 0 6 32.69 65.381 1.42619 5.4 1.7 1.6 5.9 104 8 0 0 32.856 65.711 1.41981 12.8 4.0 3.9 5.9 105 2 6 4 32.967 65.934 1.41555 21.8 6.9 6.6 5.9 106 6 4 2 33.033 66.065 1.41305 8.9 2.8 2.7 5.9 107 0 2 8 33.151 66.302 1.40858 7.0 2.2 2.1 5.9 108 6 0 -8 34.48 68.96 1.36063 3.6 1.1 1.1 5.9 109 8 2 -5 34.519 69.038 1.35929 3.7 1.2 1.1 5.9 110 1 5 -7 35.056 70.112 1.34107 6.5 2.0 1.9 5.9 111 3 5 -7 35.107 70.214 1.33938 8.1 2.5 2.4 5.9 112 2 0 8 35.528 71.057 1.32554 6.8 2.1 2.0 5.9 113 6 6 -2 35.653 71.307 1.32151 4.8 1.5 1.5 5.9 114 9 1 -1 36.808 73.616 1.28566 3.7 1.2 1.1 6.0 115 6 6 -4 36.935 73.87 1.28186 16.4 5.2 4.9 6.0 116 7 3 3 37.186 74.372 1.27444 3.6 1.1 1.1 6.0 117 9 1 -5 37.514 75.029 1.26491 4.3 1.4 1.3 6.0 118 7 5 1 37.936 75.873 1.25292 12.9 4.1 3.8 6.0 119 8 2 -7 38.314 76.627 1.24245 4.4 1.4 1.3 6.0 120 5 7 -4 38.559 77.118 1.23577 3.8 1.2 1.1 6.0 121 9 1 -6 38.97 77.94 1.22478 7.5 2.4 2.2 6.0 122 3 7 4 39.063 78.127 1.22232 5.9 1.8 1.7 6.0 123 6 6 2 39.312 78.625 1.21582 4.2 1.3 1.2 6.0 124 0 8 4 39.412 78.824 1.21324 4.3 1.3 1.3 6.0 125 4 0 8 41.205 82.411 1.16929 6.9 2.2 2.0 6.1 126 6 2 6 41.285 82.571 1.16743 8.8 2.8 2.6 6.1 127 9 3 -6 41.394 82.788 1.16492 10.9 3.4 3.2 6.1 128 2 8 4 41.671 83.342 1.15857 3.9 1.2 1.1 6.1 129 2 6 -8 41.734 83.468 1.15714 3.6 1.1 1.0 6.1 130 10 2 -2 41.944 83.888 1.15241 3.8 1.2 1.1 6.1 131 3 5 -9 42.386 84.771 1.14265 3.6 1.1 1.0 6.1 132 0 2 10 42.449 84.898 1.14127 10.2 3.2 3.0 6.1 133 1 3 -10 42.735 85.47 1.13509 4.2 1.3 1.2 6.1 134 7 3 -9 42.853 85.705 1.13258 8.3 2.6 2.4 6.1 135 3 9 -2 43.022 86.044 1.12898 6.8 2.1 2.0 6.1 136 7 7 -1 43.113 86.226 1.12707 3.9 1.2 1.1 6.1 137 7 7 -4 43.76 87.519 1.11371 5.2 1.6 1.5 6.2 138 7 7 0 43.895 87.79 1.11098 7.9 2.5 2.3 6.2 139 3 9 2 44.789 89.579 1.09337 3.9 1.2 1.1 6.2 140 6 4 6 44.879 89.758 1.09165 5.1 1.6 1.5 6.2 Reference: Chichagov A.V. et al. Information-Calculating System on Crystal Structure Data of Minerals (MINCRYST) - Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian) |