Institute of Experimental Mineralogy Russian Academy of Sciences ------------------------------------------------- 142432, Chernogolovka, Moscow district A.V. Chichagov +7(496)52-22320 *** *** W W W - X R A Y P O L *** *********************** AMICITE 1, f-zeolites, sf-thomsonite, ZL K(4)Na(4)[Al(8)Si(8)O(32)].10H(2)O Monoclinic I 2 Z = 1 R =0.041 NR =1245 15 .5 .1990 Ref.Str.: A. Alberti, G. Vezzalini (1979) * Acta Cryst.., B 35, 2866-2869 Initial data from BDM-file Lattice parameters (cub. angs.,degr.): a = 10.226 alpha = 90.0 b = 10.422 beta = 88.32 c = 9.884 gamma = 90.0 Unit cell volume (cub. angs.) = 1052.94 Molar volume ( cub.cm/mol.) = 634.22 Co-ordinates, thermal parameters, occupation for atomic positions: NoP x/a y/b z/c B(j) atom / occupation 1 0.1523 0.9867 0.3261 0.46 Si = 1.00 2 0.1534 0.2615 0.8263 0.4 Si = 1.00 3 0.1546 0.2491 0.1546 0.43 Al = 1.00 4 0.1582 0.0027 0.6512 0.44 Al = 1.00 5 0.001 0.9529 0.3037 1.21 O = 1.00 6 0.997 0.2956 0.2047 1.14 O = 1.00 7 0.2031 0.1401 0.7354 0.96 O = 1.00 8 0.181 0.0304 0.4785 1.18 O = 1.00 9 0.1712 0.2264 0.9833 1.13 O = 1.00 10 0.1989 0.1018 0.2263 1.0 O = 1.00 11 0.262 0.361 0.2184 1.09 O = 1.00 12 0.7558 0.3812 0.2177 0.73 O = 1.00 13 0.4312 0.2559 0.6716 2.53 Na = 1.00 14 0.3071 0.996 0.9692 2.09 K = 1.00 15 0.3435 0.2507 0.4539 2.65 H(2)O = 1.00 16 0.4779 0.0682 0.2179 2.76 H(2)O = 1.00 17 0.0 0.3191 0.5 2.7 H(2)O = 1.00 18 0.5 0.4729 0.5 2.35 H(2)O = 1.00 Co-ordinates for all atomic positions : No NoP x/a y/b z/c 1 1 0.1523 0.9867 0.3261 2 2 0.1534 0.2615 0.8263 3 3 0.1546 0.2491 0.1546 4 4 0.1582 0.0027 0.6512 5 5 0.001 0.9529 0.3037 6 6 0.997 0.2956 0.2047 7 7 0.2031 0.1401 0.7354 8 8 0.181 0.0304 0.4785 9 9 0.1712 0.2264 0.9833 10 10 0.1989 0.1018 0.2263 11 11 0.262 0.361 0.2184 12 12 0.7558 0.3812 0.2177 13 13 0.4312 0.2559 0.6716 14 14 0.3071 0.996 0.9692 15 15 0.3435 0.2507 0.4539 16 16 0.4779 0.0682 0.2179 17 17 0.0 0.3191 0.5 18 18 0.5 0.4729 0.5 19 1 0.8477 0.9867 0.6739 20 2 0.8466 0.2615 0.1737 21 3 0.8454 0.2491 0.8454 22 4 0.8418 0.0027 0.3488 23 5 0.999 0.9529 0.6963 24 6 0.003 0.2956 0.7953 25 7 0.7969 0.1401 0.2646 26 8 0.819 0.0304 0.5215 27 9 0.8288 0.2264 0.0167 28 10 0.8011 0.1018 0.7737 29 11 0.738 0.361 0.7816 30 12 0.2442 0.3812 0.7823 31 13 0.5688 0.2559 0.3284 32 14 0.6929 0.996 0.0308 33 15 0.6565 0.2507 0.5461 34 16 0.5221 0.0682 0.7821 35 1 0.6523 0.4867 0.8261 36 2 0.6534 0.7615 0.3263 37 3 0.6546 0.7491 0.6546 38 4 0.6582 0.5027 0.1512 39 5 0.501 0.4529 0.8037 40 6 0.497 0.7956 0.7047 41 7 0.7031 0.6401 0.2354 42 8 0.681 0.5304 0.9785 43 9 0.6712 0.7264 0.4833 44 10 0.6989 0.6018 0.7263 45 11 0.762 0.861 0.7184 46 12 0.2558 0.8812 0.7177 47 13 0.9312 0.7559 0.1716 48 14 0.8071 0.496 0.4692 49 15 0.8435 0.7507 0.9539 50 16 0.9779 0.5682 0.7179 51 17 0.5 0.8191 0.0 52 18 0.0 0.9729 0.0 53 1 0.3477 0.4867 0.1739 54 2 0.3466 0.7615 0.6737 55 3 0.3454 0.7491 0.3454 56 4 0.3418 0.5027 0.8488 57 5 0.499 0.4529 0.1963 58 6 0.503 0.7956 0.2953 59 7 0.2969 0.6401 0.7646 60 8 0.319 0.5304 0.0215 61 9 0.3288 0.7264 0.5167 62 10 0.3011 0.6018 0.2737 63 11 0.238 0.861 0.2816 64 12 0.7442 0.8812 0.2823 65 13 0.0688 0.7559 0.8284 66 14 0.1929 0.496 0.5308 67 15 0.1565 0.7507 0.0461 68 16 0.0221 0.5682 0.2821 X-ray density (g/cm cub.) = 2.23 MU (1/cm) = 90.828 Mass attenuation coefficient (cm**2/g) = 40.657 Selected interatomic distances (cation-anion,anion-anion): NoP Atom Rad.sph. C.N. Distance NoP N. (angs.) (angs.) 1 Si 2.268 4 1.6084 5 1.6089 8 1.616 10 1.6294 11 2 Si 2.268 4 1.6247 7 1.6098 9 1.6165 6 1.6075 12 3 Al 2.484 4 1.7409 6 1.7131 9 1.7558 10 1.7334 11 4 Al 2.484 4 1.7252 7 1.7401 8 1.7538 5 1.7522 12 5 O 3.432 7 2.6855 8 2.6454 10 2.8912 7 2.9181 8 3.0093 18 2.6092 11 2.7444 12 6 O 3.432 8 2.8729 9 2.9006 10 2.8014 11 2.6225 12 2.9301 17 2.6633 7 2.6681 9 2.9554 16 7 O 3.432 8 2.7999 8 2.6215 9 3.3011 15 2.8912 5 2.6633 6 2.5917 12 3.3918 16 2.7561 12 8 O 3.432 7 2.6855 5 2.7999 7 2.6027 10 2.8405 15 2.9181 5 2.9494 12 2.6791 11 9 O 3.432 7 2.8729 6 2.6215 7 2.7523 10 2.8907 11 2.6681 6 2.6495 12 3.171 18 10 O 3.432 9 2.6454 5 2.9006 6 2.6027 8 2.7523 9 2.7779 11 3.1385 15 2.8732 16 3.3484 18 2.6018 11 11 O 3.432 8 2.8014 6 2.8907 9 2.7779 10 2.7473 15 2.6092 5 2.6791 8 2.6018 10 3.3147 16 12 O 3.432 7 2.6225 6 2.5917 7 2.6495 9 2.7561 7 2.9494 8 2.7444 5 3.4236 16 13 Na 2.976 7 2.6849 7 2.3559 15 2.9011 18 2.537 12 2.585 15 2.4379 16 2.5464 5 14 K 3.396 9 2.9784 7 2.7758 9 2.9551 10 3.1482 16 2.9294 16 2.8218 12 2.7236 17 3.1554 18 3.0686 15 15 H(2)O 3.6 7 3.3011 7 2.8405 8 3.1385 10 2.7473 11 3.2802 16 2.8591 18 3.3535 15 16 H(2)O 3.6 7 2.8732 10 3.2802 15 3.3918 7 3.3765 17 2.9554 6 3.3147 11 3.4236 12 17 H(2)O 3.6 6 2.9301 6 3.5357 8 2.9301 6 3.5357 8 3.3765 16 3.3765 16 18 H(2)O 3.6 8 2.8591 15 2.8591 15 3.0093 5 3.171 9 3.3484 10 3.0093 5 3.171 9 3.3484 10 X-ray diffraction powder data (II), X-Ray W.L. = 1.54056(angs.): No H K L Theta 2*Theta S LPG MF F I int. ( degree ) *100 1 1 1 0 6.059 12.118 0.069 176.54 4 79.4 401.1 2 1 0 1 6.133 12.265 0.069 172.27 2 20.6 13.2 3 0 1 1 6.167 12.334 0.07 170.32 4 34.1 71.6 4 1 0 -1 6.316 12.632 0.071 162.3 2 13.2 5.1 5 0 2 0 8.501 17.001 0.096 88.59 2 35.4 20.1 6 2 0 0 8.668 17.337 0.098 85.11 2 131.6 266.0 7 0 0 2 8.971 17.942 0.101 79.32 2 120.9 209.2 8 1 2 1 10.509 21.017 0.118 57.22 4 141.5 413.3 9 2 1 1 10.557 21.114 0.119 56.68 4 38.3 30.0 10 1 2 -1 10.618 21.236 0.12 56.0 4 105.3 223.9 11 1 1 2 10.746 21.492 0.121 54.62 4 22.3 9.8 12 2 1 -1 10.774 21.548 0.121 54.33 4 50.4 49.9 13 1 1 -2 10.96 21.919 0.123 52.43 4 39.8 29.9 14 2 2 0 12.187 24.374 0.137 42.0 4 46.9 33.3 15 2 0 2 12.337 24.674 0.139 40.94 2 15.7 1.8 16 0 2 2 12.407 24.815 0.139 40.45 4 47.5 32.9 17 2 0 -2 12.71 25.42 0.143 38.45 2 14.5 1.4 18 1 3 0 13.543 27.087 0.152 33.62 4 98.8 118.4 19 0 3 1 13.594 27.187 0.153 33.36 4 27.7 9.2 20 3 0 1 13.708 27.416 0.154 32.77 2 35.1 7.3 21 3 1 0 13.76 27.519 0.154 32.51 4 130.7 200.2 22 3 0 -1 13.963 27.926 0.157 31.52 2 17.1 1.7 23 1 0 3 14.101 28.201 0.158 30.86 2 9.1 0.5 24 0 1 3 14.199 28.399 0.159 30.41 4 192.7 407.5 25 1 0 -3 14.349 28.698 0.161 29.74 2 38.0 7.7 26 2 2 2 15.059 30.118 0.169 26.82 4 65.8 41.9 27 2 2 -2 15.371 30.741 0.172 25.67 4 10.2 1.0 28 2 3 1 16.139 32.278 0.18 23.1 4 59.8 29.8 29 3 2 1 16.218 32.436 0.181 22.86 4 144.4 172.0 30 1 3 2 16.267 32.535 0.182 22.71 4 29.2 7.0 31 2 3 -1 16.286 32.573 0.182 22.65 4 14.1 1.6 32 3 1 2 16.305 32.61 0.182 22.6 4 92.7 70.1 33 1 3 -2 16.414 32.827 0.183 22.28 4 77.0 47.7 34 3 2 -1 16.438 32.875 0.184 22.21 4 227.9 415.9 35 2 1 3 16.516 33.032 0.185 21.98 4 56.3 25.1 36 1 2 3 16.557 33.113 0.185 21.86 4 188.5 280.3 37 3 1 -2 16.739 33.478 0.187 21.35 4 120.8 112.5 38 1 2 -3 16.772 33.544 0.187 21.26 4 67.5 34.9 39 2 1 -3 16.946 33.891 0.189 20.78 4 39.0 11.4 40 0 4 0 17.196 34.391 0.192 20.13 2 230.8 193.5 41 4 0 0 17.544 35.087 0.196 19.27 2 2.9 0.0 42 0 0 4 18.171 36.343 0.202 17.84 2 105.1 35.6 43 1 4 1 18.321 36.643 0.204 17.52 4 39.1 9.6 44 1 4 -1 18.387 36.775 0.205 17.39 4 6.4 0.3 45 3 3 0 18.461 36.922 0.206 17.23 4 23.6 3.5 46 4 1 1 18.533 37.065 0.206 17.09 4 93.4 53.8 47 3 0 3 18.693 37.386 0.208 16.77 2 21.3 1.4 48 4 1 -1 18.793 37.586 0.209 16.57 4 24.0 3.4 49 0 3 3 18.801 37.603 0.209 16.55 4 63.6 24.2 50 1 1 4 19.095 38.191 0.212 16.0 4 59.6 20.5 51 3 0 -3 19.27 38.541 0.214 15.68 2 37.9 4.1 52 1 1 -4 19.349 38.699 0.215 15.54 4 79.9 35.8 53 2 4 0 19.38 38.761 0.215 15.48 4 19.6 2.1 54 0 4 2 19.526 39.052 0.217 15.23 4 81.6 36.6 55 4 0 2 19.59 39.18 0.218 15.12 2 17.4 0.8 56 4 2 0 19.617 39.233 0.218 15.07 4 60.4 19.8 57 2 0 4 20.021 40.043 0.222 14.4 2 105.7 29.0 58 4 0 -2 20.085 40.17 0.223 14.3 2 98.9 25.2 59 0 2 4 20.189 40.378 0.224 14.14 4 44.4 10.1 60 3 3 2 20.489 40.978 0.227 13.68 4 40.1 7.9 61 2 0 -4 20.507 41.015 0.227 13.65 2 23.2 1.3 62 2 3 3 20.663 41.326 0.229 13.42 4 47.2 10.8 63 3 2 3 20.667 41.335 0.229 13.42 4 21.9 2.3 64 3 3 -2 20.848 41.695 0.231 13.16 4 57.6 15.7 65 2 3 -3 21.019 42.039 0.233 12.92 4 18.3 1.6 66 3 2 -3 21.2 42.399 0.235 12.68 4 7.1 0.2 67 2 4 2 21.393 42.786 0.237 12.42 4 108.4 52.7 68 4 2 2 21.496 42.991 0.238 12.29 4 26.7 3.2 69 2 4 -2 21.624 43.249 0.239 12.12 4 105.6 48.8 70 2 2 4 21.896 43.791 0.242 11.79 4 15.5 1.0 71 4 2 -2 21.955 43.91 0.243 11.72 4 19.9 1.7 72 1 5 0 22.157 44.315 0.245 11.48 4 35.2 5.1 73 0 5 1 22.19 44.38 0.245 11.44 4 17.6 1.3 74 3 4 1 22.265 44.53 0.246 11.35 4 59.4 14.5 75 2 2 -4 22.348 44.697 0.247 11.26 4 44.7 8.1 76 4 3 1 22.36 44.72 0.247 11.24 4 78.4 25.0 77 3 4 -1 22.433 44.866 0.248 11.16 4 24.0 2.3 78 5 0 1 22.49 44.981 0.248 11.1 2 37.2 2.8 79 1 4 3 22.525 45.05 0.249 11.06 4 43.1 7.4 80 4 1 3 22.537 45.073 0.249 11.05 4 7.1 0.2 81 5 1 0 22.58 45.16 0.249 11.0 4 72.1 20.6 82 4 3 -1 22.584 45.167 0.249 10.99 4 33.5 4.4 83 1 4 -3 22.692 45.383 0.25 10.88 4 77.4 23.5 84 3 1 4 22.762 45.524 0.251 10.8 4 33.6 4.4 85 5 0 -1 22.768 45.536 0.251 10.79 2 71.9 10.1 86 1 3 4 22.844 45.689 0.252 10.71 4 6.4 0.2 87 1 3 -4 23.064 46.128 0.254 10.48 4 30.1 3.4 88 4 1 -3 23.198 46.396 0.256 10.35 4 15.4 0.9 89 1 0 5 23.258 46.516 0.256 10.29 2 8.8 0.1 90 0 1 5 23.377 46.753 0.258 10.17 4 71.1 18.5 91 3 1 -4 23.419 46.837 0.258 10.13 4 53.0 10.3 92 1 0 -5 23.529 47.057 0.259 10.02 2 11.9 0.3 93 2 5 1 23.941 47.882 0.263 9.63 4 22.3 1.7 94 1 5 2 24.033 48.067 0.264 9.55 4 16.5 0.9 95 2 5 -1 24.047 48.094 0.265 9.54 4 7.8 0.2 96 1 5 -2 24.139 48.279 0.265 9.45 4 38.9 5.2 97 5 2 1 24.211 48.421 0.266 9.39 4 85.2 24.6 98 5 1 2 24.22 48.441 0.266 9.38 4 69.5 16.4 99 5 2 -1 24.474 48.947 0.269 9.16 4 49.6 8.1 100 5 1 -2 24.744 49.487 0.272 8.94 4 40.6 5.3 101 2 1 5 24.857 49.714 0.273 8.84 4 22.7 1.6 102 1 2 5 24.938 49.875 0.274 8.78 4 67.9 14.6 103 4 4 0 24.974 49.948 0.274 8.75 4 138.1 60.2 104 1 2 -5 25.195 50.389 0.276 8.58 4 103.6 33.2 105 4 0 4 25.298 50.596 0.277 8.5 2 107.8 17.8 106 2 1 -5 25.371 50.741 0.278 8.44 4 85.9 22.5 107 0 4 4 25.45 50.899 0.279 8.38 4 65.5 13.0 108 3 5 0 25.672 51.343 0.281 8.22 4 99.8 29.5 109 3 4 3 25.851 51.701 0.283 8.09 4 2.4 0.0 110 4 3 3 25.886 51.771 0.283 8.06 4 74.5 16.1 111 5 3 0 25.925 51.849 0.284 8.04 4 35.0 3.5 112 0 5 3 25.935 51.869 0.284 8.03 4 147.0 62.6 113 5 0 3 25.952 51.904 0.284 8.02 2 6.0 0.1 114 3 3 4 26.089 52.178 0.285 7.92 4 117.9 39.7 115 4 0 -4 26.106 52.212 0.286 7.91 2 111.2 17.6 116 3 4 -3 26.3 52.601 0.288 7.78 4 38.7 4.2 117 0 6 0 26.324 52.649 0.288 7.76 2 38.1 2.0 118 3 0 5 26.415 52.83 0.289 7.7 2 31.8 1.4 119 4 3 -3 26.484 52.967 0.289 7.66 4 84.1 19.5 120 4 4 2 26.552 53.104 0.29 7.61 4 106.0 30.9 121 0 3 5 26.646 53.292 0.291 7.55 4 16.4 0.7 122 3 3 -4 26.684 53.368 0.291 7.53 4 120.1 39.1 123 5 0 -3 26.697 53.394 0.292 7.52 2 16.0 0.3 124 6 0 0 26.882 53.763 0.293 7.4 2 189.9 48.1 125 4 2 4 26.883 53.766 0.294 7.4 4 71.4 13.6 126 2 4 4 26.894 53.789 0.294 7.39 4 29.2 2.3 127 4 4 -2 26.945 53.89 0.294 7.36 4 33.2 2.9 128 1 6 1 27.138 54.277 0.296 7.24 4 62.1 10.1 129 3 0 -5 27.151 54.302 0.296 7.23 2 39.7 2.1 130 1 6 -1 27.187 54.374 0.297 7.21 4 80.7 16.9 131 3 5 2 27.269 54.538 0.297 7.16 4 19.1 0.9 132 2 4 -4 27.284 54.568 0.298 7.15 4 90.9 21.3 133 2 5 3 27.41 54.819 0.299 7.08 4 34.9 3.1 134 5 3 2 27.415 54.831 0.299 7.08 4 48.5 6.0 135 5 2 3 27.51 55.021 0.3 7.02 4 43.5 4.8 136 6 1 1 27.549 55.098 0.3 7.0 4 36.2 3.3 137 3 5 -2 27.559 55.118 0.3 6.99 4 48.1 5.8 138 4 2 -4 27.658 55.317 0.301 6.94 4 20.5 1.1 139 2 5 -3 27.698 55.397 0.302 6.91 4 16.8 0.7 140 6 1 -1 27.837 55.674 0.303 6.84 4 35.7 3.1 141 0 0 6 27.891 55.782 0.304 6.81 2 156.7 30.2 142 5 3 -2 27.895 55.791 0.304 6.8 4 13.3 0.4 143 2 6 0 27.928 55.857 0.304 6.78 4 60.5 9.0 144 3 2 5 27.955 55.911 0.304 6.77 4 70.1 12.0 145 2 3 5 28.0 55.999 0.305 6.75 4 66.1 10.6 146 0 6 2 28.039 56.078 0.305 6.72 4 66.5 10.7 147 5 2 -3 28.227 56.454 0.307 6.62 4 12.9 0.4 148 6 0 2 28.29 56.581 0.308 6.59 2 12.8 0.2 149 6 2 0 28.405 56.81 0.309 6.53 4 40.4 3.8 150 2 3 -5 28.473 56.946 0.309 6.49 4 65.0 9.9 151 1 1 6 28.515 57.031 0.31 6.47 4 95.8 21.4 152 3 2 -5 28.664 57.329 0.311 6.4 4 54.9 7.0 153 1 1 -6 28.797 57.594 0.313 6.33 4 6.7 0.1 154 4 5 1 28.803 57.605 0.313 6.33 4 41.5 3.9 155 6 0 -2 28.854 57.708 0.313 6.3 2 11.5 0.2 156 5 4 1 28.911 57.822 0.314 6.27 4 45.0 4.6 157 4 5 -1 28.989 57.979 0.315 6.24 4 37.0 3.1 158 5 4 -1 29.144 58.288 0.316 6.16 4 51.9 6.0 159 2 0 6 29.16 58.32 0.316 6.15 2 18.0 0.4 160 5 1 4 29.186 58.372 0.317 6.14 4 31.2 2.2 161 1 5 4 29.208 58.416 0.317 6.13 4 10.9 0.3 162 0 2 6 29.38 58.759 0.318 6.05 4 28.6 1.8 163 1 5 -4 29.393 58.786 0.319 6.04 4 61.0 8.1 164 4 1 5 29.428 58.855 0.319 6.03 4 54.2 6.4 165 2 6 2 29.488 58.976 0.32 6.0 4 18.9 0.8 166 1 4 5 29.556 59.112 0.32 5.97 4 36.8 2.9 167 2 6 -2 29.672 59.344 0.321 5.92 4 30.0 1.9 168 2 0 -6 29.713 59.427 0.322 5.9 2 31.4 1.0 169 6 2 2 29.766 59.532 0.322 5.88 4 37.8 3.0 170 1 4 -5 29.786 59.571 0.322 5.87 4 53.1 6.0 171 5 1 -4 30.105 60.209 0.326 5.73 4 15.7 0.5 172 3 6 1 30.185 60.371 0.326 5.69 4 94.5 18.4 173 6 2 -2 30.312 60.625 0.328 5.64 4 25.1 1.3 174 3 6 -1 30.321 60.643 0.328 5.64 4 132.2 35.6 175 4 1 -5 30.341 60.683 0.328 5.63 4 42.6 3.7 176 1 6 3 30.396 60.791 0.328 5.61 4 84.1 14.3 177 6 3 1 30.501 61.002 0.329 5.56 4 39.5 3.1 178 1 6 -3 30.531 61.062 0.33 5.55 4 22.4 1.0 179 6 1 3 30.553 61.106 0.33 5.54 4 99.9 19.9 180 2 2 6 30.609 61.218 0.331 5.52 4 34.2 2.3 181 6 3 -1 30.771 61.542 0.332 5.46 4 63.6 8.0 182 2 2 -6 31.147 62.294 0.336 5.31 4 11.3 0.2 183 3 1 6 31.255 62.51 0.337 5.27 4 57.4 6.3 184 4 4 4 31.307 62.614 0.337 5.25 4 43.1 3.5 185 6 1 -3 31.359 62.717 0.338 5.23 4 114.1 24.6 186 1 3 6 31.41 62.82 0.338 5.21 4 128.4 31.0 187 1 7 0 31.522 63.044 0.339 5.17 4 47.1 4.1 188 0 7 1 31.547 63.095 0.34 5.16 4 38.7 2.8 189 1 3 -6 31.676 63.351 0.341 5.12 4 14.8 0.4 190 4 5 3 31.82 63.64 0.342 5.07 4 27.8 1.4 191 5 5 0 31.854 63.709 0.343 5.06 4 38.1 2.6 192 5 4 3 31.879 63.757 0.343 5.05 4 19.0 0.7 193 3 5 4 31.999 63.998 0.344 5.01 4 50.8 4.7 194 4 4 -4 32.014 64.028 0.344 5.0 4 27.1 1.3 195 5 3 4 32.044 64.088 0.344 4.99 4 15.6 0.4 196 3 1 -6 32.05 64.101 0.344 4.99 4 66.8 8.0 197 7 0 1 32.071 64.142 0.345 4.98 2 21.0 0.4 198 7 1 0 32.185 64.371 0.346 4.94 4 82.6 12.2 199 4 3 5 32.273 64.545 0.347 4.91 4 105.3 19.7 200 3 4 5 32.286 64.572 0.347 4.91 4 5.2 0.0 201 5 0 5 32.287 64.574 0.347 4.91 2 39.8 1.4 202 4 5 -3 32.347 64.693 0.347 4.89 4 77.5 10.6 203 7 0 -1 32.377 64.755 0.348 4.88 2 24.7 0.5 204 4 6 0 32.425 64.851 0.348 4.86 4 21.3 0.8 205 0 5 5 32.49 64.98 0.349 4.84 4 27.2 1.3 206 3 5 -4 32.524 65.047 0.349 4.83 4 54.4 5.2 207 5 4 -3 32.535 65.07 0.349 4.83 4 49.1 4.2 208 6 4 0 32.699 65.397 0.351 4.78 4 160.4 44.3 209 6 0 4 32.799 65.598 0.352 4.75 2 10.8 0.1 210 0 6 4 32.829 65.658 0.352 4.74 4 26.3 1.2 211 5 3 -4 32.915 65.831 0.353 4.71 4 48.1 3.9 212 3 4 -5 32.938 65.876 0.353 4.7 4 40.9 2.8 213 2 7 1 32.946 65.892 0.353 4.7 4 55.5 5.2 214 1 7 2 33.021 66.042 0.354 4.68 4 35.5 2.1 215 2 7 -1 33.032 66.065 0.354 4.67 4 9.9 0.2 216 1 7 -2 33.107 66.215 0.355 4.65 4 69.2 8.0 217 4 3 -5 33.141 66.282 0.355 4.64 4 27.3 1.2 218 3 6 3 33.171 66.343 0.355 4.63 4 75.1 9.4 219 5 5 2 33.174 66.347 0.355 4.63 4 22.5 0.8 220 1 0 7 33.281 66.562 0.356 4.6 2 28.4 0.7 221 4 0 6 33.3 66.6 0.356 4.6 2 75.0 4.7 222 6 3 3 33.343 66.685 0.357 4.58 4 52.5 4.5 223 5 0 -5 33.37 66.74 0.357 4.57 2 18.9 0.3 224 7 1 2 33.412 66.823 0.357 4.56 4 31.5 1.6 225 0 1 7 33.418 66.836 0.357 4.56 4 9.4 0.1 226 7 2 1 33.447 66.894 0.358 4.55 4 42.2 2.9 227 3 6 -3 33.558 67.116 0.359 4.52 4 73.1 8.7 228 1 0 -7 33.581 67.163 0.359 4.51 2 13.3 0.1 229 0 4 6 33.599 67.199 0.359 4.51 4 175.8 50.3 230 5 5 -2 33.603 67.206 0.359 4.51 4 31.3 1.6 231 5 2 5 33.658 67.316 0.36 4.49 4 24.9 1.0 232 2 5 5 33.697 67.393 0.36 4.48 4 42.6 2.9 233 7 2 -1 33.747 67.493 0.361 4.47 4 28.6 1.3 234 4 6 2 33.776 67.551 0.361 4.46 4 24.7 1.0 235 6 0 -4 33.831 67.662 0.361 4.44 2 2.5 0.0 236 6 4 2 33.958 67.916 0.363 4.41 4 16.7 0.4 237 7 1 -2 34.01 68.021 0.363 4.4 4 26.5 1.1 238 3 3 6 34.013 68.025 0.363 4.4 4 87.2 12.0 239 2 6 4 34.072 68.145 0.364 4.38 4 10.3 0.2 240 6 3 -3 34.112 68.224 0.364 4.37 4 93.0 13.6 241 4 6 -2 34.116 68.233 0.364 4.37 4 35.9 2.0 242 2 5 -5 34.123 68.246 0.364 4.37 4 6.5 0.1 243 6 2 4 34.159 68.319 0.364 4.36 4 33.4 1.8 244 4 0 -6 34.324 68.649 0.366 4.31 2 91.7 6.5 245 3 7 0 34.375 68.749 0.366 4.3 4 60.0 5.6 246 2 6 -4 34.412 68.824 0.367 4.29 4 53.8 4.5 247 6 4 -2 34.468 68.935 0.367 4.28 4 19.7 0.6 248 2 1 7 34.524 69.048 0.368 4.26 4 38.8 2.3 249 0 7 3 34.595 69.191 0.369 4.24 4 62.6 6.0 250 1 2 7 34.632 69.264 0.369 4.23 4 29.0 1.3 251 4 2 6 34.651 69.301 0.369 4.23 4 31.1 1.5 252 5 2 -5 34.72 69.439 0.37 4.21 4 54.1 4.5 253 2 4 6 34.745 69.49 0.37 4.21 4 27.6 1.2 254 3 3 -6 34.775 69.55 0.37 4.2 4 79.1 9.5 255 7 0 3 34.801 69.603 0.37 4.19 2 60.2 2.7 256 7 3 0 34.905 69.809 0.371 4.17 4 151.2 34.4 257 1 2 -7 34.927 69.854 0.372 4.16 4 15.8 0.4 258 2 1 -7 35.114 70.227 0.373 4.12 4 64.8 6.2 259 6 2 -4 35.172 70.344 0.374 4.1 4 14.5 0.3 260 2 4 -6 35.249 70.498 0.375 4.09 4 85.8 10.9 261 4 2 -6 35.657 71.314 0.378 3.99 4 20.0 0.6 262 7 0 -3 35.681 71.362 0.379 3.99 2 23.7 0.4 263 3 7 2 35.73 71.461 0.379 3.98 4 71.8 7.4 264 3 0 7 35.773 71.546 0.379 3.97 2 20.4 0.3 265 5 6 1 35.848 71.697 0.38 3.95 4 58.0 4.8 266 2 7 3 35.851 71.702 0.38 3.95 4 72.5 7.5 267 6 5 1 35.971 71.942 0.381 3.93 4 6.7 0.1 268 3 7 -2 35.98 71.96 0.381 3.92 4 89.8 11.4 269 5 6 -1 36.056 72.112 0.382 3.91 4 28.5 1.1 270 7 3 2 36.086 72.172 0.382 3.9 4 55.3 4.3 271 0 3 7 36.092 72.184 0.382 3.9 4 89.1 11.2 272 2 7 -3 36.1 72.2 0.382 3.9 4 50.1 3.5 273 7 2 3 36.126 72.252 0.383 3.89 4 141.2 28.0 274 6 5 -1 36.22 72.44 0.384 3.87 4 62.8 5.5 275 0 8 0 36.247 72.495 0.384 3.87 2 162.6 18.4 276 6 1 5 36.363 72.726 0.385 3.84 4 55.6 4.3 277 1 6 5 36.426 72.851 0.385 3.83 4 21.1 0.6 278 5 1 6 36.627 73.253 0.387 3.79 4 43.9 2.6 279 1 6 -5 36.632 73.264 0.387 3.79 4 58.2 4.6 280 3 0 -7 36.643 73.285 0.387 3.79 2 14.5 0.1 281 7 3 -2 36.665 73.329 0.388 3.78 4 80.0 8.7 282 1 5 6 36.811 73.621 0.389 3.76 4 98.5 13.2 283 1 8 1 36.931 73.861 0.39 3.73 4 63.0 5.3 284 1 8 -1 36.972 73.943 0.39 3.73 4 49.3 3.3 285 7 2 -3 36.992 73.985 0.391 3.72 4 79.4 8.5 286 1 5 -6 37.057 74.114 0.391 3.71 4 45.3 2.8 287 4 7 1 37.062 74.125 0.391 3.71 4 5.2 0.0 288 8 0 0 37.075 74.151 0.391 3.71 2 13.9 0.1 289 3 2 7 37.083 74.166 0.391 3.7 4 68.5 6.3 290 2 3 7 37.162 74.325 0.392 3.69 4 24.3 0.8 291 4 7 -1 37.226 74.453 0.393 3.68 4 43.4 2.5 292 5 5 4 37.4 74.8 0.394 3.65 4 50.1 3.3 293 1 7 4 37.419 74.838 0.394 3.64 4 22.6 0.7 294 7 4 1 37.425 74.85 0.394 3.64 4 36.1 1.7 295 7 1 4 37.544 75.089 0.396 3.62 4 22.3 0.6 296 1 7 -4 37.582 75.165 0.396 3.61 4 14.9 0.3 297 6 1 -5 37.595 75.191 0.396 3.61 4 31.3 1.3 298 8 1 1 37.597 75.194 0.396 3.61 4 20.3 0.5 299 2 8 0 37.602 75.205 0.396 3.61 4 104.7 14.3 300 4 5 5 37.613 75.226 0.396 3.61 4 35.9 1.7 301 5 4 5 37.627 75.253 0.396 3.61 4 29.8 1.2 302 0 8 2 37.697 75.394 0.397 3.59 4 29.6 1.1 303 7 4 -1 37.711 75.422 0.397 3.59 4 11.2 0.2 304 2 3 -7 37.735 75.47 0.397 3.59 4 71.3 6.6 305 5 1 -6 37.856 75.712 0.398 3.57 4 62.1 5.0 306 8 1 -1 37.923 75.847 0.399 3.56 4 26.8 0.9 307 3 2 -7 37.941 75.883 0.399 3.55 4 132.3 22.4 308 4 6 4 38.013 76.026 0.4 3.54 4 48.3 3.0 309 6 4 4 38.106 76.211 0.401 3.53 4 16.1 0.3 310 8 0 2 38.189 76.379 0.401 3.51 2 54.2 1.9 311 5 5 -4 38.215 76.43 0.402 3.51 4 15.9 0.3 312 4 1 7 38.324 76.648 0.403 3.49 4 126.0 20.0 313 8 2 0 38.369 76.738 0.403 3.48 4 53.8 3.6 314 4 5 -5 38.427 76.854 0.403 3.48 4 36.1 1.6 315 5 6 3 38.538 77.075 0.404 3.46 4 46.7 2.7 316 1 4 7 38.559 77.117 0.405 3.46 4 28.5 1.0 317 4 4 6 38.576 77.153 0.405 3.45 4 68.7 5.9 318 0 0 8 38.589 77.177 0.405 3.45 2 34.7 0.8 319 6 5 3 38.617 77.233 0.405 3.45 4 105.7 13.9 320 5 4 -5 38.643 77.285 0.405 3.44 4 9.8 0.1 321 4 6 -4 38.662 77.324 0.406 3.44 4 23.0 0.7 322 7 1 -4 38.682 77.365 0.406 3.44 4 69.5 6.0 323 8 0 -2 38.838 77.675 0.407 3.41 2 46.6 1.3 324 1 4 -7 38.842 77.683 0.407 3.41 4 35.9 1.6 325 3 6 5 38.913 77.826 0.408 3.4 4 72.6 6.5 326 6 3 5 38.952 77.905 0.408 3.4 4 57.0 4.0 327 2 8 2 38.954 77.908 0.408 3.4 4 16.4 0.3 328 6 4 -4 39.077 78.155 0.409 3.38 4 8.1 0.1 329 1 1 8 39.08 78.161 0.409 3.38 4 36.3 1.6 330 2 8 -2 39.115 78.23 0.41 3.37 4 40.9 2.0 331 5 6 -3 39.144 78.287 0.41 3.37 4 1.7 0.0 332 5 3 6 39.21 78.42 0.41 3.36 4 7.6 0.1 333 3 5 6 39.249 78.498 0.411 3.35 4 98.2 11.7 334 6 6 0 39.295 78.59 0.411 3.35 4 47.7 2.8 335 6 5 -3 39.343 78.686 0.412 3.34 4 153.1 28.3 336 1 1 -8 39.403 78.805 0.412 3.33 4 46.5 2.6 337 4 1 -7 39.455 78.91 0.412 3.33 4 25.7 0.8 338 8 2 2 39.471 78.942 0.413 3.32 4 35.7 1.5 339 3 6 -5 39.517 79.035 0.413 3.32 4 70.3 5.9 340 4 4 -6 39.545 79.089 0.413 3.31 4 44.9 2.4 341 3 8 1 39.568 79.136 0.413 3.31 4 24.2 0.7 342 2 0 8 39.596 79.191 0.414 3.31 2 27.0 0.4 343 3 8 -1 39.688 79.377 0.415 3.29 4 17.9 0.4 344 1 8 3 39.754 79.509 0.415 3.29 4 73.7 6.4 345 4 7 3 39.763 79.525 0.415 3.29 4 31.6 1.2 346 5 7 0 39.794 79.588 0.415 3.28 4 20.9 0.5 347 6 0 6 39.866 79.731 0.416 3.27 2 78.7 3.7 348 0 2 8 39.866 79.733 0.416 3.27 4 31.1 1.1 349 1 8 -3 39.875 79.749 0.416 3.27 4 21.9 0.6 350 3 7 4 39.926 79.851 0.417 3.26 4 58.6 4.0 351 3 5 -6 39.973 79.945 0.417 3.26 4 66.0 5.1 352 7 4 3 39.998 79.995 0.417 3.26 4 50.7 3.0 353 7 5 0 40.096 80.192 0.418 3.24 4 60.5 4.3 354 7 3 4 40.108 80.217 0.418 3.24 4 26.0 0.8 355 8 2 -2 40.113 80.226 0.418 3.24 4 49.2 2.8 356 8 1 3 40.126 80.253 0.418 3.24 4 45.4 2.4 357 0 6 6 40.134 80.268 0.418 3.24 4 20.5 0.5 358 6 3 -5 40.158 80.317 0.419 3.24 4 40.5 1.9 359 8 3 1 40.16 80.32 0.419 3.23 4 8.5 0.1 360 2 0 -8 40.237 80.475 0.419 3.23 2 5.2 0.0 361 4 7 -3 40.244 80.487 0.419 3.22 4 54.1 3.4 362 7 0 5 40.29 80.581 0.42 3.22 2 5.5 0.0 363 0 7 5 40.375 80.75 0.42 3.21 4 27.2 0.9 364 3 7 -4 40.406 80.812 0.421 3.21 4 70.6 5.8 365 5 3 -6 40.414 80.828 0.421 3.2 4 77.4 6.9 366 6 6 2 40.47 80.941 0.421 3.2 4 66.7 5.1 367 8 3 -1 40.48 80.961 0.421 3.2 4 16.9 0.3 368 7 4 -3 40.837 81.675 0.424 3.16 4 39.0 1.7 369 5 0 7 40.847 81.694 0.425 3.15 2 5.9 0.0 370 2 2 8 40.865 81.731 0.425 3.15 4 16.1 0.3 371 4 3 7 40.874 81.747 0.425 3.15 4 48.1 2.6 372 3 4 7 40.926 81.851 0.425 3.15 4 6.3 0.0 373 6 6 -2 40.949 81.899 0.425 3.14 4 42.1 2.0 374 5 7 2 41.005 82.011 0.426 3.14 4 74.3 6.2 375 8 1 -3 41.085 82.17 0.427 3.13 4 44.6 2.2 376 6 2 6 41.133 82.266 0.427 3.12 4 30.5 1.0 377 2 6 6 41.211 82.422 0.428 3.12 4 15.6 0.3 378 7 5 2 41.226 82.452 0.428 3.11 4 34.8 1.4 379 7 3 -4 41.226 82.453 0.428 3.11 4 6.5 0.0 380 0 5 7 41.231 82.463 0.428 3.11 4 23.0 0.6 381 6 0 -6 41.304 82.608 0.428 3.11 2 130.2 9.5 382 3 1 8 41.4 82.8 0.429 3.1 4 25.8 0.7 383 5 7 -2 41.404 82.807 0.429 3.1 4 40.0 1.8 384 2 7 5 41.49 82.981 0.43 3.09 4 8.8 0.1 385 2 2 -8 41.503 83.005 0.43 3.09 4 25.7 0.7 386 7 2 5 41.555 83.11 0.431 3.08 4 41.0 1.9 387 4 8 0 41.581 83.161 0.431 3.08 4 73.4 6.0 388 1 3 8 41.618 83.237 0.431 3.07 4 17.9 0.4 389 7 0 -5 41.686 83.372 0.432 3.07 2 1.6 0.0 390 2 6 -6 41.688 83.377 0.432 3.07 4 27.3 0.8 391 3 4 -7 41.761 83.523 0.432 3.06 4 15.0 0.2 392 7 5 -2 41.783 83.565 0.433 3.06 4 23.2 0.6 393 2 7 -5 41.888 83.776 0.433 3.05 4 83.6 7.7 394 1 3 -8 41.936 83.873 0.434 3.04 4 31.4 1.1 395 0 8 4 41.95 83.899 0.434 3.04 4 26.9 0.8 396 4 3 -7 41.988 83.975 0.434 3.04 4 35.9 1.4 397 1 9 0 42.024 84.047 0.435 3.04 4 12.2 0.2 398 0 9 1 42.047 84.093 0.435 3.03 4 5.1 0.0 399 5 2 7 42.108 84.217 0.435 3.03 4 13.7 0.2 400 8 0 4 42.112 84.224 0.435 3.03 2 30.5 0.5 401 8 4 0 42.179 84.358 0.436 3.02 4 33.1 1.2 402 5 0 -7 42.239 84.477 0.436 3.02 2 21.5 0.3 403 2 5 7 42.263 84.527 0.437 3.01 4 14.3 0.2 404 3 8 3 42.264 84.528 0.437 3.01 4 34.8 1.3 405 3 1 -8 42.353 84.707 0.437 3.01 4 23.2 0.6 406 6 2 -6 42.563 85.126 0.439 2.99 4 35.0 1.3 407 3 8 -3 42.621 85.241 0.44 2.98 4 14.8 0.2 408 8 3 3 42.651 85.302 0.44 2.98 4 19.5 0.4 409 2 5 -7 42.818 85.636 0.441 2.97 4 89.1 8.5 410 4 8 2 42.822 85.644 0.441 2.97 4 52.6 3.0 411 9 0 1 42.876 85.752 0.442 2.96 2 29.0 0.4 412 7 2 -5 42.943 85.887 0.442 2.96 4 31.7 1.1 413 9 1 0 43.019 86.037 0.443 2.95 4 38.1 1.5 414 2 8 4 43.098 86.195 0.444 2.95 4 56.9 3.4 415 4 8 -2 43.139 86.277 0.444 2.94 4 6.0 0.0 416 4 0 8 43.215 86.43 0.444 2.94 2 43.0 1.0 417 9 0 -1 43.232 86.464 0.445 2.94 2 9.0 0.0 418 8 4 2 43.26 86.52 0.445 2.93 4 37.1 1.5 419 2 9 1 43.313 86.626 0.445 2.93 4 31.9 1.1 420 8 2 4 43.368 86.736 0.446 2.93 4 38.7 1.6 421 8 0 -4 43.379 86.758 0.446 2.93 2 2.9 0.0 422 1 9 2 43.382 86.763 0.446 2.93 4 26.7 0.8 423 2 9 -1 43.392 86.784 0.446 2.93 4 25.9 0.7 424 2 8 -4 43.414 86.828 0.446 2.92 4 2.5 0.0 425 1 9 -2 43.461 86.922 0.446 2.92 4 24.0 0.6 426 5 2 -7 43.494 86.988 0.447 2.92 4 21.0 0.5 427 8 3 -3 43.6 87.201 0.448 2.91 4 32.9 1.1 428 6 7 1 43.631 87.262 0.448 2.91 4 27.7 0.8 429 0 4 8 43.649 87.298 0.448 2.91 4 45.6 2.2 430 7 6 1 43.772 87.545 0.449 2.9 4 5.9 0.0 431 6 7 -1 43.868 87.736 0.45 2.89 4 36.5 1.4 432 8 4 -2 43.892 87.785 0.45 2.89 4 23.0 0.6 433 3 3 8 43.913 87.826 0.45 2.89 4 13.2 0.2 434 5 6 5 43.967 87.934 0.451 2.89 4 8.5 0.1 435 6 5 5 44.005 88.009 0.451 2.88 4 68.3 4.9 436 7 6 -1 44.049 88.098 0.451 2.88 4 50.1 2.6 437 9 1 2 44.058 88.116 0.451 2.88 4 12.7 0.2 438 9 2 1 44.13 88.26 0.452 2.88 4 58.8 3.6 439 5 5 6 44.257 88.514 0.453 2.87 4 15.1 0.2 440 7 1 6 44.317 88.635 0.453 2.87 4 110.0 12.5 441 6 6 4 44.432 88.863 0.454 2.86 4 24.8 0.6 442 1 7 6 44.433 88.866 0.454 2.86 4 66.3 4.5 443 4 2 8 44.468 88.936 0.455 2.86 4 19.2 0.4 444 4 0 -8 44.48 88.959 0.455 2.86 2 2.1 0.0 445 9 2 -1 44.485 88.97 0.455 2.86 4 69.3 4.9 446 6 1 7 44.615 89.23 0.456 2.85 4 43.8 2.0 447 3 9 0 44.632 89.264 0.456 2.85 4 59.7 3.7 448 8 2 -4 44.632 89.264 0.456 2.85 4 33.5 1.2 449 2 4 8 44.635 89.271 0.456 2.85 4 18.3 0.3 450 1 7 -6 44.67 89.34 0.456 2.85 4 18.5 0.4 451 1 0 9 44.71 89.421 0.457 2.84 2 8.2 0.0 452 5 8 1 44.767 89.534 0.457 2.84 4 22.8 0.5 453 9 1 -2 44.769 89.537 0.457 2.84 4 13.7 0.2 454 0 9 3 44.838 89.676 0.458 2.84 4 96.7 9.6 455 3 3 -8 44.861 89.722 0.458 2.84 4 34.0 1.2 456 1 6 7 44.872 89.745 0.458 2.83 4 50.2 2.6 457 0 1 9 44.876 89.751 0.458 2.83 4 32.2 1.1 458 4 6 6 44.89 89.779 0.458 2.83 4 25.7 0.7 459 6 4 6 44.901 89.801 0.458 2.83 4 60.4 3.7 460 5 6 -5 44.954 89.908 0.459 2.83 4 32.1 1.1 461 5 8 -1 44.964 89.928 0.459 2.83 4 33.5 1.1 X-ray diffraction powder data (I)...X-Ray wave length = 1.54056 (angs.): No H K L Theta 2*Theta d I int I int.n. I p.h.n. H(Si) ( degree ) (angstrem) *100 *100 1 1 1 0 6.059 12.118 7.29759 401.1 86.5 87.8 5.6 2 1 0 1 6.133 12.265 7.21024 13.2 2.8 2.9 5.6 3 0 1 1 6.167 12.334 7.17008 71.6 15.4 15.7 5.6 4 1 0 -1 6.316 12.632 7.00198 5.1 1.1 1.1 5.6 5 0 2 0 8.501 17.001 5.211 20.1 4.3 4.4 5.6 6 2 0 0 8.668 17.337 5.1108 266.0 57.4 58.0 5.6 7 0 0 2 8.971 17.942 4.93988 209.2 45.1 45.6 5.6 8 1 2 1 10.509 21.017 4.22345 413.3 89.2 90.0 5.6 9 2 1 1 10.557 21.114 4.20426 30.0 6.5 6.5 5.6 10 1 2 -1 10.618 21.236 4.18037 223.9 48.3 48.7 5.6 11 2 1 -1 10.774 21.548 4.12053 59.7 12.9 13.0 5.6 12 1 1 -2 10.96 21.919 4.05159 29.9 6.5 6.5 5.6 13 2 2 0 12.187 24.374 3.64879 33.3 7.2 7.2 5.6 14 0 2 2 12.407 24.815 3.58504 32.9 7.1 7.1 5.6 15 1 3 0 13.543 27.087 3.28922 118.4 25.5 25.7 5.6 16 0 3 1 13.594 27.187 3.2773 9.2 2.0 2.0 5.6 17 3 0 1 13.708 27.416 3.25054 7.3 1.6 1.6 5.6 18 3 1 0 13.76 27.519 3.23853 200.2 43.2 43.4 5.6 19 0 1 3 14.199 28.399 3.14021 407.5 87.9 88.2 5.6 20 1 0 -3 14.349 28.698 3.10809 7.7 1.7 1.7 5.6 21 2 2 2 15.059 30.118 2.96477 41.9 9.0 9.1 5.6 22 2 3 1 16.139 32.278 2.77108 29.8 6.4 6.4 5.6 23 3 2 1 16.218 32.436 2.75796 172.0 37.1 37.1 5.6 24 1 3 2 16.267 32.535 2.74982 8.6 1.9 1.9 5.6 25 3 1 2 16.305 32.61 2.74367 70.1 15.1 15.1 5.6 26 3 2 -1 16.438 32.875 2.72213 463.6 100.0 100.0 5.6 27 2 1 3 16.516 33.032 2.70953 25.1 5.4 5.4 5.6 28 1 2 3 16.557 33.113 2.7031 280.3 60.5 60.5 5.6 29 3 1 -2 16.739 33.478 2.67443 112.5 24.3 24.2 5.7 30 1 2 -3 16.772 33.544 2.66934 34.9 7.5 7.5 5.7 31 2 1 -3 16.946 33.891 2.64278 11.4 2.5 2.5 5.7 32 0 4 0 17.196 34.391 2.6055 193.5 41.7 41.7 5.7 33 0 0 4 18.171 36.343 2.46994 35.6 7.7 7.6 5.7 34 1 4 1 18.321 36.643 2.45042 9.6 2.1 2.1 5.7 35 4 1 1 18.533 37.065 2.42346 53.8 11.6 11.6 5.7 36 0 3 3 18.801 37.603 2.39003 27.6 6.0 5.9 5.7 37 1 1 4 19.095 38.191 2.35458 20.5 4.4 4.4 5.7 38 1 1 -4 19.349 38.699 2.32484 35.8 7.7 7.7 5.7 39 0 4 2 19.526 39.052 2.30458 36.6 7.9 7.8 5.7 40 4 2 0 19.617 39.233 2.29438 19.8 4.3 4.2 5.7 41 2 0 4 20.021 40.043 2.24985 29.0 6.3 6.2 5.7 42 4 0 -2 20.085 40.17 2.24302 25.2 5.4 5.4 5.7 43 0 2 4 20.189 40.378 2.23192 10.1 2.2 2.2 5.7 44 3 3 2 20.489 40.978 2.20062 9.3 2.0 2.0 5.7 45 2 3 3 20.663 41.326 2.18289 13.1 2.8 2.8 5.7 46 3 3 -2 20.848 41.695 2.16441 15.7 3.4 3.4 5.7 47 2 4 2 21.393 42.786 2.11172 52.7 11.4 11.3 5.7 48 2 4 -2 21.624 43.249 2.09019 48.8 10.5 10.4 5.7 49 1 5 0 22.157 44.315 2.04237 5.1 1.1 1.1 5.7 50 3 4 1 22.265 44.53 2.03301 14.5 3.1 3.1 5.7 51 4 3 1 22.36 44.72 2.02478 33.1 7.1 7.1 5.7 52 1 4 3 22.525 45.05 2.01073 7.6 1.6 1.6 5.7 53 5 1 0 22.58 45.16 2.00609 25.1 5.4 5.3 5.7 54 1 4 -3 22.692 45.383 1.99672 23.5 5.1 5.0 5.7 55 5 0 -1 22.768 45.536 1.99037 14.5 3.1 3.1 5.7 56 0 1 5 23.377 46.753 1.94137 18.5 4.0 3.9 5.7 57 3 1 -4 23.419 46.837 1.93807 10.3 2.2 2.2 5.7 58 1 5 -2 24.139 48.279 1.88352 5.2 1.1 1.1 5.7 59 5 2 1 24.211 48.421 1.8783 40.9 8.8 8.7 5.7 60 5 2 -1 24.474 48.947 1.85935 8.1 1.8 1.7 5.7 61 5 1 -2 24.744 49.487 1.84031 5.3 1.1 1.1 5.7 62 1 2 5 24.938 49.875 1.82691 14.6 3.1 3.1 5.7 63 4 4 0 24.974 49.948 1.8244 60.2 13.0 12.8 5.7 64 1 2 -5 25.195 50.389 1.80946 33.2 7.2 7.0 5.8 65 4 0 4 25.298 50.596 1.80256 17.8 3.8 3.8 5.8 66 2 1 -5 25.371 50.741 1.79774 22.5 4.8 4.8 5.8 67 0 4 4 25.45 50.899 1.79252 13.0 2.8 2.7 5.8 68 3 5 0 25.672 51.343 1.77806 29.5 6.4 6.2 5.8 69 4 3 3 25.886 51.771 1.76437 16.1 3.5 3.4 5.8 70 0 5 3 25.935 51.869 1.76126 66.2 14.3 14.0 5.8 71 3 3 4 26.089 52.178 1.75156 57.4 12.4 12.1 5.8 72 3 4 -3 26.3 52.601 1.73847 6.2 1.3 1.3 5.8 73 4 3 -3 26.484 52.967 1.7273 19.5 4.2 4.1 5.8 74 4 4 2 26.552 53.104 1.72317 30.9 6.7 6.5 5.8 75 3 3 -4 26.684 53.368 1.71528 39.5 8.5 8.3 5.8 76 6 0 0 26.882 53.763 1.7036 64.0 13.8 13.5 5.8 77 1 6 1 27.138 54.277 1.68869 12.1 2.6 2.6 5.8 78 1 6 -1 27.187 54.374 1.6859 16.9 3.7 3.6 5.8 79 2 4 -4 27.284 54.568 1.68037 21.3 4.6 4.5 5.8 80 5 3 2 27.415 54.831 1.67293 9.1 2.0 1.9 5.8 81 5 2 3 27.51 55.021 1.6676 4.8 1.0 1.0 5.8 82 3 5 -2 27.559 55.118 1.66489 9.2 2.0 1.9 5.8 83 0 0 6 27.891 55.782 1.64663 30.6 6.6 6.4 5.8 84 3 2 5 27.955 55.911 1.64315 21.0 4.5 4.4 5.8 85 2 3 5 28.0 55.999 1.64076 10.6 2.3 2.2 5.8 86 0 6 2 28.039 56.078 1.63865 10.7 2.3 2.3 5.8 87 2 3 -5 28.473 56.946 1.6157 9.9 2.1 2.1 5.8 88 1 1 6 28.515 57.031 1.61351 21.4 4.6 4.5 5.8 89 3 2 -5 28.664 57.329 1.60582 7.0 1.5 1.5 5.8 90 5 4 -1 29.144 58.288 1.58167 6.3 1.4 1.3 5.8 91 1 5 -4 29.393 58.786 1.56946 9.9 2.1 2.1 5.8 92 4 1 5 29.428 58.855 1.56776 6.4 1.4 1.3 5.8 93 1 4 -5 29.786 59.571 1.55062 9.0 1.9 1.9 5.8 94 3 6 1 30.185 60.371 1.53199 18.4 4.0 3.8 5.8 95 4 1 -5 30.341 60.683 1.52485 40.5 8.7 8.5 5.8 96 1 6 3 30.396 60.791 1.52239 14.3 3.1 3.0 5.8 97 6 1 3 30.553 61.106 1.51529 21.0 4.5 4.4 5.8 98 6 3 -1 30.771 61.542 1.5056 8.0 1.7 1.7 5.8 99 3 1 6 31.255 62.51 1.4846 6.3 1.4 1.3 5.8 100 6 1 -3 31.359 62.717 1.48019 24.6 5.3 5.1 5.8 101 1 3 6 31.41 62.82 1.47802 31.0 6.7 6.5 5.9 102 1 7 0 31.522 63.044 1.47331 6.9 1.5 1.4 5.9 103 3 5 4 31.999 63.998 1.45362 6.0 1.3 1.2 5.9 104 3 1 -6 32.05 64.101 1.45154 8.4 1.8 1.7 5.9 105 7 1 0 32.185 64.371 1.4461 12.2 2.6 2.5 5.9 106 4 3 5 32.273 64.545 1.44261 21.1 4.6 4.4 5.9 107 4 5 -3 32.347 64.693 1.43967 10.6 2.3 2.2 5.9 108 3 5 -4 32.524 65.047 1.43269 9.4 2.0 1.9 5.9 109 6 4 0 32.699 65.397 1.42586 44.3 9.6 9.2 5.9 110 5 3 -4 32.915 65.831 1.41752 6.8 1.5 1.4 5.9 111 2 7 1 32.946 65.892 1.41635 5.2 1.1 1.1 5.9 112 1 7 -2 33.107 66.215 1.41022 8.0 1.7 1.7 5.9 113 3 6 3 33.171 66.343 1.40782 10.3 2.2 2.1 5.9 114 4 0 6 33.3 66.6 1.40301 4.7 1.0 1.0 5.9 115 6 3 3 33.343 66.685 1.40142 4.8 1.0 1.0 5.9 116 3 6 -3 33.558 67.116 1.39346 8.9 1.9 1.8 5.9 117 0 4 6 33.599 67.199 1.39195 51.9 11.2 10.7 5.9 118 3 3 6 34.013 68.025 1.37703 13.2 2.8 2.7 5.9 119 6 3 -3 34.112 68.224 1.37351 15.7 3.4 3.2 5.9 120 4 0 -6 34.324 68.649 1.36604 6.5 1.4 1.3 5.9 121 3 7 0 34.375 68.749 1.36429 5.6 1.2 1.2 5.9 122 0 7 3 34.595 69.191 1.35666 6.0 1.3 1.2 5.9 123 5 2 -5 34.72 69.439 1.35241 5.6 1.2 1.2 5.9 124 3 3 -6 34.775 69.55 1.35053 12.2 2.6 2.5 5.9 125 7 3 0 34.905 69.809 1.34615 34.8 7.5 7.2 5.9 126 2 1 -7 35.114 70.227 1.33916 6.2 1.3 1.3 5.9 127 2 4 -6 35.249 70.498 1.33467 10.9 2.3 2.2 5.9 128 3 7 2 35.73 71.461 1.31904 7.4 1.6 1.5 5.9 129 2 7 3 35.851 71.702 1.31519 12.3 2.7 2.5 5.9 130 3 7 -2 35.98 71.96 1.31112 11.4 2.5 2.3 5.9 131 0 3 7 36.092 72.184 1.3076 20.2 4.3 4.1 5.9 132 7 2 3 36.126 72.252 1.30652 28.0 6.0 5.7 5.9 133 0 8 0 36.247 72.495 1.30275 24.0 5.2 4.9 5.9 134 1 6 -5 36.632 73.264 1.29096 7.4 1.6 1.5 6.0 135 7 3 -2 36.665 73.329 1.28997 8.7 1.9 1.8 6.0 136 1 5 6 36.811 73.621 1.28558 13.2 2.8 2.7 6.0 137 1 8 1 36.931 73.861 1.28199 5.3 1.2 1.1 6.0 138 7 2 -3 36.992 73.985 1.28015 11.7 2.5 2.4 6.0 139 3 2 7 37.083 74.166 1.27747 9.2 2.0 1.9 6.0 140 5 5 4 37.4 74.8 1.26821 5.7 1.2 1.2 6.0 141 4 5 5 37.613 75.226 1.26207 18.9 4.1 3.9 6.0 142 2 3 -7 37.735 75.47 1.25861 6.6 1.4 1.3 6.0 143 5 1 -6 37.856 75.712 1.25519 5.0 1.1 1.0 6.0 144 3 2 -7 37.941 75.883 1.25278 22.4 4.8 4.6 6.0 145 4 1 7 38.324 76.648 1.24218 20.0 4.3 4.1 6.0 146 4 4 6 38.576 77.153 1.2353 6.6 1.4 1.3 6.0 147 6 5 3 38.617 77.233 1.23421 14.0 3.0 2.8 6.0 148 7 1 -4 38.682 77.365 1.23244 6.0 1.3 1.2 6.0 149 3 6 5 38.913 77.826 1.22629 6.5 1.4 1.3 6.0 150 3 5 6 39.249 78.498 1.21746 11.7 2.5 2.4 6.0 151 6 5 -3 39.343 78.686 1.21502 28.3 6.1 5.7 6.0 152 3 6 -5 39.517 79.035 1.21054 8.3 1.8 1.7 6.0 153 1 8 3 39.754 79.509 1.20451 7.6 1.6 1.5 6.0 154 6 0 6 39.866 79.731 1.20171 5.4 1.2 1.1 6.0 155 3 5 -6 39.973 79.945 1.19903 8.1 1.8 1.6 6.0 156 7 5 0 40.096 80.192 1.19596 7.9 1.7 1.6 6.0 157 5 3 -6 40.414 80.828 1.18814 12.7 2.7 2.6 6.1 158 6 6 2 40.47 80.941 1.18677 5.5 1.2 1.1 6.1 159 5 7 2 41.005 82.011 1.17398 6.2 1.3 1.3 6.1 160 6 0 -6 41.304 82.608 1.167 9.5 2.0 1.9 6.1 161 4 8 0 41.581 83.161 1.16063 7.9 1.7 1.6 6.1 162 2 7 -5 41.888 83.776 1.15367 7.7 1.7 1.5 6.1 163 2 5 -7 42.818 85.636 1.13331 11.5 2.5 2.3 6.1 164 6 5 5 44.005 88.009 1.10877 4.9 1.0 1.0 6.2 165 7 1 6 44.317 88.635 1.10255 12.5 2.7 2.5 6.2 166 9 2 -1 44.485 88.97 1.09926 4.9 1.1 1.0 6.2 167 3 9 0 44.632 89.264 1.09641 7.1 1.5 1.4 6.2 168 0 9 3 44.838 89.676 1.09243 10.8 2.3 2.1 6.2 169 6 4 6 44.901 89.801 1.09123 8.0 1.7 1.6 6.2 Reference: Chichagov A.V. et al. Information-Calculating System on Crystal Structure Data of Minerals (MINCRYST) - Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian) |